CN107338000A - A kind of fireproof coating and preparation method thereof - Google Patents
A kind of fireproof coating and preparation method thereof Download PDFInfo
- Publication number
- CN107338000A CN107338000A CN201710690459.2A CN201710690459A CN107338000A CN 107338000 A CN107338000 A CN 107338000A CN 201710690459 A CN201710690459 A CN 201710690459A CN 107338000 A CN107338000 A CN 107338000A
- Authority
- CN
- China
- Prior art keywords
- coating
- soluble polymeric
- initiator
- chlorinated paraffin
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/322—Ammonium phosphate
- C08K2003/323—Ammonium polyphosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses a kind of fireproof coating and preparation method thereof.Its main constituents and weight proportion are：Water-soluble polymeric adhesive 15% 25%, polyphosphoric acid ammonia 40% 55%, initiator 3% 5%, titanium dioxide 5% 8%, acrylic acid 0.8% 1%, fluorine richness surfactant 0.5% 1%, chlorinated paraffin 2% 5%, solvent 15% 20%.The present invention provides a kind of fireproof coating and preparation method thereof, and it adds fire proofing polyphosphoric acid ammonia and chlorinated paraffin, has a light waterproof modulation characteristic, at the same also can effective insulation and fire-retardant, be easy to prevent fires.
Description
Technical field
The present invention relates to technical field of coatings, specially a kind of fireproof coating and preparation method thereof.
Background technology
Coating is that one kind can firmly be covered in body surface protection, decoration, sign industry, with the continuous hair of economy
Exhibition, scientific and technical continuous progress, its application field is also increasingly wider, in some application fields, its to surface heat-insulating property and
Fire protecting performance has certain requirement, therefore has insulation and fireproof coating by applying last layer on surface, is solution
The certainly effective way of this problem.
The content of the invention
It is an object of the invention to provide a kind of fireproof coating and preparation method thereof, its add fire proofing polyphosphoric acid ammonia and
Chlorinated paraffin, has a light waterproof modulation characteristic, at the same also can effective insulation and fire-retardant, be easy to prevent fires.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of fireproof coating, its main constituents and weight proportion are：Water-soluble polymeric adhesive 15%-25%, polyphosphoric acid ammonia
40%-55%, initiator 3%-5%, titanium dioxide 5%-8%, acrylic acid 0.8%-1%, fluorine richness surfactant 0.5%-1%,
Chlorinated paraffin 2%-5%, solvent 15%-20%.
Initiator：For cracking type initiator, UV energy is can absorb, the energy needed for functional group is provided for film；
Titanium dioxide：Assign the more preferable ductility of film；
Acrylic acid：Wetting is provided for coating, improves film coated surface tension force；
Fluorine richness surfactant：Film levelability is provided, improves film coated surface activity.
A kind of preparation method of fireproof coating, its preparation flow mainly include the following steps that：
（1）Stock：By water-soluble polymeric adhesive, water-soluble polymeric adhesive, polyphosphoric acid ammonia, initiator, titanium dioxide, acrylic acid
Polymer, fluorine richness surfactant, chlorinated paraffin and solvent are stocked up according to above-mentioned weight proportion；
（2）Batch mixing：By initiator and stirring solvent to being completely dissolved, polyphosphoric acid ammonia, titanium dioxide, acrylic acid polymerization are sequentially added
Thing, fluorine richness surfactant, chlorinated paraffin, are stirred to dissolving, are added water-soluble polymeric adhesive, are fully stirred
Mix uniformly, obtain coating；
（3）Try film：On experimental products film it is above-mentioned made of coating, stand to being completely dried；
（4）Performance test：After test products film is completely dried, to its surface resistance to 99.5% absolute ethyl alcohol 500g power back and forth 500
Secondary, film is without show-through；The not bottom drain of the paper tape of resistance to RCA 175g power wear-resisting test 200 times；Cross-cut methods adhesive force 100% is tested, 0 grade；
（5）Finished product packing：Step will be passed through（4）The coating of performance test carries out finished product packing.
The beneficial effects of the invention are as follows：It provides a kind of fireproof coating and preparation method thereof, and it adds the poly- phosphorus of fire proofing
Sour ammonia and chlorinated paraffin, have a light waterproof modulation characteristic, at the same also can effective insulation and fire-retardant, be easy to prevent fires.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects
Enclose.
A kind of fireproof coating, its main constituents and weight proportion are：Water-soluble polymeric adhesive 15%-25%, poly- phosphorus
Sour ammonia 40%-55%, initiator 3%-5%, titanium dioxide 5%-8%, acrylic acid 0.8%-1%, fluorine richness surfactant 0.5%-
1%, chlorinated paraffin 2%-5%, solvent 15%-20%.
Initiator：For cracking type initiator, UV energy is can absorb, the energy needed for functional group is provided for film；
Titanium dioxide：Assign the more preferable ductility of film；
Acrylic acid：Wetting is provided for coating, improves film coated surface tension force；
Fluorine richness surfactant：Film levelability is provided, improves film coated surface activity.
A kind of preparation method of fireproof coating, its preparation flow mainly include the following steps that：
（1）Stock：By water-soluble polymeric adhesive, water-soluble polymeric adhesive, polyphosphoric acid ammonia, initiator, titanium dioxide, acrylic acid
Polymer, fluorine richness surfactant, chlorinated paraffin and solvent are stocked up according to above-mentioned weight proportion；
（2）Batch mixing：By initiator and stirring solvent to being completely dissolved, polyphosphoric acid ammonia, titanium dioxide, acrylic acid polymerization are sequentially added
Thing, fluorine richness surfactant, chlorinated paraffin, are stirred to dissolving, are added water-soluble polymeric adhesive, are fully stirred
Mix uniformly, obtain coating；
（3）Try film：On experimental products film it is above-mentioned made of coating, stand to being completely dried；
（4）Performance test：After test products film is completely dried, to its surface resistance to 99.5% absolute ethyl alcohol 500g power back and forth 500
Secondary, film is without show-through；The not bottom drain of the paper tape of resistance to RCA 175g power wear-resisting test 200 times；Cross-cut methods adhesive force 100% is tested, 0 grade；
（5）Finished product packing：Step will be passed through（4）The coating of performance test carries out finished product packing.
Embodiment 1：
Water-soluble polymeric adhesive 18%, polyphosphoric acid ammonia 45%, initiator 4%, titanium dioxide 6%, acrylic acid 1%, fluorine richness table
Face activating agent 1%, chlorinated paraffin 5%, solvent 20%.
Embodiment 2：
Water-soluble polymeric adhesive 25%, polyphosphoric acid ammonia 40%, initiator 5%, titanium dioxide 5%, acrylic acid 0.8%, fluorine richness
Surfactant 0.6%, chlorinated paraffin 3.6%, solvent 20%.
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic,
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in the present invention's
Within protection domain.
Claims (2)
1. a kind of fireproof coating, it is characterised in that its main constituents and weight proportion are：Water-soluble polymeric adhesive 15%-
25%, polyphosphoric acid ammonia 40%-55%, initiator 3%-5%, titanium dioxide 5%-8%, acrylic acid 0.8%-1%, fluorine richness surface is lived
Property agent 0.5%-1%, chlorinated paraffin 2%-5%, solvent 15%-20%.
2. a kind of preparation method of fireproof coating, it is characterised in that its preparation flow mainly includes the following steps that：
（1）Stock：By water-soluble polymeric adhesive, water-soluble polymeric adhesive, polyphosphoric acid ammonia, initiator, titanium dioxide, acrylic acid
Polymer, fluorine richness surfactant, chlorinated paraffin and solvent are stocked up according to above-mentioned weight proportion；
（2）Batch mixing：By initiator and stirring solvent to being completely dissolved, polyphosphoric acid ammonia, titanium dioxide, acrylic acid polymerization are sequentially added
Thing, fluorine richness surfactant, chlorinated paraffin, are stirred to dissolving, are added water-soluble polymeric adhesive, are fully stirred
Mix uniformly, obtain coating；
（3）Try film：On experimental products film it is above-mentioned made of coating, stand to being completely dried；
（4）Performance test：After test products film is completely dried, to its surface resistance to 99.5% absolute ethyl alcohol 500g power back and forth 500
Secondary, film is without show-through；The not bottom drain of the paper tape of resistance to RCA 175g power wear-resisting test 200 times；Cross-cut methods adhesive force 100% is tested, 0 grade；
（5）Finished product packing：Step will be passed through（4）The coating of performance test carries out finished product packing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710690459.2A CN107338000A (en) | 2017-08-14 | 2017-08-14 | A kind of fireproof coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710690459.2A CN107338000A (en) | 2017-08-14 | 2017-08-14 | A kind of fireproof coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107338000A true CN107338000A (en) | 2017-11-10 |
Family
ID=60216962
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710690459.2A Pending CN107338000A (en) | 2017-08-14 | 2017-08-14 | A kind of fireproof coating and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107338000A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115109601A (en) * | 2022-06-30 | 2022-09-27 | 广东电网有限责任公司 | Environment-friendly flame retardant and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1397613A (en) * | 2002-03-20 | 2003-02-19 | 许勇 | Fire-proof water paint for wood and its preparing process |
| CN101343507A (en) * | 2007-07-12 | 2009-01-14 | 中宏（天津）实业有限公司 | Preparation method for wood-construction water-based fire-proof paint |
| CN101597454A (en) * | 2009-06-25 | 2009-12-09 | 裘陆军 | The environment-friendly cable fire-refractory coating of high-weatherability and preparation technology |
| CN103923545A (en) * | 2014-05-07 | 2014-07-16 | 娄志 | Fireproof coating |
-
2017
- 2017-08-14 CN CN201710690459.2A patent/CN107338000A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1397613A (en) * | 2002-03-20 | 2003-02-19 | 许勇 | Fire-proof water paint for wood and its preparing process |
| CN101343507A (en) * | 2007-07-12 | 2009-01-14 | 中宏（天津）实业有限公司 | Preparation method for wood-construction water-based fire-proof paint |
| CN101597454A (en) * | 2009-06-25 | 2009-12-09 | 裘陆军 | The environment-friendly cable fire-refractory coating of high-weatherability and preparation technology |
| CN103923545A (en) * | 2014-05-07 | 2014-07-16 | 娄志 | Fireproof coating |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115109601A (en) * | 2022-06-30 | 2022-09-27 | 广东电网有限责任公司 | Environment-friendly flame retardant and preparation method and application thereof |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171110 |
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