CN107233421A - Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract and preparation method thereof - Google Patents
Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract and preparation method thereof Download PDFInfo
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- CN107233421A CN107233421A CN201710526565.7A CN201710526565A CN107233421A CN 107233421 A CN107233421 A CN 107233421A CN 201710526565 A CN201710526565 A CN 201710526565A CN 107233421 A CN107233421 A CN 107233421A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/758—Zanthoxylum, e.g. pricklyash
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
- A61K47/12—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The invention discloses lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is made up of the raw material of following weight：Chinese prickly ash branch or 1 part of Chinese pricklyash root extract, 0.03 0.05 parts of dehydroactic acid sodium；Chinese prickly ash bath used among the people, the bath of Chinese prickly ash branch or the bath of Chinese prickly ash tree root have good mitigation to a variety of pain, have a wide range of applications, wherein Chinese prickly ash price is high, and Chinese prickly ash branch and Chinese prickly ash tree root are the accessory substance that Chinese prickly ash is produced, it is cheap and easy to get, therefore, the present invention prepares lavipeditum powder using Chinese prickly ash branch and Chinese prickly ash tree root as raw material.Its is simple to operate, easy to use, and without the dregs of a decoction, environment is made and does not become pollution；Chinese prickly ash plantation has territorial characteristics, does not plant that the application of Chinese prickly ash area is inconvenient, and the extract of Chinese prickly ash tree root branch has been carried out into working process in the present invention, with convenient transportation, advantage simple to operate has been used so that when and where patient is no matter can use.
Description
Technical field
Lavipeditum powder prepared the present invention relates to a kind of utilization bunge pricklyash root branch extract and preparation method thereof.
Background technology
Chinese prickly ash branch and Chinese prickly ash tree root are rutaceae Chinese prickly ash（Zanthoxylum bungeanum Maxim.）Branch
Dry and root, is the byproduct of Chinese prickly ash production.Chinese prickly ash is in Chinese plantation extensively, with edible and medical value, while being mountain region again
Ecological Afforestation, the important species of water and soil conservation.Chinese prickly ash branch and Chinese prickly ash tree root have the work(of " cold dispelling, dehumidifying, analgesic, desinsection "
Effect, main component includes volatile oil, alkaloid, flavones, cumarin etc..
There is a bubble pin side in the Chinese department of traditional Chinese medicine institute Lu Guangxin researcher of late traditional Chinese medical science great master, health experience, i.e., with flower
Green pepper bubble pin, its method is：With 50 grams of Chinese prickly ashes of a cotton bag, tightened, added water after boiling with line, with the Chinese prickly ash bubble boiled
Pin.Chinese prickly ash bag can be with Reusability, the Chinese prickly ash bag that a Zhou Houzai more renews.Mr. Lu Guangxin thinks, with Chinese prickly ash bubble pin, have
Promoting blood circulation and removing blood stasis, clearing and activating the channels and collaterals effect, can make whole body unobstructed vessel, and feel relief happiness.The external application of Popular Utilization pricklyash twig is smoked
Wash, treat colpomycosis, curative effect is good；Pricklyash twig middle benefit gas to boil water of having drunk relieves the pain, the effect for the antidiarrheal that dehumidifies, and treats a variety of pains
Pain and bruises and sprains.
Also there are the dipping side of many Chinese prickly ashes or pricklyash twig for raw material, such as five analgesia soup in Traditional Chinese medicine medicated bath side：With ramulus mori, osmanthus
Branch, grape branch, old eggplant branch, pricklyash twig decocting balneation, can disappear bodily pain, decocting washout, to arthralgia, and various arthritis cards have good
Good adjuvant treatment effect；The lavipeditum side that psoralea corylifolia, Chinese prickly ash, radix cyathulae, levisticum, saltcake are prepared cures mainly all kinds of talagias；Rhizoma Sparganii,
The lavipeditum side that curcuma zedoary, Artemisia anomala, motherwort, Chinese prickly ash are prepared cures mainly sprain of ankle joint；Notopterygium root, levisticum, monkshood, earthworm, folium artemisiae argyi, five
Plus the lavipeditum side that skin, pericarpium zanthoxyli are prepared cures mainly lower limb osteoproliferation.
Chinese prickly ash bath used among the people, pricklyash twig bath or bunge pricklyash root bath have good mitigation to a variety of pain, with wide
General application, wherein Chinese prickly ash price are high, and Chinese prickly ash branch and Chinese prickly ash tree root are the accessory substance that Chinese prickly ash is produced, cheap and easy to get.The medicine
Bath conventional use is that Chinese prickly ash branch and the heating of Chinese prickly ash tree root are boiled certain time, is used after cooling, complex operation and the consumption energy,
The dregs of a decoction pollute the environment.The plantation of its Chinese prickly ash also has territorial characteristics, the application of Chinese prickly ash area is not planted inconvenient.
The content of the invention
Lavipeditum powder prepared it is an object of the invention to provide a kind of utilization bunge pricklyash root branch extract and preparation method thereof.
The technical scheme is that：Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is by following parts by weight
The raw material of proportioning is made：Chinese prickly ash branch or 1 part of Chinese pricklyash root extract, 0.03-0.05 parts of dehydroactic acid sodium, the Chinese prickly ash branch
Or Chinese pricklyash root extract is extract of the Extraction solvent in Chinese prickly ash branch or Chinese prickly ash tree root.
It is preferred that, the preparation method of lavipeditum powder prepared by a kind of described utilization bunge pricklyash root branch extract, including following step
Suddenly：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 0.5-20mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, extracted with Extraction solvent, Extraction solvent and the Chinese prickly ash branch
Or the mass ratio of Chinese prickly ash tree root is 1:3-20 kg/ L, merge extract solution, then are concentrated, and dry, obtain extract A；
（3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40-80 DEG C, air blast
Dry 10-20 min and obtain dry powder B；
（4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80-100 mesh, is placed in ultraviolet sterilizer, ultraviolet
After radiation sterilization 10-15 min, package encapsulation is got product.
It is preferred that, the Extraction solvent is the mixed solution or volume for the methanol/water that water, percentage by volume are 30-100%
Percentage is 30-100% ethanol/water mixed solution.
It is preferred that, the method that described Extraction solvent is extracted have room temperature cold soaking, be heated to reflux, seepage and ultrasound are carried
Take.
It is preferred that, the extracting method room temperature cold soaking needs the Chinese prickly ash branch or Chinese prickly ash after Extraction solvent and coarse crushing every time
Tree root soaks 5-9 days, and extracting times are 1-4 times.
It is preferred that, the heating-up temperature that the extracting method is heated to reflux is 70-100 DEG C, is extracted 1.0-3.0 hours every time,
Extraction time is 1-4 times.
It is preferred that, the extracting method seepage is needed the Chinese prickly ash branch after Extraction solvent and coarse crushing or the immersion of Chinese prickly ash tree root
18-24h, then it is placed in seepage equipment.
It is preferred that, the Extracting temperature of the extracting method ultrasonic extraction is 40-60 DEG C, and frequency is 20-50Hz, and power is
70-1000W, is extracted 0.5-2.0 hours every time, and extraction time is 1-4 times.
Beneficial effects of the present invention are：
（1）Chinese prickly ash plantation has territorial characteristics, does not plant Chinese prickly ash tree root branch in Chinese prickly ash area application inconvenience, the present invention
Extract has carried out working process, with convenient transportation, uses advantage simple to operate so that when and where patient regardless of
It can use.
（2）Chinese prickly ash bath used among the people, the bath of Chinese prickly ash branch or the bath of Chinese prickly ash tree root have good mitigation to a variety of pain,
Have a wide range of applications, wherein Chinese prickly ash price is high, and Chinese prickly ash branch and Chinese prickly ash tree root are the accessory substance that Chinese prickly ash is produced, it is cheap easy
, therefore, the present invention prepares lavipeditum powder using Chinese prickly ash branch and Chinese prickly ash tree root as raw material.Its is simple to operate, easy to use, and without medicine
Slag, makes to environment and does not become pollution.
（3）The dehydroactic acid sodium used in the present invention is the another Dai Xin after sodium benzoate, nipalgin, potassium sorbate
Food preservative freshness retaining agent, with broad-spectrum antiseptic ability, has good inhibiting effect to mould, saccharomycete, bacterium, suppresses effective
Concentration is 0.05%-0.1%, and general consumption is 0.03%-0.05%, is widely used in the processing industry of beverage, food, feed, in fortune
Storage period can be extended when defeated, it is to avoid loss of going mouldy.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.
Embodiment 1：
Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is made up of the raw material of following weight：Chinese prickly ash branch
Or 1 part of Chinese pricklyash root extract, 0.03 part of dehydroactic acid sodium.
Its preparation method comprises the following steps：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 10mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, heating and refluxing extraction is carried out with water, heating-up temperature is 90 DEG C, is extracted
2.0 hours, the mass volume ratio of water and Chinese prickly ash branch or Chinese prickly ash tree root was 1:10 kg/ L, merge extract solution, then are concentrated,
Dry, obtain extract A；
3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40 DEG C, forced air drying
10 min obtain dry powder B；
4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80 mesh, is placed in ultraviolet sterilizer, ultraviolet irradiation
Sterilize after 10 min, package encapsulation is got product.
Embodiment 2
Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is made up of the raw material of following weight：Chinese prickly ash branch
Or 1 part of Chinese pricklyash root extract, 0.04 part of dehydroactic acid sodium.
Its preparation method comprises the following steps：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 15mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, room temperature cold soaking extraction is carried out with water and 80% methanol, will be extracted molten
Chinese prickly ash branch or Chinese prickly ash tree root after agent and coarse crushing soak 8 days, the quality of water and 80% methanol and Chinese prickly ash branch or Chinese prickly ash tree root
Volume ratio is 1:5 kg/ L, merge extract solution, then are concentrated, and dry, obtain extract A；
3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40 DEG C, forced air drying
15 min obtain dry powder B；
4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80 mesh, is placed in ultraviolet sterilizer, ultraviolet irradiation
Sterilize after 12 min, package encapsulation is got product.
Embodiment 3
Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is made up of the raw material of following weight：Chinese prickly ash branch
Or 1 part of Chinese pricklyash root extract, 0.05 part of dehydroactic acid sodium.
Its preparation method comprises the following steps：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 15mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, seepage extraction is carried out with water and 80% ethanol, by Extraction solvent and
The quality volume of Chinese prickly ash branch or Chinese prickly ash tree root immersion 20h after coarse crushing, water and 80% ethanol and Chinese prickly ash branch or Chinese prickly ash tree root
Than for 1:15kg/ L, merge extract solution, then are concentrated, and dry, obtain extract A；
3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40 DEG C, forced air drying
17min obtains dry powder B；
4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80 mesh, is placed in ultraviolet sterilizer, ultraviolet irradiation
Sterilize after 10 min, package encapsulation is got product.
Embodiment 4
Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is made up of the raw material of following weight：Chinese prickly ash branch
Or 1 part of Chinese pricklyash root extract, 0.05 part of dehydroactic acid sodium.
Its preparation method comprises the following steps：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 15mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, ultrasonic extraction is carried out with water and 60% ethanol, Extracting temperature is 50
DEG C, frequency is 40Hz, and power is 500W, is carried 1.0 hours, water and 60% ethanol and Chinese prickly ash branch or the mass body of Chinese prickly ash tree root
Product is than being 1:15kg/ L, merge extract solution, then are concentrated, and dry, obtain extract A；
3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40 DEG C, forced air drying
17min obtains dry powder B；
4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80 mesh, is placed in ultraviolet sterilizer, ultraviolet irradiation
Sterilize after 10 min, package encapsulation is got product.
Claims (8)
1. lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract, it is characterised in that：It by following weight raw material
It is made：Chinese prickly ash branch or 1 part of Chinese pricklyash root extract, 0.03-0.05 parts of dehydroactic acid sodium, the Chinese prickly ash branch or Chinese prickly ash tree root
Extract is extract of the Extraction solvent in Chinese prickly ash branch or Chinese prickly ash tree root.
2. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 1, its feature
It is to comprise the following steps：
（1）Chinese prickly ash branch or Chinese prickly ash tree root are cleaned, dried in the shade, then carries out coarse crushing, smashing fineness is 0.5-20mm；
（2）By the Chinese prickly ash branch or Chinese prickly ash tree root after coarse crushing, extracted with Extraction solvent, Extraction solvent and the Chinese prickly ash branch
Or the mass ratio of Chinese prickly ash tree root is 1:3-20 kg/ L, merge extract solution, then are concentrated, and dry, obtain extract A；
（3）After addition dehydroactic acid sodium stirs in extract A, it is put into the drying equipment that temperature is 40-80 DEG C, air blast
Dry 10-20 min and obtain dry powder B；
（4）Obtained dry powder B is placed in crusher for Chinese herbal medicine, is crushed to 80-100 mesh, is placed in ultraviolet sterilizer, ultraviolet
After radiation sterilization 10-15 min, package encapsulation is got product.
3. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 1 or 2, it is special
Levy and be：The Extraction solvent is that the mixed solution or percentage by volume of the methanol/water that water, percentage by volume are 30-100% are
30-100% ethanol/water mixed solution.
4. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 2, its feature
It is：The method that described Extraction solvent is extracted have room temperature cold soaking, be heated to reflux, seepage or ultrasonic extraction.
5. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 4, its feature
It is：The extracting method room temperature cold soaking needs the Chinese prickly ash branch after Extraction solvent and coarse crushing or Chinese prickly ash tree root immersion 5- every time
9 days, extracting times were 1-4 times.
6. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 4, its feature
It is：The heating-up temperature that the extracting method is heated to reflux is 70-100 DEG C, is extracted 1.0-3.0 hours every time, and extraction time is
1-4 times.
7. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 4, its feature
It is：The extracting method seepage is needed the Chinese prickly ash branch after Extraction solvent and coarse crushing or Chinese prickly ash tree root immersion 18-24h, then
It is placed in seepage equipment.
8. the preparation method of lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract according to claim 4, its feature
It is：The Extracting temperature of the extracting method ultrasonic extraction is 40-60 DEG C, and frequency is 20-50Hz, and power is 70-1000W, often
Secondary extraction 0.5-2.0 hours, extraction time is 1-4 times.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710526565.7A CN107233421A (en) | 2017-06-30 | 2017-06-30 | Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710526565.7A CN107233421A (en) | 2017-06-30 | 2017-06-30 | Lavipeditum powder prepared by a kind of utilization bunge pricklyash root branch extract and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113350412A (en) * | 2021-06-24 | 2021-09-07 | 王先奇 | Foot bath bag and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101890102A (en) * | 2009-05-18 | 2010-11-24 | 邱宏亮 | Velamen or stem bark extract of Zanthoxylum simulans, extracting method and oral cavity medicinal composite thereof |
| CN106619961A (en) * | 2015-11-03 | 2017-05-10 | 贾书超 | Traditional Chinese medicine footbath health-maintaining and health-care prescription capable of promoting blood circulation and removing blood stasis and relaxing muscles and tendons and removing obstruction from meridians |
-
2017
- 2017-06-30 CN CN201710526565.7A patent/CN107233421A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101890102A (en) * | 2009-05-18 | 2010-11-24 | 邱宏亮 | Velamen or stem bark extract of Zanthoxylum simulans, extracting method and oral cavity medicinal composite thereof |
| CN106619961A (en) * | 2015-11-03 | 2017-05-10 | 贾书超 | Traditional Chinese medicine footbath health-maintaining and health-care prescription capable of promoting blood circulation and removing blood stasis and relaxing muscles and tendons and removing obstruction from meridians |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113350412A (en) * | 2021-06-24 | 2021-09-07 | 王先奇 | Foot bath bag and preparation method thereof |
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Application publication date: 20171010 |
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