CN107268328A - A kind of preparation method of cigarette body paper - Google Patents
A kind of preparation method of cigarette body paper Download PDFInfo
- Publication number
- CN107268328A CN107268328A CN201710511664.8A CN201710511664A CN107268328A CN 107268328 A CN107268328 A CN 107268328A CN 201710511664 A CN201710511664 A CN 201710511664A CN 107268328 A CN107268328 A CN 107268328A
- Authority
- CN
- China
- Prior art keywords
- body paper
- cigarette body
- preparation
- solution
- carboxymethyl cellulose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H15/00—Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution
- D21H15/02—Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution characterised by configuration
- D21H15/10—Composite fibres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
- C08J3/075—Macromolecular gels
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
- C08J3/246—Intercrosslinking of at least two polymers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/17—Ketenes, e.g. ketene dimers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
- D21H17/30—Alginic acid or alginates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/54—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen
- D21H17/55—Polyamides; Polyaminoamides; Polyester-amides
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2305/00—Characterised by the use of polysaccharides or of their derivatives not provided for in groups C08J2301/00 or C08J2303/00
- C08J2305/04—Alginic acid; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2401/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2401/08—Cellulose derivatives
- C08J2401/26—Cellulose ethers
- C08J2401/28—Alkyl ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paper (AREA)
Abstract
The invention discloses a kind of preparation method of cigarette body paper, first carboxymethyl cellulose is fully coordinated with ferrous ion cmc soln and copperas solution blending and obtain carboxymethyl cellulose Complexing Iron, then mixed with sodium alginate soln, again ferriferrous oxide nano-particle is uniformly generated by adjusting the oxidation of oxygen in pH and air in system situ, freeze-drying after calcium chloride solution be crosslinked obtaining plural gel, finally by plural gel and wood pulp, sizing agent, the raw materials such as filler are well mixed, manufactured paper with pulp by online, squeezing, dry, press polish, coiled process obtains cigarette body paper.Cigarette body paper produced by the invention not only meets index in the physical property such as tensile strength, and with the auxiliaring effect of inhaling taste comfort level and reducing tar and reducing harm is improved, is suitably applied medium-to-high grade cigarette field.
Description
Technical field
The present invention relates to cigarette material technical field, more particularly to a kind of preparation method of cigarette body paper.
Background technology
Cigarette tipping paper is a kind of dedicated paper that filter tip and Cigarette cigarette are got up, and is the important materials for producing cigarette
One of.In recent years, due to the continuous improvement of state's inner wrap strip technology, the kind of cigarette tipping paper increases, and processing technology is also constantly sent out
Exhibition.Raw material composition, physical characteristic, the sanitary index of cigarette tipping paper can have a direct impact to the quality of cigarette product, with
Lifting of the consumer to cigarette product quality requirements, cigarette tipping paper is not required nothing more than and meets finger in the physical properties such as tensile strength
Mark, it plays a part of also receiving more and more attention in terms of cigarette quality is influenceed.Existing cigarette tipping paper typically leads to
Cross punching to improve air permeability, so as to dilute flue gas, reduction cigarette, harmful components, improve cigarette quality, but this method is only capable of
Limited reducing tar and reducing harm effect is played, the improvement to cigarette odor-absorbing comfortableness is not good., can be right to reach more preferable effect
The performance of cigarette body paper makes improvements.
The content of the invention
The object of the invention be exactly in order to make up the defect of prior art there is provided one kind be conducive to improve inhale taste comfort level and
The preparation method of the cigarette body paper of reducing tar and reducing harm effect.
The present invention is achieved by the following technical solutions：
A kind of preparation method of cigarette body paper, comprises the following steps：
（1）Carboxymethyl cellulose is first added to the water stirring and dissolving and obtains cmc soln completely, then to the carboxylic
Copperas solution, and the stirring reaction 0.5-1h under logical nitrogen protective condition are slowly added dropwise in methocel solution, obtains
Carboxymethyl cellulose is complexed ferrous solution, and the volume ratio of the cmc soln and copperas solution is 2：（0.5-1）；
（2）By sodium alginate soln and step（1）Obtained carboxymethyl cellulose complexing ferrous solution by volume 1：（0.1-
0.15）It is well mixed, pH is then adjusted to 10-11 with sodium hydroxide and 0.5-1h is stirred, pH is then adjusted to neutrality, freezing is dry
It is dry and by obtained solid abrasive to 100-200 mesh, 0.5-1h is then soaked in calcium chloride solution and carries out cross-linking reaction, will
To plural gel be washed with deionized it is standby；
（3）Mashing is first handled into obtained softwood pulp, hardwood pulp by volume（1.2-1.8）：1 preparation obtains mixing slurry,
Then the AKD sizing agents equivalent to mixing slurry weight 0.5-1%, poly- third equivalent to mixing slurry weight 0.3-0.5% are sequentially added
Acrylamide, the calcium carbonate equivalent to mixing slurry weight 5-10% and the step of equivalent to mixing slurry weight 5-10%（2）The washing
Rear plural gel is well mixed, and is manufactured paper with pulp, is squeezed by online, drying, press polish, coiled process obtain cigarette body paper.
The mass fraction of the cmc soln is 1-2%.
The mass fraction of the copperas solution is 3-5%.
The mass fraction of the sodium alginate soln is 2-3%.
The mass fraction of the calcium chloride solution is 4-6%.
The beating consistency of the softwood pulp is 2.5-3%.
The beating consistency of the hardwood pulp is 2-2.5%.
It is an advantage of the invention that：
Cmc soln is first made carboxymethyl cellulose be filled with ferrous ion by the present invention with copperas solution blending
Distribution position obtains carboxymethyl cellulose Complexing Iron, then is well mixed to form composite solution system with sodium alginate soln, and lead to
The oxidation for overregulating oxygen in pH and air uniformly generates ferriferrous oxide nano grain in composite solution system situ
Son, freeze-drying carries out being crosslinked and obtaining plural gel after calcium chloride solution, then by plural gel and wood pulp, sizing agent, filler
It is well mixed Deng raw material, manufacture paper with pulp, squeeze by online, drying, press polish, coiled process obtain cigarette body paper.Present invention system
On the one hand the cigarette body paper obtained has loose structure, can improve air permeability, is harmful into so as to dilute flue gas, reduction cigarette
Point, another aspect uniform load ferriferrous oxide nano-particle can effectively adsorb a variety of harmful components in flue gas, and can increase
Moisture in smoke adding gas, reduces gas drying sense and excitant, improves flue gas mouthfeel and comfort level, not only tensile strength
Etc. meeting index in physical property, and with the auxiliaring effect of inhaling taste comfort level and reducing tar and reducing harm is improved, it is suitably applied
Medium-to-high grade cigarette field.
Embodiment
A kind of preparation method of cigarette body paper, comprises the following steps：
（1）Carboxymethyl cellulose is first added to the water stirring and dissolving and obtains cmc soln completely, then to the carboxylic
Copperas solution, and the stirring reaction 0.5h under logical nitrogen protective condition are slowly added dropwise in methocel solution, carboxylic is obtained
Methylcellulose is complexed ferrous solution, and the volume ratio of the cmc soln and copperas solution is 2：0.5；
（2）By sodium alginate soln and step（1）Obtained carboxymethyl cellulose complexing ferrous solution by volume 1：0.1 mixing is equal
It is even, pH is then adjusted to 10 with sodium hydroxide and 0.5h is stirred, pH is then adjusted to neutrality, is freeze-dried and by obtained solid
100 mesh are ground to, 0.5h is then soaked in calcium chloride solution carries out cross-linking reaction, by obtained plural gel deionized water
Washing is standby；
（3）Mashing is first handled into obtained softwood pulp, hardwood pulp by volume 1.2：1 preparation obtains mixing slurry, Ran Houyi
It is secondary add equivalent to the AKD sizing agents of mixing slurry weight 0.5%, the polyacrylamide equivalent to mixing slurry weight 0.3%, equivalent to
The calcium carbonate of mixing slurry weight 5% and the step of equivalent to mixing slurry weight 5%（2）Plural gel mixing after the washing is equal
It is even, manufacture paper with pulp, squeeze by online, drying, press polish, coiled process obtain cigarette body paper.
The mass fraction of the cmc soln is 1%.
The mass fraction of the copperas solution is 3%.
The mass fraction of the sodium alginate soln is 2%.
The mass fraction of the calcium chloride solution is 4%.
The beating consistency of the softwood pulp is 2.5%.
The beating consistency of the hardwood pulp is 2%.
Claims (7)
1. a kind of preparation method of cigarette body paper, it is characterised in that comprise the following steps：
（1）Carboxymethyl cellulose is first added to the water stirring and dissolving and obtains cmc soln completely, then to the carboxylic
Copperas solution, and the stirring reaction 0.5-1h under logical nitrogen protective condition are slowly added dropwise in methocel solution, obtains
Carboxymethyl cellulose is complexed ferrous solution, and the volume ratio of the cmc soln and copperas solution is 2：（0.5-1）；
（2）By sodium alginate soln and step（1）Obtained carboxymethyl cellulose complexing ferrous solution by volume 1：（0.1-
0.15）It is well mixed, pH is then adjusted to 10-11 with sodium hydroxide and 0.5-1h is stirred, pH is then adjusted to neutrality, freezing is dry
It is dry and by obtained solid abrasive to 100-200 mesh, 0.5-1h is then soaked in calcium chloride solution and carries out cross-linking reaction, will
To plural gel be washed with deionized it is standby；
（3）Mashing is first handled into obtained softwood pulp, hardwood pulp by volume（1.2-1.8）：1 preparation obtains mixing slurry,
Then the AKD sizing agents equivalent to mixing slurry weight 0.5-1%, poly- third equivalent to mixing slurry weight 0.3-0.5% are sequentially added
Acrylamide, the calcium carbonate equivalent to mixing slurry weight 5-10% and the step of equivalent to mixing slurry weight 5-10%（2）The washing
Rear plural gel is well mixed, and is manufactured paper with pulp, is squeezed by online, drying, press polish, coiled process obtain cigarette body paper.
2. a kind of preparation method of cigarette body paper according to claim 1, it is characterised in that the carboxymethyl cellulose
The mass fraction of plain solution is 1-2%.
3. the preparation method of a kind of cigarette body paper according to claim 1, it is characterised in that the ferrous sulfate is molten
The mass fraction of liquid is 3-5%.
4. the preparation method of a kind of cigarette body paper according to claim 1, it is characterised in that the sodium alginate is molten
The mass fraction of liquid is 2-3%.
5. a kind of preparation method of cigarette body paper according to claim 1, it is characterised in that the calcium chloride solution
Mass fraction be 4-6%.
6. the preparation method of a kind of cigarette body paper according to claim 1, it is characterised in that the softwood pulp
Beating consistency is 2.5-3%.
7. the preparation method of a kind of cigarette body paper according to claim 1, it is characterised in that the hardwood pulp
Beating consistency is 2-2.5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710511664.8A CN107268328A (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of cigarette body paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710511664.8A CN107268328A (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of cigarette body paper |
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| Publication Number | Publication Date |
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| CN107268328A true CN107268328A (en) | 2017-10-20 |
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ID=60070705
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710511664.8A Pending CN107268328A (en) | 2017-06-29 | 2017-06-29 | A kind of preparation method of cigarette body paper |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109567272A (en) * | 2018-12-26 | 2019-04-05 | 湖南中烟工业有限责任公司 | One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn |
| CN109567271A (en) * | 2018-12-26 | 2019-04-05 | 湖南中烟工业有限责任公司 | One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn |
| CN109588770A (en) * | 2018-12-26 | 2019-04-09 | 湖南中烟工业有限责任公司 | A kind of cooling mouth stick and cigarette |
| CN114622443A (en) * | 2022-03-16 | 2022-06-14 | 龙游塔恩纸业有限公司 | Cigarette tipping paper based on water-based touch oil and processing technology thereof |
| CN115341403A (en) * | 2022-05-07 | 2022-11-15 | 浙江唐丰特种纸有限公司 | Production method of high-smoothness tipping base paper for cigarettes |
Citations (5)
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|---|---|---|---|---|
| CN101143733A (en) * | 2007-08-28 | 2008-03-19 | 武汉大学 | Method for preparing magnetic ferric oxide nano particles |
| CN103290721A (en) * | 2013-05-21 | 2013-09-11 | 牡丹江恒丰纸业股份有限公司 | Production method of tipping base paper for flame-retardant cigarettes |
| CN105019292A (en) * | 2015-06-26 | 2015-11-04 | 安徽省三环纸业(集团)有限公司 | Production technology for tipping base paper for cigarette |
| CN105601983A (en) * | 2016-03-10 | 2016-05-25 | 云南中烟工业有限责任公司 | Natural polysaccharide aerogel, preparation method thereof and application thereof in cigarettes |
| CN106040190A (en) * | 2016-06-21 | 2016-10-26 | 西南科技大学 | Preparation method of iron ion croscarmellose in-situ growing Prussian-blue microsphere adsorbing material |
-
2017
- 2017-06-29 CN CN201710511664.8A patent/CN107268328A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101143733A (en) * | 2007-08-28 | 2008-03-19 | 武汉大学 | Method for preparing magnetic ferric oxide nano particles |
| CN103290721A (en) * | 2013-05-21 | 2013-09-11 | 牡丹江恒丰纸业股份有限公司 | Production method of tipping base paper for flame-retardant cigarettes |
| CN105019292A (en) * | 2015-06-26 | 2015-11-04 | 安徽省三环纸业(集团)有限公司 | Production technology for tipping base paper for cigarette |
| CN105601983A (en) * | 2016-03-10 | 2016-05-25 | 云南中烟工业有限责任公司 | Natural polysaccharide aerogel, preparation method thereof and application thereof in cigarettes |
| CN106040190A (en) * | 2016-06-21 | 2016-10-26 | 西南科技大学 | Preparation method of iron ion croscarmellose in-situ growing Prussian-blue microsphere adsorbing material |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109567272A (en) * | 2018-12-26 | 2019-04-05 | 湖南中烟工业有限责任公司 | One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn |
| CN109567271A (en) * | 2018-12-26 | 2019-04-05 | 湖南中烟工业有限责任公司 | One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn |
| CN109588770A (en) * | 2018-12-26 | 2019-04-09 | 湖南中烟工业有限责任公司 | A kind of cooling mouth stick and cigarette |
| CN114622443A (en) * | 2022-03-16 | 2022-06-14 | 龙游塔恩纸业有限公司 | Cigarette tipping paper based on water-based touch oil and processing technology thereof |
| CN115341403A (en) * | 2022-05-07 | 2022-11-15 | 浙江唐丰特种纸有限公司 | Production method of high-smoothness tipping base paper for cigarettes |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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Application publication date: 20171020 |