CN107254257A - A kind of fireproof coating for being used to build modification - Google Patents
A kind of fireproof coating for being used to build modification Download PDFInfo
- Publication number
- CN107254257A CN107254257A CN201610993921.1A CN201610993921A CN107254257A CN 107254257 A CN107254257 A CN 107254257A CN 201610993921 A CN201610993921 A CN 201610993921A CN 107254257 A CN107254257 A CN 107254257A
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- auxiliary agent
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- coating
- fireproof coating
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D193/00—Coating compositions based on natural resins; Coating compositions based on derivatives thereof
- C09D193/04—Rosin
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
It is used for the fireproof coating of building modification the invention discloses a kind of, by weight, including：30 60 parts of emulsion carriers, 20 40 parts of pigment, 5 25 parts of base-material, 2 15 parts of auxiliary agent, the emulsion carriers select 1 butyric acid and 2 methacrylaldehyde, base-material includes sodium silicate, Ludox, rosin, and pigment is at least one of anatase titanium dioxide zinc oxide, lithopone, stibium trioxide, and auxiliary agent includes defoamer, film forming agent, dispersant, thickener, nertralizer and preservative.The materials such as rosin, sodium silicate, Ludox and the barite of fireproof coating addition of the present invention improve the fire protecting performance of coating；Rosin, coating agent which has to be dissolved in alcohol before use and barite can also strengthen the glossiness of coating simultaneously so that the sight of this coating is more preferably.
Description
Technical field
The present invention relates to building material field, a kind of fireproof coating for being used to build modification is specifically referred to.
Background technology
Traditional fire proofing material mainly has the fire resistant flexible materials such as fire prevention coiled material, fireproof coating, sealing cement, and with water
Based on mud base material, the rigid fire proofing material of addition liquid medicine agent and other auxiliary agents.China's major part FPE is anti-using tradition
Fiery material, traditional fire proofing material exist loss of properties on aging, tensile strength it is low, it is temperature sensitive the shortcomings of.Tradition fire prevention is applied
Material is used for roofing fire prevention, easily cause aging, it is dry and cracked, the phenomenon such as deform, fracture, being layered；It is multiple for shape for indoor fire safety
Miscellaneous place, constructional difficulties, and to Seepage, quality is more difficult to ensure, people's every few years will spend substantial amounts of fund
Reprocessed with labour, not only confused the normal life, work and the production order of people, and influence whole building building
Service life.
The content of the invention
Can effectively be prevented fires it is an object of the invention to provide one kind, color is various, good luster be used for build modification
Coating.
The present invention is achieved through the following technical solutions：A kind of fireproof coating for being used to build modification, by weight, bag
Include：30-60 parts of emulsion carriers, 20-40 parts of pigment, 5-25 parts of base-material, 2-15 parts of auxiliary agent, the emulsion carriers from 1- butyric acid and
2- methacrylaldehyde, base-material includes sodium silicate, Ludox, rosin, wherein；
Rosin is soluble in various organic solvents, and easily film forming, glossy, is one of base stock of coating；Rosin is in paint
In effect be to make paint bright in color, fast drying, paint film is smooth difficult for drop-off；
Sodium silicate is sodium silicate aqueous solution, and molecular formula is Na2OmSiO2.KP1 is potassium silicate aqueous solution, molecular formula
For K2OmSiO2；M in sodium silicate molecular formula is referred to as the modulus of waterglass, represents Na2O and SiO2 mol ratio, right and wrong
Often important parameter.M values are bigger, and the viscosity of waterglass is higher；Sodium silicate generally uses silica flour（SiO2）Plus soda ash
（Na2CO3）, the calcining generation liquid sodium silicate at a high temperature of 1300~1400 DEG C, from furnace discharge mouthful outflow, clamp dog or water quenching into
Particle.Dissolved again in high temperature or high-temperature high pressure water, obtained solution shape waterglass product.
Ludox inorganic polymer coating grew up in recent years.The key technology of the coating is prepared with special
Method removes water miscible sodium ion in waterglass.The methods such as ion exchange, sour neutralization, water decomposition, electrodialysis can typically be used
To realize, to generate a kind of gluey aqueous solution of superfine silica ultramicron, particle diameter is 580nm（General emulsion particle is
800-1000nm）The ratio of wherein Si2O contents 20%-30%, Na2O content 0.3%$, silica and sodium oxide molybdena is more than 40%.
Using this silicon solution/glue as base-material, coordinate pigment and various auxiliary agents and Ludox inorganic polymer coating is made.Silicon solution is losing
When removing moisture, monomeric silicic acid gradually aggregates into high poly- silica gel, and with the evaporation of moisture, colloid molecules increase eventually forms-SIO-O-
SIO- films：Contents of the IO-SI-OH+HO-SI-OH because of NA2O in Ludox is low, and Ludox has a certain amount of film forming dissolving
Characteristic, its water resistance, heat resistance are substantially better than organic coating.Film is fine and close and harder, does not produce various dirt in electrostatic, air
Angstrom difficult adhesion.
Further, the base-material also includes at least one of coating agent which has to be dissolved in alcohol before use and barite.
Further, the pigment is at least one of anatase titanium dioxide zinc oxide, lithopone, stibium trioxide.
Further, the auxiliary agent includes defoamer, film forming agent, dispersant, thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 30%~50%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 20%~40%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 2%~10%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, the thickener account for the mass percent of the auxiliary agent for 2%~
10%；
The nertralizer is low molecule organic amine compound, the nertralizer account for the mass percent of the auxiliary agent for 2%~
10%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 2%~10%.
Further, the fireproof coating also includes 3-10 parts of deionized water.
Its preparation method is as follows：Above-mentioned all raw materials are mixed, and are ground to 5 microns of granularity ＜, then heating makes to own
Solid material melts, and continues stirring 1 hour, to be made.
The materials such as rosin, sodium silicate, Ludox and the barite of fireproof coating addition of the present invention improve coating
Fire protecting performance；Rosin, coating agent which has to be dissolved in alcohol before use and barite can also strengthen the glossiness of coating simultaneously so that the sight of this coating is more
It is good.
Embodiment
The present invention is described in further detail with reference to embodiment, but the implementation of the present invention is not limited to this,
Without departing from the idea case in the present invention described above, according to ordinary skill knowledge and customary means, various replace is made
Change and change, all should be included within the scope of the invention.
Embodiment 1：
A kind of fireproof coating for being used to build modification described in the present embodiment, by weight, including：40 parts of emulsion carriers, pigment
30 parts, 10 parts of base-material, 5 parts of auxiliary agent, the emulsion carriers select 1- butyric acid and 2- methacrylaldehyde, and it is molten that base-material includes sodium silicate, silicon
Glue, rosin, the pigment is at least one of anatase titanium dioxide zinc oxide, lithopone, stibium trioxide, the auxiliary agent include defoamer, into
Film, dispersant, thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 34%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 34%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 8%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, and the mass percent that the thickener accounts for the auxiliary agent is 8%；
The nertralizer is low molecule organic amine compound, and the mass percent that the nertralizer accounts for the auxiliary agent is 8%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 8%.
Flameproof effect is tested：
According to country building material industry standard JC/T984-2005 to having done impermeability test using the embodiment of the present invention, by 6.3cm,
It is tested after 6.4cm, 6.5cm shaping, it was demonstrated that its impermeability pressure reaches 3.4MPa, there is good impervious effect.
According to country building material industry standard JC/T984-2005 to being tested using the shrinkage factor of the embodiment of the present invention,
Shrinkage factor is 0.05%.
According to country building material industry standard JC/T958-2005 to having carried out abrasion test using the embodiment of the present invention, in mill
When wiping 200 times, 0.06g only have lost.
According to country building material industry standard JC/T894-2001 to having carried out degradation using the embodiment of the present invention, 3 are done
Block 10 × 10 × 40CM test blocks, its compression strength is tested after 45 degree of ultraviolets irradiate 250 hours, and for 64.5MPa, (blank is real
Block is 45.2MPa).
The experiment of freeze thawing resistance Rapid Circulation has been carried out to what is be made using the embodiment of the present invention according to GBJ82-85 national standards,
Its mass loss 0%, relative resilient modulus 90.3%.
Embodiment 2：
A kind of fireproof coating for being used to build modification described in the present embodiment, by weight, including：50 parts of emulsion carriers, pigment
40 parts, 20 parts of base-material, 10 parts of auxiliary agent, the emulsion carriers select 1- butyric acid and 2- methacrylaldehyde, base-material include rosin, calcium silicates,
Coating agent which has to be dissolved in alcohol before use and barite, the pigment be anatase titanium dioxide zinc oxide, lithopone, the auxiliary agent include defoamer, film forming agent, dispersant,
Thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 50%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 40%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 2%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, and the mass percent that the thickener accounts for the auxiliary agent is 2%；
The nertralizer is low molecule organic amine compound, and the mass percent that the nertralizer accounts for the auxiliary agent is 2%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 4%.
Flameproof effect is tested：
According to country building material industry standard JC/T984-2005 to having done impermeability test using the embodiment of the present invention, by 6.3cm,
It is tested after 6.4cm, 6.5cm shaping, it was demonstrated that its impermeability pressure reaches 3.2MPa, there is good impervious effect.
According to country building material industry standard JC/T984-2005 to being tested using the shrinkage factor of the embodiment of the present invention,
Shrinkage factor is 0.05%.
According to country building material industry standard JC/T958-2005 to having carried out abrasion test using the embodiment of the present invention, in mill
When wiping 200 times, 0.07g only have lost.
According to country building material industry standard JC/T894-2001 to having carried out degradation using the embodiment of the present invention, 3 are done
Block 10 × 10 × 40CM test blocks, its compression strength is tested after 45 degree of ultraviolets irradiate 250 hours, and for 66.3MPa, (blank is real
Block is 45.2MPa).
The experiment of freeze thawing resistance Rapid Circulation has been carried out to what is be made using the embodiment of the present invention according to GBJ82-85 national standards,
Its mass loss 0%, relative resilient modulus 88.9%.
The other parts of the present embodiment are same as the previously described embodiments, repeat no more.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that：Not
A variety of change, modification, replacement and modification can be carried out to these embodiments by departing under the principle and objective of the present invention, of the invention
Scope is limited by claim and its equivalent.
Claims (5)
1. a kind of fireproof coating for being used to build modification, it is characterised in that by weight, including：30-60 parts of emulsion carriers,
20-40 parts of pigment, 5-25 parts of base-material, 2-15 parts of auxiliary agent, the emulsion carriers select 1- butyric acid and 2- methacrylaldehyde, and base-material includes sodium
Waterglass, Ludox, rosin.
2. a kind of fireproof coating for being used to build modification according to claim 1, it is characterised in that the base-material also includes
At least one of coating agent which has to be dissolved in alcohol before use and barite.
3. a kind of fireproof coating for being used to build modification according to claim 1 or 2, it is characterised in that the pigment is
At least one of anatase titanium dioxide zinc oxide, lithopone, stibium trioxide.
4. a kind of fireproof coating for being used to build modification according to claim 3, it is characterised in that the auxiliary agent includes disappearing
Infusion, film forming agent, dispersant, thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 30%~50%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 20%~40%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 2%~10%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, the thickener account for the mass percent of the auxiliary agent for 2%~
10%；
The nertralizer is low molecule organic amine compound, the nertralizer account for the mass percent of the auxiliary agent for 2%~
10%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 2%~10%.
5. a kind of fireproof coating for being used to build modification according to claim 1 or 2, it is characterised in that the fire prevention is applied
Material also includes 3-10 parts of deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610993921.1A CN107254257A (en) | 2016-11-11 | 2016-11-11 | A kind of fireproof coating for being used to build modification |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610993921.1A CN107254257A (en) | 2016-11-11 | 2016-11-11 | A kind of fireproof coating for being used to build modification |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107254257A true CN107254257A (en) | 2017-10-17 |
Family
ID=60027139
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610993921.1A Withdrawn CN107254257A (en) | 2016-11-11 | 2016-11-11 | A kind of fireproof coating for being used to build modification |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107254257A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1046175A (en) * | 1989-04-08 | 1990-10-17 | 赵敏 | Flame retardant paint |
| CN105462298A (en) * | 2015-12-25 | 2016-04-06 | 李宏亮 | Fireproof coating and H steel structural member coated by same for building |
-
2016
- 2016-11-11 CN CN201610993921.1A patent/CN107254257A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1046175A (en) * | 1989-04-08 | 1990-10-17 | 赵敏 | Flame retardant paint |
| CN105462298A (en) * | 2015-12-25 | 2016-04-06 | 李宏亮 | Fireproof coating and H steel structural member coated by same for building |
Non-Patent Citations (1)
| Title |
|---|
| 赵雨森等: "《林业概论》", 30 September 2004, 东北林业大学出版社 * |
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Application publication date: 20171017 |
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