CN107232599B - Deer skin glue and preparation method thereof - Google Patents
Deer skin glue and preparation method thereof Download PDFInfo
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- CN107232599B CN107232599B CN201710591105.2A CN201710591105A CN107232599B CN 107232599 B CN107232599 B CN 107232599B CN 201710591105 A CN201710591105 A CN 201710591105A CN 107232599 B CN107232599 B CN 107232599B
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- 239000003292 glue Substances 0.000 title claims abstract description 114
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- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 235000021323 fish oil Nutrition 0.000 claims abstract description 26
- 238000000034 method Methods 0.000 claims abstract description 15
- 235000012424 soybean oil Nutrition 0.000 claims abstract description 13
- 239000003549 soybean oil Substances 0.000 claims abstract description 13
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 9
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- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000282985 Cervus Species 0.000 description 1
- 241000283026 Cervus elaphus Species 0.000 description 1
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- 206010002156 anal fistula Diseases 0.000 description 1
- 210000003056 antler Anatomy 0.000 description 1
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- RNFNDJAIBTYOQL-UHFFFAOYSA-N chloral hydrate Chemical compound OC(O)C(Cl)(Cl)Cl RNFNDJAIBTYOQL-UHFFFAOYSA-N 0.000 description 1
- 229960002327 chloral hydrate Drugs 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 1
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- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/20—Meat products; Meat meal; Preparation or treatment thereof from offal, e.g. rinds, skins, marrow, tripes, feet, ears or snouts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to the technical field of food processing, and particularly relates to deerskin glue and a preparation method thereof. The deer skin glue is mainly prepared from the following raw materials in parts by weight: 2000-2500 parts of deerskin, 100-300 parts of fish oil, 5-8 parts of yellow wine, 5-10 parts of soybean oil and 10-15 parts of rock candy. The deerskin gelatin provided by the invention is mainly prepared from deerskin and fish oil, and can safely and effectively stimulate secretion of sex hormone. The invention adopts the specific and preferred technology to process and treat the deerskin, so that the prepared deerskin glue has the advantages of rich nutrition, safety, sanitation and good preservation of active ingredients.
Description
Technical Field
The invention relates to the technical field of food processing, and particularly relates to deerskin glue and a preparation method thereof.
Background
With the rapid development of economy in China and the improvement of living standard of people, people put forward higher and higher requirements on food. The deer is a treasure on the whole body, so that the deer antler has good health care effect and medicinal efficacy, and other deer products such as deer penis, deer tendon, deer heart blood, deer fetus ointment and the like have good health care and medicinal values. The development and utilization of the deer skin health care product are still in the exploration stage. The deerskin is a traditional and famous traditional Chinese medicine recorded in ancient books of compendium of materia Medica, Chinese pharmacopoeia, Shen nong Ben Cao Jing, Sichuan traditional Chinese medicine Zhi and the like, has the effects of resisting fatigue, tonifying qi and blood, enhancing immunity, maintaining beauty and keeping young and the like, has a long medicinal history which is more than 500 years earlier than that of donkey-hide gelatin, and has been used as a medicine for nearly 3000 years. The description of the property of deer skin in Ben Cao gang mu written by the Ming Dynasty Li Shizhen is warm in nature and salty in taste; has effects in removing toxic materials, invigorating qi, arresting seminal emission, tonifying blood, stopping bleeding, invigorating kidney, and supporting yang; mainly treats anal fistula, leucorrhea, metrorrhagia and metrostaxis, and treats all sores. Decocting cortex Cervi Pantotrichum with Cervus nippon Temminck or Cervus elaphus Linnaeus to obtain Cervus Cervi glue. The deerskin glue is generally brownish red, hard and crisp in texture, bright in section, semitransparent to illumination and has the special fragrance of deerskin glue.
The traditional deerskin glue product has the problems of large viscosity, low purity, unfavorable digestion and absorption, low effective components, poor use effect and the like of deerskin glue, so that improvement of the deerskin glue product is urgently needed.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
The invention aims to provide deerskin glue and a preparation method thereof, so as to solve the problems.
In order to achieve the above purpose of the present invention, the following technical solutions are adopted:
the invention relates to deerskin glue which is mainly prepared from the following raw materials in parts by weight:
2000-2500 parts of deerskin, 100-300 parts of fish oil, 5-8 parts of yellow wine, 5-10 parts of soybean oil and 10-15 parts of rock candy.
The health food is mainly prepared from deerskin and fish oil serving as main raw materials. Although the deerskin and fish oil are known in the field as medicinal and edible products with health care and health preserving effects, the prior art does not describe that the combined use of the raw materials has the effect of improving the sex hormone level. The invention unexpectedly discovers that the deer skin is taken as the main material, and the fish oil is matched with the deer skin to have the effect of promoting the secretion of human sex hormones. Compared with the traditional artificially synthesized sex hormone, the health food disclosed by the invention is a pure natural marine health product, is safe and free from toxic and side effects, and does not have the risk of malignant tumors after being taken.
The invention also relates to a preparation method of the deer skin glue, which comprises the following steps:
1) cleaning deer skin for depilation, removing residual meat and fat on the inner layer of the skin surface, and soaking in alkaline water;
2) soaking again in clear water and washing the deer skin to remove alkaline water;
3) cutting the deer skin obtained in the step 2), blanching the skin through steam, and cleaning again;
4) adding the deer skin obtained in the step 3) into water, pressurizing and melting the skin to discharge the glue juice;
5) filtering the glue juice obtained in the step 4), separating oil and fat, heating to slightly boil, and removing floating foam floating on the surface layer of the water surface;
6) concentrating the glue juice obtained in the step 5) until the water content reaches 35-45%, adding fish oil, yellow wine, soybean oil and rock candy, mixing uniformly, continuing to concentrate until the water content reaches 26-28%, discharging glue, pouring the glue into a glue box, and solidifying into glue blocks;
7) freezing the rubber block at low temperature to form rubber lumps, cutting the rubber lumps, and drying the rubber lumps;
8) sealing and sealing the aired rubber blocks for sealing, taking out after 2-4 days, and repeatedly cooling the rubber blocks according to the method in the step 7); repeating the operation until the water content of the rubber block reaches 14-15%; sterilizing, and packaging.
The deer skin gelatin prepared by the method has low viscosity and high purity, and is more suitable for absorption by human body.
Compared with the prior art, the invention has the beneficial effects that:
1) the deerskin gelatin provided by the invention is mainly prepared from deerskin and fish oil, and can safely and effectively stimulate the organism to secrete sex hormone.
2) The invention adopts the specific and preferred technology to process and treat the deerskin, so that the prepared deerskin glue has the advantages of safety and sanitation, and well-preserved nutrient substances and active ingredients.
Detailed Description
The invention relates to deerskin glue which is mainly prepared from the following raw materials in parts by weight:
2000-2500 parts of deerskin, 100-300 parts of fish oil, 5-8 parts of yellow wine, 5-10 parts of soybean oil and 10-15 parts of rock candy.
Preferably, the deer skin glue is mainly prepared from the following raw materials in parts by weight:
2200-2300 parts of deerskin, 150-250 parts of fish oil, 6-7 parts of yellow wine, 7-8 parts of soybean oil and 10-15 parts of rock candy.
More preferably, the deer skin glue is mainly prepared from the following raw materials in parts by weight:
2500 parts of deerskin, 170-230 parts of fish oil, 6.5 parts of yellow wine, 7.5 parts of soybean oil and 13 parts of rock candy.
Preferably, the deer skin is the skin of sika deer (Cervus nippon Temminck).
Preferably, the fish oil is shark oil. The shark oil is rich in squalene, vitamin A, D, and nutrition, and has effect in tonifying yang.
The invention also relates to a preparation method of the deer skin glue, which comprises the following steps:
1) cleaning deer skin for depilation, removing residual meat and fat on the inner layer of the skin surface, and soaking in alkaline water;
2) soaking again in clear water and washing the deer skin to remove alkaline water;
3) cutting the deer skin obtained in the step 2), blanching the skin through steam, and cleaning again;
4) adding the deer skin obtained in the step 3) into water, pressurizing and melting the skin to discharge the glue juice;
5) filtering the glue juice obtained in the step 4), separating oil and fat, heating to slightly boil, and removing floating foam floating on the surface layer of the water surface;
6) concentrating the glue juice obtained in the step 5) until the water content reaches 35-45%, adding fish oil, yellow wine, soybean oil and rock candy, mixing uniformly, continuing to concentrate until the water content reaches 26-28%, discharging glue, pouring the glue into a glue box, and solidifying into glue blocks;
7) freezing the rubber block at low temperature to form rubber lumps, cutting the rubber lumps, and drying the rubber lumps;
8) sealing and sealing the aired rubber blocks for sealing, taking out after 2-4 days, and repeatedly cooling the rubber blocks according to the method in the step 7); repeating the operation until the water content of the rubber block reaches 14-15%; sterilizing, and packaging.
Preferably, in the preparation method, in the step 1), the alkali water is soaked in alkali water with a pH of 10-11 for 24-48 hours;
more preferably, in the step 1), the alkali water is soaked in alkali water with a pH of 10.5 for 30 to 42 hours.
Preferably, the preparation method as described above, step 4) specifically includes: adding the deerskin obtained in the step 3) into water with the volume 2-5 times of that of the deerskin, melting the deerskin for 4-6 hours under the pressure of 0.15-0.2 MPa, and repeating melting for 2-4 times by the same method;
more preferably, step 4) specifically comprises: adding the deerskin obtained in the step 3) into water which is 3-4 times of the volume of the deerskin, melting the deerskin for 5 hours under the pressure of 0.17-0.18 MPa, and repeating the melting for 3 times by using the same method.
Preferably, in the preparation method as described above, in step 5), the filtering of the glue juice specifically includes:
filtering the glue juice by a screen with 100-140 meshes, and then filtering by 3-5 layers of gauze;
more preferably, in step 5), the gum juice filtration specifically comprises:
filtering the glue juice by a 120-mesh screen and then filtering by 4 layers of gauze.
Preferably, in the preparation method as described above, in step 5), the specific parameters of oil-fat separation are as follows: passing the obtained glue juice through an oil-fat separator at the flow rate of 80-120L/h and the rotation speed of 18000-22000 r/min;
more preferably, in step 5), the specific parameters of the oil-fat separation are as follows: passing the obtained glue juice through an oil-fat separator at a flow rate of 100L/h and a rotation speed of 20000 r/min.
Preferably, in the preparation method, in the step 7), the low-temperature freezing is performed at-10 ℃ to-15 ℃ for 20h to 30 h;
more preferably, in the step 7), the low-temperature freezing condition is-12 ℃ to-13 ℃ for 25 h.
Preferably, in the preparation method as described above, in step 7), the conditions of the cooling glue are as follows:
cooling the glue in a glue cooling room at the temperature of 25-30 ℃ and the relative humidity of 40-60% for 6-8 days;
more preferably, in step 7), the conditions for cooling the gel are as follows:
the temperature is 27-28 ℃, and the relative humidity is 45-55 percent.
Embodiments of the present invention will be described in detail below with reference to examples, but it will be understood by those skilled in the art that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
Example 1
1. Taking 2000g of fresh deerskin, adding 3 times of water (the volume ratio of the added water is the volume ratio) and repeatedly cleaning for 2-3 times;
2. carrying out hair removal treatment on the deerskin obtained in the step 1, wherein the deerskin cannot be damaged in the process, and then removing residual meat and fat on the inner layer of the deerskin surface;
3. soaking the deerskin obtained in the step 2 in alkaline water (pH is 10-11) for 24 hours,
4. cleaning the deerskin obtained in the step 3 for 2-3 times, adding 2 times of water, and soaking for 24 hours until the deerskin is neutral;
5. cutting the deerskin obtained in the step 4 into small blocks of 15-20 cm;
6. putting the small deerskin blocks obtained in the step 5 into a steaming ball, adding 1.5 times of water, heating to 90-100 ℃ for scalding the deerskin, washing off part of grease, and repeatedly washing for 2-3 times with water;
7. adding 2 times of water into the small pieces of the clean deerskin obtained in the step 6, melting the deerskin for 6 hours under the pressure of 0.15MPa, discharging the glue juice after melting the deerskin, and repeating the melting for 4 times by the same method;
8. mixing the juices, filtering with 100 mesh screen, and filtering with 5 layers of gauze;
9. enabling the glue juice obtained in the step 8 to pass through a grease separator, wherein the flow rate is 80L/h, and the rotating speed is 18000 r/min;
10. heating the glue solution obtained in the step 9 to slightly boil, so that impurities in the glue solution can float on the water surface conveniently, beating out floating foam with foam, and repeating the beating for 10-15 times;
11. continuously concentrating the glue juice obtained in the step 10 until the water content reaches about 35%, adding 300g of fish oil, 8g of yellow wine, 5g of soybean oil and 10g of rock sugar, and uniformly mixing;
12. continuously concentrating the glue juice obtained in the step 11 until the water content reaches 26%, pouring the glue into a glue box, and solidifying for 24 hours at room temperature;
13. transferring the rubber blocks in the step 12 to-10 ℃ for freezing for 30 hours to form rubber lumps;
14. pouring out the glue lumps, cleaning four sides of the glue lumps, cutting the glue lumps into large strips of 4-5 cm, and cutting the large strips into small strips of 10 multiplied by 3 multiplied by 1 cm;
15. transferring the strips cut in the step 14 to a cold glue room with the temperature of 30 ℃ and the relative humidity of 60% for cooling glue for 8 days, and turning over the glue blocks 2 times every day;
16. putting the aired rubber blocks in the step 15 into a wooden box, sealing and sealing the wooden box, taking out the wooden box after 3 days, repeatedly cooling the rubber, and repeating the steps for three times until the rubber blocks are aired until the water content reaches 15%;
17. and (4) sterilizing and packaging the molded rubber block obtained in the step (16).
Example 2
1. Taking 2500g of fresh deerskin, adding 5 times of water (the volume ratio of the added water is the volume ratio) and repeatedly cleaning for 2-3 times;
2. carrying out hair removal treatment on the deerskin obtained in the step 1, wherein the deerskin cannot be damaged in the process, and then removing residual meat and fat on the inner layer of the deerskin surface;
3. soaking the deerskin obtained in the step 2 in alkaline water (pH is 10-11) for 48 hours,
4. cleaning the deerskin obtained in the step 3 for 2-3 times, adding 2 times of water, and soaking for 24 hours until the deerskin is neutral;
5. cutting the deerskin obtained in the step 4 into small blocks of 15-20 cm;
6. putting the small deerskin blocks obtained in the step 5 into a steaming ball, adding 2 times of water, heating to 90-100 ℃ for scalding the deerskin, washing off part of grease, and repeatedly washing for 2-3 times with water;
7. adding 5 times of water into the small pieces of the clean deerskin obtained in the step 6, melting the deerskin for 4 hours under the pressure of 0.2MPa, discharging the glue juice after melting the deerskin, and repeating the melting for 2 times by the same method;
8. mixing the juices, filtering with 140 mesh screen, and filtering with 3 layers of gauze;
9. enabling the glue juice obtained in the step 8 to pass through a grease separator, wherein the flow rate is 120L/h, and the rotating speed is 22000 r/min;
10. heating the glue solution obtained in the step 9 to slightly boil, so that impurities in the glue solution can float on the water surface conveniently, beating out floating foam with foam, and repeating the beating for 10-15 times;
11. continuously concentrating the glue juice obtained in the step 10 until the water content reaches about 45%, adding 100g of fish oil, 5g of yellow wine, 10g of soybean oil and 15g of rock sugar, and uniformly mixing;
12. continuously concentrating the glue juice obtained in the step 11 until the water content reaches 28%, pouring the glue into a glue box, and solidifying for 24 hours at room temperature;
13. transferring the rubber blocks in the step 12 to-15 ℃ for freezing for 20 hours to form rubber lumps;
14. pouring out the glue lumps, cleaning four sides of the glue lumps, cutting the glue lumps into large strips of 4-5 cm, and cutting the large strips into small strips of 10 multiplied by 3 multiplied by 1 cm;
15. transferring the small strips cut in the step 14 to a cold glue room with the temperature of 25 ℃ and the relative humidity of 40% for cooling glue for 6 days, and turning over the glue blocks 2 times every day;
16. putting the aired rubber blocks in the step 15 into a wooden box, sealing and sealing the wooden box, taking out the wooden box after 3 days, repeatedly cooling the rubber, and repeating the steps for three times until the rubber blocks are aired until the water content reaches 14%;
17. and (4) sterilizing and packaging the molded rubber block obtained in the step (16).
Example 3
1. Taking 2300g of fresh deerskin, adding 4 times of water (the volume ratio of the added water is the volume ratio) and repeatedly cleaning for 2-3 times;
2. carrying out hair removal treatment on the deerskin obtained in the step 1, wherein the deerskin cannot be damaged in the process, and then removing residual meat and fat on the inner layer of the deerskin surface;
3. soaking the deerskin obtained in the step 2 in alkaline water (pH is 10-11) for 36 hours,
4. cleaning the deerskin obtained in the step 3 for 2-3 times, adding 2 times of water, and soaking for 24 hours until the deerskin is neutral;
5. cutting the deerskin obtained in the step 4 into small blocks of 15-20 cm;
6. putting the small deerskin blocks obtained in the step 5 into a steaming ball, adding 1.8 times of water, heating to 90-100 ℃ for scalding the deerskin, washing off part of grease, and repeatedly washing for 2-3 times with water;
7. adding 3 times of water into the small pieces of the clean deerskin obtained in the step 6, melting the deerskin for 5 hours under the pressure of 0.17MPa, discharging the glue juice after melting the deerskin, and repeating the melting for 3 times by the same method;
8. mixing the juices, filtering with 120 mesh sieve, and filtering with 4 layers of gauze;
9. passing the glue juice obtained in the step 8 through an oil-fat separator at the flow rate of 100L/h and the rotation speed of 20000 r/min;
10. heating the glue solution obtained in the step 9 to slightly boil, so that impurities in the glue solution can float on the water surface conveniently, beating out floating foam with foam, and repeating the beating for 10-15 times;
11. continuously concentrating the glue juice obtained in the step 10 until the water content reaches about 40%, adding 200g of fish oil, 6g of yellow wine, 7g of soybean oil and 13g of rock sugar, and uniformly mixing;
12. continuously concentrating the glue juice obtained in the step 11 until the water content reaches 27%, pouring the glue into a glue box, and solidifying for 24 hours at room temperature;
13. transferring the rubber blocks in the step 12 to-13 ℃ for freezing for 25 hours to form rubber lumps;
14. pouring out the glue lumps, cleaning four sides of the glue lumps, cutting the glue lumps into large strips of 4-5 cm, and cutting the large strips into small strips of 10 multiplied by 3 multiplied by 1 cm;
15. transferring the small strips cut in the step 14 to a cold glue room with the temperature of 27 ℃ and the relative humidity of 50% for cooling glue for 7 days, and turning over the glue blocks 2 times every day;
16. putting the aired rubber blocks in the step 15 into a wooden box, sealing and sealing the wooden box, taking out the wooden box after 3 days, repeatedly cooling the rubber, and repeating the steps for three times until the rubber blocks are aired until the water content reaches 14.5%;
17. and (4) sterilizing and packaging the molded rubber block obtained in the step (16).
Experimental example 1 deer skin glue functional animal experimental verification
1.1 Experimental animals and groups
1.1.1 animal selection
Rats were used as experimental animals.
1.1.2 animal groups
64 male SPF-grade Wistar rats (purchased from Weitonglihua, Beijing) were used and weighed 270. + -.50 g. Rats were fed and drunk freely, and were randomly divided into 8 groups of 8 rats, i.e., a blank control group (C1), an example 1 group (L1), an example 2 group (L2), an example 3 group (L3), a positive control group (a), a fish oil-free control group (F1), a fish oil control group (F2), a castration control group (C2), and a castrated deer skin gelatin dose group (L0). After adaptive feeding for one week, castration treatment is carried out on the castration control group and the castration deer skin gelatin dosage group to make an animal model. The specific operation is as follows.
Wherein the deer glue prepared in the examples 1-3 is fed in the examples 1-3 respectively, and the preparation method of the fish oil-free control group is the same as that of the example 3, except that fish oil is not added; the fish oil control group was administered only with fish oil, and the deer skin gelatin dose group was fed with deer gelatin prepared in example 3 to castrated rats.
1.2 animal treatment
The castration groups were castrated to create castration animal models. First, a rat was anesthetized with 4% chloral hydrate (0.7ml/100g) by intraperitoneal injection, then, the rat was fixed on an operating table, the abdomen was cut with hair, after conventional sterilization, both testicles were excised through an abdominal incision, and the muscle and skin incisions were sutured in order. After surgery, each rat was given an intramuscular penicillin injection (18000U/(kg. d)) for 7 consecutive days to prevent infection.
1.3 treatment with drug
Seven days after operation, the medicine feeding treatment is carried out for ten days according to the medicine feeding mode shown in the following table.
TABLE 1 Experimental animal drug feeding mode
| Group of | Medicine feeding mode |
| Blank control group | Normally raising |
| EXAMPLE 1 group | Gavage with 0.1 g/(kg. d) deer glue solution |
| EXAMPLE 2 group | Gavage with 0.1 g/(kg. d) deer glue solution |
| EXAMPLE 3 group | Gavage with 0.1 g/(kg. d) deer glue solution |
| Positive control group | 5 mg/(kg. d) testosterone propionate intramuscular injection |
| Control group without fish oil | Gavage with 0.1 g/(kg. d) deer glue solution |
| Fish oil control group | 0.1ml/(kg d) pure shark oil intragastric |
| Castration control group | After castration, feeding normally |
| Castration deer skin gelatin dosage group | After castration, 0.1 g/(kg. d) deer-horn gelatin solution is used for intragastric administration |
1.4 hormone assay
After the treatment was completed, the rats were sacrificed by cervical dislocation. Blood is taken out through heart puncture and placed in a sterilized disposable centrifuge tube, after standing for 30min at room temperature, the centrifuge tube is centrifuged for 10min at 4000r/min in a low-temperature centrifuge, serum is separated, and the content of testosterone and luteinizing hormone is detected by using a full-automatic micro-particle chemiluminescence immunoassay analyzer (Beckman Coulter Access).
2 results of the experiment
2.1 hormone content
Compared with the group C1, the rats in the group C2 were castrated, and the serum testosterone and luteinizing hormone contents were remarkably reduced. After the deer skin glue is taken, compared with the C2 group, the contents of testosterone and luteinizing hormone in serum of the L0 group are obviously improved (p is less than 0.05). The contents of serum testosterone and luteinizing hormone in the L1, L2 and L3 groups are remarkably improved compared with the C1 group (p is less than 0.01). Compared with the group C1, the contents of serum testosterone and luteinizing hormone are also obviously improved in the groups F1 and F2 (p is less than 0.05).
TABLE 2 serum hormone content
*p＜0.05；**p＜0.01。
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.
Claims (9)
1. The deer skin glue is characterized by being prepared from the following raw materials in parts by weight:
2000-2500 parts of deerskin, 100-300 parts of fish oil, 5-8 parts of yellow wine, 5-10 parts of soybean oil and 10-15 parts of rock candy;
the preparation method of the deer skin glue comprises the following steps:
1) cleaning deer skin for depilation, removing residual meat and fat on the inner layer of the skin surface, and soaking in alkaline water;
2) soaking again in clear water and washing the deer skin to remove alkaline water;
3) cutting the deer skin obtained in the step 2), blanching the skin through steam, and cleaning again;
4) adding the deer skin obtained in the step 3) into water, pressurizing and melting the skin to discharge the glue juice;
5) filtering the glue juice obtained in the step 4), separating oil and fat, heating to slightly boil, and removing floating foam floating on the surface layer of the water surface;
6) concentrating the glue juice obtained in the step 5) until the water content reaches 35-45%, adding fish oil, yellow wine, soybean oil and rock candy, mixing uniformly, continuing to concentrate until the water content reaches 26-28%, discharging glue, pouring the glue into a glue box, and solidifying into glue blocks;
7) freezing the rubber block at low temperature to form rubber lumps, cutting the rubber lumps, and drying the rubber lumps;
8) sealing and sealing the aired rubber blocks for sealing, taking out after 2-4 days, and repeatedly cooling the rubber blocks according to the method in the step 7); repeating the operation until the water content of the rubber block reaches 14-15%; sterilizing, and packaging.
2. The deerskin glue according to claim 1, characterized by being prepared from the following raw materials in parts by weight:
2200-2300 parts of deerskin, 150-250 parts of fish oil, 6-7 parts of yellow wine, 7-8 parts of soybean oil and 10-15 parts of rock candy.
3. Deerskin glue according to claim 1 or 2, characterized in that said fish oil is shark oil.
4. The deer skin glue according to claim 1, wherein in step 1), the alkali water soaking is to be specifically soaking in alkali water with a pH of 10-11 for 24-48 hours.
5. The deer-hide glue of claim 1, wherein step 4) specifically comprises: adding the deerskin obtained in the step 3) into water with the volume 2-5 times of that of the deerskin, melting the deerskin for 4-6 hours under the pressure of 0.15-0.2 MPa, and repeating melting for 2-4 times by the same method.
6. The deer skin glue according to claim 1, wherein in step 5), the glue juice filtration specifically comprises:
filtering the glue juice by a screen with 100-140 meshes, and then filtering by 3-5 layers of gauze.
7. The deerskin glue according to claim 1, wherein in step 5), the specific parameters of oil separation are as follows: the obtained glue juice passes through an oil-fat separator, the flow rate is 80L/h-120L/h, and the rotating speed is 18000 r/min-22000 r/min.
8. The deer skin glue according to claim 1, wherein in the step 7), the low-temperature freezing condition is-10 ℃ to-15 ℃ for 20h to 30 h.
9. The deer-hide glue of claim 1, wherein in step 7), the glue cooling conditions are as follows:
and cooling the glue in the glue cooling room for 6-8 days at the temperature of 25-30 ℃ and the relative humidity of 40-60%.
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| CN107712881A (en) * | 2017-11-22 | 2018-02-23 | 吉林海王健康生物科技有限公司 | A kind of preparation method of deerskin glue |
| CN109091527A (en) * | 2018-08-22 | 2018-12-28 | 宋子刚 | The Traditional Chinese medicinal prescription and preparation method of one deer horn glue |
| CN109078024B (en) * | 2018-10-25 | 2020-09-29 | 贵州广济堂药业有限公司 | Preparation method of deer glue as traditional Chinese medicine decoction pieces |
| CN111358008A (en) * | 2019-04-18 | 2020-07-03 | 吉林省东鳌鹿业科技开发有限公司 | Dried fruit deer-horn gelatin cake and preparation method thereof |
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Application publication date: 20171010 Assignee: Shenzhen Xihan health Co.,Ltd. Assignor: INSTITUTE OF SPECIAL ANIMAL AND PLANT SCIENCES OF CAAS Contract record no.: X2023980032542 Denomination of invention: A deerskin glue and its preparation method Granted publication date: 20200811 License type: Common License Record date: 20230227 |
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