CN107410310A - A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof - Google Patents
A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof Download PDFInfo
- Publication number
- CN107410310A CN107410310A CN201710709885.6A CN201710709885A CN107410310A CN 107410310 A CN107410310 A CN 107410310A CN 201710709885 A CN201710709885 A CN 201710709885A CN 107410310 A CN107410310 A CN 107410310A
- Authority
- CN
- China
- Prior art keywords
- acid
- peracetic acid
- compound
- disinfection solution
- ingredient
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
Abstract
The invention discloses a kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof, is mainly made up of propellant, PH conditioning agents, compound stabilizer, compound corrosion inhibitor and purified water, and the beneficial effect that the present invention is reached is：Packed for unitary, it is not necessary to which hybrid reaction 24h is directly used.The Peracetic acid of generation need not dilute, and can directly use.In terms of application field is extended to medicine equipment, corrosivity is greatly reduced.Service life extends, and immersion medicine equipment, endoscope is most long is used continuously 7 days.Traditional two-component packaging shelf life of products is long, but can only preserve 24h 48h or so upon mixing and decompose, and the peracetic acid in single-ingredient disinfection solution term of validity of Recipe production is 2 years.
Description
Technical field
The present invention relates to a kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof, belongs to thimerosal manufacturing technology field.
Background technology
The main application fields of traditional Peracetic acid are food-processing industry, because its use is extremely inconvenient, during use
A liquid is needed to carry out more than hybrid reaction 24h with B liquid, the main component of A liquid is high-strength hydrogen peroxide, and B liquid main component is ice
Acetic acid, the concentrated sulfuric acid.It is higher, it is necessary to used after diluting to react the peroxyacetic acid concentration of generation, but service life is short, can typically make
With 24h-48h or so.
The content of the invention
The present invention provides a kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof.
In order to solve the above-mentioned technical problem, the invention provides following technical scheme：
A kind of peracetic acid in single-ingredient disinfection solution of the present invention, include the preparing raw material of following parts by weight：Propellant 10-20 parts, PH are adjusted
Save agent 5-10 parts, compound stabilizer 5-10 parts, compound corrosion inhibitor 5-10 parts, remaining be purified water.
As a preferred technical solution of the present invention, described propellant includes solid hydrogen peroxide, glacial acetic acid, dense sulphur
Acid, tetraacetyl ethylene diamine, surfactant；Described PH conditioning agents include SODIUM PERCARBONATE, disodium hydrogen phosphate；Described compounding is steady
Determining agent includes glacial acetic acid, hydrogen peroxide；Described compound corrosion inhibitor includes salicylic acid, tartaric acid, sodium pyrophosphate.
As a preferred technical solution of the present invention, described propellant is by solid hydrogen peroxide, four acetyl second two
Amine, glacial acetic acid, the concentrated sulfuric acid, surfactant press 2-10:1-5:0.2-1:0.5-3：The compound that 1-5 ratio mixes.
As a preferred technical solution of the present invention, described PH conditioning agents be by SODIUM PERCARBONATE, disodium hydrogen phosphate by
1-5:The compound that 1-5 ratio mixes.
As a preferred technical solution of the present invention, described compound stabilizer is by 1 by glacial acetic acid, hydrogen peroxide:
The compound that 3.47 ratio mixes.
As a preferred technical solution of the present invention, described compound corrosion inhibitor is by salicylic acid, tartaric acid, pyrophosphoric acid
Sodium presses 1-5:1.5-8:The compound that 2-10 ratio mixes.
Present invention also offers the preparation method of above-mentioned peracetic acid in single-ingredient disinfection solution：
Step（1）, solid hydrogen peroxide is soluble in water, tetraacetyl ethylene diamine, surfactant, stirring to mixing are added immediately
Uniformly, now material is not completely dissolved.
Step（2）, PH regulation agent sodium percarbonates are slowly added to, adjust PH to 7.0-7.5；40min-60min is stirred to thing
Material is completely dissolved, and adds glacial acetic acid, the concentrated sulfuric acid, reacts 1h, generates Peracetic acid.
Step（3）, in step S2）Compound stabilizer, compound corrosion inhibitor stirring 30min are added in the mixture of generation, extremely
Well mixed, now solution is in acidity.
Step（4）, pH value is adjusted between 2.0-3.0 with disodium hydrogen phosphate.
Step（5）, Peracetic acid content is detected, is adjusted to 0.2%-0.3%, peracetic acid in single-ingredient disinfection solution finished product is made.
The beneficial effect that is reached of the present invention is：
1st, packed for unitary, it is not necessary to which hybrid reaction 24h is directly used.
2nd, the Peracetic acid of generation need not dilute, and can directly use.
3rd, in terms of application field is extended to medicine equipment, corrosivity is greatly reduced.
4th, service life extends, and immersion medicine equipment, endoscope is most long is used continuously 7 days.
5th, traditional two-component packaging shelf life of products is long, but can only preserve 24h or so upon mixing and decompose, and this is matched somebody with somebody
The peracetic acid in single-ingredient disinfection solution term of validity of square technique productions is 2 years.
Embodiment
The preferred embodiments of the present invention are illustrated below, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
A kind of peracetic acid in single-ingredient disinfection solution of the present invention, propellant 10-20 parts, PH conditioning agent 5-10 parts, compound stabilizer 5-10
Part, compound corrosion inhibitor 5-10 parts, remaining be purified water.
Propellant includes solid hydrogen peroxide, glacial acetic acid, the concentrated sulfuric acid, tetraacetyl ethylene diamine, surfactant；PH conditioning agents
Including SODIUM PERCARBONATE, disodium hydrogen phosphate；Compound stabilizer includes glacial acetic acid, hydrogen peroxide；Compound corrosion inhibitor includes salicylic acid, wine
Stone acid, sodium pyrophosphate.
Product process flow：
1st, it is solid hydrogen peroxide is soluble in water, tetraacetyl ethylene diamine, surfactant are added immediately, are stirred to well mixed,
Now material is not completely dissolved.
2nd, PH regulation agent sodium percarbonates are slowly added to, adjust ph to 7.0-7.5.It is complete to material to stir 40min-60min
Dissolving, add glacial acetic acid, strong sulfuric acid response 1h.
3rd, compound stabilizer, compound corrosion inhibitor stirring 30min are added, to being well mixed, now solution is in acidity.
4th, Ph values are adjusted between 2.0-3.0 with disodium hydrogen phosphate.
5th, Peracetic acid content is detected, is adjusted to 0.2%-0.3%.
Compound stabilizer：Glacial acetic acid is 1 with hydrogen peroxide harmonic proportion:It is 3.47 now with the current.
Compound corrosion inhibitor：Salicylic acid, tartaric acid and sodium pyrophosphate harmonic proportion are 1-5:1.5-8:2-10.
Peracetic acid in single-ingredient disinfection solution of the present invention, including propellant：Solid hydrogen peroxide, glacial acetic acid, the concentrated sulfuric acid, four acetyl
Ethylenediamine, surfactant.PH conditioning agents：SODIUM PERCARBONATE, disodium hydrogen phosphate.Compound stabilizer：Glacial acetic acid, hydrogen peroxide.It is multiple
With corrosion inhibiter：Salicylic acid, tartaric acid, sodium pyrophosphate.Remaining is purified water.
Packed during preparation for unitary, it is not necessary to which hybrid reaction 24h is directly used.The Peracetic acid of generation need not dilute,
Can directly it use.In terms of application field is extended to medicine equipment, corrosivity is greatly reduced.Service life extends, immersion
Medicine equipment, endoscope are most long to be used continuously 7 days.Traditional two-component packaging shelf life of products is long, but upon mixing only
24h or so can be preserved to decompose, the peracetic acid in single-ingredient disinfection solution term of validity of Recipe production is 2 years.
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic.
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in the present invention's
Within protection domain.
Claims (7)
1. a kind of peracetic acid in single-ingredient disinfection solution, it is characterised in that include the preparing raw material of following parts by weight：Propellant 10-20
Part, PH conditioning agent 5-10 parts, compound stabilizer 5-10 parts, compound corrosion inhibitor 5-10 parts, remaining be purified water.
2. a kind of peracetic acid in single-ingredient disinfection solution according to claim 1, it is characterised in that described propellant includes solid
Body hydrogen peroxide, glacial acetic acid, the concentrated sulfuric acid, tetraacetyl ethylene diamine, surfactant；Described PH conditioning agents include SODIUM PERCARBONATE,
Disodium hydrogen phosphate；Described compound stabilizer includes glacial acetic acid, hydrogen peroxide；Described compound corrosion inhibitor includes salicylic acid, wine
Stone acid, sodium pyrophosphate.
3. a kind of peracetic acid in single-ingredient disinfection solution according to claim 1, it is characterised in that described propellant is by solid
Body hydrogen peroxide, glacial acetic acid, the concentrated sulfuric acid, tetraacetyl ethylene diamine, surfactant press 2-10:1-5:0.2-1:0.5-3：1-5's
The compound that ratio mixes.
A kind of 4. peracetic acid in single-ingredient disinfection solution according to claim 1, it is characterised in that described PH conditioning agents be by
SODIUM PERCARBONATE, disodium hydrogen phosphate press 1-5:The compound that 1-5 ratio mixes.
5. a kind of peracetic acid in single-ingredient disinfection solution according to claim 1, it is characterised in that described compound stabilizer is
1 is pressed by glacial acetic acid, hydrogen peroxide:The compound that 3.47 ratio mixes.
6. a kind of peracetic acid in single-ingredient disinfection solution according to claim 1, it is characterised in that described compound corrosion inhibitor is
1-5 is pressed by salicylic acid, tartaric acid, sodium pyrophosphate:1.5-8:The compound that 2-10 ratio mixes.
7. the preparation method of a kind of peracetic acid in single-ingredient disinfection solution according to claim 2, it is characterised in that including following
Step,
S1）Solid hydrogen peroxide is soluble in water, tetraacetyl ethylene diamine, surfactant are added immediately, are stirred to well mixed,
Now material is not completely dissolved；
S2）PH regulation agent sodium percarbonates are slowly added to, adjust PH to 7.0-7.5；It is completely molten to material to stir 40min-60min
Solution, glacial acetic acid, the concentrated sulfuric acid are added, react 1h, generate Peracetic acid；
S3）In step S2）Compound stabilizer, compound corrosion inhibitor stirring 30min are added in the mixture of generation, is extremely well mixed,
Now solution is in acidity；
S4）PH value is adjusted between 2.0-3.0 with disodium hydrogen phosphate；
S5）Peracetic acid content is detected, is adjusted to 0.2%-0.3%, peracetic acid in single-ingredient disinfection solution finished product is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710709885.6A CN107410310A (en) | 2017-08-18 | 2017-08-18 | A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710709885.6A CN107410310A (en) | 2017-08-18 | 2017-08-18 | A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107410310A true CN107410310A (en) | 2017-12-01 |
Family
ID=60433931
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710709885.6A Pending CN107410310A (en) | 2017-08-18 | 2017-08-18 | A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107410310A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108849893A (en) * | 2018-07-27 | 2018-11-23 | 佛山市南海东方澳龙制药有限公司 | Peroxyacetic acid disinfectant and preparation method thereof |
| CN109077054A (en) * | 2018-09-27 | 2018-12-25 | 四川省畜牧科学研究院 | A kind of Peracetic acid composite disinfectant and preparation method thereof |
| CN111296443A (en) * | 2020-03-16 | 2020-06-19 | 山东消博士消毒科技股份有限公司 | Disinfectant for cleaning endoscope and preparation method thereof |
| CN111357761A (en) * | 2018-12-26 | 2020-07-03 | 哈尔滨三联药业股份有限公司 | Peroxyacetic acid disinfectant and application thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102964285A (en) * | 2012-11-28 | 2013-03-13 | 北京红辉力上科技有限公司 | Peroxyacetic acid generator and preparation method thereof |
| WO2014089633A1 (en) * | 2012-12-14 | 2014-06-19 | Saban Ventures Pty Limited | Disinfectant |
| CN105961430A (en) * | 2016-06-08 | 2016-09-28 | 连云港奥凯医疗设备科技有限公司 | Disinfectant and preparation method thereof |
| CN106689197A (en) * | 2016-12-27 | 2017-05-24 | 广州迈高化学有限公司 | Monobasic stable type peroxyacetic acid disinfection solution and preparation method of monobasic stable type peroxyacetic acid disinfection solution |
| CN106857513A (en) * | 2017-01-11 | 2017-06-20 | 北京长江脉医药科技有限责任公司 | A kind of unitary Peracetic acid solid particle disinfectant |
| CN106879593A (en) * | 2017-01-11 | 2017-06-23 | 北京长江脉医药科技有限责任公司 | A kind of alkalescent low corrosion Peracetic acid effervescent tablet disinfectant |
-
2017
- 2017-08-18 CN CN201710709885.6A patent/CN107410310A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102964285A (en) * | 2012-11-28 | 2013-03-13 | 北京红辉力上科技有限公司 | Peroxyacetic acid generator and preparation method thereof |
| WO2014089633A1 (en) * | 2012-12-14 | 2014-06-19 | Saban Ventures Pty Limited | Disinfectant |
| CN105961430A (en) * | 2016-06-08 | 2016-09-28 | 连云港奥凯医疗设备科技有限公司 | Disinfectant and preparation method thereof |
| CN106689197A (en) * | 2016-12-27 | 2017-05-24 | 广州迈高化学有限公司 | Monobasic stable type peroxyacetic acid disinfection solution and preparation method of monobasic stable type peroxyacetic acid disinfection solution |
| CN106857513A (en) * | 2017-01-11 | 2017-06-20 | 北京长江脉医药科技有限责任公司 | A kind of unitary Peracetic acid solid particle disinfectant |
| CN106879593A (en) * | 2017-01-11 | 2017-06-23 | 北京长江脉医药科技有限责任公司 | A kind of alkalescent low corrosion Peracetic acid effervescent tablet disinfectant |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108849893A (en) * | 2018-07-27 | 2018-11-23 | 佛山市南海东方澳龙制药有限公司 | Peroxyacetic acid disinfectant and preparation method thereof |
| CN109077054A (en) * | 2018-09-27 | 2018-12-25 | 四川省畜牧科学研究院 | A kind of Peracetic acid composite disinfectant and preparation method thereof |
| CN111357761A (en) * | 2018-12-26 | 2020-07-03 | 哈尔滨三联药业股份有限公司 | Peroxyacetic acid disinfectant and application thereof |
| CN111296443A (en) * | 2020-03-16 | 2020-06-19 | 山东消博士消毒科技股份有限公司 | Disinfectant for cleaning endoscope and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107410310A (en) | A kind of peracetic acid in single-ingredient disinfection solution and preparation method thereof | |
| SI9300695B (en) | Compositions comprising dilute aqueous solutions of lower aliphatic peracids and their use as disifectants | |
| JPH034545B2 (en) | ||
| CN103896217B (en) | A kind of stabilizing agent of hydrogen peroxide | |
| JPH07500378A (en) | Stabilizing composition for inorganic peroxide solutions | |
| CN106857513A (en) | A kind of unitary Peracetic acid solid particle disinfectant | |
| CN108849893A (en) | Peroxyacetic acid disinfectant and preparation method thereof | |
| CN109392903B (en) | Peroxycarboxylic acid disinfectant and preparation method thereof | |
| CN108996629A (en) | Potassium Monopersulfate compound effervescent tablet and preparation method thereof for the improvement of water quality substrate | |
| CN106342883A (en) | Compound hydrogen peroxide sterilization powder | |
| CN102696675A (en) | Stable activation-state javelle water and preparation method thereof | |
| CN108849972A (en) | High concentration peroxy acid disinfectant and preparation method thereof | |
| CN106689197A (en) | Monobasic stable type peroxyacetic acid disinfection solution and preparation method of monobasic stable type peroxyacetic acid disinfection solution | |
| CN102511478B (en) | Stable peroxyacetic acid solution, preparation method thereof and stabilizer for preparation | |
| CN106521507A (en) | Aluminum alloy chemical polishing additive | |
| CN104322488A (en) | High concentrations high stability one-element peracetic acid disinfectant and preparation method thereof | |
| CN114145296A (en) | Peroxyacetic acid liquid generating agent and using method thereof | |
| CN111449067A (en) | Alkalescent peroxyacetic acid solution | |
| JP2010184868A (en) | Peracetic acid aqueous solution excellent in stability | |
| CA2890831C (en) | Method for producing equilibrium peracetic acid and equilibrium peracetic acid obtainable by the method | |
| CN107286482A (en) | A kind of electronic instrument shell plastics | |
| CN107034507A (en) | 7 series alloys process of surface treatment | |
| CN109706464A (en) | A kind of neutrality rust remover and preparation method thereof | |
| WO2005030648A3 (en) | Potassium monopersulfate triple salt with increased active oxygen content and substantially no k2s2o8 | |
| CN110122486A (en) | A kind of stable sodium hypochlorite solution and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171201 |
|
| RJ01 | Rejection of invention patent application after publication |