CN107304322A - A kind of preparation method of novel heat-insulation coating for metal door and window - Google Patents
A kind of preparation method of novel heat-insulation coating for metal door and window Download PDFInfo
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- CN107304322A CN107304322A CN201710621429.6A CN201710621429A CN107304322A CN 107304322 A CN107304322 A CN 107304322A CN 201710621429 A CN201710621429 A CN 201710621429A CN 107304322 A CN107304322 A CN 107304322A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A kind of preparation method of novel heat-insulation coating for metal door and window, including following preparation process:A, aqueous acrylic emulsion is placed in the stirring of dispersion tank high speed, SiO 2 powder, guar gum, thickener, defoamer, coalescents and dispersant are added under stirring, it is scattered to obtain mixture one;Mixture two is obtained after b, addition filler, levelling agent and auxiliary rheological agents into mixture one, stirring, scattered, standing;C, addition UV absorbers, light stabilizer and antimildew disinfectant into mixture two, adjust pH, add talcum powder, cenosphere, land plaster and slip agent, and heating, stirring obtain mixture three;D, mixture three is subjected to ultrasonic wave stirring.The coating that the present invention is made has that gloss is high, the characteristic that gloss retention is good, outdoor weathe resistance is strong, also with good heat-insulated, UV resistant, temperature variation resistant, anti-mildew.
Description
Technical field
The invention belongs to the preparing technical field of door and window coating, and in particular to a kind of novel heat-insulation for metal door and window is applied
The preparation method of material.
Background technology
Door and window are important parts in buildings exterior-protected structure system, to be had respectively according to different design requirements
There is the function such as insulation, heat-insulated, sound insulation, waterproof, fire prevention.Also be the important component of architectural image, its shape, size, ratio,
Arrangement, color, moulding etc. will very big influences to the moulded of building.With people's life household mode become increasingly abundant it is many
Sample, the demand for life household mode is also improved therewith, wherein the raising for construction quality requirement more seems especially prominent,
Requirement to building doors and windows is protruded the most, and door and window used now has metal, plastics system, wooden etc. several, so making
The material of door and window turns into the object mainly studied.
Material is the mainstay of current science and technology, and because being that human social development and all scientific and technical bases are aobvious
It is particularly important, the development in science and technology degree of material can directly influence the change of productivity, and the material science of rising in recent years is tool
There is one of scientific domain of overall importance;Each economic power of the world brings up to Materials the strategic height of economic development, material
Scientific and engineering just enters a unprecedented high-speed developing period, and social development, the progress of human civilization shows, to material
The requirement more and more higher of material.Instantly the shortcoming of the composition metal door and window of in the market is that effect of heat insulation is poor, the heat conduction of composition metal
Performance is high so that effect of heat insulation is short of, but composition metal door and window has that energy consumption is low, cost is low, corrosion-resistant, service life length etc.
Advantage.
In summary, it is therefore desirable to which a kind of more preferable heat-insulating method improves the deficiencies in the prior art.
The content of the invention
It is an object of the invention to provide a kind of preparation method of the novel heat-insulation coating for metal door and window, the present invention is made
Coating have that gloss is high, the characteristic that gloss retention is good, outdoor weathe resistance is strong, also with good heat-insulated, UV resistant, heatproof
Change, anti-mildew.
The invention provides following technical scheme:
A kind of preparation method of novel heat-insulation coating for metal door and window, including following preparation process:
A, aqueous acrylic emulsion is placed in the stirring of dispersion tank high speed, rotating speed is 600-800r/min, stirs 23-45min, so
SiO 2 powder, guar gum, thickener, defoamer, coalescents and dispersant are added under stirring afterwards, by rotating speed liter
To 900-1000r/min, disperse 20-35min, obtain mixture one;
B, addition filler, levelling agent and auxiliary rheological agents into mixture one, disperse 20- under 700-800r/min rotating speed
30min, stands after 30-40min, obtains mixture two;
C, addition UV absorbers, light stabilizer and antimildew disinfectant into mixture two, regulation mixture ph is 7.5-
8.5, talcum powder, cenosphere, land plaster and slip agent are added, is heated at 120-150 DEG C and stirs 30-50min, is stirred
Speed is 200-300r/min, obtains mixture three;
D, mixture three carries out to ultrasonic wave stirring 30-40min, the frequency and the sound intensity for controlling ultrasonic wave be respectively 20-35KHz and
6-12W/cm2, stands after 1-2h, you can obtain finished product.
It is preferred that, the novel heat-insulation coating includes the raw material of following parts by weight:48-56 parts of aqueous acrylic emulsion, two
24-32 parts of silicon oxide powder, 18-24 parts of guar gum, 12-16 parts of thickener, 12-15 parts of defoamer, 11-13 parts of coalescents,
8-13 parts of dispersant, 12-16 parts of filler, 13-18 parts of levelling agent, 14-18 parts of auxiliary rheological agents, 21-24 parts of UV absorbers,
17-20 parts of light stabilizer, 13-18 parts of antimildew disinfectant, 22-25 parts of talcum powder, 13-17 parts of cenosphere, 22-25 parts of land plaster
With 16-18 parts of slip agent.
It is preferred that, the thickener of the step a is non-ionic associative type polyurethane thickener and the poly- ammonia of non-ionic associative type
Any of ester thickener or the mixing of the two.
It is preferred that, the coalescents of the step a are dipropylene and the mixture of dipropylene glycol methyl ether, dipropyl two
Alcohol butyl ether and dipropylene glycol methyl ether in mass ratio 4:3 are mixed.
It is preferred that, the filler of the step b is any in calcium carbonate, talcum powder, bentonite, kaolin and barium sulfate
Plant or a variety of mixing.
It is preferred that, the UV absorbers of the step c are benzophenone, azimidobenzene class, acrylic nitrile derivates and
Any of oxanilide derivative or a variety of mixing.
It is preferred that, the antimildew disinfectant of the step c is propiconazole and Tebuconazole and the iodo- 2- propargyls butylamino first of 3-
The mixture of acid esters, propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates in mass ratio 2 of 3-:5 mixing.
It is preferred that, talcum powder, cenosphere, land plaster and the slip agent of the step c were ground to 300-500 mesh sieves.
The beneficial effects of the invention are as follows:
Insulating moulding coating prepared by the present invention is not required to solvent dilution, and smell is small, and it is up to standard to not only improve plant gas, discharge of wastewater, again
The respiratory system of workman will not be stimulated.
The nuisance content such as benzene, toluene, heavy metal is small in insulating moulding coating prepared by the present invention, not carcinogenic, not aberration inducing, right
Water body, soil, biohazard are small.
Insulating moulding coating prepared by the present invention is rigidly small, and suppleness is good, not easy to crack, and the degree that aging becomes fragile is low, application property
It is good, dry ratio faster at normal temperatures, easily polishing.
The filler that the present invention is added can increase the volume of coating, reduce cost, at the same can also improve the durability of filler,
The performances such as grinability, hardness, addition levelling agent can be obviously improved the feel of coating, to the wetability of base material, in addition to paint film
Resistance to blocking it is helpful.
Embodiment
Embodiment 1
A kind of preparation method of novel heat-insulation coating for metal door and window, including following preparation process:
A, aqueous acrylic emulsion is placed in the stirring of dispersion tank high speed, rotating speed is 800r/min, stirs 45min, is then stirring
Mix and SiO 2 powder, guar gum, thickener, defoamer, coalescents and dispersant are added under state, rotating speed is risen to
1000r/min, disperses 35min, obtains mixture one;
B, addition filler, levelling agent and auxiliary rheological agents into mixture one, disperse 20min under 700r/min rotating speed, quiet
Put after 40min, obtain mixture two;
C, addition UV absorbers, light stabilizer and antimildew disinfectant into mixture two, regulation mixture ph is 7.5,
Talcum powder, cenosphere, land plaster and slip agent are added, is heated at 150 DEG C and stirs 30min, mixing speed is 200r/
Min, obtains mixture three;
D, mixture three carries out to ultrasonic wave stirring 30-40min, the frequency and the sound intensity for controlling ultrasonic wave be respectively 25KHz and
12W/cm2, stands after 2h, you can obtain finished product.
Novel heat-insulation coating includes the raw material of following parts by weight:56 parts of aqueous acrylic emulsion, 32 parts of SiO 2 powder,
24 parts of guar gum, 16 parts of thickener, 15 parts of defoamer, 13 parts of coalescents, 13 parts of dispersant, 16 parts of filler, levelling agent 18
It is part, 14 parts of auxiliary rheological agents, 24 parts of UV absorbers, 17 parts of light stabilizer, 13 parts of antimildew disinfectant, 22 parts of talcum powder, hollow
16 parts of 17 parts of microballon, 22 parts of land plaster and slip agent.
Step a thickener is the mixed of non-ionic associative type polyurethane thickener and non-ionic associative type polyurethane thickener
Close.
Step a coalescents are the mixture of dipropylene and dipropylene glycol methyl ether, dipropylene and two
Propylene glycol monomethyl ether in mass ratio 4:3 are mixed.
Step b filler is the mixing of calcium carbonate, talcum powder, bentonite, kaolin and barium sulfate.
Step c UV absorbers are that benzophenone, azimidobenzene class, acrylic nitrile derivates and oxanilide derive
The mixing of thing.
Step c antimildew disinfectant is the mixing of propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates of 3-
Thing, propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates in mass ratio 2 of 3-:5 mixing.
Step c talcum powder, cenosphere, land plaster and slip agent was ground to 500 mesh sieves.
Embodiment 2
A kind of preparation method of novel heat-insulation coating for metal door and window, including following preparation process:
A, aqueous acrylic emulsion is placed in the stirring of dispersion tank high speed, rotating speed is 600r/min, stirs 25min, is then stirring
Mix and SiO 2 powder, guar gum, thickener, defoamer, coalescents and dispersant are added under state, rotating speed is risen to
900r/min, disperses 20min, obtains mixture one;
B, addition filler, levelling agent and auxiliary rheological agents into mixture one, disperse 20min under 800r/min rotating speed, quiet
Put after 30min, obtain mixture two;
C, addition UV absorbers, light stabilizer and antimildew disinfectant into mixture two, regulation mixture ph is 8.5,
Talcum powder, cenosphere, land plaster and slip agent are added, is heated at 150 DEG C and stirs 50min, mixing speed is 200r/
Min, obtains mixture three;
D, mixture three is carried out to ultrasonic wave stirring 40min, the frequency and the sound intensity for controlling ultrasonic wave are 35KHz and 12W/cm respectively
2, stand after 2h, you can obtain finished product.
Novel heat-insulation coating includes the raw material of following parts by weight:48 parts of aqueous acrylic emulsion, 24 parts of SiO 2 powder,
18 parts of guar gum, 16 parts of thickener, 15 parts of defoamer, 11 parts of coalescents, 8 parts of dispersant, 12 parts of filler, levelling agent 18
It is part, 18 parts of auxiliary rheological agents, 21 parts of UV absorbers, 17 parts of light stabilizer, 18 parts of antimildew disinfectant, 22 parts of talcum powder, hollow
18 parts of 17 parts of microballon, 25 parts of land plaster and slip agent.
Step a thickener is the mixed of non-ionic associative type polyurethane thickener and non-ionic associative type polyurethane thickener
Close.
Step a coalescents are the mixture of dipropylene and dipropylene glycol methyl ether, dipropylene and two
Propylene glycol monomethyl ether in mass ratio 4:3 are mixed.
Step b filler is the mixing of calcium carbonate, talcum powder, bentonite, kaolin and barium sulfate.
Step c UV absorbers are that benzophenone, azimidobenzene class, acrylic nitrile derivates and oxanilide derive
The mixing of thing.
Step c antimildew disinfectant is the mixing of propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates of 3-
Thing, propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates in mass ratio 2 of 3-:5 mixing.
Step c talcum powder, cenosphere, land plaster and slip agent was ground to 500 mesh sieves.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (8)
1. the preparation method of a kind of novel heat-insulation coating for metal door and window, it is characterised in that including following preparation process:
A, aqueous acrylic emulsion is placed in the stirring of dispersion tank high speed, rotating speed is 600-800r/min, stirs 23-45min, so
SiO 2 powder, guar gum, thickener, defoamer, coalescents and dispersant are added under stirring afterwards, by rotating speed liter
To 900-1000r/min, disperse 20-35min, obtain mixture one;
B, addition filler, levelling agent and auxiliary rheological agents into mixture one, disperse 20- under 700-800r/min rotating speed
30min, stands after 30-40min, obtains mixture two;
C, addition UV absorbers, light stabilizer and antimildew disinfectant into mixture two, regulation mixture ph is 7.5-
8.5, talcum powder, cenosphere, land plaster and slip agent are added, is heated at 120-150 DEG C and stirs 30-50min, is stirred
Speed is 200-300r/min, obtains mixture three;
D, mixture three carries out to ultrasonic wave stirring 30-40min, the frequency and the sound intensity for controlling ultrasonic wave be respectively 20-35KHz and
6-12W/cm2, stands after 1-2h, you can obtain finished product.
2. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The novel heat-insulation coating includes the raw material of following parts by weight:48-56 parts of aqueous acrylic emulsion, SiO 2 powder 24-32
Part, 18-24 parts of guar gum, 12-16 parts of thickener, 12-15 parts of defoamer, 11-13 parts of coalescents, 8-13 parts of dispersant, fill out
Fill 12-16 parts of agent, 13-18 parts of levelling agent, 14-18 parts of auxiliary rheological agents, 21-24 parts of UV absorbers, light stabilizer 17-20
Part, 13-18 parts of antimildew disinfectant, 22-25 parts of talcum powder, 13-17 parts of cenosphere, 22-25 parts of land plaster and slip agent 16-18
Part.
3. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The thickener of the step a is any in non-ionic associative type polyurethane thickener and non-ionic associative type polyurethane thickener
Plant or the mixing of the two.
4. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The coalescents of the step a are the mixture of dipropylene and dipropylene glycol methyl ether, dipropylene and dipropyl two
Alcohol methyl ether in mass ratio 4:3 are mixed.
5. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The filler of the step b is any of calcium carbonate, talcum powder, bentonite, kaolin and barium sulfate or a variety of mixing.
6. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The UV absorbers of the step c is in benzophenone, azimidobenzene class, acrylic nitrile derivates and oxanilide derivatives
Any one or more mixing.
7. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
The antimildew disinfectant of the step c is the mixture of propiconazole and Tebuconazole and the iodo- 2- propargyl butyl carbamates of 3-, third
Ring azoles and Tebuconazole and the iodo- 2- propargyl butyl carbamates in mass ratio 2 of 3-:5 mixing.
8. a kind of preparation method of novel heat-insulation coating for metal door and window according to claim 1, it is characterised in that
Talcum powder, cenosphere, land plaster and the slip agent of the step c was ground to 300-500 mesh sieves.
Priority Applications (1)
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CN201710621429.6A CN107304322A (en) | 2017-07-27 | 2017-07-27 | A kind of preparation method of novel heat-insulation coating for metal door and window |
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CN201710621429.6A CN107304322A (en) | 2017-07-27 | 2017-07-27 | A kind of preparation method of novel heat-insulation coating for metal door and window |
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CN201710621429.6A Withdrawn CN107304322A (en) | 2017-07-27 | 2017-07-27 | A kind of preparation method of novel heat-insulation coating for metal door and window |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108300290A (en) * | 2018-01-24 | 2018-07-20 | 合肥万之景门窗有限公司 | A kind of heat preservation environment protection metal door and window coating and preparation method thereof |
CN109233473A (en) * | 2018-08-28 | 2019-01-18 | 巢湖市兰天大诚门窗幕墙有限公司 | The coating for composite energy-saving door and window with fire protecting performance |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105315819A (en) * | 2015-12-07 | 2016-02-10 | 苏州市神龙门窗有限公司 | Thermal-insulating anti-oxidation coating for outdoor doors and windows and preparation method thereof |
-
2017
- 2017-07-27 CN CN201710621429.6A patent/CN107304322A/en not_active Withdrawn
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105315819A (en) * | 2015-12-07 | 2016-02-10 | 苏州市神龙门窗有限公司 | Thermal-insulating anti-oxidation coating for outdoor doors and windows and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108300290A (en) * | 2018-01-24 | 2018-07-20 | 合肥万之景门窗有限公司 | A kind of heat preservation environment protection metal door and window coating and preparation method thereof |
CN109233473A (en) * | 2018-08-28 | 2019-01-18 | 巢湖市兰天大诚门窗幕墙有限公司 | The coating for composite energy-saving door and window with fire protecting performance |
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