CN107285921A - Composite microorganism foliage fertilizer based on PAL materials and preparation method thereof - Google Patents
Composite microorganism foliage fertilizer based on PAL materials and preparation method thereof Download PDFInfo
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- CN107285921A CN107285921A CN201710683855.2A CN201710683855A CN107285921A CN 107285921 A CN107285921 A CN 107285921A CN 201710683855 A CN201710683855 A CN 201710683855A CN 107285921 A CN107285921 A CN 107285921A
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- pal
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- acid solution
- ball
- foliar fertilizer
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of composite microorganism foliage fertilizer based on PAL materials and preparation method thereof, the preparation method includes：1）By PAL（Palygorskite）Soaked in acid solution, then filter to take filter cake and carry out ball milling PAL powder is made；2）PAL powder, amino acid, cyclodextrin and water are carried out into hydro-thermal reaction modified PAL is made；3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans carry out spontaneous fermentation, then add modified PAL foliar fertilizer is made.There is excellent adhesive force and then so that the nutrient in foliar fertilizer is able to effectively absorb by the composite microorganism foliage fertilizer based on PAL materials made from this method, and the preparation method has the advantages that process is simple and raw material is easy to get.
Description
Technical field
The present invention relates to foliar fertilizer, in particular it relates to a kind of composite microorganism foliage fertilizer and its preparation based on PAL materials
Method.
Background technology
Plant needs a series of nutrients（Macronutrient and micronutrient）To ensure healthy growth.In some environment
In, abiotic constraints can hinder it is relevant must nutrition in enough these of Root Absorption into soil via addition fertilizer
The availability of element.This can be due to caused by following factor：The content of the soluble form of mineral nutrient is not in the soil liquid
Low organic matter content in foot, the water deficit in topsoil, basic soil pH, high soil carbonate content, soil with
And it is other can limiting nutrients can availability critical soil factor.
Cereal and seed crop and fruit tree are especially needed during the flourish stage quickly and densely by a large amount of ore deposits
Matter nutrient nutrient supply is to flower, young tender seed, pod and fruit, root activity and unfavorable soil that this may be with reduction
Exist simultaneously with weather conditions, so as to cause the nutrient for meeting this quick demand to supply outdated and do not fill
Point.In addition, in seed, cereal and fruit micronutrient it is continuous remove may in exhausted soil available nutrient deposit
Storage.In these cases, accurate, timely and effective nutrient can be provided to plant propagation organ using foliar fertilizer to supply
Answer, and required rate of application that can be more much lower than soil and fertilizer is carried out.This can not only cause and yield disorderly to nutrient
The quick amendment or prevention of loss, and the improvement of crop quality can be caused.
Under such conditions, it has been found that foliage dressing is provided in terms of the health plant improved and crop yield is produced
Very big benefit.Foliage dressing is that liquid fertilizer is applied directly on aerial plant part, rather than is administered to surrounding plants
Soil.Fertilizer one or both of any entered in leaf epidermis by penetrate through in air vent openings and cuticula and is absorbed to plant
In thing.
Typical foliar fertilizer can be solution or insoluble fertilising compound of the soluble compounds in water in water
Dispersion/suspended substance.Wherein, in general suspended substance foliar fertilizer is inorganic mineral compound, and suspended substance foliar fertilizer is often
Because the bad distribution on blade surface and adhesive force it is smaller cause fertilising compound be difficult to effectively be absorbed.
The content of the invention
It is an object of the invention to provide a kind of composite microorganism foliage fertilizer based on PAL materials and preparation method thereof, pass through
Composite microorganism foliage fertilizer based on PAL materials made from this method has excellent adhesive force and then causes battalion in foliar fertilizer
Foster element is able to effectively absorb, and the preparation method has the advantages that process is simple and raw material is easy to get.
To achieve these goals, the invention provides a kind of preparation of the composite microorganism foliage fertilizer based on PAL materials
Method, the preparation method includes：
1）By PAL（Palygorskite）Soaked in acid solution, then filter to take filter cake and carry out ball milling PAL powder is made；
2）PAL powder, amino acid, cyclodextrin and water are carried out into hydro-thermal reaction modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans carry out spontaneous fermentation, then add modified PAL to be made
Foliar fertilizer.
, should be based on the compound micro- of PAL materials present invention also offers a kind of composite microorganism foliage fertilizer based on PAL materials
Biological foliage fertilizer is prepared by above-mentioned preparation method.
In the above-mentioned technical solutions, the present invention first by acid to PAL（Palygorskite）Activated；Then ball milling reduces it
Particle diameter；Then by amino acid, cyclodextrin to PAL（Palygorskite）Carry out modification and make it have and can be carried out by force with plant surface
Strong attachment；Finally, beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans carry out spontaneous fermentation, while will be modified
PAL effectively absorbs the nutritional ingredient after spontaneous fermentation and then obtained foliar fertilizer is had effective fertility and excellent attachment
Power.Meanwhile, the preparation method has the advantages that process is simple and raw material is easy to get.
Other features and advantages of the present invention will be described in detail in subsequent embodiment part.
Embodiment
The embodiment to the present invention is described in detail below.It should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The invention provides a kind of preparation method of the composite microorganism foliage fertilizer based on PAL materials, the preparation method bag
Include：
1）By PAL（Palygorskite）Soaked in acid solution, then filter to take filter cake and carry out ball milling PAL powder is made；
2）PAL powder, amino acid, cyclodextrin and water are carried out into hydro-thermal reaction modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans carry out spontaneous fermentation, then add modified PAL to be made
Foliar fertilizer.
In the step 1 of the present invention）In, the consumption of each material can be selected in wide scope, but in order that obtained
Foliar fertilizer has more excellent fertility and adhesive force, it is preferable that in step 1）In, PAL（Palygorskite）Weight ratio with acid solution is
1：10-15, and the pH of acid solution is 6-6.5.
In the step 1 of the present invention）In, the consumption of each material can be selected in wide scope, but in order that obtained
Foliar fertilizer has more excellent fertility and adhesive force, it is preferable that in step 1）In, the immersion at least meets following condition：Leaching
It is 15-35 DEG C to steep temperature, and soak time is 4-8h.
In the step 1 of the present invention）In, the specific species of acid solution can be selected in wide scope, but in order that be made
Foliar fertilizer have more excellent fertility and adhesive force, it is preferable that in step 1）In, acid solution selection hydrochloric acid solution or sulfuric acid are molten
Liquid.
In the step 1 of the present invention）In, the actual conditions of ball milling can be selected in wide scope, but in order that be made
Foliar fertilizer have more excellent fertility and adhesive force, it is preferable that in step 1）In, ball milling at least meets following condition：Big ball
Mass ratio with bead is 2：The mass ratio of 1.3-1.6, abrading-ball and material is 10：0.8-1.2, rotating speed is 1500-2000rpm,
Ball-milling Time is 25-35min.
In the step 2 of the present invention）In, the consumption of each material can be selected in wide scope, but in order that obtained
Foliar fertilizer has more excellent fertility and adhesive force, it is preferable that in step 2）In, PAL powder, amino acid, the weight of cyclodextrin and water
Amount is than being 1：0.3-0.5：0.5-0.7：15-20.
In the step 3 of the present invention）In, the condition of hydro-thermal reaction can be selected in wide scope, but in order that be made
Foliar fertilizer have more excellent fertility and adhesive force, it is preferable that in step 2）In, hydro-thermal reaction at least meets following condition：
Reaction temperature is 80-100 DEG C, and the reaction time is 8-10h.
In the step 3 of the present invention）In, the consumption of each material can be selected in wide scope, but in order that obtained
Foliar fertilizer has more excellent fertility and adhesive force, it is preferable that in step 3）In, beast poultry manure, silkworm slough off, bacillus, cottonseed
Shell, dregs of beans, modified PAL weight ratio are 1：0.2-0.5：0.1-0.3：0.2-0.4：1-1.5：1-1.3.
In the step 3 of the present invention）In, the condition of spontaneous fermentation can be selected in wide scope, but in order that be made
Foliar fertilizer have more excellent fertility and adhesive force, it is preferable that in step 3）In, spontaneous fermentation at least meets following condition：
Fermentation temperature is 60-80 DEG C, and fermentation time is 10-15 days.
, should be based on the compound micro- of PAL materials present invention also offers a kind of composite microorganism foliage fertilizer based on PAL materials
Biological foliage fertilizer is prepared by above-mentioned preparation method.
The present invention will be described in detail by way of examples below.
Embodiment 1
1）By PAL（Palygorskite）, pH be 6.3 acid solution（Hydrochloric acid solution）According to 1：13 weight ratio is soaked at 25 DEG C
5h, then filters to take filter cake and carries out ball milling（The mass ratio of big ball and bead is 2：1.5, the mass ratio of abrading-ball and material is 10：1,
Rotating speed is 1800rpm, and Ball-milling Time is 30min）So that PAL powder is made；
2）By PAL powder, amino acid（Aspartic acid）, cyclodextrin and water is according to 1：0.4：0.6：18 weight ratio is in hydro-thermal at 90 DEG C
9h is reacted modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans are carried out at spontaneous fermentation 13 days at 70 DEG C, then addition changes
Property PAL be made foliar fertilizer A1（Beast poultry manure, silkworm slough off, bacillus, cotton seed hulls, dregs of beans, modified PAL weight ratio are 1：
0.4：0.2：0.23：1.3：1.2）.
Embodiment 2
1）By PAL（Palygorskite）, pH be 6 acid solution（Sulfuric acid solution）According to 1：10-15 weight ratio is soaked at 15 DEG C
4h, then filters to take filter cake and carries out ball milling（The mass ratio of big ball and bead is 2：1.3, the mass ratio of abrading-ball and material is 10：
0.8, rotating speed is 1500rpm, and Ball-milling Time is 25min）So that PAL powder is made；
2）By PAL powder, amino acid（Valine）, cyclodextrin and water is according to 1：0.3：0.5：15 weight ratio is anti-in hydro-thermal at 80 DEG C
8h is answered modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans are carried out at spontaneous fermentation 10 days at 60 DEG C, then addition changes
Property PAL be made foliar fertilizer A2（Beast poultry manure, silkworm slough off, bacillus, cotton seed hulls, dregs of beans, modified PAL weight ratio are 1：
0.2：0.1：0.2：1：1）.
Embodiment 3
1）By PAL（Palygorskite）, pH be 6.5 acid solution（Sulfuric acid solution）According to 1：15 weight ratio is soaked at 35 DEG C
8h, then filters to take filter cake and carries out ball milling（The mass ratio of big ball and bead is 2：1.6, the mass ratio of abrading-ball and material is 10：
1.2, rotating speed is 2000rpm, and Ball-milling Time is 35min）So that PAL powder is made；
2）By PAL powder, amino acid（Leucine）, cyclodextrin and water is according to 1：0.5：0.7：20 weight ratio is in hydro-thermal at 100 DEG C
10h is reacted modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans are carried out at spontaneous fermentation 15 days at 80 DEG C, then addition changes
Property PAL be made foliar fertilizer A3（Beast poultry manure, silkworm slough off, bacillus, cotton seed hulls, dregs of beans, modified PAL weight ratio are 1：
0.5：0.3：0.4：1.5：1.3）.
Comparative example 1
Foliar fertilizer B1 is prepared Following the procedure of Example 1, unlike, step 1）In be not used acid solution.
Comparative example 2
Foliar fertilizer B2 is prepared Following the procedure of Example 1, unlike, step 1）In do not carry out ball milling.
Comparative example 3
Foliar fertilizer B3 is prepared Following the procedure of Example 1, unlike, step 1）In be not used cyclodextrin.
Comparative example 4
Foliar fertilizer B4 is prepared Following the procedure of Example 1, unlike, step 1）In be not used amino acid.
Detect example 1
Above-mentioned foliar fertilizer is added respectively to a piece of different peach in florescence, and each peach is then counted when fruiting period
On fruiting rate（The number of flowers of number of results/female flower）, concrete outcome is shown in Table 1.
Table 1
| Foliar fertilizer | A1 | A2 | A3 | B1 | B2 | B3 | B4 |
| Fruiting rate/% | 80.5 | 81.2 | 80.0 | 58.2 | 62.3 | 54.8 | 48.9 |
By above-described embodiment, comparative example and detection example, the foliar fertilizer provided of the invention has excellent fertility and attached
Put forth effort.
The preferred embodiment of the present invention described in detail above, still, the present invention are not limited in above-mentioned embodiment
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (9)
1. a kind of preparation method of the composite microorganism foliage fertilizer based on PAL materials, it is characterised in that the preparation method bag
Include：
1）By PAL（Palygorskite）Soaked in acid solution, then filter to take filter cake and carry out ball milling PAL powder is made；
2）The PAL powder, amino acid, cyclodextrin and water are carried out into hydro-thermal reaction modified PAL is made；
3）Beast poultry manure, silkworm are sloughed off, bacillus, cotton seed hulls, dregs of beans carry out spontaneous fermentation, then add the modified PAL with
The foliar fertilizer is made.
2. preparation method according to claim 1, wherein, in step 1）In, the PAL（Palygorskite）With the weight of acid solution
Than for 1：10-15, and the pH of the acid solution is 6-6.5；
Preferably, the immersion at least meets following condition：Soaking temperature is 15-35 DEG C, and soak time is 4-8h.
3. preparation method according to claim 1, wherein, in step 1）In, the acid solution selection hydrochloric acid solution or sulfuric acid
Solution.
4. preparation method according to claim 1, wherein, in step 1）In, the ball milling at least meets following condition：Greatly
The mass ratio of ball and bead is 2：The mass ratio of 1.3-1.6, abrading-ball and material is 10：0.8-1.2, rotating speed is 1500-
2000rpm, Ball-milling Time is 25-35min.
5. the preparation method according to any one in claim 1-4, wherein, in step 2）In, the PAL powder, amino
The weight ratio of acid, cyclodextrin and water is 1：0.3-0.5：0.5-0.7：15-20.
6. preparation method according to claim 5, wherein, in step 2）In, the hydro-thermal reaction at least meets following bar
Part：Reaction temperature is 80-100 DEG C, and the reaction time is 8-10h.
7. preparation method according to claim 5, wherein, in step 3）In, the beast poultry manure, silkworm slough off, bacillus,
Cotton seed hulls, dregs of beans, modified PAL weight ratio are 1：0.2-0.5：0.1-0.3：0.2-0.4：1-1.5：1-1.3.
8. preparation method according to claim 5, wherein, in step 3）In, the spontaneous fermentation at least meets following bar
Part：Fermentation temperature is 60-80 DEG C, and fermentation time is 10-15 days.
9. a kind of composite microorganism foliage fertilizer based on PAL materials, it is characterised in that the composite microbial based on PAL materials
Thing foliar fertilizer is prepared by the preparation method in any one in claim 1-8.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710683855.2A CN107285921A (en) | 2017-08-11 | 2017-08-11 | Composite microorganism foliage fertilizer based on PAL materials and preparation method thereof |
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|---|---|---|---|
| CN201710683855.2A CN107285921A (en) | 2017-08-11 | 2017-08-11 | Composite microorganism foliage fertilizer based on PAL materials and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108046925A (en) * | 2017-12-29 | 2018-05-18 | 安徽乐农环保科技有限公司 | One kind is based on attapulgite material composite microorganism foliage fertilizer preparation method |
| CN108264427A (en) * | 2017-12-29 | 2018-07-10 | 安徽乐农环保科技有限公司 | A kind of method that cultivated soil renovation agent is prepared based on PAL-M materials and plant residue |
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| CN105152805A (en) * | 2015-08-05 | 2015-12-16 | 马鞍山科邦生态肥有限公司 | Mineral foliar fertilizer suitable for fruit trees and preparation method of fertilizer |
| CN105272621A (en) * | 2015-11-02 | 2016-01-27 | 中国科学院寒区旱区环境与工程研究所 | Preparation and application of composite bioactive material taking attapulgite to load bacillus |
| CN106116788A (en) * | 2016-06-16 | 2016-11-16 | 安徽乐农环保科技有限公司 | The special organic mineral fertilizer of Rhizoma Solani tuber osi prepared by a kind of PAL material |
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- 2017-08-11 CN CN201710683855.2A patent/CN107285921A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105152805A (en) * | 2015-08-05 | 2015-12-16 | 马鞍山科邦生态肥有限公司 | Mineral foliar fertilizer suitable for fruit trees and preparation method of fertilizer |
| CN105272621A (en) * | 2015-11-02 | 2016-01-27 | 中国科学院寒区旱区环境与工程研究所 | Preparation and application of composite bioactive material taking attapulgite to load bacillus |
| CN106116788A (en) * | 2016-06-16 | 2016-11-16 | 安徽乐农环保科技有限公司 | The special organic mineral fertilizer of Rhizoma Solani tuber osi prepared by a kind of PAL material |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108046925A (en) * | 2017-12-29 | 2018-05-18 | 安徽乐农环保科技有限公司 | One kind is based on attapulgite material composite microorganism foliage fertilizer preparation method |
| CN108264427A (en) * | 2017-12-29 | 2018-07-10 | 安徽乐农环保科技有限公司 | A kind of method that cultivated soil renovation agent is prepared based on PAL-M materials and plant residue |
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