CN107354721A - A kind of preparation method of multiple-effect non-woven fabrics - Google Patents
A kind of preparation method of multiple-effect non-woven fabrics Download PDFInfo
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- CN107354721A CN107354721A CN201710542061.4A CN201710542061A CN107354721A CN 107354721 A CN107354721 A CN 107354721A CN 201710542061 A CN201710542061 A CN 201710542061A CN 107354721 A CN107354721 A CN 107354721A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2243—Mono-, di-, or triglycerides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/228—Cyclic esters, e.g. lactones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/20—Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention discloses a kind of preparation method of multiple-effect non-woven fabrics, including following operating procedure：（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter after 90 100 μm, to be well mixed with the activated carbon that average grain diameter is 40 60 μm, it is standby after drying；（2）After ester gum, frankincense gum are mixed, 45 60 DEG C are heated the mixture to using heating water bath, then adds additive thereto, continues to add step thereto after stirring（1）Gained material, continue after stirring, maceration extract is made；（3）By step（2）Gained maceration extract is cooled to 35 40 DEG C, then puts into maceration extract non-woven fabrics after stopping 2 5min, takes out finished product after pressure roller is dried.The preparation technology of multiple-effect non-woven fabrics provided by the invention is simple, and obtained non-woven fabrics adsorption capacity is superior, and the adsorbing medium in non-woven fabrics is evenly distributed, difficult for drop-off during use, and service life is longer, greatly improves the quality of non-woven fabrics.
Description
Technical field
The invention belongs to non-woven fabrics preparation field, and in particular to a kind of preparation method of multiple-effect non-woven fabrics.
Background technology
Bonded fabric product is rich in color, bright-coloured bright and beautiful, Eco-Fashion, widely used, elegant in appearance, and pattern and style are all more
Sample, and it is light, environmentally friendly, recyclable, by the internationally recognized environment-friendly products for ecology of preserving our planet.Suitable for agricultural film,
The industries such as shoemaking, process hides, mattress, child-mother-covering, decoration, chemical industry, printing, automobile, building materials, furniture, and dress lining cloth, health care
The gift bag of disposable surgical clothing, mouth mask, cap, sheet, the disposable tablecloth in hotel, beauty, Saunas or even current fashion, fine work
Bag, shopping bag, advertising bag etc..There is the active carbon nonwoven fabric for having stronger adsorption capacity to harmful substance in air in the market
Sell, it is to be bonded together activated carbon and non-woven fabrics with binding agent, but its comparison of ingredients is single, therefore its adsorption effect
It is not very notable, and binding agent is perishable, causes activated carbon to be easy to come off, and greatly affected the quality of non-woven fabrics.
The content of the invention
It is an object of the invention to provide a kind of preparation method of multiple-effect non-woven fabrics.
The present invention is achieved by the following technical solutions.
A kind of preparation method of multiple-effect non-woven fabrics, including following operating procedure：
（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter as after 90-100 μm, with average grain diameter
It is well mixed for 40-60 μm of activated carbon, it is standby after drying；
（2）After ester gum, frankincense gum are mixed, 45-60 DEG C is heated the mixture to using heating water bath, then add mixing thereto
0.01 times of heavy additive of thing gross weight, continues to add step thereto after stirring（1）Gained material, continue to stir
Afterwards, maceration extract is made, wherein additive is made up of the component of following parts by weight：4- dodecalactone 5-7 parts, lilac daphne 33-36 parts, five
Color plum 32-34 parts, balsamine 20-25 parts, D-ALPHA-Hydroxypropionic acid methyl esters 3-5 parts, dispersant 1-2 parts, surfactant 1-2 parts；
（3）By step（2）Gained maceration extract is cooled to 35-40 DEG C, then puts into non-woven fabrics in maceration extract after stopping 2-5min,
Take out finished product after pressure roller is dried.
Specifically, the step（1）In drying temperature be 40-50 DEG C, the time of drying is 80-100min.
Specifically, the step（2）The mass ratio of middle ester gum and frankincense gum is 1:1, and ester gum and step（1）Middle mixture
Mass ratio be 1:10-15.
Specifically, the step（2）In dispersant for glyceryl monostearate, it is any one in glyceryl tristearate
Kind.
Specifically, the step（2）In surfactant for fatty glyceride, fatty acid sorbitan, polysorbate
In any one.
Specifically, the step（2）The preparation method of middle additive includes following operating procedure：（1）By lilac daphne, the five colors
After plum, balsamine mixing, 6 times of heavy absolute ethyl alcohols of its weight are added, refluxing extraction filtered extract solution after 2 hours, then will filter
The colored extract solution of mixing is made after crossing liquid recovery ethanol；（2）By step（1）In the extract solution and 4- 12 of the mixing flower of gained
After ester, D-ALPHA-Hydroxypropionic acid methyl esters, dispersant, surfactant are well mixed, additive is made.
Technical scheme more than, the beneficial effects of the invention are as follows：
The preparation technology of multiple-effect non-woven fabrics provided by the invention is simple, and obtained non-woven fabrics adsorption capacity is superior, in non-woven fabrics
Adsorbing medium is evenly distributed, difficult for drop-off during use, and service life is longer, greatly improves the product of non-woven fabrics
Matter.Wherein, after betel nut maturation dry seed, Aplotaxis auriculata dry root and activated carbon synergy, the energy of adsorption of activated carbon can be increased
Power, and after betel nut maturation dry seed, Aplotaxis auriculata dry root are ground into powder, itself also has excellent adsorption capacity,
And with the function of suppressing pathogen growth breeding；D-ALPHA-Hydroxypropionic acid methyl esters, 4- dodecalactones can not only strengthen ester gum, frankincense gum it is viscous
Knot ability, and its unique perfume for having, it can effectively lift the quality of non-woven fabrics；Having in lilac daphne, Lantana camara, balsamine
After imitating composition synergy, the oxidation resistance of binding agent can be not only lifted, the material oxidation for preventing binding agent to be adsorbed
Cohesive force is lost, extends the shelf-life of binding agent, and the germ to being infected with thereon has potent inhibitory action, finally makes
The obtained existing excellent absorption cleaning effect of non-woven fabrics, has excellent fungistatic effect again.
Embodiment
In order that those skilled in the art can be further understood that the feature and technology contents of the present invention, referring to following has
Close detailed description of the invention.
Embodiment 1
A kind of preparation method of multiple-effect non-woven fabrics, including following operating procedure：
（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter to be 40 μ with average grain diameter after 90 μm
M activated carbon is well mixed, standby after drying；
（2）After ester gum, frankincense gum are mixed, 45 DEG C are heated the mixture to using heating water bath, then add mixture thereto
0.01 times of heavy additive of gross weight, continues to add step thereto after stirring（1）Gained material, continue to stir
Afterwards, maceration extract is made, wherein additive is made up of the component of following parts by weight：5 parts of 4- dodecalactones, 33 parts of lilac daphne, Lantana camara
32 parts, 20 parts of balsamine, 3 parts of D-ALPHA-Hydroxypropionic acid methyl esters, 1 part of dispersant, 1 part of surfactant；
（3）By step（2）Gained maceration extract is cooled to 35 DEG C, then puts into maceration extract non-woven fabrics after stopping 2min, takes out
Finished product after pressure roller is dried.
Specifically, the step（1）In drying temperature be 40 DEG C, the time of drying is 80min.
Specifically, the step（2）The mass ratio of middle ester gum and frankincense gum is 1:1, and ester gum and step（1）Middle mixture
Mass ratio be 1:10.
Specifically, the step（2）In dispersant be glyceryl monostearate.
Specifically, the step（2）In surfactant be fatty glyceride.
Specifically, the step（2）The preparation method of middle additive includes following operating procedure：（1）By lilac daphne, the five colors
After plum, balsamine mixing, 6 times of heavy absolute ethyl alcohols of its weight are added, refluxing extraction filtered extract solution after 2 hours, then will filter
The colored extract solution of mixing is made after crossing liquid recovery ethanol；（2）By step（1）In the extract solution and 4- 12 of the mixing flower of gained
After ester, D-ALPHA-Hydroxypropionic acid methyl esters, dispersant, surfactant are well mixed, additive is made.
Embodiment 2
A kind of preparation method of multiple-effect non-woven fabrics, including following operating procedure：
（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter to be 50 μ with average grain diameter after 95 μm
M activated carbon is well mixed, standby after drying；
（2）After ester gum, frankincense gum are mixed, 50 DEG C are heated the mixture to using heating water bath, then add mixture thereto
0.01 times of heavy additive of gross weight, continues to add step thereto after stirring（1）Gained material, continue to stir
Afterwards, maceration extract is made, wherein additive is made up of the component of following parts by weight：6 parts of 4- dodecalactones, 35 parts of lilac daphne, Lantana camara
33 parts, 23 parts of balsamine, 4 parts of D-ALPHA-Hydroxypropionic acid methyl esters, 1 part of dispersant, 2 parts of surfactant；
（3）By step（2）Gained maceration extract is cooled to 37 DEG C, then puts into maceration extract non-woven fabrics after stopping 3min, takes out
Finished product after pressure roller is dried.
Specifically, the step（1）In drying temperature be 45 DEG C, the time of drying is 90min.
Specifically, the step（2）The mass ratio of middle ester gum and frankincense gum is 1:1, and ester gum and step（1）Middle mixture
Mass ratio be 1:13.
Specifically, the step（2）In dispersant be glyceryl tristearate.
Specifically, the step（2）In surfactant be fatty acid sorbitan.
Specifically, the step（2）The preparation method of middle additive includes following operating procedure：（1）By lilac daphne, the five colors
After plum, balsamine mixing, 6 times of heavy absolute ethyl alcohols of its weight are added, refluxing extraction filtered extract solution after 2 hours, then will filter
The colored extract solution of mixing is made after crossing liquid recovery ethanol；（2）By step（1）In the extract solution and 4- 12 of the mixing flower of gained
After ester, D-ALPHA-Hydroxypropionic acid methyl esters, dispersant, surfactant are well mixed, additive is made.
Embodiment 3
A kind of preparation method of multiple-effect non-woven fabrics, including following operating procedure：
（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter to be 60 with average grain diameter after 100 μm
μm activated carbon be well mixed, it is standby after drying；
（2）After ester gum, frankincense gum are mixed, 60 DEG C are heated the mixture to using heating water bath, then add mixture thereto
0.01 times of heavy additive of gross weight, continues to add step thereto after stirring（1）Gained material, continue to stir
Afterwards, maceration extract is made, wherein additive is made up of the component of following parts by weight：7 parts of 4- dodecalactones, 36 parts of lilac daphne, Lantana camara
34 parts, 25 parts of balsamine, 5 parts of D-ALPHA-Hydroxypropionic acid methyl esters, 2 parts of dispersant, 2 parts of surfactant；
（3）By step（2）Gained maceration extract is cooled to 40 DEG C, then puts into maceration extract non-woven fabrics after stopping 5min, takes out
Finished product after pressure roller is dried.
Specifically, the step（1）In drying temperature be 50 DEG C, the time of drying is 100min.
Specifically, the step（2）The mass ratio of middle ester gum and frankincense gum is 1:1, and ester gum and step（1）Middle mixture
Mass ratio be 1:15.
Specifically, the step（2）In dispersant be glyceryl tristearate.
Specifically, the step（2）In surfactant be polysorbate.
Specifically, the step（2）The preparation method of middle additive includes following operating procedure：（1）By lilac daphne, the five colors
After plum, balsamine mixing, 6 times of heavy absolute ethyl alcohols of its weight are added, refluxing extraction filtered extract solution after 2 hours, then will filter
The colored extract solution of mixing is made after crossing liquid recovery ethanol；（2）By step（1）In the extract solution and 4- 12 of the mixing flower of gained
After ester, D-ALPHA-Hydroxypropionic acid methyl esters, dispersant, surfactant are well mixed, additive is made.
Comparative example 1
Betel nut maturation dry seed and Aplotaxis auriculata dry root composition are not added, and remaining manufacture method is identical with embodiment 1.
Multiple-effect non-woven fabrics is made with the method in embodiment and comparative example respectively, wherein non-woven fabrics is melt spraying non-woven fabrics,
Material is polypropylene, and the energy of adsorption of non-woven fabrics is then tested according to the method in national standard GB/T 13803.1-13803.5-1999
Power, test result are as shown in table 1：
The adsorption effect checking of the multiple-effect non-woven fabrics of table 1
| Project | Iodine sorption value mg/g | Adsorption of Phenol value mg/g |
| Embodiment 1 | 597 | 86.4 |
| Embodiment 2 | 602 | 87.8 |
| Embodiment 3 | 608 | 89.0 |
| Comparative example | 493 | 60.1 |
As shown in Table 1, multiple-effect non-woven fabrics adsorption capacity produced by the present invention is notable, and service life is longer, the absorption adhered to
Property medium is difficult for drop-off, and has certain fungistatic effect, greatly improves the quality of non-woven fabrics.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the technology of invention
Scheme is modified or equivalent substitution, and without departing from the scope of technical solution of the present invention, it all should cover the power in the present invention
In sharp claimed range.
Claims (6)
1. a kind of preparation method of multiple-effect non-woven fabrics, it is characterised in that including following operating procedure：
（1）Betel nut maturation dry seed and Aplotaxis auriculata dry root are ground into average grain diameter as after 90-100 μm, with average grain diameter
It is well mixed for 40-60 μm of activated carbon, it is standby after drying；
（2）After ester gum, frankincense gum are mixed, 45-60 DEG C is heated the mixture to using heating water bath, then add mixing thereto
0.01 times of heavy additive of thing gross weight, continues to add step thereto after stirring（1）Gained material, continue to stir
Afterwards, maceration extract is made, wherein additive is made up of the component of following parts by weight：4- dodecalactone 5-7 parts, lilac daphne 33-36 parts, five
Color plum 32-34 parts, balsamine 20-25 parts, D-ALPHA-Hydroxypropionic acid methyl esters 3-5 parts, dispersant 1-2 parts, surfactant 1-2 parts；
（3）By step（2）Gained maceration extract is cooled to 35-40 DEG C, then puts into non-woven fabrics in maceration extract after stopping 2-5min,
Take out finished product after pressure roller is dried.
2. according to a kind of preparation method of multiple-effect non-woven fabrics described in claim 1, it is characterised in that step（1）In baking
Dry temperature is 40-50 DEG C, and the time of drying is 80-100min.
3. according to a kind of preparation method of multiple-effect non-woven fabrics described in claim 1, it is characterised in that step（2）Middle ester gum
Mass ratio with frankincense gum is 1:1, and ester gum and step（1）The mass ratio of middle mixture is 1:10-15.
4. according to a kind of preparation method of multiple-effect non-woven fabrics described in claim 1, it is characterised in that step（2）In point
Powder is any one in glyceryl monostearate, glyceryl tristearate.
5. according to a kind of preparation method of multiple-effect non-woven fabrics described in claim 1, it is characterised in that step（2）In table
Face activating agent is any one in fatty glyceride, fatty acid sorbitan, polysorbate.
6. according to a kind of preparation method of multiple-effect non-woven fabrics described in claim 1, it is characterised in that step（2）Middle addition
The preparation method of agent includes following operating procedure：（1）After lilac daphne, Lantana camara, balsamine are mixed, it is heavy to add 6 times of its weight
Absolute ethyl alcohol, refluxing extraction filtered extract solution after 2 hours, then the colored extract solution of mixing is made after filtered solution is reclaimed into ethanol；
（2）By step（1）The extract solution of the mixing flower of gained mixes with 4- dodecalactones, D-ALPHA-Hydroxypropionic acid methyl esters, dispersant, surfactant
After uniformly, additive is made.
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| CN201710542061.4A CN107354721A (en) | 2017-07-05 | 2017-07-05 | A kind of preparation method of multiple-effect non-woven fabrics |
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| CN201710542061.4A CN107354721A (en) | 2017-07-05 | 2017-07-05 | A kind of preparation method of multiple-effect non-woven fabrics |
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Citations (3)
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| CN101161140A (en) * | 2007-11-28 | 2008-04-16 | 盛虹集团有限公司 | Healthy tie capable of permanently emitting negative ions |
| CN101225598A (en) * | 2007-11-28 | 2008-07-23 | 盛虹集团有限公司 | Color lining cloth capable of emitting negative ions |
| CN105054401A (en) * | 2014-07-06 | 2015-11-18 | 耿云花 | Modified nanometer bamboo charcoal mask |
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2017
- 2017-07-05 CN CN201710542061.4A patent/CN107354721A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101161140A (en) * | 2007-11-28 | 2008-04-16 | 盛虹集团有限公司 | Healthy tie capable of permanently emitting negative ions |
| CN101225598A (en) * | 2007-11-28 | 2008-07-23 | 盛虹集团有限公司 | Color lining cloth capable of emitting negative ions |
| CN105054401A (en) * | 2014-07-06 | 2015-11-18 | 耿云花 | Modified nanometer bamboo charcoal mask |
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