CN107308481A - Alcohol-free air freshener and preparation method thereof - Google Patents
Alcohol-free air freshener and preparation method thereof Download PDFInfo
- Publication number
- CN107308481A CN107308481A CN201710524738.1A CN201710524738A CN107308481A CN 107308481 A CN107308481 A CN 107308481A CN 201710524738 A CN201710524738 A CN 201710524738A CN 107308481 A CN107308481 A CN 107308481A
- Authority
- CN
- China
- Prior art keywords
- essence
- parts
- alcohol
- air freshener
- free air
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/04—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
- A61L9/044—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating with the help of an organic compound other than a macromolecular compound
Landscapes
- Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses alcohol-free air freshener and preparation method thereof.The alcohol-free air freshener includes the component of following parts by weight：6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant；Solubility≤9 (the cal/cm of the essence3)1/2, the flash-point of the essence is 40 DEG C 95 DEG C, and vapour pressure of the essence at 25 DEG C is in 0.1mmHg 5mmHg, volatility >=50% of the essence；Solubility≤8.5 (cal/cm3) 1/2 of the non-polar solven, boiling range is at 135 DEG C 260 DEG C, and flash-point is at 30 DEG C 100 DEG C；Preparation method is that raw material is mixed evenly.Alcohol-free air freshener of the present invention, is not required to addition surfactant and alcohol, and aroma strength is high, and the duration is long, will not block cotton core, and air freshener liquid residual is few, and in the absence of potential safety hazard.
Description
Technical field
The present invention relates to air freshener technical field, and in particular to alcohol-free air freshener and preparation method thereof.
Background technology
The existing liquid air freshener of in the market, usually with alcohol, surfactant, pure water and essence are constituted,
The high volatile by alcohol is needed, is evaporate into by swab stick in air, therefore alcohol content is higher, deposits certain safety
Hidden danger.Essence is needed by surfactant and alcohol, could be compatible with pure water, and surfactant is a kind of original of difficult volatilization
Material, how much is the addition of surfactant, and great role is played in the volatilization to perfume.Current liquid air freshener on the market
Essence addition it is general in 3%-6%, use time was at 30 days or so.Because essence addition is few, overall aroma strength ratio
Weaker, use time is shorter.If wanting to improve the addition of essence, to improve aroma strength, extend perfume substantiation, then table
The amount of face activating agent also wants corresponding raising, and the problem of this brings is exactly that surfactant blocks cotton core, causes liquia air
The residual of freshener is a lot.
The content of the invention
Based on this, the present invention provides a kind of alcohol-free air freshener, and it is not required to addition surfactant and alcohol, fragrance
Intensity is high, and the duration is long, will not block cotton core, and air freshener liquid residual is few, and in the absence of potential safety hazard.
The present invention also provides a kind of preparation method of the alcohol-free air freshener.
In order to realize the purpose of the present invention, the present invention uses following technical scheme：
A kind of alcohol-free air freshener, includes the component of following parts by weight：
6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant；Solubility≤9 of the essence
(cal/cm3)1/2, the flash-point of the essence is 40 DEG C -95 DEG C, and vapour pressure of the essence at 25 DEG C is in 0.1mmHg-
5mmHg, volatility >=50% of the essence；Solubility≤8.5 (the cal/cm of the non-polar solven3)1/2, boiling range is 135
DEG C -260 DEG C, flash-point is 30 DEG C -100 DEG C.Product is under fixed profile and structure, and the surfactant influence volatilization is direct
Remove, while the very low solvent flashing alcohol of flash-point (12 DEG C) is also removed, add suitable essence and solvent, control is matched,
Further investigate and screen in the selection of essence and volatilization auxiliary agent simultaneously, using preferred essence and nonpolar solvent flashing
To realize the parameters of the formula of liquid air freshener, control essence and non-polar solven so that essence is directly dissolved in non-
Polar solvent, forms air freshener, the aroma strength and use time of the air freshener all improve 2 times or 3 times even more
It is high.
In wherein some embodiments, described alcohol-free air freshener is made up of the component of following parts by weight：Essence
7~80 parts, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.2~1.2 part of ultra-violet absorber.
In wherein some embodiments, described alcohol-free air freshener is made up of the component of following parts by weight：Essence
7~80 parts, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.5~1 part of ultra-violet absorber, pigment 0.01~
0.05 part.
In wherein some embodiments, the ultra-violet absorber can be dissolved in grease.
In wherein some embodiments, described alcohol-free air freshener is made up of the component of following parts by weight：Essence
20~65 parts, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.5~1 part of ultra-violet absorber, pigment 0.01
~0.05 part.
In wherein some embodiments, the solubility≤8 (cal/cm of the essence3)1/2, the flash-point of the essence is 50
DEG C -80 DEG C, vapour pressure of the essence at 25 DEG C is 0.2mmHg-3mmHg, volatility >=65% of the essence.
In wherein some embodiments, the solubility≤7.8 (cal/cm of the non-polar solven3)1/2, boiling range is 150
DEG C -220 DEG C, flash-point is 40 DEG C -93 DEG C.
The present invention is also adopted the following technical scheme that：
A kind of preparation method of alcohol-free air freshener, it comprises the following steps：
6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant are provided；
Under conditions of room temperature and to Shi Du≤65%, above-mentioned essence and non-polar solven is taken to mix,
Stir, then add antioxidant, stirring is to being completely dissolved.
In wherein some embodiments, the preparation method of described alcohol-free air freshener also provides ultraviolet radiation absorption
0.5~1 part of agent, the ultra-violet absorber is added in the lump with antioxidant, and is stirred to being completely dissolved.
In wherein some embodiments, the preparation method of described alcohol-free air freshener, also provide pigment 0.01~
0.05 part, by described pigmentolysis into 1% pigment solution, with 6-10 layers of hospital gauze filtering several times, it is added to the perfume (or spice)
In the mixed liquor of essence and non-polar solven, stir.
Alcohol-free air freshener of the present invention, product is under fixed profile and structure, the surface of influence volatilization
Activating agent directly removes, while the very low solvent flashing alcohol of flash-point (12 DEG C) is also removed, adds suitable essence and solvent,
Control proportioning, while furtheing investigate and screening in the selection of essence and volatilization auxiliary agent, using preferred essence and non-pole
Property solvent flashing realize the formula of liquid air freshener, parameters of control essence and non-polar solven so that essence
Be directly dissolved in non-polar solven, form air freshener, the aroma strength and use time of the air freshener all improve 2 times or
3 times of even more highs.
Embodiment
For the ease of understanding the present invention, the present invention will be described more fully below.The present invention can be with many not
With form realize, however it is not limited to embodiment described herein.On the contrary, the purpose for providing these embodiments is made to this
The understanding of the disclosure of invention is more thorough comprehensive.
Unless otherwise defined, all of technologies and scientific terms used here by the article is with belonging to technical field of the invention
The implication that technical staff is generally understood that is identical.Term used in the description of the invention herein is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.
Alcohol-free air freshener of the present invention, includes the component of following parts by weight：
6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant；, wherein it is desired to control essence and non-
The parameter of polar solvent, it is ensured that both can be mutually dissolved, the solubility≤9 (cal/cm of the essence3)1/2, the essence
Flash-point is 40 DEG C -95 DEG C, the vapour pressure when essence is 25 DEG C in 0.1mmHg-5mmHg, the volatility of the essence >=
50%；Solubility≤8.5 (the cal/cm of the non-polar solven3)1/2, boiling range is 135 DEG C -260 DEG C, and flash-point is 30 DEG C -100
℃.Solubility≤8 (the cal/cm of preferably described essence3)1/2, the flash-point of the essence is 50 DEG C -80 DEG C, and the essence exists
Vapour pressure at 25 DEG C is in 0.2mmHg-3mmHg, volatility >=65% of the essence.The solubility of the non-polar solven≤
7.8(cal/cm3)1/2, boiling range is at 150 DEG C -220 DEG C, and flash-point is at 40 DEG C -93 DEG C.
Wherein, flash-point is determined according to ASTM D93-15 methods.Volatility is determined as follows：In 50 DEG C of constant temperature rings
In border, 5-20g essence is weighed, is put into 100ml-250ml beaker, continuous constant temperature 7 days, front and rear contrast of weighing determines essence
Volatility.
Essence therein can select to include lemon, Cologne, honey peach, the essence for the various tastes such as meeting by chance, and selection can
Reach the effect of above-mentioned each parameter.Non-polar solven can select de- arene, isoparaffin class, n-alkane
The combination of the single or multiple solvent of class, arene, silicone oil etc..The specific non-limiting example of solvent combination includes：It is purchased from
Exxon ChemicalCompany (Exxon Mobil Corporation) de- arene product, referred to as Exxon D30Fluid,
Exxon D40Fluid、Exxon D60Fluid、Exxon D80Fluid。
Purchased from Exxon ChemicalCompany (Exxon Mobil Corporation) isoparaffin class product, referred to as Isopar
G、Isopar H、Isopar L、Isopar M.Purchased from IDEMITSUKOSAN (Japanese light extraction) isoparaffin class product, it is referred to as
IPCLEANLX, IP1620, IP CLEANHX, IP2028.
Other non-limiting examples of applicable branched-chain hydrocarbons include：Purchased from Preperse, Inc., South Plainfield,
NewJersey, U.S.A. product be referred to as Permethyl 99A (Permethyl 99A), Permethyl 102A (Isoeicosane),
Permethyl 101A (different hexadecane) and combinations thereof.
The non-limiting example of other applicable branched-chain hydrocarbons includes petroleum distillate, is such as purchased from Phillips Chemical production
Product Soltrol 130, Soltrol 170, and purchased from Shell product Shell Sol-70, -71 and -2033.
Purchased from Exxon ChemicalCompany (Exxon Mobil Corporation) N-alkanes hydrocarbon products, referred to as Norpar
12Fluid、Norpar 13Fluid、Norpar 14Fluid。
Other non-limiting examples of applicable arene, purchased from Exxon ChemicalCompany, (Exxon Mobil is public
Department) arene product, referred to as Solvesso 100Fluid, Solvesso 150Fluid.
Other non-limiting examples of applicable silicone oil, including purchased from the silicone oil product of Dow corning, referred to as PMX-
0245, PMX-0345 etc..
Antioxidant selection can be dissolved in grease, and the material of good antioxidation is played to grease.Conventional has butyl hydroxyl
The artificial synthesized oil-soluble such as base anisole (BHA), dibutyl hydroxy toluene (BHT) and propylgallate (PG) is anti-oxidant
Agent；The natural oil-soluble inhibitor such as mixed tocopherol concentrate and guaiac resin.Other non-limiting examples：It is preferred that BHA and
BHT。
Described alcohol-free air freshener, can also add ultra-violet absorber, and selection can be dissolved in grease, can absorb sun
Ultraviolet part in light and fluorescence light source, and itself does not change.Conventional has to the stupid formic acid system of amino, cinnamic acid
System, carboxyl benzophenone system, salicylic acid system.Other non-limiting examples：It is preferred that Octocrilene, Avobenzone, 2- (2H- BTAs-
2- yls) -6- dodecyl -4- cresols.I.e. described alcohol-free air freshener is made up of the component of following parts by weight：Essence 7
~80 parts, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.2~1.2 part of ultra-violet absorber.
Described alcohol-free air freshener, can also add pigment, and pigment selects fat-soluble toner, color or liquid color
Element, selection has good compatibility, easy dispersing and dissolving, colour stable, the pigment of safety non-toxic in polar solvent.It is i.e. described
Alcohol-free air freshener be made up of the component of following parts by weight：7~80 parts of essence, 40~80 parts of non-polar solven, antioxygen
0.2~0.8 part of agent, 0.5~1 part of ultra-violet absorber, 0.01~0.05 part of pigment.
The preparation method of above-mentioned alcohol-free air freshener, comprises the following steps：In room temperature and to Shi Du≤65%
Under conditions of, take above-mentioned essence and non-polar solven to mix, stir；Then antioxidant and ultraviolet are added
Absorbent, stirring is to being completely dissolved；By described pigmentolysis into 1% pigment solution, filter several with 6-10 layers of hospital gauze
It is secondary, add in above-mentioned mixed liquor.
Alcohol-free air freshener of the present invention, product is under fixed profile and structure, the surface of influence volatilization
Activating agent directly removes, while the very low solvent flashing alcohol of flash-point (12 DEG C) is also removed, adds suitable essence and solvent,
Control proportioning, while furtheing investigate and screening in the selection of essence and volatilization auxiliary agent, using preferred essence and non-pole
Property solvent flashing realize the formula of liquid air freshener, parameters of control essence and non-polar solven so that essence
Be directly dissolved in non-polar solven, form air freshener, the aroma strength and use time of the air freshener all improve 2 times or
3 times of even more highs.
The embodiment of the present invention will be illustrated by several embodiments below, wherein, after measured, in each embodiment
Essence and solvent parameter all in above-mentioned scope, do not illustrate one by one.
Embodiment one
Alcohol-free air freshener of the present invention, includes the component of following parts by weight：6 parts of essence, non-polar solven
83.09 parts, 0.2 part of antioxidant, 0.2 part of ultra-violet absorber, 0.01 part of pigment., wherein it is desired to control essence and nonpolar
The parameter of solvent, it is ensured that both can be mutually dissolved, the solubility≤9 (cal/cm of the essence3)1/2, the flash-point of the essence
For 40 DEG C -95 DEG C, vapour pressure of the essence at 25 DEG C is in 0.1mmHg-5mmHg, volatility >=50% of the essence；Institute
State the solubility≤8.5 (cal/cm of non-polar solven3)1/2, boiling range is at 135 DEG C -260 DEG C, and flash-point is at 30 DEG C -100 DEG C.
Essence selects lemon flavour essence, needs to determine parameters when selecting essence, described to guarantee to meet
Parameter Conditions.Non-polar solven includes 13.09 parts of 60 parts of Isopar G, 20 parts of Isopar H and IPCLEAN LX, resists
Oxidant is 0.2 part of butylated hydroxy anisole, and ultra-violet absorber is 0.2 part of Avobenzone, 0.01 part of pigment.
The preparation method of above-mentioned alcohol-free air freshener is：Under conditions of room temperature and to Shi Du≤65%, take
Above-mentioned essence and non-polar solven is mixed, and is stirred；Then antioxidant and ultra-violet absorber, stirring are added
To being completely dissolved；By described pigmentolysis into 1% pigment solution, with 10 layers of hospital gauze filtering several times, add above-mentioned
In mixed liquor.
After tested, the alcohol-free air freshener of the present embodiment, after using 62 days, fragrance just can slowly disappear.
Embodiment two
Alcohol-free air freshener of the present invention, includes the component of following parts by weight：8 parts of essence, non-polar solven
91.48 parts, 0.2 part of antioxidant, 0.3 part of ultra-violet absorber, 0.02 part of pigment., wherein it is desired to control essence and nonpolar
The parameter of solvent, it is ensured that both can be mutually dissolved, the solubility≤8.5 (cal/cm of the essence3)1/2, the sudden strain of a muscle of the essence
Point is 45 DEG C -85 DEG C, and vapour pressure of the essence at 25 DEG C is in 0.2mmHg-3mmHg, volatility >=65% of the essence；
Solubility≤8 (cal/cm3) 1/2 of the non-polar solven, boiling range is at 150 DEG C -220 DEG C, and flash-point is at 35 DEG C -95 DEG C.
Taste essence is met in essence selection by chance, needs to determine parameters when selecting essence, described to guarantee to meet
Parameter Conditions.Non-polar solven includes 55 parts of Exxon D40Fluid, 25 parts of Exxon D40Fluid and Isopar M
1.48 parts, 10 parts of IP CLEAN HX, antioxidant are 0.2 part of dibutyl hydroxy toluene, and ultra-violet absorber is Octocrilene
0.1 part, 0.1 part of Avobenzone and 2- (2H- BTA -2- bases) 0.1 part of -6- dodecyl -4- cresols, pigment 0.02
Part.
The preparation method of above-mentioned alcohol-free air freshener is：Under conditions of room temperature and to Shi Du≤65%, take
Above-mentioned essence and non-polar solven is mixed, and is stirred；Then antioxidant and ultra-violet absorber, stirring are added
To being completely dissolved；By described pigmentolysis into 1% pigment solution, with 10 layers of hospital gauze filtering several times, add above-mentioned
In mixed liquor.
After tested, the alcohol-free air freshener of the present embodiment, after using 65 days, fragrance just can slowly disappear.
Embodiment three
Alcohol-free air freshener of the present invention, includes the component of following parts by weight：10 parts of essence, non-polar solven
89.17 parts, 0.2 part of antioxidant, 0.5 part of ultra-violet absorber, 0.03 part of pigment., wherein it is desired to control essence and nonpolar
The parameter of solvent, it is ensured that both can be mutually dissolved, the solubility≤8 (cal/cm of the essence3)1/2, the flash-point of the essence
For 50 DEG C -80 DEG C, vapour pressure of the essence at 25 DEG C is in 0.2mmHg-3mmHg, volatility >=65% of the essence；Institute
State the solubility≤7.8 (cal/cm of non-polar solven3)1/2, boiling range is at 160 DEG C -200 DEG C, and flash-point is at 40 DEG C -93 DEG C.
Need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven
Including 22.17 parts of 25 parts of Isopar G, 10 parts of Isopar H and Isopar L, 32 parts of IPCLEAN LX, antioxidant
For 0.2 part of dibutyl hydroxy toluene, ultra-violet absorber is 0.2 part of Octocrilene, 0.1 part of Avobenzone and 2- (2H- benzos
Triazole -2- bases) 0.2 part of -6- dodecyl -4- cresols, 0.03 part of pigment.
The preparation method of above-mentioned alcohol-free air freshener is：Under conditions of room temperature and to Shi Du≤65%, take
Above-mentioned essence and non-polar solven is mixed, and is stirred；Then antioxidant and ultra-violet absorber, stirring are added
To being completely dissolved；By described pigmentolysis into 1% pigment solution, with 10 layers of hospital gauze filtering several times, add above-mentioned
In mixed liquor.
After tested, the alcohol-free air freshener of the present embodiment, after using 73 days, fragrance just can slowly disappear.
Example IV
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：15 parts of essence, 84.15 parts of non-polar solven, 0.4 part of antioxidant, 0.4 part of ultra-violet absorber, 0.05 part of pigment.Its
In, essence selection apple taste essence needs to determine parameters when selecting essence, to guarantee to meet described parameter
Condition.Non-polar solven include 43 parts of IP1620,21 parts of Norpar12Fluid, 15 parts of Solvesso 100Fluid,
5.15 parts of Solvesso 150Fluid, antioxidant is 0.3 part of butylated hydroxy anisole, 0.1 part of dibutyl hydroxy toluene, purple
Ultraviolet absorbers are 0.2 part of Octocrilene, 0.2 part of Avobenzone, 0.05 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 85 days, fragrance just can slowly disappear.
Embodiment five
Alcohol-free air freshener of the present invention, and unlike embodiment two, it includes the group of following parts by weight
Point：20 parts of essence, 79.08 parts of non-polar solven, 0.5 part of antioxidant, 0.4 part of ultra-violet absorber, 0.02 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
27 parts of Exxon D80Fluid, 17.08 parts of IP1620,25 parts of PMX-0245,10 parts of PMX-0345, antioxidant is butyl
0.2 part of BHA, 0.3 part of dibutyl hydroxy toluene, ultra-violet absorber are 0.2 part of Avobenzone, 2- (2H- benzos three
Azoles -2- bases) 0.2 part of -6- dodecyl -4- cresols, 0.02 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 92 days, fragrance just can slowly disappear.
Embodiment six
Alcohol-free air freshener of the present invention, and unlike embodiment three, it includes the group of following parts by weight
Point：30 parts of essence, 68.96 parts of non-polar solven, 0.5 part of antioxidant, 0.5 part of ultra-violet absorber, 0.04 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
28.96 parts of Isopar H, 20 parts of Isopar L, 5 parts of Isopar L, 15 parts of IP2028, antioxidant are butylhydroxy fennel
Fragrant 0.5 part of ether, ultra-violet absorber is 0.1 part of Octocrilene, 0.3 part of Avobenzone, 2- (2H- BTA -2- bases) -6- ten
0.1 part of dialkyl group -4- cresols, 0.04 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 86 days, fragrance just can slowly disappear.
Embodiment seven
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：35 parts of essence, 64.07 parts of non-polar solven, 0.6 part of antioxidant, 0.3 part of ultra-violet absorber, 0.03 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
21 parts of Exxon D60Fluid, 16 parts of Exxon D80Fluid, 20 parts of IP1620,7.07 parts of Solvesso 100Fluid,
Antioxidant is 0.6 part of dibutyl hydroxy toluene, and ultra-violet absorber is 0.3 part of Octocrilene, 0.03 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 73 days, fragrance just can slowly disappear.
Embodiment eight
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：40 parts of essence, 58.85 parts of non-polar solven, 0.6 part of antioxidant, 0.5 part of ultra-violet absorber, 0.05 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
40 parts of Isopar G, 18.85 parts of Isopar L, antioxidant are 0.1 part of butylated hydroxy anisole, dibutyl hydroxy toluene
0.5 part, ultra-violet absorber is 0.5 part of Avobenzone, 0.05 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 64 days, fragrance just can slowly disappear.
Embodiment nine
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：45 parts of essence, 52.78 parts of non-polar solven, 0.7 part of antioxidant, 0.5 part of ultra-violet absorber, 0.02 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
30 parts of Exxon D60Fluid, 5 parts of Exxon D80Fluid, 17.78 parts of IPCLEAN LX, antioxidant is butylhydroxy
0.2 part of anisole, 0.5 part of dibutyl hydroxy toluene, ultra-violet absorber are 0.3 part of Avobenzone, 2- (2H- BTAs -2-
Base) 0.2 part of -6- dodecyl -4- cresols, 0.02 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 67 days, fragrance just can slowly disappear.
Embodiment ten
Alcohol-free air freshener of the present invention, and unlike embodiment two, it includes the group of following parts by weight
Point：50 parts of essence, 48.79 parts of non-polar solven, 0.7 part of antioxidant, 0.5 part of ultra-violet absorber, 0.01 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
10 parts of Isopar L, 8 parts of Isopar M, HX20 parts of IP CLEAN, 10.79 parts of Norpar 12Fluid, antioxidant is
0.7 part of dibutyl hydroxy toluene, ultra-violet absorber is 0.4 part of Octocrilene, 0.1 part of Avobenzone, 0.01 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 65 days, fragrance just can slowly disappear.
Embodiment 11
Alcohol-free air freshener of the present invention, and unlike embodiment three, it includes the group of following parts by weight
Point：60 parts of essence, 38.36 parts of non-polar solven, 0.7 part of antioxidant, 0.9 part of ultra-violet absorber, 0.04 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
20 parts of Solvesso 150Fluid, 13 parts of PMX-0245,5.36 parts of PMX-0345, antioxidant is butylated hydroxy anisole
0.5 part, 0.2 part of dibutyl hydroxy toluene, ultra-violet absorber are 0.3 part of Octocrilene, 0.3 part of Avobenzone, 2- (2H- benzene
And triazole -2- bases) 0.3 part of -6- dodecyl -4- cresols, 0.04 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 66 days, fragrance just can slowly disappear.
Embodiment 12
Alcohol-free air freshener of the present invention, and unlike embodiment two, it includes the group of following parts by weight
Point：65 parts of essence, 33.28 parts of non-polar solven, 0.8 part of antioxidant, 0.9 part of ultra-violet absorber, 0.02 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
28 parts of Isopar L, 5.28 parts of IP1620, antioxidant are 0.8 part of butylated hydroxy anisole, and ultra-violet absorber is Losec
Vertical 0.5 part of woods, 0.3 part of Avobenzone, 2- (2H- BTA -2- bases) 0.1 part of -6- dodecyl -4- cresols, pigment 0.02
Part.
After tested, the alcohol-free air freshener of the present embodiment, after using 86 days, fragrance just can slowly disappear.
Embodiment 13
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：70 parts of essence, 28.25 parts of non-polar solven, 1.3 parts of antioxidant, 0.9 part of ultra-violet absorber, 0.05 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
18.25 parts of Exxon D60Fluid, 10 parts of Isopar G, antioxidant are 0.8 part of butylated hydroxy anisole, dibutyl hydroxy
0.5 part of toluene, ultra-violet absorber is 0.4 part of Octocrilene, 2- (2H- BTA -2- bases) -6- dodecyl -4- cresols
0.5 part, 0.05 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 79 days, fragrance just can slowly disappear.
Embodiment 14
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：75 parts of essence, 23.17 parts of non-polar solven, 0.8 part of antioxidant, 1.0 parts of ultra-violet absorber, 0.03 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
8.17 parts of IP1620,15 parts of IP CLEAN HX, antioxidant are 0.2 part of butylated hydroxy anisole, dibutyl hydroxy toluene
0.6 part, ultra-violet absorber is 0.8 part of Avobenzone, 2- (2H- BTA -2- bases) -6- dodecyl -4- cresols 0.2
Part, 0.03 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 72 days, fragrance just can slowly disappear.
Embodiment 15
Alcohol-free air freshener of the present invention, and unlike embodiment three, it includes the group of following parts by weight
Point：85 parts of essence, 13.08 parts of non-polar solven, 0.8 part of antioxidant, 1.1 parts of ultra-violet absorber, 0.02 part of pigment.Its
In, need to determine parameters when selecting essence, to guarantee to meet described Parameter Conditions.Non-polar solven includes
5.08 parts of Exxon D40Fluid, 8 parts of IP2028, antioxidant are 0.8 part of dibutyl hydroxy toluene, and ultra-violet absorber is
0.5 part of Octocrilene, 0.4 part of Avobenzone, 2- (2H- BTA -2- bases) 0.2 part of -6- dodecyl -4- cresols, pigment
0.02 part.
After tested, the alcohol-free air freshener of the present embodiment, after using 81 days, fragrance just can slowly disappear.
Embodiment 16
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：7 parts of essence, 95 parts of non-polar solven, 0.1 part of antioxidant, 0.2 part of ultra-violet absorber, 0.01 part of pigment.It is nonpolar molten
Agent includes 20 parts of Exxon D40Fluid, and antioxidant is 0.1 part of dibutyl hydroxy toluene, and ultra-violet absorber is vertical for Losec
0.2 part of woods, 0.01 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 60 days, fragrance just can slowly disappear.
Embodiment 17
Alcohol-free air freshener of the present invention, and unlike embodiment one, it includes the group of following parts by weight
Point：80 parts of essence, 20 parts of non-polar solven, 1.0 parts of antioxidant, 1.2 parts of ultra-violet absorber, 0.01 part of pigment.It is nonpolar
Solvent includes 95 parts of IP2028, and antioxidant is 1.0 parts of dibutyl hydroxy toluene, and ultra-violet absorber is Octocrilene 1.2
Part, 0.02 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 81 days, fragrance just can slowly disappear.
Embodiment 18
Alcohol-free air freshener of the present invention, and unlike embodiment two, it includes the group of following parts by weight
Point：10 parts of essence, 40 parts of non-polar solven, 0.5 part of antioxidant, 0.2 part of ultra-violet absorber, 0.02 part of pigment.It is nonpolar
Solvent includes 20 parts of Exxon D60Fluid, 20 parts of Isopar G, and antioxidant is 0.5 part of dibutyl hydroxy toluene, ultraviolet
Light absorbers are 0.2 part of Octocrilene, 0.02 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 56 days, fragrance just can slowly disappear.
Embodiment 19
Alcohol-free air freshener of the present invention, and unlike embodiment three, it includes the group of following parts by weight
Point：30 parts of essence, 80 parts of non-polar solven, 0.5 part of antioxidant, 0.2 part of ultra-violet absorber, 0.02 part of pigment.It is nonpolar
Solvent includes 30 parts of Isopar L, 8 parts of Isopar M, HX42 parts of IP CLEAN, and antioxidant is dibutyl hydroxy toluene
0.5 part, ultra-violet absorber is 0.2 part of Octocrilene, 0.02 part of pigment.
After tested, the alcohol-free air freshener of the present embodiment, after using 75 days, fragrance just can slowly disappear.
Embodiment described above only expresses the several embodiments of the present invention, and it describes more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of alcohol-free air freshener, it is characterised in that include the component of following parts by weight：
6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant；Solubility≤9 (the cal/ of the essence
cm3)1/2, the flash-point of the essence is 40 DEG C -95 DEG C, and vapour pressure of the essence at 25 DEG C is described in 0.1mmHg-5mmHg
Volatility >=50% of essence；Solubility≤8.5 (the cal/cm of the non-polar solven3)1/2, boiling range is 135 DEG C -260 DEG C,
Flash-point is 30 DEG C -100 DEG C.
2. alcohol-free air freshener according to claim 1, it is characterised in that：It is made up of the component of following parts by weight：
7~80 parts of essence, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.2~1.2 part of ultra-violet absorber.
3. alcohol-free air freshener according to claim 1 or 2, it is characterised in that：By the component group of following parts by weight
Into：7~80 parts of essence, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.5~1 part of ultra-violet absorber, color
0.01~0.05 part of element.
4. alcohol-free air freshener according to claim 3, it is characterised in that：The ultra-violet absorber can be dissolved in
Grease.
5. alcohol-free air freshener according to claim 3, it is characterised in that：It is made up of the component of following parts by weight：
20~65 parts of essence, 40~80 parts of non-polar solven, 0.2~0.8 part of antioxidant, 0.5~1 part of ultra-violet absorber, pigment
0.01~0.05 part.
6. alcohol-free air freshener according to claim 1, it is characterised in that：Solubility≤8 (the cal/ of the essence
cm3)1/2, the flash-point of the essence is 50 DEG C -80 DEG C, and vapour pressure of the essence at 25 DEG C is 0.2mmHg-3mmHg, described
Volatility >=65% of essence.
7. alcohol-free air freshener according to claim 1, it is characterised in that：The solubility of the non-polar solven≤
7.8(cal/cm3)1/2, boiling range is 150 DEG C -220 DEG C, and flash-point is 40 DEG C -93 DEG C.
8. a kind of preparation method of alcohol-free air freshener, it is characterised in that comprise the following steps：
6~85 parts of essence, 20~95 parts of non-polar solven, 0.1~1 part of antioxidant are provided；Solubility≤9 of the essence
(cal/cm3)1/2, the flash-point of the essence is 40 DEG C -95 DEG C, and vapour pressure of the essence at 25 DEG C is 0.1mmHg-
5mmHg, volatility >=50% of the essence；Solubility≤8.5 (the cal/cm of the non-polar solven3)1/2, boiling range is 135
DEG C -260 DEG C, flash-point is 30 DEG C -100 DEG C；
Under conditions of room temperature and to Shi Du≤65%, take above-mentioned essence and non-polar solven to mix, stir
Uniformly, antioxidant is then added, stirring is to being completely dissolved.
9. the preparation method of alcohol-free air freshener according to claim 8, it is characterised in that ultraviolet is also provided and inhaled
0.5~1 part of agent is received, the ultra-violet absorber is added in the lump with antioxidant, and stirring is to being completely dissolved.
10. the preparation method of alcohol-free air freshener according to claim 8 or claim 9, it is characterised in that pigment is also provided
0.01~0.05 part, by described pigmentolysis into 1% pigment solution, with 6-10 layers of hospital gauze filtering several times, it is added to
In the mixed liquor of the essence and non-polar solven, stir.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710524738.1A CN107308481A (en) | 2017-06-30 | 2017-06-30 | Alcohol-free air freshener and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710524738.1A CN107308481A (en) | 2017-06-30 | 2017-06-30 | Alcohol-free air freshener and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107308481A true CN107308481A (en) | 2017-11-03 |
Family
ID=60179942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710524738.1A Pending CN107308481A (en) | 2017-06-30 | 2017-06-30 | Alcohol-free air freshener and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107308481A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112704762A (en) * | 2019-10-25 | 2021-04-27 | 广东爱车小屋电子商务科技有限公司 | Solid air freshener and preparation method thereof |
| CN113599559A (en) * | 2021-08-20 | 2021-11-05 | 广东爱车小屋电子商务科技有限公司 | Alcohol-free air freshener and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1265579A (en) * | 1997-06-23 | 2000-09-06 | 普罗克特和甘保尔公司 | Anhydrous gel deodorant compositions containing volatile nonpolar solvents |
| CN1393542A (en) * | 2001-06-29 | 2003-01-29 | 雷军 | Non-polar essence additive and essence containing it |
| CN106362181A (en) * | 2016-08-30 | 2017-02-01 | 广东爱车小屋实业发展股份有限公司 | Liquid air freshener and preparation method thereof |
-
2017
- 2017-06-30 CN CN201710524738.1A patent/CN107308481A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1265579A (en) * | 1997-06-23 | 2000-09-06 | 普罗克特和甘保尔公司 | Anhydrous gel deodorant compositions containing volatile nonpolar solvents |
| CN1393542A (en) * | 2001-06-29 | 2003-01-29 | 雷军 | Non-polar essence additive and essence containing it |
| CN106362181A (en) * | 2016-08-30 | 2017-02-01 | 广东爱车小屋实业发展股份有限公司 | Liquid air freshener and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112704762A (en) * | 2019-10-25 | 2021-04-27 | 广东爱车小屋电子商务科技有限公司 | Solid air freshener and preparation method thereof |
| CN113599559A (en) * | 2021-08-20 | 2021-11-05 | 广东爱车小屋电子商务科技有限公司 | Alcohol-free air freshener and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Quach et al. | An improved method for the extraction and thin-layer chromatography of chlorophyll a and b from spinach | |
| CN102703215B (en) | Perfume essence and preparation method thereof | |
| CN107308481A (en) | Alcohol-free air freshener and preparation method thereof | |
| US5298184A (en) | Paint stripper composition | |
| JP5208728B2 (en) | Functional UV paint, building material using the same, and method for producing the paint | |
| Takahashi et al. | Carotenoids extraction from Japanese persimmon (Hachiya-kaki) peels by supercritical CO2 with ethanol | |
| Johns et al. | Early diagenesis of phytyl esters in a contemporary temperate intertidal sediment | |
| JPS63145367A (en) | Carotenoid pigment composition | |
| CN106635516A (en) | Keyboard cleaning agent | |
| Aziz et al. | Study of anthocyanin stability derived from the fruit pulp of Melastoma malabathricum in a coating system | |
| CN107510859A (en) | Champignon and preparation method thereof | |
| DE60310850T2 (en) | Liquid toners and electrographic inks with reduced odors | |
| CN103911039B (en) | Nondiscoloration water color ink containing Flos Hibisci extract and preparation method thereof | |
| US20070178169A1 (en) | Extraction method of active molecular structures from natural resins and/or essential oils | |
| EP2918295B1 (en) | Release system for fragrances with optical end-of-life indicator | |
| Nurdianti et al. | Formulation and evaluation of astaxanthin lotions as natural antioxidants for the skin | |
| CN104524614B (en) | Possesses composition of noctilucent function and preparation method thereof | |
| CN107397688A (en) | A kind of water-in-oil type cosmetic and preparation method containing melanin | |
| CN108969788A (en) | A kind of the rattan scent liquid and its preparation process of lasting fragrance | |
| Desnita et al. | Span 60 as surfactant of topical microemulsion of purple sweet potato (Ipomoea batatas L.) ethanol extract and antioxidant activity test using dpph method | |
| CN103911040B (en) | Nondiscoloration water color ink containing Flos abelmoschi manihot extract and preparation method thereof | |
| JP2003313596A (en) | Detergent for screen printing plate and method production for the same | |
| CN104312268A (en) | Environment-friendly printing ink with high adhesive force | |
| US2320527A (en) | Coating composition and process of producing the same | |
| Kotak et al. | Photostability of aniline blue (CI 42755) and methyl blue (CI 42780) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: 523808 No. 16, Science and Technology Fourth Road, Songshan Lake Park, Dongguan City, Guangdong Province Applicant after: Guangdong Love Car Cabin Electronic Commerce Technology Co., Ltd. Address before: 523000 Dongguan, Guangdong province Dongcheng District fire lotus tree community Dongguan Avenue 11 Taiwan business building 4801-4810 room. Applicant before: Wujiang City Li Da Lustre Finished Products Co., Ltd. |
|
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171103 |