CN107344056A - A kind of pure plant removes the preparation method of formaldehyde formulations - Google Patents

A kind of pure plant removes the preparation method of formaldehyde formulations Download PDF

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Publication number
CN107344056A
CN107344056A CN201710746843.XA CN201710746843A CN107344056A CN 107344056 A CN107344056 A CN 107344056A CN 201710746843 A CN201710746843 A CN 201710746843A CN 107344056 A CN107344056 A CN 107344056A
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CN
China
Prior art keywords
preparation
removes
plant
formaldehyde
formaldehyde formulations
Prior art date
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Pending
Application number
CN201710746843.XA
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Chinese (zh)
Inventor
刘庆勇
孙德强
刘鸣
刘一鸣
刘玉伟
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Shandong Hengnuo Environmental Protection Technology Co Ltd
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Shandong Hengnuo Environmental Protection Technology Co Ltd
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Priority to CN201710746843.XA priority Critical patent/CN107344056A/en
Publication of CN107344056A publication Critical patent/CN107344056A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702Hydrocarbons
    • B01D2257/7022Aliphatic hydrocarbons

Abstract

The present invention discloses the preparation method that a kind of pure plant removes formaldehyde formulations, formulation composition is simple, sophisticated technologies, the harmful substance in formaldehyde and air can effectively be removed, and human body can be helped to discharge harmful substance, reduce harm of the pernicious gas to body, the present invention can also effectively economize on resources, and reduce use cost, do not have secondary pollution to human body and environment.

Description

A kind of pure plant removes the preparation method of formaldehyde formulations
Technical field
The present invention relates to remove the preparation method of formaldehyde formulations except formaldehyde technical field, more particularly to a kind of pure plant.
Background technology
State Administration for Quality Supervision and Inspection and Quarantine and national standardization administration committee ratified to send out on December 10th, 2001 Cloth, and 10 standards on indoor decorating and refurnishing materials limits of harmful substances implemented on January 1st, 2002, wherein just having 8 Item is related to formaldehyde.Formaldehyde (HCHO) is a kind of colourless readily soluble irritative gas, can be absorbed through respiratory tract, by world health Tissue is defined as suspicious carcinogenic and causes deformed material.Influence of the formaldehyde to health is mainly manifested in allotriosmia, stimulation, mistake Quick, abnormal pulmonary function, dysfunction of liver, immunologic dysfunction etc..Just have when content is 0.lmg/m3 in room air Peculiar smell and sense of discomfort;0.5mg/m3 can stimulate eyes to cause and shed tears;Cause throat discomfort or pain during 0.6mg/m3;Concentration is high again Nausea and vomiting, cough, uncomfortable in chest, asthma even pulmonary emphysema can be caused;Death can be caused at once when reaching 30mg/m3 in air.
The existing formaldehyde scavenger in China is generally inefficient, and the overwhelming majority is chemical reagent formaldehyde scavenger, easily Cause secondary pollution.For the main feature of current room air pollution, for the purpose of eliminating formaldehyde pollution and microorganism pollution, The formaldehyde scavenger that in the market is almost prepared without selection natural plants and traditional Chinese herbal medicine for raw material.Natural plants and natural Chinese herbal medicine, nature is come from, and be the material that humans and animals are most easily accepted by, and the composition portion of human environment ecosystem circulation Point, therefore say on the whole, natural goods and Chinese herbal medicine will not form malicious secondary residual and public hazards.
The content of the invention
The present invention mainly solves the technical problem present in existing product, so as to provide a kind of plant except formaldehyde formulations Preparation method, methods described step are as follows:
(1)3 parts of Tea Polyphenols, 4 parts of aloe, 0.5 part of theanine, 0.4 part of radix glycyrrhizae, 0.3 part of the tuber of dwarf lilyturf, 0.1 part of selenium, natural antibacterial are taken 2 parts of Chinese herbal medicine, after mixing, then carry out residue filter and go out large particulate matter, obtain the liquid of preparation 95%;
(2)Toward step(1)Glycerine and pure water are added in obtained fine liquid, is completely dissolved with after adsorption precipitation, obtains Clear liquid;
(3)By step(2)Obtained supernatant is put into rotary evaporator, and by 1:0.5 ratio adds DBSA The immersion of sodium, centrifuge 40 minutes, collect high-purity supernatant;
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)The middle aqueous solution using neopelex, Soak time is l-3 hours, is produced under temperature=34 DEG C, pressure=8.1MP states.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, and the natural antibacterial Chinese herbal medicine is honeysuckle, folium artemisiae argyi, mattress Old and dried orange peel.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(1)Also comprise the following steps before:
Honeysuckle 259, folium artemisiae argyi 259, oriental wormwood 259, dried orange peel 259 are weighed, is fitted into after mashing in distilling flask, is sequentially added by upper table Distilled water, it is heated to reflux after soaking the regular hour, volatile oil together volatilizees in company with vapor, condenses in extractor, distills Finish.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(2)The glycerine of middle addition is the sweet of 25%-60.5% Oil.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)Also comprise the following steps afterwards:
Plant is put into high-purity supernatant, the diffusion of high-purity supernatant is penetrated into inside plant and in internal capillary gap, led to The solution crossed in the micropore passage of plant diffuses to the stepping of going forward side by side of plant surface and enters solvent.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, the active matter content of described neopelex For 30%~40%, unsaponifiable matter content 3%, pH value is about 8.
Above formulation composition is simple, sophisticated technologies, can effectively remove the harmful substance in formaldehyde and air, and can be with Human body discharge harmful substance is helped, reduces harm of the pernicious gas to body, the present invention can also effectively economize on resources, and reduce Use cost, there is no secondary pollution to human body and environment.
Embodiment
With reference to specific embodiment, the invention will be further described:
Embodiment one:
A kind of plant removes the preparation method of formaldehyde formulations, and methods described step is as follows:
(1)3 parts of Tea Polyphenols, 4 parts of aloe, 0.5 part of theanine, 0.4 part of radix glycyrrhizae, 0.3 part of the tuber of dwarf lilyturf, 0.1 part of selenium, natural antibacterial are taken 2 parts of Chinese herbal medicine, after mixing, then carry out residue filter and go out large particulate matter, obtain the liquid of preparation 95%;
(2)Toward step(1)Glycerine and pure water are added in obtained fine liquid, is completely dissolved with after adsorption precipitation, obtains Clear liquid;
(3)By step(2)Obtained supernatant is put into rotary evaporator, and by 1:0.5 ratio adds DBSA The immersion of sodium, centrifuge 40 minutes, collect high-purity supernatant;
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)The middle aqueous solution using neopelex, Soak time is l-3 hours, is produced under temperature=34 DEG C, pressure=8.1MP states.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, and the natural antibacterial Chinese herbal medicine is honeysuckle, folium artemisiae argyi, mattress Old and dried orange peel.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(1)Also comprise the following steps before:
Honeysuckle 259, folium artemisiae argyi 259, oriental wormwood 259, dried orange peel 259 are weighed, is fitted into after mashing in distilling flask, is sequentially added by upper table Distilled water, it is heated to reflux after soaking the regular hour, volatile oil together volatilizees in company with vapor, condenses in extractor, distills Finish.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(2)The glycerine of middle addition is the sweet of 25%-60.5% Oil.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)Also comprise the following steps afterwards:
Plant is put into high-purity supernatant, the diffusion of high-purity supernatant is penetrated into inside plant and in internal capillary gap, led to The solution crossed in the micropore passage of plant diffuses to the stepping of going forward side by side of plant surface and enters solvent.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, the active matter content of described neopelex For 30%~40%, unsaponifiable matter content 3%, pH value is about 8.
Embodiment two:
(1)3.5 parts of Tea Polyphenols is taken, 3 parts of aloe, 1.5 parts of theanine, 0.2 part of radix glycyrrhizae, 0.5 part of the tuber of dwarf lilyturf, 0.3 part of selenium is natural anti- 3 parts of bacterium Chinese herbal medicine, after mixing, then carry out residue filter and go out large particulate matter, obtain the liquid of preparation 95%;
(2)Toward step(1)Glycerine and pure water are added in obtained fine liquid, is completely dissolved with after adsorption precipitation, obtains Clear liquid;
(3)By step(2)Obtained supernatant is put into rotary evaporator, and by 1:0.7 ratio adds DBSA The immersion of sodium, centrifuge 50 minutes, collect high-purity supernatant;
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)The middle aqueous solution using neopelex, Soak time is l-2.5 hours, is produced under temperature=40 DEG C, pressure=8.2MP states.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, and the natural antibacterial Chinese herbal medicine is honeysuckle, folium artemisiae argyi, mattress Old and dried orange peel.
Embodiment three:
(1)2.5 parts of Tea Polyphenols, 1 part of aloe, 3 parts of theanine, 0.7 part of radix glycyrrhizae, 0.9 part of the tuber of dwarf lilyturf, 0.5 part of selenium, natural antibacterial are taken 5 parts of Chinese herbal medicine, after mixing, then carry out residue filter and go out large particulate matter, obtain the liquid of preparation 95%;
(2)Toward step(1)Glycerine and pure water are added in obtained fine liquid, is completely dissolved with after adsorption precipitation, obtains Clear liquid;
(3)By step(2)Obtained supernatant is put into rotary evaporator, and by 1:0.9 ratio adds DBSA The immersion of sodium, centrifuge 60 minutes, collect high-purity supernatant;
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, step(3)The middle aqueous solution using neopelex, Soak time is l-2 hours, is produced under temperature=50 DEG C, pressure=9MP states.
A kind of above-mentioned plant removes the preparation method of formaldehyde formulations, and the natural antibacterial Chinese herbal medicine is honeysuckle, folium artemisiae argyi, mattress Old and dried orange peel.
Obviously, above-described embodiment is only intended to clearly illustrate example, rather than whole embodiments, and does not have to To limit the present invention.For those of ordinary skill in the field, within the spirit and principles of the invention, made Any modification, equivalent substitution and improvements etc., should be included in the scope of the protection.

Claims (7)

1. a kind of plant removes the preparation method of formaldehyde formulations, it is characterised in that methods described step is as follows:
(1)3 parts of Tea Polyphenols, 4 parts of aloe, 0.5 part of theanine, 0.4 part of radix glycyrrhizae, 0.3 part of the tuber of dwarf lilyturf, 0.1 part of selenium, natural antibacterial are taken 2 parts of Chinese herbal medicine, after mixing, then carry out residue filter and go out large particulate matter, obtain the liquid of preparation 95%;
(2)Toward step(1)Glycerine and pure water are added in obtained fine liquid, is completely dissolved with after adsorption precipitation, obtains Clear liquid;
(3)By step(2)Obtained supernatant is put into rotary evaporator, and by 1:0.5 ratio adds DBSA The immersion of sodium, centrifuge 40 minutes, collect high-purity supernatant.
2. a kind of plant according to claim 1 removes the preparation method of formaldehyde formulations, it is characterised in that step(3)Middle use The aqueous solution of neopelex, soak time are l-3 hours, are made under temperature=34 DEG C, pressure=8.1MP states Take.
3. a kind of plant according to claim 1 removes the preparation method of formaldehyde formulations, it is characterised in that the natural antibacterial Chinese herbal medicine is honeysuckle, folium artemisiae argyi, oriental wormwood and dried orange peel.
4. a kind of plant according to claim 3 removes the preparation method of formaldehyde formulations, it is characterised in that step(1)Also before Comprise the following steps:
Honeysuckle 259, folium artemisiae argyi 259, oriental wormwood 259, dried orange peel 259 are weighed, is fitted into after mashing in distilling flask, is sequentially added by upper table Distilled water, it is heated to reflux after soaking the regular hour, volatile oil together volatilizees in company with vapor, condenses in extractor, distills Finish.
5. a kind of plant according to claim 1 removes the preparation method of formaldehyde formulations, it is characterised in that step(2)Middle addition Glycerine be 25%-60.5% glycerine.
6. a kind of plant according to claim 1 removes the preparation method of formaldehyde formulations, it is characterised in that step(3)Afterwards also Comprise the following steps:
Plant is put into high-purity supernatant, the diffusion of high-purity supernatant is penetrated into inside plant and in internal capillary gap, led to The solution crossed in the micropore passage of plant diffuses to the stepping of going forward side by side of plant surface and enters solvent.
7. a kind of plant according to claim 1 removes the preparation method of formaldehyde formulations, described neopelex Active matter content be 30%~40%, unsaponifiable matter content 3%, pH value is about 8.
CN201710746843.XA 2017-08-27 2017-08-27 A kind of pure plant removes the preparation method of formaldehyde formulations Pending CN107344056A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111345296A (en) * 2018-12-21 2020-06-30 南京科翼新材料有限公司 Glyphosate aqueous agent synergistic auxiliary agent with formaldehyde removing function and preparation method thereof

Citations (5)

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Publication number Priority date Publication date Assignee Title
CN103721288A (en) * 2013-12-10 2014-04-16 宿州军创佳美环保科技有限公司 Traditional Chinese medicine aldehyde-removing air purifying agent and preparation method thereof
CN104785088A (en) * 2015-04-02 2015-07-22 龚娟 Preparation method for formaldehyde scavenger
CN105920998A (en) * 2016-07-07 2016-09-07 山东冬瑞高新技术开发有限公司 Formaldehyde degradation spray for Chinese herbal components
CN108522554A (en) * 2017-03-06 2018-09-14 金远来 A kind of compound and preparation method thereof to eliminate the unusual smell except formaldehyde plant extraction liquid
CN109381983A (en) * 2018-10-31 2019-02-26 龙舟 A kind of compound formaldehyde of pure plant, odor scavenging agent and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103721288A (en) * 2013-12-10 2014-04-16 宿州军创佳美环保科技有限公司 Traditional Chinese medicine aldehyde-removing air purifying agent and preparation method thereof
CN104785088A (en) * 2015-04-02 2015-07-22 龚娟 Preparation method for formaldehyde scavenger
CN105920998A (en) * 2016-07-07 2016-09-07 山东冬瑞高新技术开发有限公司 Formaldehyde degradation spray for Chinese herbal components
CN108522554A (en) * 2017-03-06 2018-09-14 金远来 A kind of compound and preparation method thereof to eliminate the unusual smell except formaldehyde plant extraction liquid
CN109381983A (en) * 2018-10-31 2019-02-26 龙舟 A kind of compound formaldehyde of pure plant, odor scavenging agent and preparation method thereof

Non-Patent Citations (1)

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Title
谢洪柱: "中草药空气清新剂的制备及其净化室内空气的研究", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111345296A (en) * 2018-12-21 2020-06-30 南京科翼新材料有限公司 Glyphosate aqueous agent synergistic auxiliary agent with formaldehyde removing function and preparation method thereof

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