CN107418733A - A kind of compound method of banana flavor flavouring essence for tobacco - Google Patents

A kind of compound method of banana flavor flavouring essence for tobacco Download PDF

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Publication number
CN107418733A
CN107418733A CN201710542953.4A CN201710542953A CN107418733A CN 107418733 A CN107418733 A CN 107418733A CN 201710542953 A CN201710542953 A CN 201710542953A CN 107418733 A CN107418733 A CN 107418733A
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CN
China
Prior art keywords
acetate
mixed liquor
flavouring essence
tobacco
stirred
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710542953.4A
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Chinese (zh)
Inventor
赵黎明
艾训儒
姚兰
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Hubei University for Nationalities
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Hubei University for Nationalities
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Publication date
Application filed by Hubei University for Nationalities filed Critical Hubei University for Nationalities
Priority to CN201710542953.4A priority Critical patent/CN107418733A/en
Publication of CN107418733A publication Critical patent/CN107418733A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
    • A24F47/008
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0026Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Confectionery (AREA)

Abstract

The invention discloses a kind of compound method of banana flavor flavouring essence for tobacco, comprise the following steps:(1) preparation raw material;(2) propane diols, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and terpinol are stirred;(3) amylalcohol, ethyl acetate, butyl acetate, benzyl acetate, diethyl malonate and Leaf Acetate are added in mixed liquor A obtained by upper step, is well mixed;(4) pentyl acetate, hexyl acetate, ethyl butyrate, isoamyl butyrate and the triacetyl glycerine of above-mentioned preparation are added in mixed liquid B obtained by upper step, is well mixed;(5) it is aged.The raw material of the banana flavor flavouring essence for tobacco is simple and easy to get, makes simply, cost is cheap, has the strong new sweet fragrance of fresh bananas, with rich flavor mellow and lasting.

Description

A kind of compound method of banana flavor flavouring essence for tobacco
Technical field
The present invention relates to a kind of flavouring essence for tobacco, specifically a kind of compound method of banana flavor flavouring essence for tobacco.
Background technology
Electronic cigarette also known as virtual cigarette, electronic atomizer, it is mainly used in smoking cessation and cigarette substitute.It has as cigarette Outward appearance, with the approximate taste of cigarette, or even than general cigarette taste to have more a lot, also like cigarette it is the same can suction out cigarette, Taste is suctioned out with feeling to come.Electronic cigarette does not have other harmful components such as tar in cigarette, suspended particulates, is mainly used for giving up smoking And cigarette substitute.
Electronic cigarette is made up of lithium battery, atomizer and cigarette bullet, and electronic cigarette passes through high-tech silicon and air flow sensor control Tobacco curing mist output quantity and working condition, nicotine are atomized, and by the solution atomization containing nicotine and essence into particulate, are inhaled by lung Receive, while the simulation smoke that spues.So electronics flavouring essence for tobacco is the indispensable important component of electronic cigarette.
Because the taste of each present smoker is all different, in order to cater to the hobby of consumer, in the market needs It the flavouring essence for tobacco of diverse fragrant flavour style, so can just expand consumption market, obtain the interests of maximum.Therefore, the present invention provides one The compound method of kind banana flavor flavouring essence for tobacco.
The content of the invention
It is an object of the invention to provide a kind of compound method of banana flavor flavouring essence for tobacco, to solve in above-mentioned background technology The problem of proposition.
To achieve the above object, the present invention provides following technical scheme:
A kind of compound method of banana flavor flavouring essence for tobacco, comprises the following steps:
(1) raw material of following quality permillage is prepared:
(2) by the propane diols of above-mentioned preparation, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and pine tar Alcohol is stirred 35-50min in closed space, obtains mixed liquor A;
(3) in mixed liquor A obtained by upper step, amylalcohol, ethyl acetate, butyl acetate, the acetic acid of above-mentioned preparation are sequentially added Benzyl ester, diethyl malonate and Leaf Acetate, 18-25min is stirred in closed space, obtains mixed liquid B;
(4) in mixed liquid B obtained by upper step, sequentially add the pentyl acetate of above-mentioned preparation, hexyl acetate, ethyl butyrate, Isoamyl butyrate and triacetyl glycerine, 20-30min is stirred in closed space, what is be uniformly mixed is mixed Close liquid C;
(5) mixed liquor C is placed at 28-38 DEG C and is aged 40-72h.
As the further scheme of the present invention:Step (2) is by the propane diols of above-mentioned preparation, second position damascenone, acetic acid, fourth Acid, clove bud oil, spearmint oil and terpinol are stirred 42min in closed space, obtain mixed liquor A.
As the further scheme of the present invention:Step (3) sequentially adds above-mentioned preparation in mixed liquor A obtained by upper step Amylalcohol, ethyl acetate, butyl acetate, benzyl acetate, diethyl malonate and Leaf Acetate, stirred in closed space mixed 21min is closed, obtains mixed liquid B.
As the further scheme of the present invention:Step (4) sequentially adds above-mentioned preparation in mixed liquid B obtained by upper step Pentyl acetate, hexyl acetate, ethyl butyrate, isoamyl butyrate and triacetyl glycerine, it is stirred in closed space 26min, the mixed liquor C being uniformly mixed.
As the further scheme of the present invention:Mixed liquor C is placed at 32 DEG C and is aged 62h by step (5).
Compared with prior art, the beneficial effects of the invention are as follows:
The raw material of the banana flavor flavouring essence for tobacco is simple and easy to get, makes simply, and cost is cheap, and making the electronic cigarette come has The special strong new sweet fragrance of fresh bananas, it is with rich flavor mellow and lasting, make the breath freshening of user;With energy and cigarette Gas is coordinated, increases light fragrant and sweet, fruity, add the fine and smooth soft sense of flue gas, reduce the advantages of stimulation.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Embodiment 1
A kind of compound method of banana flavor flavouring essence for tobacco, comprises the following steps:
(1) raw material of following quality permillage is prepared:
(2) by the propane diols of above-mentioned preparation, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and pine tar Alcohol is stirred 35min in closed space, obtains mixed liquor A;
(3) in mixed liquor A obtained by upper step, amylalcohol, ethyl acetate, butyl acetate, the acetic acid of above-mentioned preparation are sequentially added Benzyl ester, diethyl malonate and Leaf Acetate, 18min is stirred in closed space, obtains mixed liquid B;
(4) in mixed liquid B obtained by upper step, sequentially add the pentyl acetate of above-mentioned preparation, hexyl acetate, ethyl butyrate, Isoamyl butyrate and triacetyl glycerine, 20min is stirred in closed space, the mixed liquor being uniformly mixed C;
(5) mixed liquor C is placed at 28 DEG C and is aged 40h.
Embodiment 2
A kind of compound method of banana flavor flavouring essence for tobacco, comprises the following steps:
(1) raw material of following quality permillage is prepared:
(2) by the propane diols of above-mentioned preparation, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and pine tar Alcohol is stirred 50min in closed space, obtains mixed liquor A;
(3) in mixed liquor A obtained by upper step, amylalcohol, ethyl acetate, butyl acetate, the acetic acid of above-mentioned preparation are sequentially added Benzyl ester, diethyl malonate and Leaf Acetate, 25min is stirred in closed space, obtains mixed liquid B;
(4) in mixed liquid B obtained by upper step, sequentially add the pentyl acetate of above-mentioned preparation, hexyl acetate, ethyl butyrate, Isoamyl butyrate and triacetyl glycerine, 30min is stirred in closed space, the mixed liquor being uniformly mixed C;
(5) mixed liquor C is placed at 38 DEG C and is aged 72h.
Embodiment 3
A kind of compound method of banana flavor flavouring essence for tobacco, comprises the following steps:
(1) raw material of following quality permillage is prepared:
(2) by the propane diols of above-mentioned preparation, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and pine tar Alcohol is stirred 42min in closed space, obtains mixed liquor A;
(3) in mixed liquor A obtained by upper step, amylalcohol, ethyl acetate, butyl acetate, the acetic acid of above-mentioned preparation are sequentially added Benzyl ester, diethyl malonate and Leaf Acetate, 21min is stirred in closed space, obtains mixed liquid B;
(4) in mixed liquid B obtained by upper step, sequentially add the pentyl acetate of above-mentioned preparation, hexyl acetate, ethyl butyrate, Isoamyl butyrate and triacetyl glycerine, 26min is stirred in closed space, the mixed liquor being uniformly mixed C;
(5) mixed liquor C is placed at 32 DEG C and is aged 62h.
The raw material of the banana flavor flavouring essence for tobacco is simple and easy to get, makes simply, and cost is cheap, and making the electronic cigarette come has The special strong new sweet fragrance of fresh bananas, it is with rich flavor mellow and lasting, make the breath freshening of user;With energy and cigarette Gas is coordinated, increases light fragrant and sweet, fruity, add the fine and smooth soft sense of flue gas, reduce the advantages of stimulation.
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party Formula, can also be on the premise of this patent objective not be departed from one skilled in the relevant art's possessed knowledge Make a variety of changes.

Claims (5)

1. a kind of compound method of banana flavor flavouring essence for tobacco, it is characterised in that comprise the following steps:
(1) raw material of following quality permillage is prepared:
(2) propane diols of above-mentioned preparation, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and terpinol are existed 35-50min is stirred in closed space, obtains mixed liquor A;
(3) in mixed liquor A obtained by upper step, sequentially add the amylalcohol of above-mentioned preparation, ethyl acetate, butyl acetate, benzyl acetate, Diethyl malonate and Leaf Acetate, 18-25min is stirred in closed space, obtains mixed liquid B;
(4) in mixed liquid B obtained by upper step, pentyl acetate, hexyl acetate, ethyl butyrate, the butyric acid of above-mentioned preparation are sequentially added Isopentyl ester and triacetyl glycerine, 20-30min is stirred in closed space, the mixed liquor being uniformly mixed C;
(5) mixed liquor C is placed at 28-38 DEG C and is aged 40-72h.
2. the compound method of banana flavor flavouring essence for tobacco according to claim 1, it is characterised in that step (2) is matched somebody with somebody above-mentioned Propane diols, second position damascenone, acetic acid, butyric acid, clove bud oil, spearmint oil and the terpinol of system stir in closed space 42min is mixed, obtains mixed liquor A.
3. the compound method of banana flavor flavouring essence for tobacco according to claim 1, it is characterised in that step (3) is in upper step institute In mixed liquor A, sequentially add the amylalcohol of above-mentioned preparation, ethyl acetate, butyl acetate, benzyl acetate, diethyl malonate and Leaf Acetate, 21min is stirred in closed space, obtains mixed liquid B.
4. the compound method of banana flavor flavouring essence for tobacco according to claim 1, it is characterised in that step (4) is in upper step institute Obtain in mixed liquid B, pentyl acetate, hexyl acetate, ethyl butyrate, isoamyl butyrate and three acetic acid for sequentially adding above-mentioned preparation are sweet Grease, 26min is stirred in closed space, the mixed liquor C being uniformly mixed.
5. the compound method of banana flavor flavouring essence for tobacco according to claim 1, it is characterised in that step (5) is by mixed liquor C It is placed at 32 DEG C and is aged 62h.
CN201710542953.4A 2017-07-05 2017-07-05 A kind of compound method of banana flavor flavouring essence for tobacco Pending CN107418733A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103695171A (en) * 2012-09-27 2014-04-02 邢娜 Banana flavored cigarette essence
CN103849465A (en) * 2014-02-27 2014-06-11 恩施市锦华生物工程有限责任公司 Preparation method of essence for electronic cigarette with strawberry flavor
CN104087414A (en) * 2014-07-28 2014-10-08 嘉兴市得百科新材料科技有限公司 Electronic cigarette liquid with blueberry flavor and preparation method thereof
CN104382223A (en) * 2014-10-22 2015-03-04 浙江中烟工业有限责任公司 Solvent suitable for preparation of fruity nicotine liquid, and nicotine liquid and electronic cigarette prepared by solvent
CN105166840A (en) * 2015-09-29 2015-12-23 上海孔雀香精香料科技有限公司 Banana essence
CN106418704A (en) * 2016-09-14 2017-02-22 河北中烟工业有限责任公司 Application of clove bud oil in electronic tobacco tar
CN106722766A (en) * 2016-11-13 2017-05-31 浙江绿晶香精有限公司 Flavoring banana essence
CN106811292A (en) * 2015-11-30 2017-06-09 青岛顺昕电子科技有限公司 A kind of flavoring banana essence

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103695171A (en) * 2012-09-27 2014-04-02 邢娜 Banana flavored cigarette essence
CN103849465A (en) * 2014-02-27 2014-06-11 恩施市锦华生物工程有限责任公司 Preparation method of essence for electronic cigarette with strawberry flavor
CN104087414A (en) * 2014-07-28 2014-10-08 嘉兴市得百科新材料科技有限公司 Electronic cigarette liquid with blueberry flavor and preparation method thereof
CN104382223A (en) * 2014-10-22 2015-03-04 浙江中烟工业有限责任公司 Solvent suitable for preparation of fruity nicotine liquid, and nicotine liquid and electronic cigarette prepared by solvent
CN105166840A (en) * 2015-09-29 2015-12-23 上海孔雀香精香料科技有限公司 Banana essence
CN106811292A (en) * 2015-11-30 2017-06-09 青岛顺昕电子科技有限公司 A kind of flavoring banana essence
CN106418704A (en) * 2016-09-14 2017-02-22 河北中烟工业有限责任公司 Application of clove bud oil in electronic tobacco tar
CN106722766A (en) * 2016-11-13 2017-05-31 浙江绿晶香精有限公司 Flavoring banana essence

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Application publication date: 20171201