CN107256668A - A kind of experimental provision of solid refractometry - Google Patents

A kind of experimental provision of solid refractometry Download PDF

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Publication number
CN107256668A
CN107256668A CN201710452496.XA CN201710452496A CN107256668A CN 107256668 A CN107256668 A CN 107256668A CN 201710452496 A CN201710452496 A CN 201710452496A CN 107256668 A CN107256668 A CN 107256668A
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CN
China
Prior art keywords
rotating disk
sample
experimental provision
polarizer
seat
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CN201710452496.XA
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Chinese (zh)
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CN107256668B (en
Inventor
乐培界
谢文明
周锦生
斯公寿
周小风
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HANGZHOU JINGKE INSTRUMENT CO Ltd
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HANGZHOU JINGKE INSTRUMENT CO Ltd
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    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09BEDUCATIONAL OR DEMONSTRATION APPLIANCES; APPLIANCES FOR TEACHING, OR COMMUNICATING WITH, THE BLIND, DEAF OR MUTE; MODELS; PLANETARIA; GLOBES; MAPS; DIAGRAMS
    • G09B23/00Models for scientific, medical, or mathematical purposes, e.g. full-sized devices for demonstration purposes
    • G09B23/06Models for scientific, medical, or mathematical purposes, e.g. full-sized devices for demonstration purposes for physics
    • G09B23/22Models for scientific, medical, or mathematical purposes, e.g. full-sized devices for demonstration purposes for physics for optics
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length
    • G01N21/43Refractivity; Phase-affecting properties, e.g. optical path length by measuring critical angle

Abstract

The invention discloses a kind of solid refractometry experimental provision.Semiconductor laser is sent Guang Bouquet to be mapped on chip solid sample through polarizer, the reflected light produced by it is penetrated is converted into voltage signal output on flexible lengths solar cell;Sample is placed on Yi on the rotating disk of the test cavity of cylindrical shape and changes Guang Bouquet incidence angles, while the rotary encoder output angle information of rotating disk lower link, coordinates analytical instrument, it is possible to measures solid refractive index, checking Fresnel law etc., and can be tested in bright room.

Description

A kind of experimental provision of solid refractometry
Technical field
The invention belongs to experiment device for teaching, more specifically, it belongs to a kind of solid folding in universities and colleges' Physical Experiment Penetrate rate measurement experiment device, it is possible to verify Fresnel law.
Background technology
Reflection and refraction can occur when light wave is by both of which even dielectric interface, at any time, incidence wave and anti- The electric vector of ejected wave may be divided into two vectors, and one (is represented) parallel to the plane of incidence with P, and one (is used S perpendicular to the plane of incidence Represent), according to Fresnel law, in the mode of propagation from optically thinner medium to optically denser medium:The reflected intensity of P light is before this with entering The increase of firing angle and be gradually reduced, occur that become zero phenomenon of reflective light intensity (shows as light during actual experiment during to a certain angle It is strong minimum), and the angle is exactly Brewster angle, once incidence angle increases above Brewster angle, reflective light intensity is just rapid Enhancing is presented.If medium is different, reflected intensity is different from the change curve of incidence angle.
According to Fresnel law, the calculating of refractive index is completed by below equation:
n2=tg θB
It is checking Fresnel law and measurement solid refractive index, it is necessary to record changing incidence angle, and track simultaneously The light intensity of reflected light is measured, the change curve of reflected intensity and incidence angle could be obtained, corresponding angle when measuring light intensity minimum, And then measure refractive index (if polarizer is rotated by 90 ° observable P or S).
But existing experimental provision is to install the rocking arm equipped with optical-electrical converter at sample rotary table edge, changes an incidence Angle, angle during with regard to reflected light light intensity maximum need to be looked for turn round rocking arm.Error is big, and very inconvenient, must also be tested in darkroom.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of solid refractometry experimental provision.
The purpose of the present invention is to be achieved by the following technical programs:A kind of solid refractometry experimental provision, bag Include base, semiconductor laser, mounting seat, rotary encoder, vertical tube, cylindric test cavity, rotary handle, sample iron seat, Analytical instrument;The vertical tube is arranged on base, and the test cavity is arranged on vertical tube upper end, and the experiment chamber inner sidewall posts soft Property solar battery sheet.Test cavity side wall is provided with laser hole, and the mounting seat front end is connected with laser hole, semiconductor laser Device is fixedly connected with installing base rear end, and polarizer is provided with mounting seat.Rotating disk and swing pinion are installed in test cavity, it is described Swing pinion is embedded in the chassis of test cavity, and the rotating disk is inverted round stage structure, is co-axially mounted with chassis, the side of bottom has With the swing pinion meshed gears structure;
Rotary handle is arranged on the lower surface on chassis, is connected by round bar with swing pinion;The rotary encoder is fixed In vertical tube, it measures axle and passes through chassis, is connected with disk middle spindle.The sample iron seat is located on rotating disk, is carried on sample Testing sample on iron seat is located in same perpendicular with disk diameter;The laser of semiconductor laser is through polarizer Afterwards, it is injected into through laser hole in the test sample being fixed on sample iron seat, sample reflexes to flexible solar electricity after tested Pond piece.Rotary encoder and the flexible solar battery piece is connected with analyzer;Analyzer gathers flexible solar battery piece Output voltage, obtain reflected light intensity of illumination, by rotary encoder obtain laser relative to test sample angle of reflection Degree.
Further, the polarizer in mounting seat is rotatable.
Further, the mounting seat drives the polarizer turning handle for being provided with and being connected with the polarizer in circumferential groove, groove.
Further, the station location marker of sample iron seat is carved with the rotating disk so that be carried on to be measured on sample iron seat Sample is located in same perpendicular with disk diameter.
Further, the station location marker is the cross hairs put centered on the rotating disk center of circle, or is tangent with disk diameter Wire.
Due to using above-mentioned technical proposal, the invention has the advantages that:
1. using flexible lengths solar cell and rotary encoder, it is not required to use rocking arm, so that it may accurate to measure reflection letter Number maximum and reflection angle.
2. can consecutive variations incidence angle, synchronism output reflected signal and angle supply analytical instrument, measurement solid refractive index, tests Demonstrate,prove Fresnel law etc..
It 3. not influenceed by external stray light, can be tested in bright room, reduce error.
Brief description of the drawings
Fig. 1 is figure of the embodiment of the present invention;
Fig. 2 is principle schematic diagram;
Fig. 3 is cylindric test cavity structural representation
In figure:Base 1, semiconductor laser 2, mounting seat 3, socket 4, test sample 5, sample iron seat 6, flexible solar Cell piece 7, rotating disk 8, test cavity 9, chassis 10, rotary handle 11, rotary encoder 12, vertical tube 13, swing pinion 14, top cover 15th, analyzer 16, polarizer turning handle 17, wire 18.
Embodiment
The present invention is described in further detail with embodiment below in conjunction with the accompanying drawings:
As depicted in figs. 1 and 2, a kind of solid refractometry experimental provision, including base 1, semiconductor laser 2, peace Fill seat 3, rotary encoder 12, vertical tube 13, cylindric test cavity 9, rotary handle 11, sample iron seat 6, analyzer 16;
The vertical tube 13 is arranged on base 1, and the test cavity 9 is arranged on the upper end of vertical tube 13, the madial wall of test cavity 9 Post flexible solar battery piece 7.The test cavity 9 is made up of closed test cavity chassis, side wall and top cover 15, can be Bright room experiment, wherein, side wall is provided with laser hole, and the mounting seat 3 is installed at the laser hole of test cavity side wall, semiconductor laser Device 2 is fixedly connected with mounting seat 3, and rotary polarizer is laid in mounting seat 3, by adjusting polarizer polarization direction, Observable P or S curve.
As shown in figure 3, being provided with rotating disk 8 and swing pinion 14 in test cavity 9, the swing pinion 14 is embedded in test cavity 9 Chassis 10 in, the rotating disk 8 be inverted round stage structure, be co-axially mounted with chassis 10, be embedded in the top of chassis 10, the bottom of rotating disk 8 Side has and the meshed gears structure of swing pinion 14;
Rotary handle 11 is arranged on the lower surface on chassis 10, is connected by round bar with swing pinion 14;The rotary coding Device 12 is fixed in vertical tube 13, and it measures axle and passes through chassis 10, is connected with rotating disk 8.By the rotatable rotary table 8 of rotary handle 11, Its anglec of rotation is read by rotary encoder 12.
The side of sample iron seat 6 is pasted, adsorbs or be mechanically anchored in the testing sample 5 vertically, and sample iron seat 6, which is placed on, to be turned On disk 8, can by setting the station location marker of sample iron seat 6 on rotating disk 8, as shown in Figure 2, it is ensured that be put into every time after sample, Testing sample 5 is located in same perpendicular with the diameter of rotating disk 8, this ensures that incident light path is consistent with reflection light path, all For the radius of wall, it is easy to calculate;Station location marker is the cross hairs put centered on the center of circle of rotating disk 8, or as shown in Figure 2 Wire, one side of wire is overlapped with the diameter of rotating disk 8.
The laser that semiconductor laser 2 is launched is incident upon on the face of test sample 5, after tested after polarizer through laser hole Sample 5 reflexes to flexible solar battery piece 7.By the rotary turnplate 8 of rotary handle 11, place superincumbent test sample 5 with Rotation, namely change the incidence angle of light, reflected light is incident upon on flexible solar battery.
The rotary encoder 12 and flexible solar battery piece 7 are connected with analyzer 16 respectively;In figure, flexible solar Cell piece 7 is connected by the socket 4 being connected on the wall of side with analyzer 16, lead-out wire and the phase of analyzer 16 of rotary encoder 12 Even, the output voltage of the collection flexible solar battery of analyzer 16 piece 7, obtains the intensity of illumination of reflected light, passes through rotary coding Device 12 obtains reflection angle of the laser relative to test sample 5.By implementing measurement, corresponding angle when obtaining light intensity minimum, And then obtain the refractive index of test sample 5.In figure, semiconductor laser 2 is powered by analyzer 16.
It should be noted that in the present invention, the mounting seat 3 of polarizer rotation can be caused to belong to the general production of this area Product, for example, mounting seat 3 opens circumferential groove, the corresponding angle of circumference of groove is 90 °, and be connected with the polarizer inclined is provided with groove Shake piece turning handle 17.By stirring polarizer turning handle 17, you can adjustment polarizer polarization direction.
Finally, it is also noted that, listed above is only the specific embodiment of the present invention.Obviously, the present invention is gone back There can be many deformations, it is all that one of ordinary skill in the art directly can export or associate from present disclosure Deformation, is considered as protection scope of the present invention.

Claims (5)

1. a kind of solid refractometry experimental provision, it is characterised in that:Including base (1), semiconductor laser (2), install Seat (3), rotary encoder (12), vertical tube (13), cylindric test cavity (9), rotary handle (11), sample iron seat (6), analysis Instrument (16);The vertical tube (13) is arranged on base (1), and the test cavity (9) is arranged on vertical tube (13) upper end, the experiment Chamber (9) madial wall posts flexible solar battery piece (7).Test cavity (9) side wall is provided with laser hole, the mounting seat (3) Front end is connected with laser hole, and semiconductor laser (2) is fixedly connected with mounting seat (3) rear end, and polarization is provided with mounting seat (3) Piece.Rotating disk (8) and swing pinion (14) are installed in test cavity (9), the swing pinion (14) is embedded in the chassis of test cavity (9) (10) in, the rotating disk (8) is inverted round stage structure, is co-axially mounted with chassis (10), and the side of bottom has and the rotary teeth Take turns (14) meshed gears structure;
Rotary handle (11) is arranged on the lower surface of chassis (10), is connected by round bar with swing pinion (14);The rotation is compiled Code device (12) is fixed in vertical tube (13), and it measures axle and passes through chassis (10), is connected with rotating disk (8) central shaft.The sample iron Seat (6) is located on rotating disk (8), and it is same vertical that the testing sample (5) being carried on sample iron seat (6) is located at rotating disk (8) diameter In plane;The laser of semiconductor laser (2) transmitting is injected into through laser hole after polarizer and is fixed on sample iron seat (6) On test sample (5) on, sample (5) reflexes to flexible solar battery piece (7) after tested.The rotary encoder (12) and Flexible solar battery piece (7) is connected with analyzer (16);The output electricity of analyzer (16) collection flexible solar battery piece (7) Pressure, obtains the intensity of illumination of reflected light, and angle of reflection of the laser relative to test sample (5) is obtained by rotary encoder (12) Degree.
2. experimental provision according to claim 1, it is characterised in that the polarizer in mounting seat (3) is rotatable.
3. experimental provision according to claim 2, it is characterised in that the mounting seat (3) is opened in circumferential groove, groove and installed There is the polarizer turning handle (17) being connected with the polarizer.
4. experimental provision according to claim 1, it is characterised in that the position of sample iron seat (6) is carved with the rotating disk (8) Put mark so that be carried on the testing sample (5) on sample iron seat (6) and be located at rotating disk (8) diameter in same perpendicular.
5. experimental provision according to claim 4, it is characterised in that the station location marker be using rotating disk (8) center of circle in The cross hairs of heart point, or be the wire tangent with rotating disk (8) diameter.
CN201710452496.XA 2017-06-15 2017-06-15 Experimental device for solid refractive index measurement Active CN107256668B (en)

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Application Number Priority Date Filing Date Title
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CN107256668B CN107256668B (en) 2022-06-17

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107782698A (en) * 2017-11-16 2018-03-09 鞍山师范学院 Experimental method and device based on fresnel formula measurement refractive index

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CN102749303A (en) * 2012-07-14 2012-10-24 浙江师范大学 Device and method for measuring refractive index of flat plate type transparent medium
CN203572632U (en) * 2013-05-16 2014-04-30 宁波大学 Device for measuring optical parameters of dielectric film
CN204405543U (en) * 2014-11-04 2015-06-17 湖南科技大学 Rotary Variable multi-angle laser light scattering instrument
CN106662519A (en) * 2014-08-20 2017-05-10 研究三角协会 Devices, systems and methods for detecting particles

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Publication number Priority date Publication date Assignee Title
DE4312812A1 (en) * 1993-04-20 1994-10-27 Deutsche Bundespost Telekom Process and arrangement for determining the end point of silylation processes of exposed varnishes for masks
CN101799413A (en) * 2010-03-05 2010-08-11 陕西师范大学 Experimental apparatus for measuring refractive indexes of liquid and measuring method thereof
CN102589452A (en) * 2012-01-17 2012-07-18 华南师范大学 Method and device for measuring thickness and refractive index of thin film
CN202421066U (en) * 2012-01-19 2012-09-05 杨立荣 Refractive index measuring instrument
CN102749303A (en) * 2012-07-14 2012-10-24 浙江师范大学 Device and method for measuring refractive index of flat plate type transparent medium
CN203572632U (en) * 2013-05-16 2014-04-30 宁波大学 Device for measuring optical parameters of dielectric film
CN106662519A (en) * 2014-08-20 2017-05-10 研究三角协会 Devices, systems and methods for detecting particles
CN204405543U (en) * 2014-11-04 2015-06-17 湖南科技大学 Rotary Variable multi-angle laser light scattering instrument

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107782698A (en) * 2017-11-16 2018-03-09 鞍山师范学院 Experimental method and device based on fresnel formula measurement refractive index
CN107782698B (en) * 2017-11-16 2024-04-12 鞍山师范学院 Experimental method and device for measuring refractive index based on Fresnel formula

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