CN107311736A - A kind of high slow release compoiste fertilizer of black mustard high yield - Google Patents

A kind of high slow release compoiste fertilizer of black mustard high yield Download PDF

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Publication number
CN107311736A
CN107311736A CN201710338604.0A CN201710338604A CN107311736A CN 107311736 A CN107311736 A CN 107311736A CN 201710338604 A CN201710338604 A CN 201710338604A CN 107311736 A CN107311736 A CN 107311736A
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parts
black mustard
powder
well mixed
compoiste fertilizer
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项永祥
童茜
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Tianchang Xiangjing Vegetable Cultivation Development Co Ltd
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Tianchang Xiangjing Vegetable Cultivation Development Co Ltd
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Priority to CN201710338604.0A priority Critical patent/CN107311736A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N55/00Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
    • A01N55/02Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur containing metal atoms
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14Boron; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/04Double-superphosphate; Triple-superphosphate; Other fertilisers based essentially on monocalcium phosphate
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil

Abstract

The invention discloses a kind of high slow release compoiste fertilizer of black mustard high yield, its raw material includes cow dung, maize straw, furfural dregs, bean cake powder, castor cake, medical stone powder, oyster shell whiting, chitin, fishbone dust, asparagus amino-acid calcium, humic acid potassium, calcium nitrate mud, magnesium nitrate mud, urea, ammonium nitrate, calcium dihydrogen phosphate, zinc-amino acid chelate, zinc sulfate, manganese sulfate, zinc acetate, molybdenum trisulfate, modified sustained release agent, mould proof auxiliary agent and antimicrobial powder.The compoiste fertilizer of the present invention has excellent sustained release and antimildew and antibacterial performance, disclosure satisfy that the nutritional need in black mustard whole growth period, improves the yield and quality of black mustard.

Description

A kind of high slow release compoiste fertilizer of black mustard high yield
Technical field
The present invention relates to the technical field of fertilizer, more particularly to a kind of high slow release compoiste fertilizer of black mustard high yield.
Background technology
Black mustard single flower basidixed, bottom has a lobate involucre, sepal petal-shaped, petal 5, is degenerated to nectar scale, and base portion is narrow thin Into pawl, 3-5cm of Hua Jing, 5-July of florescence.Top is ftractureed after capsule Long Circle, maturation, seed black.Cultivar petal increases Many, pattern has white, pale blue, pink, purplish red, faint yellow etc..Bred, sowed at the beginning of September with seeding method, germinate 15-20 DEG C of thermophilic, Sprout within 12-16 days.Seedling is intolerant to transplanting.If early spring open field live broadcast, evening at florescence and it is short.Englishman is called " sweet heart in mist ". Seed is shown in that light does not germinate, and avoids transplanting.Suitable for flower bed plantation.Ancient European people often makes dried flower with this flower.
Black mustard plantation fertilizer used is mostly organic agriculture fertilizer or inorganic fertilizer in the prior art, the slow release of organic agriculture fertilizer without Method meets the demand of actual plantation, and inorganic fertilizer easily causes soil hardening, and the perishable fermentation of organic fertilizer, the harmful substance meeting of generation The yield and quality of black mustard are reduced, so needing a kind of high slow release compoiste fertilizer of black mustard high yield of design badly to solve prior art Middle the problem of.
The content of the invention
To solve technical problem present in background technology, the present invention proposes a kind of high slow release organic composite of black mustard high yield Fertilizer, with excellent sustained release and fungicidal properties, can effectively improve the yield and quality of black mustard.
A kind of high slow release compoiste fertilizer of black mustard high yield proposed by the present invention, its raw material includes by weight:Cow dung 80- 120 parts, 2-8 parts of maize straw, 1.5-3.5 parts of furfural dregs, 3-6 parts of bean cake powder, 2-5 parts of castor cake, 3-6 parts of medical stone powder, shellfish 5-8 parts of shell powder, 2-6 parts of chitin, 1-4 parts of fishbone dust, 3-4 parts of asparagus amino-acid calcium, 2-5 parts of humic acid potassium, calcium nitrate mud 3-5 Part, 2-6 parts of magnesium nitrate mud, 20-40 parts of urea, 1-4 parts of ammonium nitrate, 2-6 parts of calcium dihydrogen phosphate, 3-5 parts of zinc-amino acid chelate, sulphur Sour zinc 4-8 parts, 6-12 parts of manganese sulfate, 4-9 parts of zinc acetate, 2-5 parts of molybdenum trisulfate, modified 2-4 parts of sustained release agent, mould proof auxiliary agent 3-6 parts, 4-8 parts of antimicrobial powder.
Preferably, modified sustained release agent is prepared by following technique:Casein and water are well mixed, 60-70 is warming up to DEG C, 20-40min is incubated, 30-50min is stirred in 650-850r/min rotating speeds, alkali lye is subsequently added into and is well mixed, in 350- 450r/min rotating speeds stir 1-3h, then heat to 80-90 DEG C, are incubated 2-4h, are cooled to room temperature and obtain being modified sustained release agent.
Preferably, in the preparation technology of modified sustained release agent, the weight ratio of casein, water and alkali lye is 3-5:2-8:1-3.
Preferably, the raw material of mould proof auxiliary agent includes by weight:3-9 parts of attapulgite, 4-8 parts of jade powder, polyvinyl alcohol 2-8 parts, 1-8 parts of dipotassium glycyrrhizinate, 2-9 parts of Tea Saponin, 4-8 parts of chlorinated paraffin, 3-9 parts of lithium base grease, ferrocenecarboxylic acid 1-5 Part, 2-9 parts of hexahydro phthalic anhydride, 3-6 parts of potassium sorbate, 4-8 parts of hexamethyl phosphoramide, 2-5 parts of sodium hydrogensulfite, boron Sour 1-5 parts, 3-9 parts of methyl benzotriazazole, 4-6 parts of pyrolkigneous liquid, 4-12 parts of deionized water.
Preferably, mould proof auxiliary agent is prepared by following technique:Attapulgite and jade powder are ground to form into 15-35 mesh, so Dipotassium glycyrrhizinate, Tea Saponin, chlorinated paraffin, lithium base grease, ferrocenecarboxylic acid, hexahydro phthalic anhydride, mountain are added afterwards Potassium sorbate, hexamethyl phosphoramide, sodium hydrogensulfite, boric acid, methyl benzotriazazole and deionized water are well mixed, grind 20- 50min, then adds polyvinyl alcohol and pyrolkigneous liquid, is well mixed, and is warming up to 120-140 DEG C, is incubated 1-4h, is cooled to room temperature, Dry, mould proof auxiliary agent is made in granulation.
Preferably, the parts by weight of raw materials of antimicrobial powder includes:2-8 parts of urea, 1-5 parts of polyvinylpyrrolidone, deionization 5-15 parts of water, 2-8 parts of sodium chloride solution, 1-6 parts of defoamer, 2-8 parts of silver nitrate solution, 1-4 parts of titanium liquid, disodium phosphate soln 4-8 parts.
Preferably, antimicrobial powder is prepared by following technique:Urea, polyvinylpyrrolidone and deionized water are mixed Uniformly, sodium chloride solution and defoamer stirring 10-30min are then added, then silver nitrate solution is added dropwise with separatory funnel and obtains thing Expect a;Titanium liquid is added with separatory funnel into material a to be well mixed, then heating water bath is cooled to after room temperature and added to 70-90 DEG C Enter disodium phosphate soln, be then aged, filtration washing is dried, is cooled to room temperature after calcining and obtains antimicrobial powder.
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes cow dung, maize straw, furfural Slag, bean cake powder, castor cake, medical stone powder, oyster shell whiting, chitin, fishbone dust, asparagus amino-acid calcium, humic acid potassium, calcium nitrate Mud, magnesium nitrate mud, urea, ammonium nitrate, calcium dihydrogen phosphate, zinc-amino acid chelate, zinc sulfate, manganese sulfate, zinc acetate, molybdenum trisulfate, Modified sustained release agent, mould proof auxiliary agent and antimicrobial powder.With cow dung, maize straw, furfural dregs, bean cake powder, castor cake, medical stone powder, Oyster shell whiting, chitin and fishbone dust are the source of organic material, with asparagus amino-acid calcium, humic acid potassium, calcium nitrate mud, magnesium nitrate Mud, urea, ammonium nitrate, calcium dihydrogen phosphate, zinc-amino acid chelate, zinc sulfate, manganese sulfate, zinc acetate and molybdenum trisulfate are inorganic growth Material source, to be modified sustained release agent, mould proof auxiliary agent and antimicrobial powder as auxiliary agent, is coordinated by organic material, inorganic growth material and auxiliary agent, Obtained compoiste fertilizer has excellent sustained release and antimildew and antibacterial performance, disclosure satisfy that the nutrition in black mustard whole growth period and needs Ask, improve the yield and quality of black mustard.Wherein, modified sustained release agent is heated up by the way that casein and water are well mixed, insulation, Stirring, is subsequently added into alkali lye and is well mixed, and then stirring heats up, and is incubated, is cooled to room temperature and obtains being modified sustained release agent, apply to In the compoiste fertilizer of the present invention, the sustained release performance of compoiste fertilizer of the present invention can be effectively improved, the plantation of black mustard is applied to In, the yield and quality of black mustard can be effectively improved.Then mould proof auxiliary agent is added sweet by the way that attapulgite and jade powder are ground Oxalic acid dipotassium, Tea Saponin, chlorinated paraffin, lithium base grease, ferrocenecarboxylic acid, hexahydro phthalic anhydride, potassium sorbate, six Methyl phosphamide, sodium hydrogensulfite, boric acid, methyl benzotriazazole and deionized water are well mixed, grinding, then add poly- second Enol and pyrolkigneous liquid, are well mixed, and heat up, and insulation is cooled to room temperature, dries, and mould proof auxiliary agent is made in granulation, applies to the present invention Compoiste fertilizer in, the fungicidal properties of compoiste fertilizer of the present invention can be effectively improved.Antimicrobial powder is by by urea, poly- second Alkene pyrrolidone and deionized water are well mixed, then add sodium chloride solution and defoamer stirring, then be added dropwise with separatory funnel Silver nitrate solution obtains material a;Titanium liquid is added with separatory funnel into material a to be well mixed, then heating water bath, is cooled to room Disodium phosphate soln is added after temperature, is then aged, filtration washing is dried, room temperature is cooled to after calcining and obtains antimicrobial powder, transports Use in compoiste fertilizer of the present invention, effectively increase the anti-microbial property of compoiste fertilizer of the present invention, it is to avoid fertilizer is because of the external world The contact of bacterium and cause the rotten of compoiste fertilizer of the present invention, in the plantation for applying to black mustard, black mustard can be effectively improved Yield and quality.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair In bright protection domain.
Embodiment 1
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes by weight:100 parts of cow dung, 5 parts of maize straw, 2.5 parts of furfural dregs, 4.5 parts of bean cake powder, 3.5 parts of castor cake, 4.5 parts of medical stone powder, 6.5 parts of oyster shell whiting, first Shell element 4 parts, 2.5 parts of fishbone dust, 3.5 parts of asparagus amino-acid calcium, 3.5 parts of humic acid potassium, 4 parts of calcium nitrate mud, 4 parts of magnesium nitrate mud, 30 parts of urea, 2.5 parts of ammonium nitrate, 4 parts of calcium dihydrogen phosphate, 4 parts of zinc-amino acid chelate, 6 parts of zinc sulfate, 9 parts of manganese sulfate, zinc acetate 6.5 parts, 3.5 parts of molybdenum trisulfate, modified 3 parts of sustained release agent, 4.5 parts of mould proof auxiliary agent, 6 parts of antimicrobial powder.
Modified sustained release agent is prepared by following technique:4 parts of casein and 5 parts of water are well mixed by weight, heated up To 65 DEG C, 30min is incubated, 40min is stirred in 750r/min rotating speeds, 2 parts of alkali lye is subsequently added into and is well mixed, turn in 400r/min Speed stirring 2h, then heats to 85 DEG C, is incubated 3h, is cooled to room temperature and obtains being modified sustained release agent.
Mould proof auxiliary agent is prepared by following technique:6 parts of attapulgites and 6 parts of jade powders are ground to form 25 by weight Mesh, then adds 4.5 parts of dipotassium glycyrrhizinates, 5.5 parts of Tea Saponins, 6 parts of chlorinated paraffins, 6 parts of lithium base greases, 3 parts of ferrocene first Acid, 5.5 parts of hexahydro phthalic anhydrides, 4.5 parts of potassium sorbates, 6 parts of hexamethyl phosphoramides, 3.5 parts of sodium hydrogensulfites, 3 parts Boric acid, 6 parts of methyl benzotriazazoles and 8 parts of deionized waters are well mixed, and are ground 35min, are then added 5 parts of polyvinyl alcohol and 5 Part pyrolkigneous liquid, is well mixed, and is warming up to 130 DEG C, is incubated 2.5h, is cooled to room temperature, dries, the obtained mould proof auxiliary agent of granulation.
Antimicrobial powder is prepared by following technique:By weight by 5 parts of urea, 3 parts of polyvinylpyrrolidones and 10 parts Deionized water is well mixed, and then adds 5 parts of sodium chloride solutions and 3.5 parts of defoamer stirring 20min, then be added dropwise with separatory funnel 5 parts of silver nitrate solutiones obtain material a;2.5 parts of titanium liquid are added with separatory funnel into material a to be well mixed, then heating water bath To 80 DEG C, 6 parts of disodium phosphate solns of addition after room temperature are cooled to, are then aged, filtration washing, dries, is cooled to after calcining Room temperature obtains antimicrobial powder.
Embodiment 2
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes by weight:80 parts of cow dung, jade 8 parts of stalk of rice, 1.5 parts of furfural dregs, 6 parts of bean cake powder, 2 parts of castor cake, 6 parts of medical stone powder, 5 parts of oyster shell whiting, 6 parts of chitin, fish 1 part of bone meal, 4 parts of asparagus amino-acid calcium, 2 parts of humic acid potassium, 5 parts of calcium nitrate mud, 2 parts of magnesium nitrate mud, 40 parts of urea, ammonium nitrate 1 Part, 6 parts of calcium dihydrogen phosphate, 3 parts of zinc-amino acid chelate, 8 parts of zinc sulfate, 6 parts of manganese sulfate, 9 parts of zinc acetate, 2 parts of molybdenum trisulfate, modification 4 parts of sustained release agent, 3 parts of mould proof auxiliary agent, 8 parts of antimicrobial powder.
Modified sustained release agent is prepared by following technique:3 parts of casein and 8 parts of water are well mixed by weight, heated up To 60 DEG C, 40min is incubated, 50min is stirred in 650r/min rotating speeds, 1 part of alkali lye is subsequently added into and is well mixed, turn in 450r/min Speed stirring 1h, then heats to 90 DEG C, is incubated 2h, is cooled to room temperature and obtains being modified sustained release agent.
Mould proof auxiliary agent is prepared by following technique:3 parts of attapulgites and 8 parts of jade powders are ground to form 15 by weight Mesh, then adds 8 parts of dipotassium glycyrrhizinates, 2 parts of Tea Saponins, 8 parts of chlorinated paraffins, 3 parts of lithium base greases, 5 parts of ferrocenecarboxylic acids, 2 Part hexahydro phthalic anhydride, 6 parts of potassium sorbates, 4 parts of hexamethyl phosphoramides, 5 parts of sodium hydrogensulfites, 1 part of boric acid, 9 parts of first Base BTA and 4 parts of deionized waters are well mixed, and are ground 50min, are then added 2 parts of polyvinyl alcohol and 6 parts of pyrolkigneous liquid, mix Close uniform, be warming up to 120 DEG C, be incubated 4h, be cooled to room temperature, dry, mould proof auxiliary agent is made in granulation.
Antimicrobial powder is prepared by following technique:2 parts of urea, 5 parts of polyvinylpyrrolidones and 5 parts are gone by weight Ionized water is well mixed, and then adds 8 parts of sodium chloride solutions and 1 part of defoamer stirring 30min, then be added dropwise 2 parts with separatory funnel Silver nitrate solution obtains material a;Add into material a 4 parts of titanium liquid with separatory funnel to be well mixed, then heating water bath is to 70 DEG C, 8 parts of disodium phosphate solns of addition after room temperature are cooled to, are then aged, filtration washing, dries, room temperature is cooled to after calcining Obtain antimicrobial powder.
Embodiment 3
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes by weight:120 parts of cow dung, 2 parts of maize straw, 3.5 parts of furfural dregs, 3 parts of bean cake powder, 5 parts of castor cake, 3 parts of medical stone powder, 8 parts of oyster shell whiting, 2 parts of chitin, 4 parts of fishbone dust, 3 parts of asparagus amino-acid calcium, 5 parts of humic acid potassium, 3 parts of calcium nitrate mud, 6 parts of magnesium nitrate mud, 20 parts of urea, ammonium nitrate 4 parts, 2 parts of calcium dihydrogen phosphate, 5 parts of zinc-amino acid chelate, 4 parts of zinc sulfate, 12 parts of manganese sulfate, 4 parts of zinc acetate, 5 parts of molybdenum trisulfate, change 2 parts of sustained release agent of property, 6 parts of mould proof auxiliary agent, 4 parts of antimicrobial powder.
Modified sustained release agent is prepared by following technique:5 parts of casein and 2 parts of water are well mixed by weight, heated up To 70 DEG C, 20min is incubated, 30min is stirred in 850r/min rotating speeds, 3 parts of alkali lye is subsequently added into and is well mixed, turn in 350r/min Speed stirring 3h, then heats to 80 DEG C, is incubated 4h, is cooled to room temperature and obtains being modified sustained release agent.
Mould proof auxiliary agent is prepared by following technique:9 parts of attapulgites and 4 parts of jade powders are ground to form 35 by weight Mesh, then adds 1 part of dipotassium glycyrrhizinate, 9 parts of Tea Saponins, 4 parts of chlorinated paraffins, 9 parts of lithium base greases, 1 part of ferrocenecarboxylic acid, 9 Part hexahydro phthalic anhydride, 3 parts of potassium sorbates, 8 parts of hexamethyl phosphoramides, 2 parts of sodium hydrogensulfites, 5 parts of boric acid, 3 parts of first Base BTA and 12 parts of deionized waters are well mixed, and are ground 20min, are then added 8 parts of polyvinyl alcohol and 4 parts of pyrolkigneous liquid, It is well mixed, 140 DEG C are warming up to, 1h is incubated, is cooled to room temperature, is dried, mould proof auxiliary agent is made in granulation.
Antimicrobial powder is prepared by following technique:By weight by 8 parts of urea, 1 part of polyvinylpyrrolidone and 15 parts Deionized water is well mixed, and then adds 2 parts of sodium chloride solutions and 6 parts of defoamer stirring 10min, then be added dropwise 8 with separatory funnel Part silver nitrate solution obtains material a;Add into material a 1 part of titanium liquid with separatory funnel to be well mixed, then heating water bath is to 90 DEG C, 4 parts of disodium phosphate solns of addition after room temperature are cooled to, are then aged, filtration washing, dries, room temperature is cooled to after calcining Obtain antimicrobial powder.
Embodiment 4
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes by weight:85 parts of cow dung, jade 7 parts of stalk of rice, 1.8 parts of furfural dregs, 5 parts of bean cake powder, 3 parts of castor cake, 5 parts of medical stone powder, 6 parts of oyster shell whiting, 5 parts of chitin, fish 2 parts of bone meal, 3.8 parts of asparagus amino-acid calcium, 3 parts of humic acid potassium, 4.5 parts of calcium nitrate mud, 3 parts of magnesium nitrate mud, 35 parts of urea, nitric acid 2 parts of ammonium, 5 parts of calcium dihydrogen phosphate, 3.5 parts of zinc-amino acid chelate, 7 parts of zinc sulfate, 7 parts of manganese sulfate, 8 parts of zinc acetate, molybdenum trisulfate 3 Part, modified 3.5 parts of sustained release agent, 4 parts of mould proof auxiliary agent, 7 parts of antimicrobial powder.
Modified sustained release agent is prepared by following technique:3.5 parts of casein and 7 parts of water are well mixed by weight, risen Temperature is incubated 35min to 62 DEG C, and 45min is stirred in 680r/min rotating speeds, is subsequently added into 1.5 parts of alkali lye and is well mixed, in 420r/ Min rotating speeds stir 1.5h, then heat to 88 DEG C, are incubated 2.5h, are cooled to room temperature and obtain being modified sustained release agent.
Mould proof auxiliary agent is prepared by following technique:4 parts of attapulgites and 7 parts of jade powders are ground to form 18 by weight Mesh, then adds 7 parts of dipotassium glycyrrhizinates, 3 parts of Tea Saponins, 7 parts of chlorinated paraffins, 4 parts of lithium base greases, 4 parts of ferrocenecarboxylic acids, 3 Part hexahydro phthalic anhydride, 5 parts of potassium sorbates, 5 parts of hexamethyl phosphoramides, 4 parts of sodium hydrogensulfites, 2 parts of boric acid, 8 parts of first Base BTA and 5 parts of deionized waters are well mixed, and are ground 45min, are then added 3 parts of polyvinyl alcohol and 5.5 parts of pyrolkigneous liquid, It is well mixed, 125 DEG C are warming up to, 3h is incubated, is cooled to room temperature, is dried, mould proof auxiliary agent is made in granulation.
Antimicrobial powder is prepared by following technique:3 parts of urea, 4 parts of polyvinylpyrrolidones and 8 parts are gone by weight Ionized water is well mixed, and then adds 7 parts of sodium chloride solutions and 2 parts of defoamer stirring 25min, then be added dropwise 3 parts with separatory funnel Silver nitrate solution obtains material a;Add into material a 3 parts of titanium liquid with separatory funnel to be well mixed, then heating water bath is to 75 DEG C, 7 parts of disodium phosphate solns of addition after room temperature are cooled to, are then aged, filtration washing, dries, room temperature is cooled to after calcining Obtain antimicrobial powder.
Embodiment 5
A kind of high slow release compoiste fertilizer of black mustard high yield of the present invention, its raw material includes by weight:115 parts of cow dung, 3 parts of maize straw, 3.2 parts of furfural dregs, 4 parts of bean cake powder, 4 parts of castor cake, 4 parts of medical stone powder, 7 parts of oyster shell whiting, 3 parts of chitin, 3 parts of fishbone dust, 3.2 parts of asparagus amino-acid calcium, 4 parts of humic acid potassium, 3.5 parts of calcium nitrate mud, 5 parts of magnesium nitrate mud, 25 parts of urea, nitre Sour 3 parts of ammonium, 3 parts of calcium dihydrogen phosphate, 4.5 parts of zinc-amino acid chelate, 5 parts of zinc sulfate, 11 parts of manganese sulfate, 5 parts of zinc acetate, molybdenum trisulfate 4 parts, modified 2.5 parts of sustained release agent, 5 parts of mould proof auxiliary agent, 5 parts of antimicrobial powder.
Modified sustained release agent is prepared by following technique:4.5 parts of casein and 3 parts of water are well mixed by weight, risen Temperature is incubated 25min to 68 DEG C, and 35min is stirred in 820r/min rotating speeds, is subsequently added into 2.5 parts of alkali lye and is well mixed, in 380r/ Min rotating speeds stir 2.5h, then heat to 82 DEG C, are incubated 3.5h, are cooled to room temperature and obtain being modified sustained release agent.
Mould proof auxiliary agent is prepared by following technique:8 parts of attapulgites and 5 parts of jade powders are ground to form 32 by weight Mesh, then adds 2 parts of dipotassium glycyrrhizinates, 8 parts of Tea Saponins, 5 parts of chlorinated paraffins, 8 parts of lithium base greases, 2 parts of ferrocenecarboxylic acids, 8 Part hexahydro phthalic anhydride, 4 parts of potassium sorbates, 7 parts of hexamethyl phosphoramides, 3 parts of sodium hydrogensulfites, 4 parts of boric acid, 4 parts of first Base BTA and 11 parts of deionized waters are well mixed, and grind 25min, then add 7 parts of polyvinyl alcohol and 4.5 portions of wooden vinegar Liquid, is well mixed, and is warming up to 135 DEG C, is incubated 2h, is cooled to room temperature, dries, and mould proof auxiliary agent is made in granulation.
Antimicrobial powder is prepared by following technique:By weight by 7 parts of urea, 2 parts of polyvinylpyrrolidones and 12 parts Deionized water is well mixed, and then adds 3 parts of sodium chloride solutions and 5 parts of defoamer stirring 15min, then be added dropwise 7 with separatory funnel Part silver nitrate solution obtains material a;Add into material a 2 parts of titanium liquid with separatory funnel to be well mixed, then heating water bath is to 85 DEG C, 5 parts of disodium phosphate solns of addition after room temperature are cooled to, are then aged, filtration washing, dries, room temperature is cooled to after calcining Obtain antimicrobial powder.
The high slow release compoiste fertilizer of black mustard high yield in 1- of embodiment of the present invention embodiments 5 is applied into actual plantation In, and blank control group is set, blank control group is to apply the black mustard that common fertilizer is planted, shown in obtained tables of data 1.
Table 1:
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (7)

1. a kind of high slow release compoiste fertilizer of black mustard high yield, it is characterised in that its raw material includes by weight:Cow dung 80-120 Part, 2-8 parts of maize straw, 1.5-3.5 parts of furfural dregs, 3-6 parts of bean cake powder, 2-5 parts of castor cake, 3-6 parts of medical stone powder, oyster shell whiting 5-8 parts, 2-6 parts of chitin, 1-4 parts of fishbone dust, 3-4 parts of asparagus amino-acid calcium, 2-5 parts of humic acid potassium, 3-5 parts of calcium nitrate mud, 2-6 parts of magnesium nitrate mud, 20-40 parts of urea, 1-4 parts of ammonium nitrate, 2-6 parts of calcium dihydrogen phosphate, 3-5 parts of zinc-amino acid chelate, sulfuric acid 4-8 parts of zinc, 6-12 parts of manganese sulfate, 4-9 parts of zinc acetate, 2-5 parts of molybdenum trisulfate, modified 2-4 part of sustained release agent, mould proof auxiliary agent 3-6 parts, resist 4-8 parts of bacterium powder body.
2. the high slow release compoiste fertilizer of black mustard high yield according to claim 1, it is characterised in that modified sustained release agent is by such as It is prepared by lower technique:Casein and water are well mixed, 60-70 DEG C is warming up to, 20-40min is incubated, in 650-850r/min Rotating speed stirs 30-50min, is subsequently added into alkali lye and is well mixed, stirs 1-3h in 350-450r/min rotating speeds, then heat to 80-90 DEG C, 2-4h is incubated, room temperature is cooled to and obtains being modified sustained release agent.
3. the high slow release compoiste fertilizer of black mustard high yield according to claim 1 or 2, it is characterised in that modified sustained release agent Preparation technology in, the weight ratio of casein, water and alkali lye is 3-5:2-8:1-3.
4. the high slow release compoiste fertilizer of black mustard high yield according to claim any one of 1-3, it is characterised in that mould proof to help The raw material of agent includes by weight:3-9 parts of attapulgite, 4-8 parts of jade powder, 2-8 parts of polyvinyl alcohol, 1-8 parts of dipotassium glycyrrhizinate, 2-9 parts of Tea Saponin, 4-8 parts of chlorinated paraffin, 3-9 parts of lithium base grease, 1-5 parts of ferrocenecarboxylic acid, hexahydro phthalic anhydride 2-9 parts, 3-6 parts of potassium sorbate, 4-8 parts of hexamethyl phosphoramide, 2-5 parts of sodium hydrogensulfite, 1-5 parts of boric acid, the nitrogen of methyl benzo three 3-9 parts of azoles, 4-6 parts of pyrolkigneous liquid, 4-12 parts of deionized water.
5. the high slow release compoiste fertilizer of black mustard high yield according to claim any one of 1-4, it is characterised in that mould proof to help Agent is prepared by following technique:Attapulgite and jade powder are ground to form into 15-35 mesh, dipotassium glycyrrhizinate, tea soap is then added Element, chlorinated paraffin, lithium base grease, ferrocenecarboxylic acid, hexahydro phthalic anhydride, potassium sorbate, hexamethyl phosphoramide, Asia Niter cake, boric acid, methyl benzotriazazole and deionized water are well mixed, grind 20-50min, then add polyvinyl alcohol And pyrolkigneous liquid, it is well mixed, is warming up to 120-140 DEG C, be incubated 1-4h, be cooled to room temperature, dry, mould proof auxiliary agent is made in granulation.
6. the high slow release compoiste fertilizer of black mustard high yield according to claim any one of 1-5, it is characterised in that antibacterial powder The parts by weight of raw materials of body includes:2-8 parts of urea, 1-5 parts of polyvinylpyrrolidone, 5-15 parts of deionized water, sodium chloride solution 2-8 Part, 1-6 parts of defoamer, 2-8 parts of silver nitrate solution, 1-4 parts of titanium liquid, 4-8 parts of disodium phosphate soln.
7. the high slow release compoiste fertilizer of black mustard high yield according to claim any one of 1-6, it is characterised in that antibacterial powder Body is prepared by following technique:Urea, polyvinylpyrrolidone and deionized water are well mixed, sodium chloride is then added molten Liquid and defoamer stirring 10-30min, then obtain material a with separatory funnel dropwise addition silver nitrate solution;With separatory funnel to material a Middle addition titanium liquid is well mixed, and then heating water bath is cooled to after room temperature to 70-90 DEG C and adds disodium phosphate soln, then Ageing, filtration washing is dried, is cooled to room temperature after calcining and obtains antimicrobial powder.
CN201710338604.0A 2017-05-12 2017-05-12 A kind of high slow release compoiste fertilizer of black mustard high yield Pending CN107311736A (en)

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