CN107375033B - Sweet osmanthus essential oil shampoo and preparation method thereof - Google Patents
Sweet osmanthus essential oil shampoo and preparation method thereof Download PDFInfo
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- CN107375033B CN107375033B CN201710688677.2A CN201710688677A CN107375033B CN 107375033 B CN107375033 B CN 107375033B CN 201710688677 A CN201710688677 A CN 201710688677A CN 107375033 B CN107375033 B CN 107375033B
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- essential oil
- osmanthus
- shampoo
- osmanthus essential
- cationic polymer
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 69
- 239000002453 shampoo Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 244000242564 Osmanthus fragrans Species 0.000 title claims description 35
- 235000019083 Osmanthus fragrans Nutrition 0.000 title claims description 35
- 239000000203 mixture Substances 0.000 claims abstract description 51
- 235000019082 Osmanthus Nutrition 0.000 claims abstract description 33
- 241000333181 Osmanthus Species 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229920006317 cationic polymer Polymers 0.000 claims abstract description 27
- 239000004094 surface-active agent Substances 0.000 claims abstract description 26
- 229920000747 poly(lactic acid) Polymers 0.000 claims abstract description 21
- 239000004626 polylactic acid Substances 0.000 claims abstract description 21
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 20
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 20
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 20
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims description 22
- 238000010008 shearing Methods 0.000 claims description 16
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 12
- 241000628997 Flos Species 0.000 claims description 10
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 9
- 229920002907 Guar gum Polymers 0.000 claims description 8
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 claims description 8
- 229940063953 ammonium lauryl sulfate Drugs 0.000 claims description 8
- 229960002154 guar gum Drugs 0.000 claims description 8
- 235000010417 guar gum Nutrition 0.000 claims description 8
- 239000000665 guar gum Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 239000004310 lactic acid Substances 0.000 claims description 6
- 235000014655 lactic acid Nutrition 0.000 claims description 6
- 239000008236 heating water Substances 0.000 claims description 2
- OPVLOHUACNWTQT-UHFFFAOYSA-N azane;2-dodecoxyethyl hydrogen sulfate Chemical compound N.CCCCCCCCCCCCOCCOS(O)(=O)=O OPVLOHUACNWTQT-UHFFFAOYSA-N 0.000 claims 2
- 239000003205 fragrance Substances 0.000 abstract description 16
- 230000002688 persistence Effects 0.000 abstract description 4
- 210000004209 hair Anatomy 0.000 description 15
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 14
- 230000000052 comparative effect Effects 0.000 description 11
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 230000003078 antioxidant effect Effects 0.000 description 4
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 3
- 230000003064 anti-oxidating effect Effects 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 210000003780 hair follicle Anatomy 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 210000004761 scalp Anatomy 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 2
- 235000011130 ammonium sulphate Nutrition 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000004456 color vision Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 239000003797 essential amino acid Substances 0.000 description 2
- 235000020776 essential amino acid Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 238000000338 in vitro Methods 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000031700 light absorption Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 229940079877 pyrogallol Drugs 0.000 description 2
- QBJWYMFTMJFGOL-UHFFFAOYSA-N 2-hexadecyloxirane Chemical compound CCCCCCCCCCCCCCCCC1CO1 QBJWYMFTMJFGOL-UHFFFAOYSA-N 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 230000023852 carbohydrate metabolic process Effects 0.000 description 1
- 235000021256 carbohydrate metabolism Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000009920 chelation Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- RBJABTJRYMHYOP-UHFFFAOYSA-N docosa-1,21-diene Chemical compound C=CCCCCCCCCCCCCCCCCCCC=C RBJABTJRYMHYOP-UHFFFAOYSA-N 0.000 description 1
- OVRWSOABJJYTBD-UHFFFAOYSA-N dodecylazanium;sulfate Chemical compound OS(O)(=O)=O.CCCCCCCCCCCCN.CCCCCCCCCCCCN OVRWSOABJJYTBD-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- FEIOASZZURHTHB-UHFFFAOYSA-N methyl 4-formylbenzoate Chemical compound COC(=O)C1=CC=C(C=O)C=C1 FEIOASZZURHTHB-UHFFFAOYSA-N 0.000 description 1
- UAVVZJIMFHIEJV-UHFFFAOYSA-N methyl 5-ethenylpyridine-3-carboxylate Chemical compound COC(=O)C1=CN=CC(C=C)=C1 UAVVZJIMFHIEJV-UHFFFAOYSA-N 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention relates to an osmanthus essential oil shampoo and a preparation method thereof, the osmanthus essential oil shampoo has fresh and natural fragrance and good fragrance persistence, and consists of an osmanthus essential oil composition, a cationic polymer, a surfactant, polydimethylsiloxane, polylactic acid and deionized water.
Description
Technical Field
The invention relates to osmanthus fragrans essential oil shampoo and a preparation method thereof, and belongs to the field of daily chemicals.
Background
The sweet osmanthus has high utilization value, not only can beautify the environment, but also can be used in chemical industry and food industry, has thick and sweet taste and rich nutrition, and is called as 'full-nutrition food' in the world. The total amino acid content in the sweet osmanthus is up to 13.78 percent, wherein the essential amino acid content in the sweet osmanthus is 6.26 percent, the essential amino acid content accounts for 45.55 percent of the total amino acid content, the proportion of the amino acid in the sweet osmanthus is reasonable, the sweet osmanthus is high-quality protein, in addition, the sweet osmanthus contains rich vitamins and various trace elements, and the contents of potassium, iron and zinc are obviously higher than those of common plants, so the sweet osmanthus has certain effects of beautifying and whitening, activating blood and enriching the blood, promoting the growth and development of human bodies, improving the immunity, reducing the blood pressure, promoting the carbohydrate metabolism and the like.
The osmanthus essential oil is a main bioactive component of the osmanthus, and has important significance for researching chemical components and bioactivity of the osmanthus essential oil. The osmanthus essential oil contains components such as alcohol, ketone, aldehyde, acid, ester, alkane, terpenes and oxygenated derivatives thereof, mainly esters and similar components, contains various bioactive components with application value, and has high content of 5-vinyl-3-pyridinecarboxylic acid methyl ester, p-formylbenzoic acid methyl ester, palmitic acid, 1, 21-docosadiene and 1, 2-epoxyoctadecane, good in-vitro antioxidant activity, and very obvious total reducing power and chelation effect on metal ions.
The main component of hair is protein, which has no physiological function and no self-cleaning or self-repairing function. The hair is polluted due to the fact that the hair is exposed for a long time and does not continuously adsorb dust in the air, the hair becomes greasy and unsmooth, and the protein is easy to be damaged by ultraviolet rays and becomes withered and yellow, hair forks, loops and the like. The osmanthus essential oil shampoo is used as a cleanser for cleaning hair, not only has the function of removing sludge of the hair, but also has unique fragrance, so that people can feel cool and natural, and finally the osmanthus essential oil has a good antioxidation function, so that oxidation aging can be reduced after scalp absorption, the healthy development of hair follicles can be promoted, the health of the hair is fundamentally ensured, however, the osmanthus essential oil has strong volatility and weak adsorbability, and how to retain the osmanthus essential oil in the hair and the scalp for a long time is a great problem.
Disclosure of Invention
In order to achieve the purpose, the invention provides the osmanthus fragrans essential oil shampoo which has lasting fragrance and the effect of repairing hair follicles and hairs, and the embodiment of the invention is as follows:
the osmanthus essential oil shampoo is composed of an osmanthus essential oil composition, a cationic polymer, a surfactant, polydimethylsiloxane, polylactic acid and deionized water, and comprises the following components in proportion:
10 to 30 percent of osmanthus essential oil composition
1 to 3 percent of cationic polymer
5 to 10 percent of surfactant
1 to 5 percent of polydimethylsiloxane
3 to 6 percent of polylactic acid
50 to 70 percent of water
The above proportions are by weight.
The sweet osmanthus essential oil composition consists of sweet osmanthus essential oil, lactic acid and water according to the weight ratio of 1:1:5 in sequence.
The preparation method of the sweet osmanthus essential oil composition comprises the following steps: stirring and mixing flos Osmanthi Fragrantis essential oil and lactic acid, heating water to 50 deg.C, stirring at constant temperature, adding the mixture of flos Osmanthi Fragrantis essential oil and lactic acid, and shearing for 5-10 min at a shearing speed of 10000r/min or more.
The sweet osmanthus essential oil is a substance which is extracted from sweet osmanthus by a conventional extraction method and has unique fragrance and the main component of volatile oil.
Further, the method for extracting the osmanthus essential oil comprises the following steps: taking a proper amount of sweet osmanthus, adding water which is 3 times of the weight of the sweet osmanthus, extracting and refluxing for 3 hours, and collecting volatile oil to obtain the sweet osmanthus essential oil.
The cationic polymer is one or two mixtures of polyquaternium-10 or guar gum hydroxypropyl trimethyl ammonium chloride.
Preferably, the cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1: 2.
The surfactant is one or a mixture of dodecyl alcohol ether ammonium sulfate and dodecyl ammonium sulfate.
Preferably, the surfactant is a mixture of ammonium lauryl alcohol ether sulfate and ammonium lauryl sulfate in a weight ratio of 1: 1.
The molecular weight of the polylactic acid is between 5000-.
The water is deionized water.
Preferably, the osmanthus fragrans essential oil shampoo is composed of the following components:
15 to 25 percent of osmanthus essential oil composition
1 to 3 percent of cationic polymer
6 to 8 percent of surfactant
2 to 4 percent of polydimethylsiloxane
4 to 6 percent of polylactic acid
55 to 65 percent of water
Further, the osmanthus fragrans essential oil shampoo is composed of the following components:
sweet osmanthus essential oil composition 20%
Cationic Polymer 2%
Surfactant 7%
3 percent of polydimethylsiloxane
5 percent of polylactic acid
63 percent of water
Further, the preparation method of the osmanthus fragrans essential oil shampoo comprises the following steps:
1) adding 70 deg.C deionized water into the flos Osmanthi Fragrantis essential oil composition, stirring to dissolve completely
2) Adding cationic polymer, stirring to dissolve completely
3) Adding surfactant, polydimethylsiloxane and polylactic acid, stirring and mixing uniformly, and shearing for 5-10 minutes at a shearing speed of 10000r/min or above.
Further, the preparation method of the osmanthus fragrans essential oil shampoo comprises the following steps:
1) adding 70 deg.C deionized water into the flos Osmanthi Fragrantis essential oil composition, stirring to dissolve completely
2) Adding cationic polymer, stirring to dissolve completely
3) Adding surfactant, polydimethylsiloxane and polylactic acid, stirring and mixing uniformly, and shearing for 8 minutes at the shearing speed of 10000 r/min.
The invention is characterized in that sweet osmanthus essential oil shampoo is composed of a sweet osmanthus essential oil composition, a cationic polymer, a surfactant, polydimethylsiloxane, polylactic acid and deionized water, wherein the sweet osmanthus essential oil has antioxidant, anti-fatigue and antibacterial effects.
The invention is also characterized in that the invention not only treats the osmanthus essential oil, but also fully researches other components, and adds a certain amount of polylactic acid, thereby having a certain slow release effect, protecting the volatilization of the osmanthus essential oil composition, and simultaneously, the polylactic acid can be combined with the grease on the scalp, thereby being convenient for grease removal and playing a role in enhancing the cleaning capability.
The invention has the beneficial effects that:
1. the invention adopts simple preparation process, is easy to enlarge and industrialize and has low cost
2. The osmanthus essential oil shampoo provided by the invention has lasting and pleasant fragrance and can protect hair follicles
Detailed Description
The above invention will now be further described in detail by way of specific examples for better understanding of the gist of the present invention, but the following examples are not to be construed as further limiting the present invention.
Comparative example 1
20 percent of osmanthus essential oil
Cationic Polymer 2%
8 percent of surfactant
3 percent of polydimethylsiloxane
5 percent of polylactic acid
62 percent of water
The cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1:2
The surface active agent is: the weight ratio of the ammonium lauryl alcohol ether sulfate to the ammonium lauryl sulfate is 1: 1.
Comparative example 2
20 percent of osmanthus essential oil
Cationic Polymer 2%
8 percent of surfactant
3 percent of polydimethylsiloxane
67% of water
Comparative example 3
The composition of comparative example 1 was prepared as follows:
1. adding 70 deg.C deionized water into flos Osmanthi Fragrantis essential oil, stirring to dissolve completely
2. Adding cationic polymer, stirring to dissolve completely
3. Adding surfactant, polydimethylsiloxane and polylactic acid, stirring and mixing uniformly, and shearing for 8 minutes at the shearing speed of 10000 r/min.
The composition of comparative example 2 was prepared as follows:
1. adding 70 deg.C deionized water into the flos Osmanthi Fragrantis essential oil composition, stirring to dissolve completely
2. Adding cationic polymer, stirring to dissolve completely
3. Adding surfactant and polydimethylsiloxane, stirring and mixing uniformly, and shearing for 8 minutes at the shearing speed of 10000 r/min.
Example 1
Sweet osmanthus essential oil composition 20%
Cationic Polymer 2%
8 percent of surfactant
3 percent of polydimethylsiloxane
5 percent of polylactic acid
62 percent of water
The cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1: 2.
The surface active agent is: mixture of ammonium lauryl alcohol ether sulfate and ammonium lauryl sulfate in a weight ratio of 1:1
Example 2
10 percent of osmanthus essential oil composition
Cationic polymer 3%
10 percent of surfactant
Polydimethylsiloxane 5%
3 percent of polylactic acid
69 percent of water
The cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1:2
The surface active agent is: the weight ratio of the ammonium lauryl alcohol ether sulfate to the ammonium lauryl sulfate is 1: 1.
Example 3
30 percent of osmanthus essential oil composition
Cationic Polymer 1%
5 percent of surfactant
1% of polydimethylsiloxane
6 percent of polylactic acid
57 percent of water
The cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1:2
The surface active agent is: the weight ratio of the ammonium lauryl alcohol ether sulfate to the ammonium lauryl sulfate is 1: 1.
Example 4
Sweet osmanthus essential oil composition 20%
Polyquaternary ammonium salt-102%
Dodecyl alcohol ether ammonium sulfate 7%
3 percent of polydimethylsiloxane
5 percent of polylactic acid
And (5) 63% of water.
Example 5
Sweet osmanthus essential oil composition 20%
Guar hydroxypropyl trimethyl ammonium chloride 2%
Ammonium lauryl sulfate 7%
3 percent of polydimethylsiloxane
5 percent of polylactic acid
And (5) 63% of water.
Example 6
The compositions obtained in examples 1 to 5 were prepared as follows:
1. adding 70 deg.C deionized water into the flos Osmanthi Fragrantis essential oil composition, stirring to dissolve completely
2. Adding cationic polymer, stirring to dissolve completely
3. Adding surfactant and polydimethylsiloxane, stirring and mixing uniformly, and shearing at the shearing speed of 10000r/min for 8 minutes to obtain the product
Fragrance of the compositions obtained in comparative examples 1-2 and examples 1 to 5 was examined
A proper amount of hair is taken, divided into 7 parts and bundled, each part is 5g, the compositions of comparative examples 1-2 and examples 1-5 are respectively coated on the weight of the hair, 10g of water is added, the hair is gently washed for 5 minutes, and the foam is washed clean by water. Five adults with normal color vision and smell sense judge the flavor of the washed hair bundle, the hair bundle is graded according to the standard of refreshing and natural fragrance, the average value is taken, the higher the grade is, the better the effect is, and the average value result of five grades is as follows:
TABLE 1 fragrance evaluation results of compositions
The compositions obtained in comparative examples 1-2 and examples 1 to 5 were examined for fragrance persistence
3g of each of the compositions of comparative examples 1 to 2 and examples 1 to 5 was applied to a stainless steel plate with an area of 5cm2,Placing in open air, selecting 5 female adults with normal color vision and smell, scoring the fragrance of the composition with refreshing and natural fragrance as standard, taking average value,the higher the score, the better the effect, and the five-digit mean score results are as follows:
TABLE 2 evaluation results of fragrance persistence of compositions
The remark "-" is that there is no fresh natural fragrance at all.
According to the analysis of the results, the osmanthus essential oil shampoo disclosed by the invention has good natural fragrance and good persistence of fragrance.
The compositions obtained in comparative examples 1-2 and examples 1 to 2 were examined for their antioxidant ability
The compositions obtained in comparative examples 1-2 and examples 1-2 were tested for their in vitro anti-oxygen radical capacity, as determined by the pyrogallol method, which produces O by autoxidation of pyrogallol2. Taking 16 tubes of 10mL test tubes with stoppers, No. 1 to No. 16, adding 4.5mL of Tris-HC1 buffer solution with pH value of 8.2, preheating in water bath at 20 ℃ for 20min, adding the composition according to the amount in the following table 3, transferring 1 mL of distilled water and 0.4 mL of pyrogallol solution (45 mmol), reacting in water bath at 25 ℃ for the reaction time as shown in the following table, adding (6 mmol) of HCl solution lmL to terminate the reaction, and measuring the light absorption A at 420nm wavelengthSample (I). And calculating the inhibition rate. Detecting the control absorbance value A by the same methodControl。
Inhibition rate = (a)Contrast-ASample (I))／AControlx 100％
In the formula AControlAbsorbance values measured for the control group; a. theSample (I)Is the light absorption value after adding the extracting solution for reaction.
TABLE 3 composition description table
TABLE 4 test tube number and test schedule
Remarking: test tube No. 1/5/9/13 was tested for antioxidant capacity for 2 hours, and so on.
TABLE 5 Oxidation resistance results table
The result shows that the shampoo disclosed by the invention has a good effect on antioxidation and also has a remarkable effect on continuous antioxidation.
The above-described embodiments are not intended to limit the present invention in any manner, and those skilled in the art can make many possible variations and modifications to the technical solution of the present invention using the above-disclosed technical contents, or modify equivalent embodiments with equivalent variations, without departing from the scope of the technical solution of the present invention. Therefore, any simple modification, equivalent change and modification made to the above embodiments according to the technical spirit of the present invention should fall within the protection scope of the technical scheme of the present invention, unless the technical spirit of the present invention departs from the content of the technical scheme of the present invention.
Claims (8)
1. The osmanthus essential oil shampoo is composed of an osmanthus essential oil composition, a cationic polymer, a surfactant, polydimethylsiloxane, polylactic acid and deionized water, and is characterized by comprising the following components in percentage by weight:
the above-mentioned proportion is a weight ratio,
the sweet osmanthus essential oil composition consists of sweet osmanthus essential oil, lactic acid and water according to the weight ratio of 1:1:5 in sequence,
the preparation method of the sweet osmanthus essential oil composition comprises the following steps: stirring and mixing flos Osmanthi Fragrantis essential oil and lactic acid, heating water to 50 deg.C, stirring at constant temperature, adding the mixture of flos Osmanthi Fragrantis essential oil and lactic acid, and shearing for 5-10 min at a shearing speed of 10000r/min or more.
2. The osmanthus essential oil shampoo as claimed in claim 1, wherein the cationic polymer is one or a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride.
3. The osmanthus essential oil shampoo as claimed in claim 2, wherein the cationic polymer is a mixture of polyquaternium-10 and guar gum hydroxypropyl trimethyl ammonium chloride in a weight ratio of 1: 2.
4. The osmanthus essential oil shampoo as claimed in claim 1, wherein the surfactant is one or a mixture of ammonium lauryl ether sulfate and ammonium lauryl sulfate.
5. The osmanthus essential oil shampoo as claimed in claim 4, wherein the surfactant is a mixture of ammonium lauryl ether sulfate and ammonium lauryl sulfate in a weight ratio of 1: 1.
6. The shampoo containing osmanthus essential oil as claimed in claim 1, wherein the molecular weight of the polylactic acid is between 5000-15000.
7. The osmanthus essential oil shampoo according to claim 1, characterized in that the osmanthus essential oil shampoo is composed of the following components:
8. the osmanthus fragrans essential oil shampoo according to claim 1, characterized in that the preparation method of the osmanthus fragrans essential oil shampoo comprises the following steps:
(1) adding 70 deg.C deionized water into the flos Osmanthi Fragrantis essential oil composition, stirring to dissolve completely,
(2) adding the cationic polymer, stirring until the cationic polymer is completely dissolved,
(3) adding surfactant, polydimethylsiloxane and polylactic acid, stirring and mixing uniformly, and shearing for 5-10 minutes at a shearing speed of 10000r/min or above.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102772326A (en) * | 2012-07-10 | 2012-11-14 | 江苏天辅星光学材料有限公司 | Hair conditioner |
| CN104248556A (en) * | 2013-06-28 | 2014-12-31 | 青岛康泰鑫环保科技有限公司 | Plant hair conditioner |
| CN104398459A (en) * | 2014-11-27 | 2015-03-11 | 青岛市市南区隆德中医药研究所 | Shampoo with flavor of osmanthus |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102772326A (en) * | 2012-07-10 | 2012-11-14 | 江苏天辅星光学材料有限公司 | Hair conditioner |
| CN104248556A (en) * | 2013-06-28 | 2014-12-31 | 青岛康泰鑫环保科技有限公司 | Plant hair conditioner |
| CN104398459A (en) * | 2014-11-27 | 2015-03-11 | 青岛市市南区隆德中医药研究所 | Shampoo with flavor of osmanthus |
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| 《桂花有效成分合成转化规律与药学研究》;王丽梅;《桂花有效成分合成转化规律与药学研究》;20090501;第12页 * |
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