CN107208358A - Multipurpose functional sanitary napkin and manufacture method - Google Patents
Multipurpose functional sanitary napkin and manufacture method Download PDFInfo
- Publication number
- CN107208358A CN107208358A CN201580068631.XA CN201580068631A CN107208358A CN 107208358 A CN107208358 A CN 107208358A CN 201580068631 A CN201580068631 A CN 201580068631A CN 107208358 A CN107208358 A CN 107208358A
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- cotton
- sanitary napkin
- weight
- functional sanitary
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- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
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- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
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- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
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- D06M11/81—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron; with boron halides; with fluoroborates
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
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- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2503/00—Domestic or personal
- D10B2503/02—Curtains
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2503/00—Domestic or personal
- D10B2503/04—Floor or wall coverings; Carpets
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2509/00—Medical; Hygiene
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
The present invention provides a kind of multipurpose functional sanitary napkin, more specifically, it is related to natural cotton, multipurpose feature mixing cotton and includes urea (UREA) aqueous solution, oleic acid (OLEIC ACID), diethylenetriamines (DETA), APP (APP), boron (B2O3), aqueous Polyoxyethylene este (PUD), bleeding agent (anion), Nano Silver (NANO SILVER), nano titanium oxide (NANO TIO2) multipurpose functional sanitary napkin manufacture composition multipurpose functional sanitary napkin and manufacture method.
Description
Technical field
The present invention relates to a kind of multipurpose functional sanitary napkin and manufacture method.
Background technology
As the multipurpose feature cotton of existing exploitation, the anti-flammability such as natural cotton (cotton) and natural numb cotton is fragile, also,
While oxidation in atmosphere, cotton itself can produce micronic dust, therefore the reason for fine dust offer fire.
Also, existing cotton wool easily produces by force mould and bacterium, taste, acarid due to hygroscopicity so that be only used on bed
It cannot be used for category or clothes in multi industries field.
In order to improve the shortcoming, in granted patent (grant number 10-1079871) multipurpose feature cotton and manufacturer
Method is mixed with the multipurpose feature of the composite fibre in the improvement invention of granted patent (application number 10-2013-0141631)
Cotton and manufacture method are in order to improve the problem of natural cotton produces fine dust and dust with bast fibre spinning by the easy breakage of impact, natural
The inner chamber infiltration multipurpose feature cotton of cotton, which is made, uses composition so that improves tension intensity and rupture strength, utilizes phosphoric acid nitrile
Synthetic fibre coupling agent strengthens cotton, and addition provides flexibility by the combination thing liquid of anion interfacial agent.
The content of the invention
The technical problem to be solved
The present invention be in view of the problems and propose, its object is to there is provided a kind of improved multipurpose function
The fire retardant of sex hygiene cotton, can be prevented due to the problem of by paragraph dust occurs for cotton block, also will not be damaged in the impact of strength, be made
Dust will not be occurred by obtaining, because cotton is soft and smooth so that greatly improve workability and productivity.Will not occur electrostatic phenomenon,
Even if the state being also not damaged before being restored to washing is washed with water, so that, it is very environmentally friendly.
Also, flexibility, touch sense, heat insulating ability and restoring force are outstanding, defended even if filling multipurpose feature in quilt
The state of raw cotton, which carries out sewing operation cotton, damaged to produce fine dust and dust, so that, operating environment comfortably improves production
Property greatly improves effect.
And suppress to add feature by the mould and bacterium of moisture absorption sexual reproduction, taste, acarid injection Nano Silver with
Nano titanium oxide carries out dual antibiotic property, bactericidal properties, sterilization type, antimite, removes taste, prevents electrostatic, also, due to
Material on Nano Silver and fire-retardant powder etc. are paid on cotton, therefore, even if occurring fine dust and powder also can be with fibre
Dimension state occurs on a small quantity so that even if being drawn into the skin or respiratory system of human body to nose or organ also being safe from harm property.And
And, Nano Silver or nano titanium oxide are crystalline texture, therefore, will not be separated with cotton, even if separation also can be damaged together with cotton,
Therefore, problem will not be turned into.
Also, day is penetrated into according to the harmless functional composition of the multipurpose functional sanitary napkin of the present invention
Right cotton, mixing cotton, straw cotton, wheat straw cotton, waste paper cotton, natural numb cotton, cocoanut fiber cotton, silk cotton, chemical cotton, bamboo fiber
Cotton, banana fiber cotton, waste cotton regeneration cotton, synthetic fibers cotton, paper pulp cotton, carbon fiber cotton, tencel, artificial silk flosssilk wadding, cuprammonium are artificial
Silk, in the tissue of low melting point thermoplastic resin so that improve the heat insulating ability of natural cotton, natural numb cotton, mixing cotton etc., cold insulation,
Thermal insulation, heat accumulation, tension intensity, rupture strength etc., moreover it is possible to permeate the Nano Silver for penetrating into inner chamber with nano titanium oxide
To inner cavity so that even if a small amount of can also increase surface area to greatest extent, the nano-particle of aggregation one by one constitutes non-
Often small air space (Fig. 2), so as to possess multi-effect and function.
Also, anti-flammability and the intensity of cotton block are improved, and the oxidation of cotton can be prevented.And possess moisture resistance, insect prevention, resist
It is bacterium, bactericidal properties, sterilising.Also, producing cost is cheap, environmental protection can be with former material after again being reclaimed using the waste materials finished
Expect to use.According to the multipurpose functional sanitary napkin of the present invention penetrate into line, rope, processing weave cotton cloth, it is non-woven fabrics, mat, quick-fried
Broken pad, sheet material, panel core, pipe sleeve, filter, flameproof fabric, resist printing wallpaper, fire prevention curtain, resist printing carpet, natural cotton, mixing
Cotton, straw cotton, wheat straw cotton, waste paper cotton, natural numb cotton, cocoanut fiber cotton, silk cotton, chemical cotton, bamboo fiber cotton, banana fiber
Cotton, waste cotton regeneration cotton, synthetic fibers cotton, paper pulp cotton, carbon fiber cotton, tencel, artificial silk flosssilk wadding, cuprammonium rayon cotton, low melting point
In the tissue such as thermoplastic resin fibre cotton, kapok so that be utilized in fiber structures such as natural cotton, natural numb cotton, mixing cottons
It is that material etc. is utilized in multi industries field.
Line or processing fabric are turned to using according to the multipurpose functional sanitary napkin product of the present invention, also, common
The functional composition of multipurpose functional sanitary napkin is permeated in bafta, cotton blended fabric etc., so as to not only possess flame-retarded
Health product can also be manufactured.
Technical scheme
The present invention provide include urea (UREA), it is oleic acid (OLEIC ACID), diethylenetriamines (DETA), water, poly-
Ammonium phosphate (APP), boron (B2O3), aqueous Polyoxyethylene este (PUD), bleeding agent (anion), Nano Silver (NANO SILVER), nanometer
Titanium dioxide (NANO TIO2) multipurpose functional sanitary napkin manufacture composition.
According to the aspect of the present invention, it is characterised in that the urea (UREA) comprising 5.1 to 5.35 weight %.
According to other aspects of the present invention, it is characterised in that include 0.11 to the 0.18 weight % oleic acid
(OLEIC ACID)。
According to the present invention other another aspects, it is characterised in that the diethylenetriamines (DETA) be 0.13 to
0.18 weight %.
According to another aspect of the present invention, it is characterised in that include 12.1 to the 12.20 weight % APP
(APP)。
According to other another aspects of the present invention, it is characterised in that include 1.62 to the 1.70 weight % boron
(B2O3)。
According to other another aspects of the present invention, it is characterised in that include the described aqueous of 0.25 to 0.32 weight %
Polyoxyethylene este (PUD).
According to other another aspects of the present invention, it is characterised in that include 0.11 to the 0.18 weight % infiltration
Agent (Alkyl Succinate anions).
According to other aspects of the present invention, it is characterised in that include 2.30 to the 2.48 weight % Nano Silver
(NANO SILVER)。
According to other aspects of the present invention, it is characterised in that Nano Silver (NANO SILVER) solution is with PH6
To 8, the acicular texture of 5~10nm size is difficult to depart from when penetrating into cotton, and will not change colour.
According to other aspects of the present invention, it is characterised in that include 1.5 to the 1.60 weight % nanometer titanium dioxide
Titanium (NANO TIO2)。
According to other aspects of the present invention, it is characterised in that in the nano titanium oxide (NANO TIO2) surface
Coating silver (Silver) is used.
Also, the present invention provides the manufacturer of the multipurpose functional sanitary napkin manufacture composition comprised the following steps
Method.
E) the step of manufacturing lysate after oleic acid, diethylenetriamines, addition water is added in aqueous solution of urea;
F) the step of dissolving APP and boron in the lysate
G) add and made after aqueous Polyoxyethylene este, bleeding agent, Nano Silver, nano titanium oxide in the lysate of the b) step
The step of making composition;And
H) the step of being dissolved after the composition is stirred ten minutes to 30 minutes;
According to the aspect of the present invention, the lysate of a) step is that 2 minutes are stirred at a temperature of 70 to 120 DEG C extremely
Heated after 3 minutes.
According to other aspects of the present invention, it is characterised in that further comprise completing cooling down 30 after the d) step
Minute a to hour.
Also, the present invention provides the multipurpose functional sanitary napkin manufactured using the composition.
According to the present invention an aspect, it is characterised in that the multipurpose functional sanitary napkin be used for by line, rope,
Processing is weaved cotton cloth, non-woven fabrics, mat, blasting mat, sheet material, panel core, pipe sleeve, filter, flameproof fabric, resist printing wallpaper, fire window
The manufacture of the material selected in the group that curtain, resist printing carpet are constituted.
According to other aspects of the present invention, it is characterised in that the multipurpose functional sanitary napkin is used for by anti-flammability
Material, anti-metachromia material, heat insulating ability material, cold insulation material, heat-barrier material, sound-absorbing material, soundproof material, absorb impact material,
Interlayer acoustic material, heating floor material, vacuum heat insulation material, ornament materials, safety, hygienic material, explosion bullet resistant material, day
The manufacture of the material selected in the group that card material, finishing material, clothing materials, bedding class material are constituted.
Also, the present invention provides the manufacture method of the multipurpose functional sanitary napkin comprised the following steps.
In natural cotton the step of the composition of hydraulic pressure jet penetration claim 1;
Dehydration infiltration has after the natural cotton of the composition, dry step;
The step of by the cotton bullet cotton;
The aspect of the present invention is, it is characterised in that the injection of the hydraulic pressure of a) step is performed ten seconds to 30 seconds
Clock.
Other aspects of the present invention are that the dehydration of (b) step is to utilize extruding (Mangle) dewaterer so that will
The moisture of cotton is dehydrated to 70 to 80%.
Other another aspects of the present invention are that the drying of (b) step is to utilize air drier by the aqueous of cotton
Rate drying is to 13% to 15%..
Also, the present invention is as the mixing cotton comprising the cotton wool, and the mixing cotton is with 1 in the cotton wool:9 to
4:6 weight are than mixing by natural cotton, the miscellaneous cotton of mixing, straw cotton, wheat straw cotton, waste paper cotton, natural numb cotton, cocoanut fiber cotton, silk
Cotton, chemical cotton, bamboo fiber cotton, banana fiber cotton, waste cotton regeneration cotton, synthetic fibers cotton, paper pulp cotton, carbon fiber cotton, tencel,
The more than one cotton selected in the group that artificial silk flosssilk wadding, cuprammonium rayon, low melting point thermoplastic resin fibre cotton are constituted.
Also, the present invention, which is provided, to permeate the composition and is immersed on bafta, cotton blended fabric or cotton face fabric
The functional sanitary fabric of manufacture.
Beneficial effect
Manufactured using the fire retardant of the improved multipurpose functional sanitary napkin according to the present invention during feature cotton, will not
Occur because of the phenomenon that dust occurs for cotton block paragraph, even if also will not be damaged by the impact of strength, so as to will not occur asking for dust
Topic.
Also, due to soft and smooth so that significantly improve workability and productivity, will not occur electrostatic phenomenon, i.e.,
Just cotton will not also be damaged by being washed with water, and can be restored to the state before washing, it is thus possible to reused after washing, therefore,
It is very environmentally friendly.
Also, cotton flexibility, touch sense, heat insulating ability and restoring force made according to the method for the present invention is remarkably, in quilt
In filling multipurpose functional sanitary napkin state carry out sewing operation also will not damaged cotton so that will not produce fine dust and
Dust, so that, operating environment comfortably improves productivity and greatly improves effect.
And suppress to add feature by the mould and bacterium of moisture absorption sexual reproduction, taste, acarid, injection Nano Silver with
Nano titanium oxide carries out dual antibiotic property, bactericidal properties, sterilization type, antimite, removes taste, prevents electrostatic, also, due to
Material on Nano Silver and fire-retardant powder etc. are paid on cotton, therefore, even if occurring fine dust and powder also can be with fibre
Dimension state occurs on a small quantity so that even if being drawn into the skin or respiratory system of human body to nose or being safe from harm property of bronchus.And
And, Nano Silver or nano titanium oxide are crystalline texture, therefore, will not be separated with cotton, even if separation also can be damaged together with cotton,
Therefore, problem will not be turned into.
Brief description of the drawings
Fig. 1 is the engineering drawing of the manufacture method of the multipurpose functional sanitary napkin according to the present invention.
Fig. 2 is the composition impregnation process for showing natural cotton (cotton) being immersed in the functional sanitary napkin according to the present invention
Cotton inner chamber front and rear figure.
Fig. 3 is the experiment grade book of the result for the antibacterial degree for testing comparative example.
Fig. 4 is the experiment grade of the experimental result for the antibacterial degree for showing the multipurpose functional sanitary napkin according to the present invention
Book.
Fig. 5 is the experiment grade book of the experimental result of the anti-metachromia of the multipurpose functional sanitary napkin according to the present invention.
Fig. 6 be show using multipurpose functional sanitary napkin and the cotton wool according to the present invention as material respectively with natural fiber crops
Mix after cotton, carbonization mixing cotton mixing with the roasting 30 seconds lab diagram of blowtorch.
Fig. 7 is the reality for baking the multipurpose functional sanitary napkin according to the present invention with blowtorch as the non-woven fabrics that material is made
Test figure.
Fig. 8 is the experiment grade book of the experimental result of the tension intensity, rupture strength, cold resistance that show comparative example.
Fig. 9 is tension intensity, the experimental result of rupture strength for showing the multipurpose functional sanitary napkin according to the present invention
Experiment grade book.
Figure 10 be show according to the present invention multipurpose functional sanitary napkin washing fastness experimental result experiment into
Achievement book.
Figure 11 is the experiment grade of the experimental result for the cold resistance for showing the multipurpose functional sanitary napkin according to the present invention
Book.
Figure 12 is the experiment grade of the experimental result for the insulation rate for showing the multipurpose functional sanitary napkin according to the present invention
Book.
Figure 13 is the bedding class figure for showing to be made with the material of the multipurpose functional sanitary napkin according to the present invention.
Embodiment
The present invention is to be related to multipurpose functional sanitary napkin, more specifically, is related to the applicant and (is authorized in prior art
Patent the 10-1079871st) improvement " multipurpose feature cotton and manufacture method " invention.The prior art it is multi-purpose
The natural cotton of way feature cotton be will not be produced while heat insulating ability, thermal insulation, ultralow warm nature, sound absorption properties are outstanding harmful components with
Trigger environmental hazard.The multipurpose feature cotton and manufacture method of the present invention is to improve multipurpose function in the prior art described
Property mixing cotton, therefore, with the addition of feature, improve fire-retardant (resist printing) physical property and relatively sanitary and comfortable multipurpose function is provided
Sex hygiene cotton.
The multipurpose feature cotton of the granted patent is 20~25 weight % of addition in the weight % of ammonia spirit 100
After ammonium dihydrogen phosphate, at a temperature of 50~70 DEG C after stirring 2~3 minutes, 0.1~0.3 weight is added in the solution of dissolving
Measure % anion interfacial agent, 1.5~3.2 weight % fluoro water proofing agent, 0.5~2.5 weight % acrylic coupling
Stir 10~30 minutes after agent to obtain the composition (fire-retardant, anti-dye liquor) that multipurpose feature cotton is made, by said composition
Dipping and containing being immersed in natural cotton.The weight ratio of natural cotton and composition (fire-retardant, anti-dye liquor) is turned into 5:1 to 5:1 is impregnated with after 3
~2 minutes, it was 70~80% to be then dehydrated to moisture content, after being dried with dielectric dryer less than 15 weight %, plays and is manufactured after cotton
Multipurpose feature cotton.
That is, the present invention is that as improved composition (fire-retardant, anti-dye liquor), there is provided include urea using the composition
(UREA), oleic acid (OLEIC ACID), diethylenetriamines (DETA), water, APP (APP), boron (B2O3), aqueous polyoxy
Ester (PUD), bleeding agent (anion), Nano Silver (NANO SILVER), nano titanium oxide (NANO TIO2) multipurpose
Functional sanitary napkin manufacture composition.
According to the aspect of the present invention, the composition includes 5.1 to 5.35 weight % urea, 0.11 to 0.18 weight
Measure % oleic acid, 0.13 to 0.18 weight % diethylenetriamines, 12.1 to 12.20 weight % APP (APP),
1.62 to 1.70 weight % boron (B2O3), 0.25 to 0.32 weight % aqueous Polyoxyethylene este (PUD), 0.11 to 0.18 weight %
Bleeding agent (anion), 2.30 to 2.48 weight % Nano Silver, 1.5 to 1.60 weight % nano titanium oxide
(NANO TIO2) and include remaining water.
Nano Silver (NANO SILVER) solution be pH6 to 8, if being entered with the acicular texture of 5 to 10nm size
In cotton, then it is difficult to depart from, and will not change colour.
Also, the present invention provides the manufacturer of the multipurpose functional sanitary napkin manufacture composition comprised the steps of
Method.
A) added in aqueous solution of urea after oleic acid, diethylenetriamines, the step of addition water is to manufacture lysate;
B) the step of dissolving APP and boron in the lysate;
C) add and made after aqueous Polyoxyethylene este, bleeding agent, Nano Silver, nano titanium oxide in the aqueous solution of the b) step
The step of making composition;And
D) the step of being dissolved after the composition is stirred ten minutes to 30 minutes;
That is, the manufacture method of composition of the invention includes 5.1 to 5.35 weight % of addition urea, 0.11 to 0.18 weight
Measure % oleic acid, 0.13 to 0.18 weight % diethylenetriamines, 72.5 to 77.15 weight % water, at 70 to 120 DEG C
At a temperature of stirring 2 to 3 minutes after carry out heating response the step of.
Carry out after the agitating and heating reaction, add 12.1 to 12.20 weight % APP, 1.62 to 1.70 weights
Measure and dissolved after % boron.Then, the aqueous weight of Polyoxyethylene este 0.25 to 0.32 % of addition, 0.11 to 0.18 weight % bleeding agent,
2.30 to 2.48 weight % Nano Silver (NANO SILVER), 1.5 to 1.60 weight % nano titanium oxide (NANO
TIO2) after, stirring and dissolving completes composition after 10 to 30 minutes.
Also, the present invention provides many thorough fare functional sanitary napkins manufactured using the composition.
As one embodiment of the invention, the multipurpose functional sanitary napkin can make line, rope, processing weave cotton cloth, nothing
Spin cloth, mat, blasting mat, sheet material, panel core, pipe sleeve, filter, flameproof fabric, resist printing wallpaper, fire prevention curtain, resist printing carpet
Material.
According to other embodiments of the invention, the multipurpose functional sanitary napkin is used for by flame-retardant materials, anti-metachromia
Material, heat insulating ability material, cold insulation material, heat-barrier material, sound-absorbing material, soundproof material, absorption impact material, interlayer sound insulation material
Material, heating floor material, vacuum heat insulation material, ornament materials, safety, hygienic material, explosion bullet resistant material, ceiling tile materials,
The manufacture of the material selected in the group that finishing material, clothing materials, bedding class material are constituted.
Also, the present invention provides the manufacture method of the multipurpose functional sanitary napkin comprised the following steps.
A) in natural cotton the step of the composition of hydraulic pressure jet penetration claim 1;
B) dehydration infiltration has after the natural cotton of the composition, dry step;And
C) by cotton bullet cotton the step of;
That is, further comprise that (a) is multi-purpose using hydraulic pressure jet penetration method infiltration fire resistant fluid (resist printing) manufacture in the cotton class
The step of way functional sanitary napkin;(b) by the cotton be dehydrated and dry step and play cotton described in cotton the step of;(c) using crowded
The step of (MANGLE) dewaterer is dehydrated the cotton is pressed, the step of drying the cotton using air drier.
The hydraulic pressure injection is to be preferably carried out 10 to 30 seconds, and the dehydration is taken off using extruding (Mangle) dewaterer
Water to cotton moisture be 70 to 80%, the drying be using air drier drying to cotton sweat rate for 13% to
15%.
According to the aspect of the present invention, the weight ratio of the natural cotton and the composition is 5:1 to 5:3.Also, institute
State multipurpose functional sanitary napkin be used for line, rope, processing weave cotton cloth, fabric, non-woven fabrics, mat, panel core, sheet material, fire prevention
Cloth, resist printing wallpaper, fire prevention curtain, resist printing carpet, pipe sleeve.The manufacture of filter material, also, for include flame-retardant materials,
Anti- metachromia material, heat insulating ability material, cold insulation material, heat-barrier material, sound-absorbing material, soundproof material, absorb impact material, interlayer every
Sound material, heating floor material, vacuum heat insulation material, ornament materials, safety, hygienic material, explosion bullet resistant material, smallpox sheet material
Material, finishing material, clothing materials, the manufacture of bedding class material, also, natural ginseng fiber is to contain having hemp, Huang
Fiber crops, flax, mestha, the manufacture of the material of the natural ginseng mixing cotton of ramie.
And there is provided the mixing cotton of the cotton wool comprising the present invention.The mixing cotton is used by natural cotton, mixing cotton, rice
It is cotton, wheat straw cotton, waste paper cotton, natural numb cotton, cocoanut fiber cotton, silk cotton, chemical cotton, bamboo fiber cotton, banana fiber cotton, useless
Cotton regeneration cotton, synthetic fibers cotton, paper pulp cotton, carbon fiber cotton, tencel, artificial silk flosssilk wadding, cuprammonium rayon, low melting point thermoplastic resin
The more than one cotton selected in the group that fat cellucotton and kapok are constituted is with the multipurpose manufactured in the present invention feature is defended
Raw cotton is with 1:9 to 4:6 weight rate mixes to manufacture.Preferably with 2:8 to 3:7 weight rate is used.
Meanwhile, the present invention is provided to permeate and be immersed in bafta, cotton blend sanitary cotton manufacture composition and knitted
The functional sanitary fabric manufactured on thing or cotton face fabric.The cotton wool manufacture is not only cotton, bafta, cotton with composition and mixed
Yarn fabric or cotton face fabric are readily applicable in any material of textile material.
In the present invention, oleic acid (OLEIC ACID) by olive oil, camellia oil etc. grease type principal component unsaturated lipid
Fat acid is constituted.Also, with softening agent for fibres aggregation cotton block cause cotton block will not paragraph can also prevent breakage so that it is strong to improve pulling force
Degree, rupture strength.
Also, in the present invention, urea ((NH2)2CO it is) strong basicity, therefore, if being dissolved in water, forms a lot
AMIN ions, when occurring fire, occur ammonia to play the fiery function that disappears.Also, it is also to possess the ability of suppressing growth of microorganism
Make cotton more soft while antimicrobial.
Also, cotton is become soft and smooth as the diethylenetriamines (DETA) of softening agent, and it is tough to possess cotton
Degree so that also will not be damaged by any impact.Also, the restoring force of cotton is strong.And bounce and elastic, durability are improved,
Shrinkage factor is reduced with improving binding function.
APP has the effect of the scattered medicine of safety, and has the effect for preventing gel and forming crystallization, flame retardant
The function that matter (resist printing) prevents from separating out as crystallization.And PH change is prevented, when promoting carbonization fire-retardant (resist printing), phosphoric acid is generated
Acid amides, and with raising dehydration, the anti-flammability of the efficiency of carbon.
Boron (B2O3) it is not only there is sterilization, desinsection, anti-corrosion function also to have fire prevention and the fiery function that disappears, moreover it is possible to strengthen cotton block.
The water proofing property of aqueous Polyoxyethylene este, washing fastness, heat resistance, least etc. are outstanding, and coating is very soft in natural cotton
Soft and touch is felt.Do not repel stickup property with a variety of medicines good.Milky anion PH is 8~10 or so and easily molten
In Xie Shui.Bleeding agent is the transparent liquid anion of ecru, is an alkyl succinic acid (ALKYL SUCCINATE).Very
Natural cotton is penetrated into the short time, so that, anti-flammability (resist printing) and drenching property are good.
Nano Silver has the effect more improved according to Nano Silver technology, especially, and silver has outstanding under nm regime
Sterilizing ability, therefore, minimum Nano Silver have the bactericidal action of very strength.Also, silver-colored composition not only improve sterilizing power with
Antimicrbial power can also remove taste, electromagnetic wave, cut-out ultraviolet, far infrared and anion, release silver particles etc. in extensive model
It is antibiotics to enclose interior use.Natural cotton is due to hygroscopicity, therefore, occur mould and bacterium, taste, acarid.Injection is received
Meter Yin Hou can prevent bacterium infection by sterilizing power and antimicrbial power and remove taste so that contribute to health and health.Nano Silver
Structure be needle-like, therefore, pay and be not easily disconnected from the inside of the inner chamber of multipurpose functional sanitary napkin, size is 5~10nm,
So as to improve surface area to greatest extent.The injection rate of Nano silver solution is 10 to 30ppm.
The photochemical catalyst of nano titanium oxide is that as catalyst the TiO 2 particles of nanosized are done into self purification
With the material of super hydrophilic effect.If as photochemical catalyst titanium dioxide by ultraviolets such as sunshine fluorescence, producing electronics e-With
Hole h', wherein hole h' are to form the hydroxide (OH RADICAL) of the oxidation with strength there is sterilization to imitate
Really.Electronics is that the oxygen adsorbed in photochemical catalyst is generated as into oxonium ion (O2-), the oxonium ion is added as reflection active material
To oxidation reaction intermediate so that with the effect for removing taste and decomposing organic matter.Especially, current construction and decoration material can be solved
Material and construction after occur new home syndrome, organic compound VOCSThe radon gas produced in problem or concrete, cement
(Rn-222)。
Gas occurs while radon gas voluntarily collapses.The gas is penetrated as alpha ray as a kind of radioactive ray than common X
Line, gamma-rays are dangerous 20 times, more dangerous five times than β ray.The reason for these turn into new home syndrome.Radon gas is used as colorless and odorless
The species that the gas in road triggers the one-level carcinogen of lung cancer to release radon gas has plasterboard, concrete, cement, sand, stone, soil
Earth, stone material, rock etc. occur from construction material.Cotton material or pad are made in order to remove radon gas multipurpose functional sanitary napkin
New home syndrome, radon gas etc. can be relaxed when being used as ceiling tile materials, wall decorations material after son, plate to construct.Nano-silica
If the shortcoming for changing titanium is to irradiate without visible rays or fluorescence etc., effect is very insignificant.Due to transmission light or
The place of fluorescence has effect, therefore, if multipurpose functional sanitary napkin is arranged at into curtain, chair, wall as material
Deng interior, then effect is very good.Due to can be produced multipurpose functional sanitary napkin as material in multi industries field
Product, therefore, the effect using the photochemical catalyst of titanium dioxide are used for cotton wool.So as to the industry beyond the building such as house
With not limited in purposes.And apply for a patent (application number the 10-2013-0141631st) disclose multipurpose feature mix
Close cotton and multi-functional functional sanitary napkin and manufacture method comprising composition.
The sanitary cotton manufactured by methods described is more special with invention than patent of invention (grant number the 10-1079871st)
The cotton of sharp (application number the 10-2013-0141634th) greatly improves insulation rate, tension intensity, rupture strength, anti-metachromia, washable
Washing property, antibacterial degree, radon gas, roasting experimental result, are an ideal cottons not broken up.Also, energy more than 99.9% is effectively
Ground prevents bacterial growth, acarid etc., so that antibiotic property is very outstanding.
Also, relax and remove organic compound, radon gas, ammonia, acetaldehyde, hydrogen sulfide, nitrogen oxides of new home syndrome etc.,
Make it possible to it is pre- it is hypo-allergenic, de-taste, taste removal, cut-out electromagnetic wave, ultraviolet and release silver particles, anion.Especially, significantly change
Kind washing fastness so that quilt can be washed, so that the washable natural cotton cotton wool who can be used.
Meanwhile, greatly reduce volume slip caused by external pressure, it is ensured that dimensional stability so that easy construction, after construction
Will not occur defect, it is lighter and handier than other materials, the cotton wool with multi-effect is used on the various buildings such as house, from
And the energy and reduction carbon are saved, it also can widely be used in train, automobile, household appliances, shipbuilding, aerospace, hospital or state
The anti-multipurpose functional sanitary napkin waited in multi industries field.
Hereinafter, in order that the definitely offer preferred embodiment and experimental example of the present invention.But, following embodiment and reality
Example is tested only for making the present invention definitely, present disclosure is not limited by following examples and experimental example.
Embodiment 1:The manufacture of the multipurpose functional sanitary napkin of the present invention
It is in the weight % of urea 5.33 with the sample of composition to manufacture multipurpose functional sanitary napkin manufacture of the invention
The weight % of water 76.14 is added after adding the weight % of oleic acid 0.15, addition diethylenetriamines 0.15 weight %, at 70 to 120 DEG C
After stirring 2 to 3 minutes, 30 minutes to 1 hours are cooled down.Then after addition APP 12.18 weight %, the weight % of boron 1.68
Dissolving.
After dissolving, aqueous the weight % of Polyoxyethylene este 0.30, the weight % of bleeding agent 0.15 and the weight % of Nano Silver 2.40 are added,
After the weight % of nano titanium oxide 1.52, stirring and dissolving 10 to 30 minutes obtains composition, impregnates natural in said composition
After cotton, ten minutes osmotic composition liquid, it is 70~80% to be then dehydrated with extruding-desiccation machine to moisture, dry with air drier
Dry moisture content is 13%~15%, so as to manufacture non-woven fabrics.Fig. 1 shows the engineering.Also, Fig. 2 shows to permeate the combination
Structure after thing.
Embodiment 2:The contrast of comparative example and the antibacterial degree of multipurpose functional sanitary napkin of the present invention
Perform comparative examples and the experiment of the antibacterial degree of the multipurpose functional sanitary napkin according to the present invention.
Test the antibacterial degree KSK0693 of comparative example and cotton wool of the present invention:2011 result, the slime mould slip of comparative example
It is staphylococcus aureus 70%, pneumococcus 54.4%, the multipurpose functional sanitary napkin of present invention is golden yellow Portugal
Grape coccus 99.9%, pneumococcus 99.9%.Therefore, very outstanding (Fig. 3, Fig. 4) of antibacterial degree
Table 1【Table 1】
Experimental bacteria | Comparative example | Multipurpose functional sanitary napkin of the present invention |
Staphylococcus aureus | 70% | 99.90% |
Pneumococcus | 54.40% | 99.90% |
Embodiment 3:Comparative example and anti-flammability (resist printing) experimental result of the multipurpose functional sanitary napkin of the present invention
Fig. 2 shows to be set according to fire fighting device and the law experiment benchmarks comparative example and the present invention of safety management are hygienic
The result of the anti-flammability (resist printing) of cotton.
Table 2【Table 2】
Distinguish | Test benchmark | Comparative example | Multipurpose functional sanitary napkin of the present invention |
After flame time (S) | Within 10 (S) | ○ | ○ |
Persistence (S) | Within 30 (S) | ○ | ○ |
Be carbonized area () | 50(cm2) within | 39.6 | 27.6 |
Char length | Within 20 (cm) | 8.2 | 7.5 |
Judge | - | It is qualified | It is qualified |
As shown in table 2, the carbonization area of the multipurpose functional sanitary napkin manufactured in the present invention is 27.6cm2Char length
It is that 7.5cm is 39.6cm than the carbonization area of multipurpose feature cotton2, char length is that 8.2cm has outstanding achievement,
So as to which it is qualified to be determined in anti-flammability experiment.(Fig. 5)
Also, Fig. 6 is to show the multipurpose functional sanitary napkin and multipurpose functional sanitary with the roasting present invention of blowtorch
The natural fiber crops mixing cotton that cotton mixes respectively, result of the carbonization mixing cotton after 30 seconds, multipurpose functional sanitary napkin is tested
The surface area for the mixing cotton that body is mixed with multipurpose functional sanitary napkin as material is all carbonized, so as to find out three species
All there is outstanding fire-retardant (resist printing) property.Also, the non-woven fabrics that is made of multi-functional functional sanitary napkin, weave cotton cloth also that it is outstanding all to have
Fire-retardant (resist printing) property (Fig. 7).
Embodiment 4:Comparative example and the tension intensity of multipurpose functional sanitary napkin of the present invention are contrasted
Comparative example is according to KS K0521:2006, C, R, E determine tension intensity, and cotton wool of the invention is according to KS
K0521:2011 (hold distance:200mm, draw speed:100mm/min) make comparisons.Result is shown respectively in Fig. 8 and Fig. 9.
As shown in table 3, comparative example is with (7.3) N/5cm (kgf/5cm) amplitudes (direction of tensile strength length (direction 1) 71
2) 149 (15.2) N/5cm (kgf/5cm) are determined, according to the tensile strength length of the multipurpose functional sanitary napkin of the present invention
(direction 1) 71N/5cm (kgf/5cm), amplitude (direction 2) 300N/5cm (kgf/5cm) are determined so that from twocouese (length,
Amplitude) complete equilibrium can find out the support force of multipurpose functional sanitary napkin by equalization so that tensile force is by very strong
Change.
Table 3【Table 3】
Embodiment 5:Comparative example is compared with the rupture strength of the multipurpose functional sanitary napkin of the present invention
Comparative example is with multipurpose functional sanitary napkin of the invention according to KSK0351:2006 compare multipurpose feature cotton
With the rupture strength (Fig. 8, Fig. 9) of multipurpose functional sanitary napkin.
Comparative example is according to KSK0351:2006 determine tensile strength, and cotton wool of the invention is according to KSKISO13938-1:
2011 (experiment area 7.3cm2) compare.Fig. 8 and Fig. 9 show result.
As shown in table 4, comparative example is determined with 1059.1KPa, and multipurpose functional sanitary napkin is determined with 4929KPa,
It can find out that the rupture strength of multipurpose functional sanitary napkin is very outstanding.
Table 4【Table 4】
Distinguish | Comparative example | The multipurpose functional sanitary napkin of the present invention |
Experimental result | 1,059.1KPa | 4,929KPa |
Experimental example 6:Comparative example is compared with the washing fastness of multipurpose functional sanitary napkin of the present invention
Comparative example and the experimental result of the multipurpose functional sanitary napkin washing fastness according to the present invention, comparative example are washings
It can not be washed repeatedly by dry result afterwards.On the contrary, the multipurpose functional sanitary napkin of the present invention can carry out ten washings
Dry, so that, washing fastness is very outstanding (Figure 10).
Also, cold resistance (trustee voluntarily experimental method) is, at -40 DEG C, comparative example or root to be shown under the conditions of 24 hours
Multipurpose functional sanitary napkin according to the present invention does not occur the disrepair phenomenon (Figure 11) of apparent tissue, insulation rate all
(KS K 0560:2011, temperature resistance method) it is also 89.9% very outstanding.
The explanation of the present invention is, for example, to can be regarded as not changing this in the those skilled in the art of the present invention
The technological thought and feature of invention can be easily deformed other concrete forms.Therefore, described embodiment and experimental example are all
Aspect is example and is not limited.
Claims (24)
1. a kind of multipurpose functional sanitary napkin manufacture composition is comprising have urea (UREA), oleic acid (OLEIC
ACID), diethylenetriamines (DETA), water, APP (APP), boron (B2O3), aqueous Polyoxyethylene este (PUD), bleeding agent (bear from
Sub- property), Nano Silver (NANO SILVER) and nano titanium oxide (NANO TIO2)。
2. composition according to claim 1, it is characterised in that include 5.1 to the 5.35 weight % urea
(UREA)。
3. composition according to claim 1, it is characterised in that include 0.11 to the 0.18 weight % oleic acid
(OLEIC ACID)。
4. composition according to claim 1, it is characterised in that include 0.13 to the 0.18 weight % diethylidene
Triamine.
5. composition according to claim 1, it is characterised in that include 12.1 to the 12.20 weight % polyphosphoric acid
Ammonium.
6. composition according to claim 1, it is characterised in that the boron (B comprising 1.62 to 1.70 weight %2O3)。
7. composition according to claim 1, it is characterised in that the aqueous polyoxy comprising 0.25 to 0.32 weight %
Ester (PUD).
8. composition according to claim 1, it is characterised in that include 0.11 to the 0.18 weight % bleeding agent.
9. composition according to claim 1, it is characterised in that include 2.30 to the 2.48 weight % Nano Silver
(NANO SILVER)。
10. composition according to claim 9, it is characterised in that the Nano Silver (NANO SILVER) be PH6 to 8,
It is difficult to depart from when penetrating into cotton with the acicular texture of 5~10nm size, and will not changes colour.
11. composition according to claim 1, it is characterised in that include 1.5 to the 1.60 weight % nano-silica
Change titanium (NANO TIO2)。
12. composition according to claim 11, it is characterised in that in the nano titanium oxide (NANO TIO2) table
Finishing coat silver (Silver) is used.
13. a kind of manufacture method of multipurpose functional sanitary napkin manufacture composition, comprises the following steps:
A) the step of manufacturing lysate after oleic acid, diethylenetriamines, addition water is added in aqueous solution of urea;
B) the step of dissolving APP and boron in the lysate;
C) manufacture group after aqueous Polyoxyethylene este, bleeding agent, Nano Silver, nano titanium oxide is added in the lysate of the b) step
The step of compound;And
D) the step of being dissolved after the composition is stirred ten minutes to 30 minutes.
14. manufacture method according to claim 13, it is characterised in that the lysate of a) step is 70 to 120
Heated after being stirred 2 minutes to 3 minutes at a temperature of DEG C.
15. manufacture method according to claim 13, it is characterised in that further comprise completing cooling down after the d) step
30 minutes to one hours.
16. the multipurpose functional sanitary napkin that a kind of usage right requires 1 composition to manufacture.
17. multipurpose functional sanitary napkin according to claim 16, it is characterised in that the multipurpose functional sanitary
Cotton be used for weaved cotton cloth by line, rope, processing, non-woven fabrics, mat, blasting mat, sheet material, panel core, pipe sleeve, filter, flameproof fabric,
The manufacture of the material selected in the group that resist printing wallpaper, fire prevention curtain and resist printing carpet are constituted.
18. multipurpose functional sanitary napkin according to claim 16, it is characterised in that the multipurpose functional sanitary
Cotton be used for by flame-retardant materials, anti-metachromia material, heat insulating ability material, cold insulation material, heat-barrier material, sound-absorbing material, soundproof material,
Absorb impact material, it is interlayer acoustic material, heating floor material, vacuum heat insulation material, ornament materials, safety, hygienic material, quick-fried
The material selected in the group that broken bullet resistant material, ceiling tile materials, finishing material, clothing materials, bedding class material are constituted
Manufacture.
19. a kind of manufacture method of multipurpose functional sanitary napkin, comprises the following steps:
A) in natural cotton the step of the composition of hydraulic pressure jet penetration claim 1;
B) dehydration infiltration has after the natural cotton of the composition, dry step;And
C) by cotton bullet cotton the step of.
20. manufacture method according to claim 19, it is characterised in that the hydraulic pressure injection of a) step is performed ten seconds
To 30 seconds.
21. manufacture method according to claim 19, it is characterised in that the dehydration of (b) step is to utilize extruding
(Mangle) moisture of cotton is dehydrated to 70 to 80% by dewaterer.
22. manufacture method according to claim 19, it is characterised in that the drying of (b) step is to utilize hot air drying
Dry machine is by the moisture content drying of cotton to 13% to 15%.
23. one kind mixing cotton, is used as the mixing cotton of the cotton wool comprising claim 16, it is characterised in that the mixing cotton is
In the cotton wool with 1:9 to 4:6 weight than mixing by natural cotton, mix miscellaneous cotton, it is straw cotton, wheat straw cotton, waste paper cotton, natural
Numb cotton, cocoanut fiber cotton, silk cotton, chemical cotton, bamboo fiber cotton, banana fiber cotton, waste cotton regeneration cotton, synthetic fibers cotton, paper
Cotton, carbon fiber cotton, tencel, artificial silk flosssilk wadding, cuprammonium rayon cotton, low melting point thermoplastic resin fibre cotton and kapok is starched to constitute
Group in the more than one cotton that selects.
24. a kind of functional sanitary fabric, by the composition of claim 1 permeate and be immersed in bafta, cotton blended fabric or
Manufactured on cotton face fabric.
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KR1020140182203A KR101517875B1 (en) | 2014-12-17 | 2014-12-17 | Functional cotton for various purpose and method for producing thereof |
KR10-2014-0182203 | 2014-12-17 | ||
PCT/KR2015/002310 WO2016098952A1 (en) | 2014-12-17 | 2015-03-10 | Multipurpose functional sanitary cotton and method for preparing same |
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CN201580068631.XA Pending CN107208358A (en) | 2014-12-17 | 2015-03-10 | Multipurpose functional sanitary napkin and manufacture method |
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KR (1) | KR101517875B1 (en) |
CN (1) | CN107208358A (en) |
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CN108867019A (en) * | 2018-08-09 | 2018-11-23 | 界首市恒仁服饰有限公司 | A kind of method for washing of colored woven jean |
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WO2017213596A1 (en) * | 2016-06-07 | 2017-12-14 | Ozyegin Universitesi | Nano-boron for textiles |
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WO2016098952A1 (en) | 2016-06-23 |
KR101517875B1 (en) | 2015-05-18 |
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