CN107410356A - Mould inhibitor preparation method with high-efficiency antimicrobial - Google Patents

Mould inhibitor preparation method with high-efficiency antimicrobial Download PDF

Info

Publication number
CN107410356A
CN107410356A CN201710772017.2A CN201710772017A CN107410356A CN 107410356 A CN107410356 A CN 107410356A CN 201710772017 A CN201710772017 A CN 201710772017A CN 107410356 A CN107410356 A CN 107410356A
Authority
CN
China
Prior art keywords
parts
mould inhibitor
menthol
bromogeramine
polyethylene glycol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710772017.2A
Other languages
Chinese (zh)
Inventor
赖金元
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu Kameiqi Footwear Co ltd
Original Assignee
Chengdu Kameiqi Footwear Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chengdu Kameiqi Footwear Co ltd filed Critical Chengdu Kameiqi Footwear Co ltd
Priority to CN201710772017.2A priority Critical patent/CN107410356A/en
Publication of CN107410356A publication Critical patent/CN107410356A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/06Oxygen or sulfur directly attached to a cycloaliphatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/12Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/06Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/10Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A01N37/38Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
    • A01N37/40Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06Aluminium; Calcium; Magnesium; Compounds thereof

Abstract

The invention discloses the mould inhibitor preparation method with high-efficiency antimicrobial, 1) salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nano-aluminum hydroxide are well mixed;2) polyethylene glycol, potassium sorbate, sodium benzoate are added, is then transferred in reactor and is stirred reaction;3) nano titanium oxide and nano silver antimicrobials are added after material is cooled to 40 DEG C;4) menthol is ground into 50 100 mesh, is added to adsorbent in step 3) and carries out uniform stirring;The preparation method of the antibacterial mildew inhibitor of the present invention, obtained antibacterial mildew inhibitor can effectively suppress foot pathomycete trichophyta and candida albicans, it is harmless and extracorporeal antifungal activity is big so that antibacterial agent for shoes has very strong antifungal activity and security, deodorization speed is fast, keeps footgear salubrious, it is all effective to a variety of peculiar smell and anti-mold effect is obvious, it is biodegradable, it is harmless, the green safe environmental protection of production technology.

Description

Mould inhibitor preparation method with high-efficiency antimicrobial
Technical field
The present invention relates to one kind Gluewater of shoes, and in particular to has the mould inhibitor preparation method of high-efficiency antimicrobial.
Background technology
Shoes have long development history.In Yangshao culture period about before more than 5000 years, there have been animal skin sewing Most original footwear.Shoes are indispensable daily necessitiess in people's life, and shoes production is one of China's hosiery industry Important component.Shoes belong to the formed product of weft-knitted fabric.Comfortable due to requiring to wear, its shape will meet pin shape, It will not come off or overturn, and require good-extensibility, good permeability, in addition, also to have good hygroscopicity and wearability.Shoes Species it is a lot, can be classified according to raw material, institutional framework, leggings length and stocking blank structure, shoes specification.The production of pedopathy It is raw most of all relevant with shoes, due to the metabolism of human body, all discharging substantial amounts of aging skin fragment daily, people's pin and The small space humiture of footwear is suitable, turns into the hotbed of germ reproduction, at a suitable temperature, the microorganism such as bacterium, fungi, acarid Bred rapidly using aging skin fragment as nutrition, make foot infected, meanwhile, it is easy to grow on shoes and breeds thin Bacterium, microorganism, especially plum rain season or it is hot and humid under the conditions of, situation that shoes can be caused to go mouldy.
The content of the invention
The technical problems to be solved by the invention are that the small space humiture of people's pin and footwear is suitable, turn into the temperature of germ reproduction Bed, at a suitable temperature, the microorganism such as bacterium, fungi, acarid breeds rapidly using aging skin fragment as nutrition, makes foot It is infected, meanwhile, growth and bacterial growth, microorganism are easy on shoes, especially in plum rain season or hot and humid bar Under part, situation that shoes go mouldy can be caused, and it is an object of the present invention to provide the mould inhibitor preparation method with high-efficiency antimicrobial, can It is effective to suppress foot pathomycete trichophyta and candida albicans, and extracorporeal antifungal activity is big, it is harmless so that footwear are used Antiseptic has very strong antifungal activity and security, and deodorization speed is fast, keeps footgear salubrious, and anti-mold effect is obvious, right A variety of peculiar smell are all effective, biodegradable, harmless, the green safe environmental protection of production technology.
The present invention is achieved through the following technical solutions:
Mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer Aluminium hydroxide is uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added to adsorbent in step 3) and carries out uniform stirring;
The mass fraction of wherein feed components is:Polyethylene glycol 40-45 parts, potassium sorbate 15-20 parts, sodium benzoate 10-13 parts, salicylanilide 6-8 parts, acid diatomite 15-25 parts, bromogeramine 1-4 parts, glacial acetic acid 2-8 parts, stearic acid Sodium 3-5 parts, calcined kaolin 10-14 parts, nano titanium oxide 1-2.5 parts, nano silver antimicrobials 1-2 parts, aluminium hydroxide 6-8 Part, adsorbent 1-3 parts, menthol 0.5-1 parts.
The mass fraction of each component is:Polyethylene glycol 42-45 parts, potassium sorbate 15-18 parts, sodium benzoate 11-13 parts, water Poplar anilide 6-8 parts, acid diatomite 17-23 parts, bromogeramine 1-3 parts, glacial acetic acid 3-7 parts, odium stearate 4-5 parts, forge Burn kaolin 11-13 parts, nano titanium oxide 1.5-2.5 parts, nano silver antimicrobials 1-2 parts, aluminium hydroxide 7-8 parts, adsorbent 1-2 parts, menthol 0.7-1 parts.
The mass fraction of each component is:43 parts of polyethylene glycol, 17 parts of potassium sorbate, 12 parts of sodium benzoate, salicylanilide 7 Part, 20 parts acid of diatomite, 3 parts of bromogeramine, 5 parts of glacial acetic acid, 4 parts of odium stearate, 12 parts of calcined kaolin, nano-silica Change 1.7 parts of titanium, 1.5 parts of nano silver antimicrobials, 7 parts of aluminium hydroxide, 2 parts of adsorbent, 0.8 part of menthol.
The preparation method of the antibacterial mildew inhibitor of the present invention, obtained antibacterial mildew inhibitor can effectively suppress foot and cause a disease very Bacterium trichophyta and candida albicans, and extracorporeal antifungal activity is big so that and antibacterial agent for shoes has very strong antifungal activity and safety Property, deodorization speed is fast, keeps footgear salubrious, and anti-mold effect is obvious, all effective to a variety of peculiar smell, biodegradable, right Human body is harmless, the green safe environmental protection of production technology.
The size of the nano titanium oxide is 50-60nm.
Also contain essence 1-2 parts in the antibacterial mildew inhibitor.
The present invention compared with prior art, has the following advantages and advantages:
1st, the present invention has the mould inhibitor preparation method of high-efficiency antimicrobial, and obtained antibacterial mildew inhibitor can effectively suppress Foot pathomycete trichophyta and candida albicans, and extracorporeal antifungal activity is big so that antibacterial agent for shoes has very strong anti-true Bacterium property and security;
2nd, the present invention has the mould inhibitor preparation method of high-efficiency antimicrobial, and obtained antibacterial mildew inhibitor deodorization speed is fast, protects It is salubrious to hold footgear, and anti-mold effect is obvious, biodegradable, harmless, production technology all effective to a variety of peculiar smell Green safe environmental protection.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment, the present invention is made Further to describe in detail, exemplary embodiment of the invention and its explanation are only used for explaining the present invention, are not intended as to this The restriction of invention.
Embodiment 1
The present invention provides the mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer Aluminium hydroxide is uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added in step 3) with adsorbent, essence and is uniformly stirred Mix;
The mass fraction of wherein feed components is:40 parts of polyethylene glycol, 15 parts of potassium sorbate, 10 parts of sodium benzoate, water 6 parts of poplar anilide, 15 parts acid of diatomite, 1 part of bromogeramine, 2 parts of glacial acetic acid, 3 parts of odium stearate, calcined kaolin 10 Part, 1 part of nano titanium oxide, 1 part of nano silver antimicrobials, 6 parts of aluminium hydroxide, 1 part of adsorbent, 0.5 part of menthol, 1 part of essence.
The antibacterial mildew inhibitor of the present embodiment, to Escherichia coli, staphylococcus aureus, fungi trichophyta and candida albicans white The bacteriums such as candida albicans, fungi are respectively provided with good antibacterial effect.Through experimental determination, reach killing rate more than 80%, it is mould proof with Eliminate the unusual smell positive effect.
Embodiment 2
The present invention provides the mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer Aluminium hydroxide is uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added in step 3) with adsorbent, essence and is uniformly stirred Mix;
The mass fraction of wherein feed components is:45 parts of polyethylene glycol, 20 parts of potassium sorbate, 13 parts of sodium benzoate, water 8 parts of poplar anilide, 25 parts acid of diatomite, 4 parts of bromogeramine, 8 parts of glacial acetic acid, 5 parts of odium stearate, calcined kaolin 14 Part, 2.5 parts of nano titanium oxide, 2 parts of nano silver antimicrobials, 8 parts of aluminium hydroxide, 3 parts of adsorbent, 1 part of menthol, 2 parts of essence.
The antibacterial mildew inhibitor of the present embodiment, to Escherichia coli, staphylococcus aureus, fungi trichophyta and candida albicans white The bacteriums such as candida albicans, fungi are respectively provided with good antibacterial effect.Through experimental determination, reach killing rate more than 80%, it is mould proof and Eliminate the unusual smell positive effect.
Embodiment 3
The present invention provides the mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer Aluminium hydroxide is uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added in step 3) with adsorbent, essence and is uniformly stirred Mix;
The mass fraction of wherein feed components is:43 parts of polyethylene glycol, 17 parts of potassium sorbate, 12 parts of sodium benzoate, water 7 parts of poplar anilide, 20 parts acid of diatomite, 3 parts of bromogeramine, 5 parts of glacial acetic acid, 4 parts of odium stearate, calcined kaolin 12 Part, 1.7 parts of nano titanium oxide, 1.5 parts of nano silver antimicrobials, 7 parts of aluminium hydroxide, 2 parts of adsorbent, 0.8 part of menthol, essence 1 part.
The antibacterial mildew inhibitor of the present embodiment, to Escherichia coli, staphylococcus aureus, fungi trichophyta and candida albicans white The bacteriums such as candida albicans, fungi are respectively provided with good antibacterial effect.Through experimental determination, reach killing rate more than 80%, it is mould proof and Eliminate the unusual smell positive effect.
Embodiment 4
The present invention provides the mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer Aluminium hydroxide is uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) after menthol being ground into 50-100 mesh, together it is added in step 2) with adsorbent, essence and is uniformly stirred Mix;
The mass fraction of wherein feed components is:43 parts of polyethylene glycol, 17 parts of potassium sorbate, 12 parts of sodium benzoate, water 7 parts of poplar anilide, 20 parts acid of diatomite, 3 parts of bromogeramine, 5 parts of glacial acetic acid, 4 parts of odium stearate, calcined kaolin 12 Part, 7 parts of aluminium hydroxide, 2 parts of adsorbent, 0.8 part of menthol, 1 part of essence.
The antibacterial mildew inhibitor of the present embodiment, the mould proof and positive effect that eliminates the unusual smell, but the effect of bacteriostasis antibiosis is relatively low, bacterium Killing rate can only achieve 30% or so.
Embodiment 5
The present invention provides the mould inhibitor preparation method with high-efficiency antimicrobial, comprises the following steps:
1) salicylanilide, acid diatomite, odium stearate, calcined kaolin, nano-aluminum hydroxide are stirred Uniformly;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred instead Should, reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added to essence in step 3) and carries out uniform stirring;
The mass fraction of wherein feed components is:30 parts of polyethylene glycol, 10 parts of potassium sorbate, 20 parts of sodium benzoate, water 1 part of poplar anilide, 5 parts acid of diatomite, 4 parts of odium stearate, 7 parts of calcined kaolin, nano titanium oxide 0.3 part, nanometer 0.1 part of silver antibacterial agent, 7 parts of aluminium hydroxide, 0.8 part of menthol, 1 part of essence.
The antibacterial mildew inhibitor of the present embodiment, to Escherichia coli, staphylococcus aureus, fungi trichophyta and candida albicans white The bacteriums such as candida albicans, fungi are respectively provided with certain antibacterial effect.Through experimental determination, reach killing rate 50% or so, but it is anti- Mould and effect that is eliminating the unusual smell is poor.
Above-described embodiment, the purpose of the present invention, technical scheme and beneficial effect are carried out further Describe in detail, should be understood that the embodiment that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc., all should include Within protection scope of the present invention.

Claims (5)

1. the mould inhibitor preparation method with high-efficiency antimicrobial, it is characterised in that comprise the following steps:
1) by salicylanilide, acid diatomite, bromogeramine, glacial acetic acid, odium stearate, calcined kaolin, nanometer hydrogen-oxygen Change aluminium to be uniformly mixed;
2) polyethylene glycol, potassium sorbate, sodium benzoate are added in step 1), is then transferred in reactor and is stirred reaction, Reaction temperature is 55-60 DEG C, time 30-60min;
3) add nano titanium oxide after material in step 2) being cooled into 40 DEG C and nano silver antimicrobials stir;
4) after menthol being ground into 50-100 mesh, together it is added to adsorbent in step 3) and carries out uniform stirring;
The mass fraction of wherein feed components is:Polyethylene glycol 40-45 parts, potassium sorbate 15-20 parts, sodium benzoate 10-13 Part, salicylanilide 6-8 parts, acid diatomite 15-25 parts, bromogeramine 1-4 parts, glacial acetic acid 2-8 parts, odium stearate 3-5 Part, calcined kaolin 10-14 parts, nano titanium oxide 1-2.5 parts, nano silver antimicrobials 1-2 parts, aluminium hydroxide 6-8 parts, absorption Agent 1-3 parts, menthol 0.5-1 parts.
2. the mould inhibitor preparation method according to claim 1 with high-efficiency antimicrobial, it is characterised in that the matter of each component Measuring number is:Polyethylene glycol 42-45 parts, potassium sorbate 15-18 parts, sodium benzoate 11-13 parts, salicylanilide 6-8 parts, acidity Diatomite 17-23 parts, bromogeramine 1-3 parts, glacial acetic acid 3-7 parts, odium stearate 4-5 parts, calcined kaolin 11-13 parts, receive Rice titanium dioxide 1.5-2.5 parts, nano silver antimicrobials 1-2 parts, aluminium hydroxide 7-8 parts, adsorbent 1-2 parts, menthol 0.7-1 Part.
3. the mould inhibitor preparation method according to claim 1 with high-efficiency antimicrobial, it is characterised in that the matter of each component Measuring number is:43 parts of polyethylene glycol, 17 parts of potassium sorbate, 12 parts of sodium benzoate, 7 parts of salicylanilide, acid diatomite 20 Part, 3 parts of bromogeramine, 5 parts of glacial acetic acid, 4 parts of odium stearate, 12 parts of calcined kaolin, 1.7 parts of nano titanium oxide, Nano Silver 1.5 parts of antiseptic, 7 parts of aluminium hydroxide, 2 parts of adsorbent, 0.8 part of menthol.
4. according to any described mould inhibitor preparation methods with high-efficiency antimicrobial of claim 1-3, it is characterised in that described The size of nano titanium oxide is 50-60nm.
5. the mould inhibitor preparation method according to claim 1 with high-efficiency antimicrobial, it is characterised in that the antibacterial is prevented Also contain essence 1-2 parts in mould dose.
CN201710772017.2A 2017-08-31 2017-08-31 Mould inhibitor preparation method with high-efficiency antimicrobial Withdrawn CN107410356A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710772017.2A CN107410356A (en) 2017-08-31 2017-08-31 Mould inhibitor preparation method with high-efficiency antimicrobial

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710772017.2A CN107410356A (en) 2017-08-31 2017-08-31 Mould inhibitor preparation method with high-efficiency antimicrobial

Publications (1)

Publication Number Publication Date
CN107410356A true CN107410356A (en) 2017-12-01

Family

ID=60435490

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710772017.2A Withdrawn CN107410356A (en) 2017-08-31 2017-08-31 Mould inhibitor preparation method with high-efficiency antimicrobial

Country Status (1)

Country Link
CN (1) CN107410356A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116117950A (en) * 2023-03-01 2023-05-16 北华大学 Wood anti-cracking agent

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102239884A (en) * 2011-04-29 2011-11-16 广东省微生物研究所 Mildewproof agent for leather shoes and preparation method thereof
CN103828807A (en) * 2014-03-18 2014-06-04 王利芬 Mildew preventive for cloth shoes
CN104686574A (en) * 2013-12-05 2015-06-10 无锡钻石地毯制造有限公司 Ecological carpet eco-friendly mildew inhibitor
CN106689209A (en) * 2016-11-15 2017-05-24 史小琳 Mildew resisting agent applied to shoes

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102239884A (en) * 2011-04-29 2011-11-16 广东省微生物研究所 Mildewproof agent for leather shoes and preparation method thereof
CN104686574A (en) * 2013-12-05 2015-06-10 无锡钻石地毯制造有限公司 Ecological carpet eco-friendly mildew inhibitor
CN103828807A (en) * 2014-03-18 2014-06-04 王利芬 Mildew preventive for cloth shoes
CN106689209A (en) * 2016-11-15 2017-05-24 史小琳 Mildew resisting agent applied to shoes

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116117950A (en) * 2023-03-01 2023-05-16 北华大学 Wood anti-cracking agent
CN116117950B (en) * 2023-03-01 2024-01-30 北华大学 Wood anti-cracking agent

Similar Documents

Publication Publication Date Title
CN103947673B (en) Antibacterial root-growing agent of a kind of slowly-releasing and preparation method thereof
CN109170228A (en) A kind of liquid compound acidulant and its preparation process with strong buffer capacity
CN111135160B (en) Foam wash-free antibacterial liquid for personal protection and preparation method thereof
CN106578839A (en) Feed mildew proofing agent and preparation method thereof
CN103668955A (en) Padding-process antibacterial polyester fabric and preparation method thereof
CN102845607A (en) Novel antibacterial antiviral feed additive
CN102988232A (en) Pet cleanser and preparation method thereof
CN101779641A (en) Alcohol-group leather sterilization mildewcide
CN105166587A (en) Drying mildewproof bactericide for feeds
CN110624012A (en) Nanometer povidone iodine oral liquid for protecting pig intestines and stomach and preparation method thereof
CN108142688B (en) Zinc oxide-free conservation material
CN107410356A (en) Mould inhibitor preparation method with high-efficiency antimicrobial
CN108210464A (en) A kind of compound florfenicol soluble powder and preparation method thereof
CN104430341A (en) Application of natural organic acid radical laminine chelate in agricultural preparations
CN105248461A (en) Domestic disinfectant and preparing method thereof
CN102000092B (en) New application of sulfadiazine sodium in preparing medicine for preventing or treating Bombyx mori septicemia
CN107162129A (en) A kind of water quality of aquaculture pond inorganic agent
CN107484773A (en) It is capable of the shoes antibacterial mildew inhibitor of deodorization
KR101052917B1 (en) Manufacturing method of feed additive for pig breeding
CN103669001A (en) Clothing finishing agent and preparation method thereof
CN104650352A (en) Poly-hexamethylene biguanide hydrochloride sterilizing and disinfecting agent
JP2002507123A (en) Method for improving the effectiveness of probiotics, preparation of nutritional additives and animal feed containing same
CN103768089A (en) Chitosan antibacterial lotion for gynecology and preparation method thereof
CN106721003A (en) Prevent and treat the feed addictive and preparation method of animal viral disease
CN102559418B (en) Phytic acid silver toilet soap and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication
WW01 Invention patent application withdrawn after publication

Application publication date: 20171201