CN107290224B - Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method - Google Patents

Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method Download PDF

Info

Publication number
CN107290224B
CN107290224B CN201710663713.XA CN201710663713A CN107290224B CN 107290224 B CN107290224 B CN 107290224B CN 201710663713 A CN201710663713 A CN 201710663713A CN 107290224 B CN107290224 B CN 107290224B
Authority
CN
China
Prior art keywords
fracturing
hydraulic
hydraulic cylinder
acoustic emission
test block
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201710663713.XA
Other languages
Chinese (zh)
Other versions
CN107290224A (en
Inventor
陈晨
朱颖
张晗
孙友宏
陈勇
李曦桐
潘栋彬
靳成才
刘书源
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jilin University
Original Assignee
Jilin University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jilin University filed Critical Jilin University
Priority to CN201710663713.XA priority Critical patent/CN107290224B/en
Publication of CN107290224A publication Critical patent/CN107290224A/en
Application granted granted Critical
Publication of CN107290224B publication Critical patent/CN107290224B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • G01N3/10Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces generated by pneumatic or hydraulic pressure
    • G01N3/12Pressure testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
    • G01N2203/0003Steady
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0019Compressive
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/003Generation of the force
    • G01N2203/0042Pneumatic or hydraulic means
    • G01N2203/0048Hydraulic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0062Crack or flaws
    • G01N2203/0064Initiation of crack
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0062Crack or flaws
    • G01N2203/0066Propagation of crack
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/022Environment of the test
    • G01N2203/0222Temperature
    • G01N2203/0226High temperature; Heating means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/025Geometry of the test
    • G01N2203/0256Triaxial, i.e. the forces being applied along three normal axes of the specimen
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/0658Indicating or recording means; Sensing means using acoustic or ultrasonic detectors

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a microwave heating device and an experimental method for a true triaxial hydraulic fracturing simulation experiment, wherein the microwave heating device comprises a triaxial pressurizing unit, a microwave heating unit, a fracturing fluid injection unit, an acoustic emission monitoring unit, a temperature monitoring unit and a control and signal acquisition unit: the invention combines the microwave heating equipment and the hydraulic fracturing equipment, avoids the change of the property of the experimental test block caused by the lack of simulated ground stress in the connection process in the existing experimental equipment, and better simulates the influence of the expansion and contraction property of the rock on the hydraulic fracturing effect; the condition that the test block is subjected to thermal expansion in the microwave heating process under the simulated ground stress condition can be monitored; the influence rule of parameters such as the ground stress condition, the heating temperature, the temperature difference between the test block and the fracturing fluid, the perforation condition and the like on the initiation and extension of the crack can be inspected.

Description

用于真三轴水力压裂模拟实验的微波加热装置及实验方法Microwave heating device and experimental method for true triaxial hydraulic fracturing simulation experiment

技术领域technical field

本发明涉及油气藏水力压裂以及微波加热研究领域,特别涉及一种真三轴水力压裂模拟实验的微波加热装置及实验方法,用以监测在模拟地应力条件下岩石热胀冷缩的性质对提高水力压裂效果的作用,并考察地应力条件、加热温度、试块与压裂液的温差和射孔条件等参数对裂缝起裂和延伸的影响规律。The present invention relates to the field of oil and gas reservoir hydraulic fracturing and microwave heating research, in particular to a microwave heating device and experimental method for a true triaxial hydraulic fracturing simulation experiment, which is used to monitor the properties of thermal expansion and contraction of rocks under simulated ground stress conditions To improve the effect of hydraulic fracturing, and investigate the influence of parameters such as ground stress conditions, heating temperature, temperature difference between test block and fracturing fluid, and perforation conditions on fracture initiation and extension.

背景技术Background technique

随着经济的迅猛发展,国家的能源需求量不断提升。水力压裂技术,是油气藏开采过程中常用的增产措施。利用水力压裂技术,可增大油气储集层的天然裂缝、形成人工裂缝、增强裂缝之间的连通性,提高油气储集层的渗透率。同时,利用岩石热胀冷缩的性质,可提高水力压裂的效率,有利于裂缝网络的形成。With the rapid development of the economy, the country's energy demand continues to increase. Hydraulic fracturing technology is a commonly used stimulation measure in the process of oil and gas reservoir exploitation. The use of hydraulic fracturing technology can increase the natural fractures of oil and gas reservoirs, form artificial fractures, enhance the connectivity between fractures, and improve the permeability of oil and gas reservoirs. At the same time, utilizing the thermal expansion and contraction properties of rocks can improve the efficiency of hydraulic fracturing and facilitate the formation of fracture networks.

微波加热技术与传导、对流等传统加热技术相比,具有瞬时加热、热损耗小以及操作方便等特点。微波加热过程,是一个加热介质内外部同时加热、升温的过程。因此,加热过程中并不存在温度梯度,大大提高了介质加热质量与加热效率。同时,其即加即停的特性有利于自动化控制的生产。Compared with traditional heating technologies such as conduction and convection, microwave heating technology has the characteristics of instantaneous heating, small heat loss and convenient operation. The microwave heating process is a process in which the inside and outside of the heating medium are heated and heated at the same time. Therefore, there is no temperature gradient in the heating process, which greatly improves the heating quality and heating efficiency of the medium. At the same time, its feature of starting and stopping is conducive to the production of automatic control.

在过去的研究中,加热油气储集层的过程中并未考虑到地应力的作用,其实验结果往往与真实地层中的加热情况有所差距。同时,现有装置未能将油气储集层加热与水力压裂的过程衔接起来,不能有效地模拟出热胀冷缩的性质对地下油气储集层水力压裂的作用。因此,设计能将油气储集层加热和水力压裂相结合的实验装置,对模拟地下油气储集层受热膨胀以及压裂过程中岩石热胀冷缩性质的作用有重要意义。In previous studies, the effect of in-situ stress was not considered in the process of heating oil and gas reservoirs, and the experimental results were often different from the heating conditions in real formations. At the same time, the existing devices fail to link the heating of oil and gas reservoirs with the process of hydraulic fracturing, and cannot effectively simulate the effects of thermal expansion and contraction on hydraulic fracturing of underground oil and gas reservoirs. Therefore, designing an experimental device that can combine heating of oil and gas reservoirs with hydraulic fracturing is of great significance for simulating the thermal expansion of underground oil and gas reservoirs and the effects of thermal expansion and contraction of rocks during fracturing.

因此,首先需要对开采区油气藏储层埋藏区的地应力条件、裂缝起裂与延伸等情况有所调查。同时,考虑到微波泄露的危害性,在实验装置使用前,必须对进行微波装置控制的所在区域进行微波泄漏检测,以“每平方厘米不超过5毫瓦”为标准。Therefore, it is first necessary to investigate the in-situ stress conditions, fracture initiation and extension of the oil and gas reservoir burial area in the production area. At the same time, considering the harmfulness of microwave leakage, microwave leakage detection must be carried out in the area where the microwave device is controlled before the experimental device is used, with the standard of "no more than 5 milliwatts per square centimeter".

发明内容Contents of the invention

本发明的目的是监测在模拟地应力条件下,岩石热胀冷缩性质对提高水力压裂效果的作用,并观察不同温度、温差及射孔条件等参数对裂缝起裂及延伸的影响,为此提供了一种用于真三轴水力压裂模拟实验的微波加热装置及实验方法。The purpose of the present invention is to monitor the effect of thermal expansion and contraction of rock on improving the effect of hydraulic fracturing under simulated ground stress conditions, and to observe the influence of parameters such as different temperatures, temperature differences and perforation conditions on fracture initiation and extension. This provides a microwave heating device and an experimental method for a true triaxial hydraulic fracturing simulation experiment.

本发明之真三轴水力压裂模拟实验的微波加热装置,包括三轴加压单元、微波加热单元、压裂液注入单元、声发射监测单元、温度监测单元和控制及信号采集单元:The microwave heating device for the true triaxial hydraulic fracturing simulation experiment of the present invention includes a triaxial pressurization unit, a microwave heating unit, a fracturing fluid injection unit, an acoustic emission monitoring unit, a temperature monitoring unit, and a control and signal acquisition unit:

所述三轴加压单元包括四个固定轴、八个螺栓、压裂室主机、推进台、三个加载板、一个后挡板、X向三通阀、Y向三通阀、Z向三通阀、X向压力传感器、Y向压力传感器、Z向压力传感器、X向加压液压缸、Y向加压液压缸、Z向加压液压缸、两个X向卸料液压缸和液压站;The three-axis pressurization unit includes four fixed shafts, eight bolts, a fracturing chamber host, a propulsion platform, three loading plates, a rear baffle, an X-direction three-way valve, a Y-direction three-way valve, and a Z-direction three-way valve. Through valve, X-direction pressure sensor, Y-direction pressure sensor, Z-direction pressure sensor, X-direction pressurization hydraulic cylinder, Y-direction pressurization hydraulic cylinder, Z-direction pressurization hydraulic cylinder, two X-direction discharge hydraulic cylinders and hydraulic station ;

其中,Y向加压液压缸、Z向加压液压缸均通过沉头螺钉固定在压裂室主机上;X向加压液压缸与压裂室主机通过四个固定轴和八个螺栓进行螺纹密封连接;推进台通过胶接连接方式,一面与X向加压液压缸的底座连接,一面与压裂室主机连接,并与试样室底边重合,以便推送实验试块进入试样室;X向退料油缸通过沉头螺钉固定在压裂室主机上;X向加压液压缸、Y向加压液压缸、Z向加压液压缸的液压杆端部分别与加载板连接,连接方式为沉头螺钉连接;在X方向上,试样室内放有后挡板,且与两个X向卸料液压缸的液压杆端部通过沉头螺钉连接;Among them, the Y-direction pressurized hydraulic cylinder and the Z-directed pressurized hydraulic cylinder are fixed on the main machine of the fracturing chamber through countersunk screws; the X-directed pressurized hydraulic cylinder and the main machine of the fracturing room are threaded through four fixed shafts and eight bolts. Sealed connection; the propulsion platform is connected by glue, one side is connected to the base of the X-direction pressurized hydraulic cylinder, and the other side is connected to the main machine of the fracturing chamber, and coincides with the bottom edge of the sample chamber, so as to push the experimental test block into the sample chamber; The X-direction material return cylinder is fixed on the main machine of the fracturing chamber through the countersunk head screw; the ends of the hydraulic rods of the X-direction pressurization hydraulic cylinder, Y-direction pressurization hydraulic cylinder, and Z-direction pressurization hydraulic cylinder are respectively connected to the loading plate. It is connected by countersunk screws; in the X direction, there is a rear baffle in the sample chamber, and it is connected with the ends of the hydraulic rods of the two X-direction unloading hydraulic cylinders through countersunk screws;

X向加压液压缸、Y向加压液压缸和Z向加压液压缸进油口连接处,分别与X向三通阀、Y向三通阀和Z向三通阀螺纹连接分成两路,一路分别与X向压力传感器、Y向压力传感器和Z向压力传感器通过螺纹密封连接,将压力信息传递给控制及信号采集单元;另一路分别与液压油运输管道连接,连接方式为六角接头螺纹连接;X向退料液压缸与液压油运输管道连接,连接方式为六角接头螺纹连接;The X-direction pressurized hydraulic cylinder, Y-directed pressurized hydraulic cylinder and Z-directed pressurized hydraulic cylinder oil inlet connections are divided into two lines with X-direction three-way valve, Y-direction three-way valve and Z-direction three-way valve respectively. , one way is respectively connected with the X-direction pressure sensor, Y-direction pressure sensor and Z-direction pressure sensor through thread sealing, and the pressure information is transmitted to the control and signal acquisition unit; the other one is respectively connected with the hydraulic oil transportation pipeline, and the connection method is hexagonal joint thread Connection; the X-direction return hydraulic cylinder is connected with the hydraulic oil transportation pipeline, and the connection method is a hexagonal joint threaded connection;

液压站包括液压阀组合、泵装置、油箱、压力控制器和囊式蓄能器,与液压油运输管道连接以提供液压源,连接方式为六角接头螺纹连接;The hydraulic station includes a hydraulic valve combination, a pump device, an oil tank, a pressure controller and a bladder accumulator, which are connected to the hydraulic oil transportation pipeline to provide a hydraulic source, and the connection method is a hexagonal joint threaded connection;

所述微波加热单元包括微波发生装置、波导管和微波天线;所述微波发生装置可在一定范围内,调节微波的频率及功率;所述微波天线固定在三轴加压单元装置的底座中,微波天线位于压裂试样室的下方;所述波导管与微波天线连接,波导管固定在三轴加压单元装置的底座中;The microwave heating unit includes a microwave generating device, a waveguide and a microwave antenna; the microwave generating device can adjust the frequency and power of the microwave within a certain range; the microwave antenna is fixed in the base of the triaxial pressurizing unit device, The microwave antenna is located below the fracturing sample chamber; the waveguide is connected to the microwave antenna, and the waveguide is fixed in the base of the triaxial pressurization unit device;

所述压裂液注入单元包括单向液压缸、压裂液泵送控制系统和压裂液管线,可控制压裂液泵送的压力及速度;所述压裂液管线穿过前六角螺栓与后六角螺栓,前六角螺栓与实验试块上固定的模拟套管通过进行螺纹密封连接,后六角螺栓与压裂室主机通过螺纹密封连接,防止微波泄露;The fracturing fluid injection unit includes a one-way hydraulic cylinder, a fracturing fluid pumping control system and a fracturing fluid pipeline, which can control the pressure and speed of the fracturing fluid pumping; the fracturing fluid pipeline passes through the front hexagon bolt and The rear hexagonal bolt, the front hexagonal bolt and the simulated casing fixed on the experimental test block are connected through thread sealing, and the rear hexagonal bolt is connected with the host machine of the fracturing chamber through thread sealing to prevent microwave leakage;

所述声发射监测单元包括通过胶接与加载板四个顶点处连接的声发射传感器,声发射传感器传输线从加载板后的槽口中伸出,声发射传感器传输线固定在固定管道中;在Y、Z方向上,固定管道一端与压裂室主机通过螺纹连接,另一端可固定传输线;固定管道材质属于微波反射材料;The acoustic emission monitoring unit includes an acoustic emission sensor connected to the four vertices of the loading plate by gluing, the transmission line of the acoustic emission sensor protrudes from the notch behind the loading plate, and the transmission line of the acoustic emission sensor is fixed in the fixed pipeline; in Y, In the Z direction, one end of the fixed pipe is threadedly connected to the main unit of the fracturing chamber, and the other end can be used to fix the transmission line; the material of the fixed pipe is a microwave reflective material;

所述温度监测单元包括通过胶接与加载板中心处连接的温度传感器,温度传感器传输线从加载板后的槽口中伸出并固定在固定管道中;The temperature monitoring unit includes a temperature sensor connected to the center of the loading plate through glue, and the temperature sensor transmission line protrudes from the notch behind the loading plate and is fixed in the fixed pipe;

所述控制及信号采集单元与压力传感器传输线连接,采集模拟地应力值并显示在显示装置上;控制及信号采集单元与液压站通过信号传输线连接,利用其三轴加压控制装置可直接控制施加的三轴应力大小;控制及信号采集单元与声发射传感器传输线连接,内置的声发射信号处理装置处理声发射信号并显示在显示装置上;控制及信号采集单元与压裂液注入单元通过信号传输线连接,采集压裂液泵送信息并显示在显示装置上;控制及信号采集单元与温度传感器传输线连接,监测实验试块加热实时信息并显示在显示装置上;The control and signal acquisition unit is connected with the pressure sensor transmission line, and the simulated ground stress value is collected and displayed on the display device; the control and signal acquisition unit is connected with the hydraulic station through the signal transmission line, and the three-axis pressurization control device can be used to directly control the applied pressure. The magnitude of the triaxial stress; the control and signal acquisition unit is connected with the transmission line of the acoustic emission sensor, and the built-in acoustic emission signal processing device processes the acoustic emission signal and displays it on the display device; the control and signal acquisition unit and the fracturing fluid injection unit pass through the signal transmission line Connect, collect the fracturing fluid pumping information and display it on the display device; the control and signal acquisition unit is connected with the temperature sensor transmission line, monitor the real-time information of the heating of the experimental test block and display it on the display device;

优选的,压裂室主机除微波天线正上方的试样室底部材质外,其余材质均属于微波反射材料;加载板、后挡板、后六角螺栓、固定管道、X向加压液压缸、Y向加压液压缸、Z向加压液压缸、两个X向卸料液压缸的缸体与液压杆均属于微波反射材料;声发射传感器与温度传感器耐高温,采用的耦合剂耐高温,方便灵敏测得信号。Preferably, except for the material at the bottom of the sample chamber directly above the microwave antenna, the other materials of the fracturing chamber host are all microwave reflective materials; The cylinders and hydraulic rods of the pressurizing hydraulic cylinder, the pressurizing hydraulic cylinder in the Z direction, and the two unloading hydraulic cylinders in the X direction are microwave reflective materials; the acoustic emission sensor and temperature sensor are resistant to high temperature, and the coupling agent used is resistant to high temperature, which is convenient Sensitively detected signal.

本发明之真三轴水力压裂模拟实验的微波加热装置的实验方法,包括如下步骤:The experimental method of the microwave heating device of the true three-axis hydraulic fracturing simulation experiment of the present invention comprises the following steps:

步骤一、计算微波频率λ:测量采集到的油气藏储层岩样的介电常数ε’与介电损耗因子ε”,以该试块的尺寸为基准,计算微波频率λ,L为实验试块上底面与微波天线之间的距离:

Figure BDA0001371236500000041
Step 1. Calculate the microwave frequency λ: measure the dielectric constant ε' and dielectric loss factor ε" of the collected oil and gas reservoir rock samples, and calculate the microwave frequency λ based on the size of the test block, where L is the experimental test Distance between the bottom surface of the block and the microwave antenna:
Figure BDA0001371236500000041

步骤二、制作实验试块:在采集的油气藏储层岩样中心位置钻得扩孔段与裸眼压裂段,并插入模拟套管,且以之为中心,浇筑混凝土制得尺寸为200*200*200mm的实验试块;Step 2. Make the experimental test block: Drill the reaming section and the open hole fracturing section at the center of the collected oil and gas reservoir rock samples, insert the simulated casing, and take it as the center, pour concrete to make a size of 200* 200*200mm experimental test block;

步骤三、实验试块到位:向制得的实验试块上的模拟套管中注水排净空气,将其与压裂液管线相连;在X、Y、Z方向上的声发射传感器面上涂抹耐高温耦合剂以便更好地测得声发射信号,并利用X向加压液压缸将实验试块推入压裂室主机的试样室内,同时将后六角螺栓与压裂室主机连接;Step 3: Put the experimental test block in place: inject water into the simulated casing on the prepared experimental test block to drain the air, and connect it to the fracturing fluid pipeline; smear on the surface of the acoustic emission sensor in the X, Y, and Z directions High-temperature-resistant couplant to better measure the acoustic emission signal, and use the X-direction pressurized hydraulic cylinder to push the experimental test block into the sample chamber of the fracturing chamber host, and at the same time connect the rear hexagonal bolt to the fracturing chamber host;

步骤四、三轴压力加载:启动控制及信号采集单元,利用三轴加压控制装置控制三轴压力加载,直至达到设定的模拟地应力值;Step 4. Triaxial pressure loading: start the control and signal acquisition unit, and use the triaxial pressure control device to control the triaxial pressure loading until the set simulated ground stress value is reached;

步骤五、微波加热:开启微波发生装置,以步骤一中计算所得的微波频率λ加热实验试块,观察声发射监测单元采集的声发射信号波形;当显示装置上的温度达到设定温度时,关闭微波发生装置;Step 5, microwave heating: turn on the microwave generating device, heat the experimental test block with the microwave frequency λ calculated in step 1, and observe the acoustic emission signal waveform collected by the acoustic emission monitoring unit; when the temperature on the display device reaches the set temperature, Turn off the microwave generator;

步骤六、进行水力压裂:开启压裂液泵系统,以一定排量按设定的泵送压力或泵送速度向实验试块泵送压裂液;通过声发射监测单元采集压裂过程中的声发射信号,观察声发射信号波形变化;观察显示装置上的水力压裂压力曲线与X、Y、Z三轴压力曲线;当水力压裂压力值以及三轴压力值归零时,水力压裂过程结束;Step 6. Carry out hydraulic fracturing: turn on the fracturing fluid pump system, pump fracturing fluid to the experimental test block with a certain displacement according to the set pumping pressure or pumping speed; collect data during the fracturing process through the acoustic emission monitoring unit Acoustic emission signal, observe the waveform change of the acoustic emission signal; observe the hydraulic fracturing pressure curve and the X, Y, Z triaxial pressure curve on the display device; when the hydraulic fracturing pressure value and the triaxial pressure value return to zero, the hydraulic fracturing pressure end of cracking process;

步骤七、取出实验试块:利用三轴加压控制装置控制X、Y、Z向的压力逐渐减少直至归零,X向加压液压缸的液压杆移出试样室,控制X向卸料液压缸及后挡板将实验试块推出;Step 7. Take out the experimental test block: Use the three-axis pressurization control device to control the pressure in the X, Y, and Z directions to gradually decrease until it returns to zero. The cylinder and the rear baffle push out the test block;

本发明的有益效果:Beneficial effects of the present invention:

本发明提供的真三轴水力压裂模拟实验的微波加热装置及实验方法,相比现有技术,结合了微波加热设备与水力压裂设备,避免了现有的实验设备中,由于连接过程中模拟地应力的缺失,而导致的实验试块性质的变化,更好地模拟岩石热胀冷缩性质对水力压裂效果的影响;能监测在模拟地应力条件下,微波加热时实验试块受热膨胀的情况;能考察地应力条件、加热温度、试块与压裂液的温差和射孔条件等参数对裂缝起裂和延伸的影响规律。Compared with the prior art, the microwave heating device and the experimental method of the true triaxial hydraulic fracturing simulation experiment provided by the present invention combine the microwave heating equipment and the hydraulic fracturing equipment, avoiding the existing experimental equipment, due to the The change of the properties of the experimental test block caused by the lack of simulated in-situ stress can better simulate the influence of rock thermal expansion and contraction on the effect of hydraulic fracturing; it can monitor the impact of the experimental test block when microwave heating is performed under the simulated in-situ stress condition. The situation of thermal expansion; it can investigate the influence of parameters such as ground stress conditions, heating temperature, temperature difference between test block and fracturing fluid, and perforation conditions on fracture initiation and extension.

附图说明Description of drawings

图1为本发明之模拟实验装置的结构示意图。Fig. 1 is the schematic structural diagram of the simulation experiment device of the present invention.

图2为本发明之三轴加压单元的立体结构示意图。Fig. 2 is a three-dimensional structure schematic diagram of the triaxial pressing unit of the present invention.

图3为本发明之三轴加压单元的结构剖视图。Fig. 3 is a structural sectional view of the triaxial pressing unit of the present invention.

图4为本发明之加载板半剖面结构示意图。Fig. 4 is a schematic diagram of the half-section structure of the loading plate of the present invention.

图5为本发明之声发射传感器与温度传感器传输结构示意图。Fig. 5 is a schematic diagram of the transmission structure of the acoustic emission sensor and the temperature sensor of the present invention.

图6为本发明中实验试块结构示意图。Fig. 6 is a schematic diagram of the structure of the experimental test block in the present invention.

图中:1.微波发生装置;2.波导管;3.微波天线;4.液压站;5.油箱;6.囊式蓄能器;7.液压阀组合;8.泵装置;9.压力控制器;10.X向加压液压缸;11.Y向加压液压缸;12.Z向加压液压缸;13.X向退料液压缸;14.螺栓;15.固定轴;16.推进台;17.压裂室主机;18.试样室;9.X向压力传感器;20.Y向压力传感器;21.Z向压力传感器;22.X向三通阀;23.Y向三通阀;24.Z向三通阀;25.加载板;26.压裂液管线;27.前六角螺栓;28.后六角螺栓;29.液压油运输管道;30.压裂液泵送控制系统;31.单向液压缸;32.信号传输线;33.固定管道;34.声发射传感器传输线;35.温度传感器传输线;36.压力传感器传输线;37.显示装置;38.三轴加压控制装置;39.声发射信号处理装置;301.后挡板;401.声发射传感器;402.温度传感器;403.槽口;601.实验试块;602.裸眼压裂段;603.扩孔段;604.模拟套管。In the figure: 1. Microwave generator; 2. Waveguide; 3. Microwave antenna; 4. Hydraulic station; 5. Oil tank; 6. Bladder accumulator; 7. Hydraulic valve combination; 8. Pump device; 9. Pressure Controller; 10. X-direction pressurized hydraulic cylinder; 11. Y-directed pressurized hydraulic cylinder; 12. Z-directed pressurized hydraulic cylinder; 13. X-directed material return hydraulic cylinder; 14. Bolts; 15. Fixed shaft; 16. 17. Fracturing chamber host; 18. Sample chamber; 9. X-direction pressure sensor; 20. Y-direction pressure sensor; 21. Z-direction pressure sensor; 22. X-direction three-way valve; 23. Y-direction three-way valve; One-way valve; 24. Z-direction three-way valve; 25. Loading plate; 26. Fracturing fluid pipeline; 27. Front hexagonal bolt; 28. Rear hexagonal bolt; 29. Hydraulic oil transportation pipeline; 30. Fracturing fluid pumping control System; 31. One-way hydraulic cylinder; 32. Signal transmission line; 33. Fixed pipeline; 34. Acoustic emission sensor transmission line; 35. Temperature sensor transmission line; 36. Pressure sensor transmission line; 37. Display device; 38. Three-axis pressurization control Device; 39. Acoustic emission signal processing device; 301. Back baffle; 401. Acoustic emission sensor; 402. Temperature sensor; 403. Notch; 601. Experimental test block; ; 604. Mock casing.

具体实施方式Detailed ways

如图1、图2、图3、图4和图5所示,本发明所述的一种真三轴水力压裂模拟实验的微波加热装置,包括三轴加压单元、微波加热单元、压裂液注入单元、声发射监测单元、温度监测单元和控制及信号采集单元:As shown in Fig. 1, Fig. 2, Fig. 3, Fig. 4 and Fig. 5, a microwave heating device for a true triaxial hydraulic fracturing simulation experiment according to the present invention includes a triaxial pressurizing unit, a microwave heating unit, a pressing Fissure fluid injection unit, acoustic emission monitoring unit, temperature monitoring unit and control and signal acquisition unit:

所述三轴加压单元包括四个固定轴15、八个螺栓14、压裂室主机17、推进台16、三个加载板25、后挡板301、X向三通阀22、Y向三通阀23、Z向三通阀24、X向压力传感器19、Y向压力传感器20、Z向压力传感器21、X向加压液压缸10、Y向加压液压缸11、Z向加压液压缸12、两个X向卸料液压缸13和液压站4;The three-axis pressurization unit includes four fixed shafts 15, eight bolts 14, a fracturing chamber host 17, a propulsion table 16, three loading plates 25, a rear baffle 301, an X-direction three-way valve 22, and a Y-direction three-way valve. One-way valve 23, Z-direction three-way valve 24, X-direction pressure sensor 19, Y-direction pressure sensor 20, Z-direction pressure sensor 21, X-direction pressurization hydraulic cylinder 10, Y-direction pressurization hydraulic cylinder 11, Z-direction pressurization hydraulic cylinder Cylinder 12, two X-direction unloading hydraulic cylinders 13 and hydraulic station 4;

其中,Y向加压液压缸11、Z向加压液压缸12均通过沉头螺钉固定在压裂室主机17上;X向加压液压缸10与压裂室主机17通过四个固定轴15和八个螺栓14进行螺纹密封连接;推进台16通过胶接连接方式,一面与X向加压液压缸10的底座连接,一面与压裂室主机17连接,并与试样室18底边重合,以便推送实验试块进入试样室18;X向退料油缸13通过沉头螺钉固定在压裂室主机17上;X向加压液压缸10、Y向加压液压缸11、Z向加压液压缸12的液压杆端部分别与加载板25连接,连接方式为沉头螺钉连接;在X方向上,试样室内放有后挡板301,且与两个X向卸料液压缸13的液压杆端部通过沉头螺钉连接;Among them, the Y-direction pressurized hydraulic cylinder 11 and the Z-directed pressurized hydraulic cylinder 12 are fixed on the main machine 17 of the fracturing chamber through countersunk screws; It is threaded and sealed with eight bolts 14; the propulsion platform 16 is connected with the base of the X-direction pressurized hydraulic cylinder 10 on one side, and connected to the main machine 17 of the fracturing chamber on the other side, and coincides with the bottom edge of the sample chamber 18 , so as to push the experimental test block into the sample chamber 18; the X-direction material return cylinder 13 is fixed on the fracturing chamber main machine 17 through countersunk screws; the X-direction pressurization hydraulic cylinder 10, the Y-direction pressurization hydraulic cylinder 11, the Z-direction pressurization The ends of the hydraulic rods of the pressure hydraulic cylinder 12 are respectively connected with the loading plate 25 by countersunk screws; in the X direction, a rear baffle 301 is placed in the sample chamber, and it is connected with two X direction unloading hydraulic cylinders 13 The end of the hydraulic rod is connected by a countersunk screw;

X向加压液压缸10、Y向加压液压缸11和Z向加压液压缸12进油口连接处,分别与X向三通阀22、Y向三通阀23和Z向三通阀24螺纹连接分成两路,一路分别与X向压力传感器19、Y向压力传感器20和Z向压力传感器21通过螺纹密封连接,将压力信息传递给控制及信号采集单元;另一路分别与液压油运输管道29连接,连接方式为六角接头螺纹连接;X向退料液压缸13与液压油运输管道29连接,连接方式为六角接头螺纹连接;X-direction pressurized hydraulic cylinder 10, Y-directed pressurized hydraulic cylinder 11 and Z-directed pressurized hydraulic cylinder 12 are connected to the oil inlet ports of X-directed three-way valve 22, Y-directed three-way valve 23 and Z-directed three-way valve respectively. 24 The thread connection is divided into two ways, one way is respectively connected with the X-direction pressure sensor 19, the Y-direction pressure sensor 20 and the Z-direction pressure sensor 21 through thread sealing, and the pressure information is transmitted to the control and signal acquisition unit; the other way is respectively connected with the hydraulic oil transportation The pipeline 29 is connected, and the connection method is a hexagonal joint threaded connection; the X-direction material return hydraulic cylinder 13 is connected to the hydraulic oil transportation pipeline 29, and the connection method is a hexagonal joint threaded connection;

液压站4包括液压阀组合7、泵装置8、油箱5、压力控制器9和囊式蓄能器6,与液压油运输管道29连接以提供液压源,连接方式为六角接头螺纹连接;The hydraulic station 4 includes a hydraulic valve combination 7, a pump device 8, a fuel tank 5, a pressure controller 9 and a bladder accumulator 6, and is connected to a hydraulic oil transportation pipeline 29 to provide a hydraulic source, and the connection method is a hexagonal joint threaded connection;

所述微波加热单元包括微波发生装置1、波导管2和微波天线3;所述微波发生装置1可在一定范围内,调节微波的频率及功率;所述微波天线3固定在三轴加压单元的底座中,微波天线3位于压裂试样室的下方;所述波导管2与微波天线3连接,波导管2固定在三轴加压单元的底座中;The microwave heating unit includes a microwave generator 1, a waveguide 2 and a microwave antenna 3; the microwave generator 1 can adjust the frequency and power of microwaves within a certain range; the microwave antenna 3 is fixed on the triaxial pressurization unit In the base, the microwave antenna 3 is located below the fracturing sample chamber; the waveguide 2 is connected to the microwave antenna 3, and the waveguide 2 is fixed in the base of the triaxial pressurization unit;

所述压裂液注入单元包括单向液压缸31、压裂液泵送控制系统30和压裂液管线26,可控制压裂液泵送的压力及速度;所述压裂液管线26穿过前六角螺栓27与后六角螺栓28,前六角螺栓27与实验试块601上固定的模拟套管604通过进行螺纹密封连接,后六角螺栓28与压裂室主机17通过螺纹密封连接,防止微波泄露;The fracturing fluid injection unit includes a one-way hydraulic cylinder 31, a fracturing fluid pumping control system 30 and a fracturing fluid pipeline 26, which can control the pressure and speed of fracturing fluid pumping; the fracturing fluid pipeline 26 passes through The front hexagonal bolt 27 and the rear hexagonal bolt 28, the front hexagonal bolt 27 and the simulated sleeve 604 fixed on the experimental test block 601 are connected by thread sealing, and the rear hexagonal bolt 28 is connected with the host machine 17 of the fracturing chamber by thread sealing to prevent microwave leakage ;

所述声发射监测单元包括通过胶接与加载板四个顶点处连接的声发射传感器401,声发射传感器传输线34从加载板25后的槽口403中伸出,声发射传感器传输线34固定在固定管道33中;在Y、Z方向上,固定管道33一端与压裂室主机17通过螺纹连接,固定管道33另一端能固定传输线;固定管道33材质属于微波反射材料;The acoustic emission monitoring unit includes an acoustic emission sensor 401 connected to the four apexes of the loading plate by gluing, the acoustic emission sensor transmission line 34 protrudes from the notch 403 behind the loading plate 25, and the acoustic emission sensor transmission line 34 is fixed on a fixed In the pipeline 33; in the Y and Z directions, one end of the fixed pipeline 33 is threadedly connected to the fracturing chamber host 17, and the other end of the fixed pipeline 33 can fix the transmission line; the material of the fixed pipeline 33 is a microwave reflective material;

所述温度监测单元包括通过胶接与加载板中心处连接的温度传感器402,温度传感器传输线35从加载板25后的槽口403中伸出并固定在固定管道33中;The temperature monitoring unit includes a temperature sensor 402 connected to the center of the loading plate by gluing, and the temperature sensor transmission line 35 protrudes from the notch 403 behind the loading plate 25 and is fixed in the fixed pipe 33;

所述控制及信号采集单元与压力传感器传输线36连接,采集模拟地应力值并显示在显示装置37上;控制及信号采集单元与液压站4通过信号传输线32连接,利用其三轴加压控制装置38可直接控制施加的三轴应力大小;控制及信号采集单元与声发射传感器传输线34连接,内置的声发射信号处理装置39处理声发射信号并显示在显示装置37上;控制及信号采集单元与压裂液注入单元通过信号传输线32连接,采集压裂液泵送信息并显示在显示装置37上;控制及信号采集单元与温度传感器传输线35连接,监测实验试块加热实时信息并显示在显示装置37上;The control and signal acquisition unit is connected with the pressure sensor transmission line 36, collects the simulated ground stress value and displays it on the display device 37; the control and signal acquisition unit is connected with the hydraulic station 4 through the signal transmission line 32, and uses its three-axis pressurization control device 38 can directly control the magnitude of the applied triaxial stress; the control and signal acquisition unit is connected to the acoustic emission sensor transmission line 34, and the built-in acoustic emission signal processing device 39 processes the acoustic emission signal and displays it on the display device 37; the control and signal acquisition unit is connected to the acoustic emission sensor transmission line 34. The fracturing fluid injection unit is connected through the signal transmission line 32, collects the fracturing fluid pumping information and displays it on the display device 37; the control and signal acquisition unit is connected with the temperature sensor transmission line 35, monitors the real-time information of the heating of the experimental test block and displays it on the display device 37 on;

优选的,压裂室主机17除微波天线3正上方的试样室18底部材质外,其余材质均属于微波反射材料;加载板25、后挡板301、后六角螺栓28、固定管道33、X向加压液压缸10、Y向加压液压缸11、Z向加压液压缸12、两个X向卸料液压缸13的缸体与液压杆均属于微波反射材料;声发射传感器401与温度传感器402耐高温,采用的耦合剂耐高温,方便灵敏测得信号。Preferably, except for the bottom material of the sample chamber 18 directly above the microwave antenna 3, the main machine 17 of the fracturing chamber is made of microwave reflective materials; The cylinder bodies and hydraulic rods of the pressurizing hydraulic cylinder 10, the Y-direction pressurizing hydraulic cylinder 11, the Z-direction pressurizing hydraulic cylinder 12, and the two X-direction unloading hydraulic cylinders 13 are microwave reflective materials; the acoustic emission sensor 401 and temperature The sensor 402 is resistant to high temperature, and the couplant used is resistant to high temperature, so it is convenient and sensitive to measure the signal.

本发明之真三轴水力压裂模拟实验的微波加热装置的实验方法,包括如下步骤:The experimental method of the microwave heating device of the true three-axis hydraulic fracturing simulation experiment of the present invention comprises the following steps:

步骤一、计算微波频率λ:测量采集到的油气藏储层岩样的介电常数ε’与介电损耗因子ε”,以该试块的尺寸为基准,计算微波频率λ,L为实验试块上底面与微波天线之间的距离:

Figure BDA0001371236500000091
Step 1. Calculate the microwave frequency λ: measure the dielectric constant ε' and dielectric loss factor ε" of the collected oil and gas reservoir rock samples, and calculate the microwave frequency λ based on the size of the test block, where L is the experimental test Distance between the bottom surface of the block and the microwave antenna:
Figure BDA0001371236500000091

步骤二、制作实验试块:在采集的油气藏储层岩样中心位置钻得扩孔段602与裸眼压裂段603,并插入模拟套管604,且以之为中心,浇筑混凝土制得尺寸为200*200*200mm的实验试块601;Step 2. Make the test block: Drill the reaming section 602 and the open hole fracturing section 603 at the center of the collected oil and gas reservoir rock sample, insert the simulated casing 604, and pour concrete to obtain the size An experimental test block 601 of 200*200*200mm;

步骤三、实验试块到位:向制得的实验试块601上的模拟套管604中注水排净空气,将其与压裂液管线26相连;在X、Y、Z方向上的声发射传感器401面上涂抹耐高温耦合剂以便更好地测得声发射信号,并利用X向加压液压缸10将实验试块推入试样室18内,同时将后六角螺栓28与压裂室主机17连接;Step 3: Put the experimental test block in place: inject water into the simulated casing 604 on the prepared experimental test block 601 to drain the air, and connect it to the fracturing fluid pipeline 26; the acoustic emission sensors in the X, Y, and Z directions Apply high-temperature-resistant couplant on the 401 surface to better measure the acoustic emission signal, and use the X-direction pressurized hydraulic cylinder 10 to push the experimental test block into the sample chamber 18, and at the same time connect the rear hexagonal bolt 28 to the main machine of the fracturing chamber 17 connections;

步骤四、三轴压力加载:启动控制及信号采集单元,利用三轴加压控制装置38控制三轴压力加载,直至达到设定的模拟地应力值;Step 4. Triaxial pressure loading: start the control and signal acquisition unit, and use the triaxial pressure control device 38 to control the triaxial pressure loading until the set simulated ground stress value is reached;

步骤五、微波加热:开启微波发生装置1,以步骤一中计算所得的微波频率λ加热实验试块,观察声发射监测单元采集的声发射信号波形;当显示装置37上的温度达到设定温度时,关闭微波发生装置1;Step 5, microwave heating: turn on the microwave generating device 1, heat the experimental test piece with the microwave frequency λ calculated in step 1, observe the acoustic emission signal waveform collected by the acoustic emission monitoring unit; when the temperature on the display device 37 reaches the set temperature , turn off the microwave generator 1;

步骤六、进行水力压裂:开启压裂液泵系统30,以一定排量按设定的泵送压力或泵送速度向实验试块泵送压裂液;通过声发射监测单元采集压裂过程中的声发射信号,观察声发射信号波形变化;观察显示装置37上的水力压裂压力曲线与X、Y、Z三轴压力曲线;当水力压裂压力值以及三轴压力值归零时,水力压裂过程结束;Step 6. Perform hydraulic fracturing: turn on the fracturing fluid pump system 30, pump fracturing fluid to the experimental test block with a certain displacement according to the set pumping pressure or pumping speed; collect the fracturing process through the acoustic emission monitoring unit Acoustic emission signal in, observe the waveform change of acoustic emission signal; Observe the hydraulic fracturing pressure curve and the X, Y, Z triaxial pressure curve on the display device 37; When the hydraulic fracturing pressure value and the triaxial pressure value return to zero, The hydraulic fracturing process ends;

步骤七、取出实验试块:利用三轴加压控制装置38控制X、Y、Z向的压力逐渐减少直至归零,X向加压液压缸10的液压杆移出试样室18,控制X向卸料液压缸13及后挡板301将实验试块601推出。Step 7. Take out the experimental test block: Use the triaxial pressurization control device 38 to control the pressure in the X, Y, and Z directions to gradually decrease until it returns to zero. The unloading hydraulic cylinder 13 and the tailgate 301 push out the experimental test block 601.

Claims (3)

1.一种真三轴水力压裂模拟实验的微波加热装置,其特征在于:包括三轴加压单元、微波加热单元、压裂液注入单元、声发射监测单元、温度监测单元和控制及信号采集单元:1. A microwave heating device for a true triaxial hydraulic fracturing simulation experiment, characterized in that it includes a triaxial pressurization unit, a microwave heating unit, a fracturing fluid injection unit, an acoustic emission monitoring unit, a temperature monitoring unit, and control and signal Acquisition unit: 所述三轴加压单元包括四个固定轴(15)、八个螺栓(14)、压裂室主机(17)、推进台(16)、三个加载板(25)、后挡板(301)、X向三通阀(22)、Y向三通阀(23)、Z向三通阀(24)、X向压力传感器(19)、Y向压力传感器(20)、Z向压力传感器(21)、X向加压液压缸(10)、Y向加压液压缸(11)、Z向加压液压缸(12)、两个X向卸料液压缸(13)和液压站(4);The triaxial pressurization unit includes four fixed shafts (15), eight bolts (14), a fracturing chamber host (17), a propulsion table (16), three loading plates (25), a rear baffle (301 ), X-direction three-way valve (22), Y-direction three-way valve (23), Z-direction three-way valve (24), X-direction pressure sensor (19), Y-direction pressure sensor (20), Z-direction pressure sensor ( 21), X-direction pressurization hydraulic cylinder (10), Y-direction pressurization hydraulic cylinder (11), Z-direction pressurization hydraulic cylinder (12), two X-direction unloading hydraulic cylinders (13) and hydraulic station (4) ; Y向加压液压缸(11)、Z向加压液压缸(12)均通过沉头螺钉固定在压裂室主机(17)上;X向加压液压缸(10)与压裂室主机(17)通过四个固定轴(15)和八个螺栓(14)进行螺纹密封连接;推进台(16)通过胶接连接方式,一面与X向加压液压缸(10)的底座连接,一面与压裂室主机(17)连接,并与试样室(18)底边重合,以便推送实验试块进入试样室(18);X向卸料液压缸(13)通过沉头螺钉固定在压裂室主机(17)上;X向加压液压缸(10)、Y向加压液压缸(11)、Z向加压液压缸(12)的液压杆端部分别与加载板(25)连接,连接方式为沉头螺钉连接;在X方向上,试样室内放有后挡板(301),且与两个X向卸料液压缸(13)的液压杆端部通过沉头螺钉连接;Y-direction pressurized hydraulic cylinder (11) and Z-directed pressurized hydraulic cylinder (12) are all fixed on the fracturing chamber host (17) by countersunk screws; X-directed pressurized hydraulic cylinder (10) is connected to the fracturing chamber host ( 17) Through four fixed shafts (15) and eight bolts (14) for thread sealing connection; the propulsion table (16) is connected by glue joint, one side is connected to the base of the X-direction pressurized hydraulic cylinder (10), and the other side is connected to the The host machine (17) of the fracturing chamber is connected and coincides with the bottom edge of the sample chamber (18), so as to push the test piece into the sample chamber (18); On the split chamber host machine (17); the hydraulic rod ends of the X-direction pressurization hydraulic cylinder (10), the Y-direction pressurization hydraulic cylinder (11), and the Z-direction pressurization hydraulic cylinder (12) are respectively connected with the loading plate (25) , the connection mode is a countersunk screw connection; in the X direction, a rear baffle (301) is placed in the sample chamber, and it is connected with the ends of the hydraulic rods of the two X-direction unloading hydraulic cylinders (13) through countersunk screws; X向加压液压缸(10)、Y向加压液压缸(11)和Z向加压液压缸(12)进油口连接处,分别与X向三通阀(22)、Y向三通阀(23)和Z向三通阀(24)螺纹连接分成两路,一路分别与X向压力传感器(19)、Y向压力传感器(20)和Z向压力传感器(21)通过螺纹密封连接,将压力信息传递给控制及信号采集单元;另一路分别与液压油运输管道(29)连接,连接方式为六角接头螺纹连接;X向卸料液压缸(13)与液压油运输管道(29)连接,连接方式为六角接头螺纹连接;X-direction pressurized hydraulic cylinder (10), Y-directed pressurized hydraulic cylinder (11), and Z-directed pressurized hydraulic cylinder (12) are connected to the oil inlet ports of the X-direction three-way valve (22) and Y-direction three-way valve respectively. The valve (23) and the Z-direction three-way valve (24) are threadedly connected into two paths, and one path is respectively connected to the X-direction pressure sensor (19), the Y-direction pressure sensor (20) and the Z-direction pressure sensor (21) through threaded sealing. The pressure information is transmitted to the control and signal acquisition unit; the other road is respectively connected to the hydraulic oil transportation pipeline (29), and the connection method is a hexagonal joint threaded connection; the X-direction unloading hydraulic cylinder (13) is connected to the hydraulic oil transportation pipeline (29) , the connection method is hexagonal joint threaded connection; 液压站(4)包括液压阀组合(7)、泵装置(8)、油箱(5)、压力控制器(9)和囊式蓄能器(6),与液压油运输管道(29)连接以提供液压源,连接方式为六角接头螺纹连接;The hydraulic station (4) includes a hydraulic valve combination (7), a pump device (8), an oil tank (5), a pressure controller (9) and a bladder accumulator (6), and is connected with a hydraulic oil transportation pipeline (29) to Provide a hydraulic source, and the connection method is a hexagonal joint threaded connection; 所述微波加热单元包括微波发生装置(1)、波导管(2)和微波天线(3);微波天线(3)固定在三轴加压单元的底座中,微波天线(3)位于压裂试样室的下方;波导管(2)与微波天线(3)连接,波导管(2)固定在三轴加压单元的底座中;The microwave heating unit includes a microwave generating device (1), a waveguide (2) and a microwave antenna (3); the microwave antenna (3) is fixed in the base of the triaxial pressurization unit, and the microwave antenna (3) is located The bottom of the sample chamber; the waveguide (2) is connected with the microwave antenna (3), and the waveguide (2) is fixed in the base of the triaxial pressurization unit; 所述压裂液注入单元包括单向液压缸(31)、压裂液泵送控制系统(30)和压裂液管线(26),可控制压裂液泵送的压力及速度;所述压裂液管线(26)穿过前六角螺栓(27)与后六角螺栓(28),前六角螺栓(27)与实验试块(601)上固定的模拟套管(604)通过进行螺纹密封连接,后六角螺栓(28)与压裂室主机(17)通过螺纹密封连接;The fracturing fluid injection unit includes a one-way hydraulic cylinder (31), a fracturing fluid pumping control system (30) and a fracturing fluid pipeline (26), which can control the pressure and speed of the fracturing fluid pumping; The cracking liquid pipeline (26) passes through the front hexagonal bolt (27) and the rear hexagonal bolt (28), and the front hexagonal bolt (27) is connected with the simulated casing (604) fixed on the experimental test block (601) by thread sealing, The rear hex bolt (28) is connected to the fracturing chamber host (17) through a threaded seal; 所述声发射监测单元包括通过胶接与加载板四个顶点处连接的声发射传感器(401),声发射传感器传输线(34)从加载板(25)后的槽口(403)中伸出,声发射传感器传输线(34)固定在固定管道(33)中;在Y、Z方向上,固定管道(33)一端与压裂室主机(17)通过螺纹连接,固定管道(33)另一端能固定传输线;The acoustic emission monitoring unit includes an acoustic emission sensor (401) connected to the four vertices of the loading plate by gluing, and the acoustic emission sensor transmission line (34) protrudes from the notch (403) behind the loading plate (25), The acoustic emission sensor transmission line (34) is fixed in the fixed pipe (33); in the Y and Z directions, one end of the fixed pipe (33) is threadedly connected to the fracturing chamber host (17), and the other end of the fixed pipe (33) can be fixed Transmission line; 所述温度监测单元包括通过胶接与加载板中心处连接的温度传感器(402),温度传感器传输线(35)从加载板(25)后的槽口(403)中伸出并固定在固定管道(33)中;The temperature monitoring unit includes a temperature sensor (402) connected to the center of the loading plate by glue, and the temperature sensor transmission line (35) protrudes from the notch (403) behind the loading plate (25) and is fixed in the fixed pipe ( 33) in; 所述控制及信号采集单元与压力传感器传输线(36)连接,采集模拟地应力值并显示在显示装置(37)上;控制及信号采集单元与液压站(4)通过信号传输线(32)连接,利用其三轴加压控制装置(38)可直接控制施加的三轴应力大小;控制及信号采集单元与声发射传感器传输线(34)连接,内置的声发射信号处理装置(39)处理声发射信号并显示在显示装置(37)上;控制及信号采集单元与压裂液注入单元通过信号传输线(32)连接,采集压裂液泵送信息并显示在显示装置(37)上;控制及信号采集单元与温度传感器传输线(35)连接,监测实验试块加热实时信息并显示在显示装置(37)上。The control and signal acquisition unit is connected with the pressure sensor transmission line (36), and the simulated ground stress value is collected and displayed on the display device (37); the control and signal acquisition unit is connected with the hydraulic station (4) through the signal transmission line (32), The applied triaxial stress can be directly controlled by using its triaxial pressure control device (38); the control and signal acquisition unit is connected with the acoustic emission sensor transmission line (34), and the built-in acoustic emission signal processing device (39) processes the acoustic emission signal And displayed on the display device (37); the control and signal acquisition unit is connected with the fracturing fluid injection unit through the signal transmission line (32), and the fracturing fluid pumping information is collected and displayed on the display device (37); the control and signal acquisition The unit is connected with the temperature sensor transmission line (35), monitors the real-time information of the heating of the experimental test block and displays it on the display device (37). 2.根据权利要求1所述的一种真三轴水力压裂模拟实验的微波加热装置,其特征在于:所述的加载板(25)、后挡板(301)、后六角螺栓(28)、固定管道(33)、X向加压液压缸(10)、Y向加压液压缸(11)、Z向加压液压缸(12)、两个X向卸料液压缸(13)的缸体与液压杆均为微波反射材料。2. A microwave heating device for a true triaxial hydraulic fracturing simulation experiment according to claim 1, characterized in that: the loading plate (25), the rear baffle (301), the rear hexagonal bolt (28) , fixed pipeline (33), X-direction pressurization hydraulic cylinder (10), Y-direction pressurization hydraulic cylinder (11), Z-direction pressurization hydraulic cylinder (12), two cylinders of X-direction discharge hydraulic cylinder (13) Body and hydraulic rod are microwave reflective materials. 3.一种权利要求1所述真三轴水力压裂模拟实验的微波加热装置的实验方法,包括如下步骤:3. an experimental method of the microwave heating device of the true triaxial hydraulic fracturing simulation experiment described in claim 1, comprising the steps: 步骤一、计算微波频率λ:测量采集到的油气藏储层岩样的介电常数ε’与介电损耗因子ε”,以该试块的尺寸为基准,计算微波频率λ,L为实验试块上底面与微波天线之间的距离:
Figure FDA0004100037670000031
Step 1. Calculate the microwave frequency λ: measure the dielectric constant ε' and dielectric loss factor ε" of the collected oil and gas reservoir rock samples, and calculate the microwave frequency λ based on the size of the test block, where L is the experimental test Distance between the bottom surface of the block and the microwave antenna:
Figure FDA0004100037670000031
步骤二、制作实验试块:在采集的油气藏储层岩样中心位置钻得扩孔段(602)与裸眼压裂段(603),并插入模拟套管(604),且以之为中心,浇筑混凝土制得尺寸为200*200*200mm的实验试块(601);Step 2. Making the experimental test block: Drill the reaming section (602) and the open hole fracturing section (603) at the center of the collected oil and gas reservoir rock sample, and insert the simulated casing (604), and take it as the center , pouring concrete to make an experimental test block (601) whose size is 200*200*200mm; 步骤三、实验试块到位:向制得的实验试块(601)上的模拟套管(604)中注水排净空气,将其与压裂液管线(26)相连;在X、Y、Z方向上的声发射传感器(401)面上涂抹耐高温耦合剂以便更好地测得声发射信号,并利用X向加压液压缸(10)将实验试块推入试样室(18)内,同时将后六角螺栓(28)与压裂室主机(17)连接;Step 3, put the experimental test block in place: inject water into the simulated casing (604) on the prepared experimental test block (601) to discharge the air, and connect it to the fracturing fluid pipeline (26); Apply high-temperature-resistant couplant on the surface of the acoustic emission sensor (401) in the direction to better measure the acoustic emission signal, and use the X-direction pressurized hydraulic cylinder (10) to push the experimental test block into the sample chamber (18) , and connect the rear hex bolt (28) with the fracturing chamber host (17) at the same time; 步骤四、三轴压力加载:启动控制及信号采集单元,利用三轴加压控制装置(38)控制三轴压力加载,直至达到设定的模拟地应力值;Step 4, triaxial pressure loading: start the control and signal acquisition unit, and use the triaxial pressure control device (38) to control the triaxial pressure loading until the set simulated ground stress value is reached; 步骤五、微波加热:开启微波发生装置(1),以步骤一中计算所得的微波频率λ加热实验试块,观察声发射监测单元采集的声发射信号波形;当显示装置(37)上的温度达到设定温度时,关闭微波发生装置(1);Step 5, microwave heating: open the microwave generating device (1), heat the experimental test block with the microwave frequency λ calculated in step 1, observe the acoustic emission signal waveform collected by the acoustic emission monitoring unit; when the temperature on the display device (37) When the set temperature is reached, the microwave generating device (1) is turned off; 步骤六、进行水力压裂:压裂液泵送控制系统(30),以一定排量按设定的泵送压力或泵送速度向实验试块泵送压裂液;通过声发射监测单元采集压裂过程中的声发射信号,观察声发射信号波形变化;观察显示装置(37)上的水力压裂压力曲线与X、Y、Z三轴压力曲线;当水力压裂压力值以及三轴压力值归零时,水力压裂过程结束;Step 6. Perform hydraulic fracturing: the fracturing fluid pumping control system (30) pumps fracturing fluid to the experimental test block with a certain displacement according to the set pumping pressure or pumping speed; Acoustic emission signal during the fracturing process, observe the waveform change of the acoustic emission signal; observe the hydraulic fracturing pressure curve and the X, Y, Z triaxial pressure curve on the display device (37); when the hydraulic fracturing pressure value and the triaxial pressure When the value returns to zero, the hydraulic fracturing process ends; 步骤七、取出实验试块:利用三轴加压控制装置(38)控制X、Y、Z向的压力逐渐减少直至归零,X向加压液压缸(10)的液压杆移出试样室(18),控制X向卸料液压缸(13)及后挡板(301)将实验试块(601)推出。Step 7. Take out the experimental test block: use the three-axis pressurization control device (38) to control the pressure in the X, Y, and Z directions to gradually decrease until it returns to zero, and the hydraulic rod of the X-direction pressurization hydraulic cylinder (10) moves out of the sample chamber ( 18), control the X-direction unloading hydraulic cylinder (13) and tailgate (301) to push out the experimental test block (601).
CN201710663713.XA 2017-08-06 2017-08-06 Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method Active CN107290224B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710663713.XA CN107290224B (en) 2017-08-06 2017-08-06 Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710663713.XA CN107290224B (en) 2017-08-06 2017-08-06 Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method

Publications (2)

Publication Number Publication Date
CN107290224A CN107290224A (en) 2017-10-24
CN107290224B true CN107290224B (en) 2023-04-18

Family

ID=60105385

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710663713.XA Active CN107290224B (en) 2017-08-06 2017-08-06 Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method

Country Status (1)

Country Link
CN (1) CN107290224B (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111594040B (en) * 2019-02-19 2021-10-01 中国石油化工股份有限公司 Microwave rock breaking test device
CN111198136A (en) * 2020-02-17 2020-05-26 北京科技大学 An experimental system and method for monitoring the frost heave expansion process of ice-bearing fracture network in rock mass
CN111894550B (en) * 2020-06-23 2022-05-17 中国矿业大学 A simulation test system and method for upward drilling low temperature fluid fracturing
CN112268818B (en) * 2020-11-11 2021-04-13 中国科学院地质与地球物理研究所 Rock true triaxial controllable shock wave fracturing test system and method
US11965860B2 (en) * 2020-12-04 2024-04-23 Northeastern University Test system for hard rock breaking by microwave intelligent loading based on true triaxial stress
CN113075112B (en) * 2021-04-26 2024-07-02 东北大学 Experimental device and method for hydraulically fracturing and microwave fracturing combined permeability-increasing shale
CN113917110A (en) * 2021-09-30 2022-01-11 中国矿业大学(北京) Multifunctional three-dimensional analog simulation test platform and test method

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4152941A (en) * 1978-05-08 1979-05-08 Terra Tek, Inc. Process for measuring the fracture toughness of rock under simulated down-hole stress conditions
CN104330310B (en) * 2014-10-29 2016-08-31 吉林大学 A kind of oil shale fracturing experimental system for simulating and the manufacture method of laboratory sample
CN104655495B (en) * 2015-02-13 2017-05-10 太原理工大学 High temperature and high pressure coal and rock true triaxial fracturing and seepage test device and test method
CN105114049A (en) * 2015-09-17 2015-12-02 中国石油大学(北京) Experimental device for simulating hydrofracture action mechanism in steam assisted gravity drainage (SAGD) process
CN105510142B (en) * 2016-01-15 2018-02-16 太原理工大学 A kind of axle crushing test device of coal petrography multiphase different fluid three and test method
CN207197948U (en) * 2017-08-06 2018-04-06 吉林大学 Microwave heating equipment for true triaxial hydraulic fracturing simulated experiment

Also Published As

Publication number Publication date
CN107290224A (en) 2017-10-24

Similar Documents

Publication Publication Date Title
CN107290224B (en) Microwave heating device for true triaxial hydraulic fracturing simulation experiment and experiment method
CN207197948U (en) Microwave heating equipment for true triaxial hydraulic fracturing simulated experiment
CN108386177B (en) Real-time monitoring experiment system and method for three-dimensional multilayer multi-well fracturing support crack
CN102174883B (en) Test method for conductivity of self-supporting fractures in clear water fracturing
CN106896043B (en) Device for simulating crack initiation and evaluating crack seepage under true triaxial stress
CN107991216B (en) A simulation device for fluid fracture seepage under high temperature stress
CN102590456B (en) Device and method for simulating volume fracturing of horizontal well on shale reservoir stratum
CN107905778A (en) Supercritical CO2The enhanced geothermal system experimental provision of fluid fracturing and method
CN103712863B (en) Based on the device and method of Study on Catastrophe Theory pressure break Rock Damage and crack propagation
CN106153856B (en) One kind evaluating apparatus of shale stability containing crack and method
CN102735548A (en) Multifunctional true triaxial flow solid coupling test system
CN105114049A (en) Experimental device for simulating hydrofracture action mechanism in steam assisted gravity drainage (SAGD) process
CN102735547A (en) Coal-rock hydraulic fracturing testing method under true triaxial state
CN103775070A (en) Full-size well wall stable simulator
CN104458918A (en) Super-critical carbon dioxide fractured shale damage positioning monitoring device and method
CN104655495A (en) High temperature and high pressure coal and rock true triaxial fracturing and seepage test device and test method
CN103266888A (en) System and method for visualization fracturing simulation experiment
CN103758513A (en) Method for evaluating simulation of full-size well wall stability
CN110005400B (en) Device for testing cementing surface of shaft sleeve and cement sheath in high-temperature and high-pressure environment of dry-hot rock stratum
CN104330310A (en) Hydraulic fracturing simulation experiment system for oil shale and manufacturing method of experiment sample
CN113514337B (en) Hot dry rock rupture pressure test device and method
CN110056335A (en) Three axis multiple cracks hydraulic fracturing experiments devices of one kind and experimental method
CN105352811A (en) Pressurizing device and method for small-sized hydrofracture three-axis assessment and test
CN205154123U (en) Experimental device for simulation SAGD in -process hydraulic fracturing mechanism
CN111257129A (en) A true triaxial hydraulic fracturing test device and hydraulic fracturing test method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant