CN107200626A - High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation - Google Patents
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation Download PDFInfo
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- CN107200626A CN107200626A CN201710334423.0A CN201710334423A CN107200626A CN 107200626 A CN107200626 A CN 107200626A CN 201710334423 A CN201710334423 A CN 201710334423A CN 107200626 A CN107200626 A CN 107200626A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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Abstract
The invention discloses a kind of elm mushroom plantation high yield organic slow-release fertilizer, its raw material includes chicken manure, rape cake, domestic sludge, lignin, stalk, mica powder, urea, urea phosphate, borax, ammonium chloride, potassium chloride, Diammonium phosphate (DAP), potassium nitrate, calcium humate, humic acid magnesium, boric acid, ammonium nitrate, potassium nitrate, ammonium molybdate, zinc carbonate, ferrous sulfate, sodium humate, manganese chloride, citric acid waste, oil shale, gangue, weathered coal, ferment bacterium, polyacrylamide, modified sustained release agent and sustained release agent tackifier.The organic slow-release fertilizer grain forming rate of the present invention is high, is difficult bulk cargo, with excellent sustained release performance, disclosure satisfy that the nutritional need in the whole growth course of elm mushroom, can efficiently release of the high texture to nutriment, effectively improve the yield and quality of elm mushroom.
Description
Technical field
High yield organic slow-release fertilizer is used the present invention relates to the technical field of fertilizer, more particularly to a kind of plantation of elm mushroom.
Background technology
Elm mushroom also known as gold oyster mushroom, goldentop mushroom, Jade Emperor mushroom, gold mushroom；Cap olive drab(O.D) is smooth to foresythia, funnel
Shape, 3-10 centimetres of diameter.Bacterial context white.Handle is wilfully.It is cap cadmium yellow, glossy, it is graceful gratifying.Elm mushroom had both had delicious flavour, perfume (or spice)
Strong, the nutritious edibility of taste, the medical value with nourishing and fit keeping function.Not only liked by Chinese, Er Qie
International market is more in great demand, and production and the more general agricultural product of effectiveness of operation are much higher.
The fertilizer that uses of elm mushroom plantation is mostly inorganic fertilizer or farm manure in the prior art, and fertilizer efficiency and nutriment are released
Put efficiency, and nutriment release quality, the actual demand of elm mushroom plantation can not be met, so it is a kind of to need design badly
Elm mushroom plantation solves the problems of the prior art with high yield organic slow-release fertilizer.
The content of the invention
To solve technical problem present in background technology, the present invention proposes that high yield organic slow-release is used in a kind of elm mushroom plantation
Fertilizer, grain forming rate is high, is difficult bulk cargo, with excellent sustained release performance, disclosure satisfy that the battalion in the whole growth course of elm mushroom
Support demand, can efficiently release of the high texture to nutriment, effectively improve the yield and quality of elm mushroom.
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 80-
120 parts, 3-9 parts of rape cake, 5-15 parts of domestic sludge, 2-8 parts of lignin, 1-5 parts of stalk, 2-5 parts of mica powder, urea 20-40
Part, 2-3 parts of urea phosphate, 2-5 parts of borax, 1-4 parts of ammonium chloride, 3-9 parts of potassium chloride, 2-5 parts of Diammonium phosphate (DAP), 1-3 parts of potassium nitrate, corruption
2-5 parts of phytic acid calcium, 3-6 parts of humic acid magnesium, 1-5 parts of boric acid, 1-4 parts of ammonium nitrate, 2-6 parts of potassium nitrate, 3-5 parts of ammonium molybdate, carbonic acid
2-4 parts of zinc, 3-5 parts of ferrous sulfate, 2-5 parts of sodium humate, 2-4 parts of manganese chloride, 1-4 parts of citric acid waste, 1-4 parts of oil shale, coal
2-6 parts of spoil, 3-5 parts of weathered coal, 1-6 parts of ferment bacterium, 6-9 parts of polyacrylamide, modified 15-25 parts of sustained release agent, sustained release agent increase
3-6 parts of stick.
Preferably, the raw material of modified sustained release agent includes by weight：5-15 parts of Tween-80,2-8 parts of n-hexane, polyethylene
3-6 parts of pyrrolidones, 1-4 parts of sodium carbonate, 2-5 parts of calcium chloride solution, 3-6 parts of disodium phosphate soln, 1-4 parts of polyvinyl alcohol,
2-5 parts of chitosan, 3-5 parts of aqueous acetic acid.
Preferably, in the raw material of modified sustained release agent, the substance withdrawl syndrome of calcium chloride solution is 1.5-3.5mol/L, carbonic acid
The substance withdrawl syndrome of disodium hydrogen solution is 0.02-0.04mol/L, and the substance withdrawl syndrome of aqueous acetic acid is 0.01-
0.03mol/L。
Preferably, modified sustained release agent is prepared by following technique：Tween-80, n-hexane and deionized water are mixed equal
It is even to obtain material a, polyvinylpyrrolidone and sodium carbonate are well mixed and obtain material b, then material a and material b is mixed
Uniformly, stir, be subsequently added into calcium chloride solution and be well mixed, stir, dry, be cooled to room temperature and obtain material c；Then to material
C and water are well mixed, are placed in thermostat water bath and heat, and then add disodium phosphate soln and are well mixed, then use hydrogen-oxygen
Change sodium regulation pH, ageing after separation, is washed, dries, be cooled to room temperature and obtain material d；Polyvinyl alcohol and distilled water are mixed equal
Even, heating and heat preservation, then adds material d and absolute ethyl alcohol is well mixed, ultrasonic disperse, stands, is cooled to room temperature, then adds
Chitosan and aqueous acetic acid are well mixed, and stirring is cooled to room temperature and obtains being modified sustained release agent.
Preferably, modified sustained release agent is prepared by following technique：Tween-80, n-hexane and deionized water are mixed equal
It is even to obtain material a, polyvinylpyrrolidone and sodium carbonate are well mixed and obtain material b, then material a and material b is mixed
Uniformly, 20-40min is stirred in 650-850r/min rotating speeds, is subsequently added into calcium chloride solution and is well mixed, in 1050-1250r/
Min rotating speeds stir 20-40min, then in 70-90 DEG C of dry 10-14h, are cooled to room temperature and obtain material c；Then to material c and
Water is well mixed, and is placed in 70-80 DEG C of thermostat water bath and is heated 20-40min, then adds disodium phosphate soln mixing equal
It is even, 1-3h is stirred in 650-850r/min rotating speeds, then pH to 10.5-11.5 is adjusted with sodium hydroxide, 1-2d, separation is aged
Afterwards, wash, in 75-85 DEG C of dry 10-14h, be cooled to room temperature and obtain material d；Polyvinyl alcohol and distilled water are well mixed, risen
Then temperature adds material d and absolute ethyl alcohol is well mixed, ultrasonic disperse 5-15min, stand 1-3h to 85-95 DEG C of insulation 1-3h,
Room temperature is cooled to, chitosan is then added and aqueous acetic acid is well mixed, 20-40min is stirred in 450-550r/min rotating speeds,
Room temperature is cooled to obtain being modified sustained release agent.
Preferably, the raw material of sustained release agent tackifier includes by weight：3-9 parts of rice bran wax, 2-5 parts of paraffin, palm wax 1-5
Part, 3-6 parts of gleditsia sinensis liquid, 2-5 parts of mineral oil, 4-5 parts of methyl-silicone oil, 2-5 parts of cocinic acid alkanolamide, coconut oil fat acyl diethyl
3-6 parts of hydramine, 1-4 parts of triethanolamine, 2-5 parts of laurel alcohol ether phosphate, 3-6 parts of oleic acid, 1-4 parts of ethylene glycol, dodecyl sweet tea
2-5 parts of dish alkali, 4-8 parts of water, 3-9 parts of alumina silicate.
Preferably, sustained release agent tackifier are prepared by following technique：Rice bran wax and paraffin are well mixed, heating is protected
Temperature, then add palm wax, gleditsia sinensis liquid, mineral oil, methyl-silicone oil, cocinic acid alkanolamide, coconut oil fat acyl diethanol amine,
Triethanolamine, laurel alcohol ether phosphate, oleic acid, ethylene glycol and empgen BB are well mixed, heat up, and insulation is cooled to
Room temperature obtains material A；Water and alumina silicate are well mixed, heated, insulation is cooled to room temperature and obtains material B；By material A and thing
Expect that B is well mixed, stirring makes its emulsification uniform, is cooled to room temperature and produces sustained release agent tackifier.
Preferably, sustained release agent tackifier are prepared by following technique：Rice bran wax and paraffin are well mixed, are heated to
95-105 DEG C, 0.5-1.5h is incubated, palm wax, gleditsia sinensis extract solution, mineral oil, methyl-silicone oil, cocinic acid alkanol is then added
Acid amides, coconut oil fat acyl diethanol amine, triethanolamine, laurel alcohol ether phosphate, oleic acid, ethylene glycol and empgen BB are mixed
Close uniform, be warming up to 75-85 DEG C, be incubated 1-3h, be cooled to room temperature and obtain material A；Water and alumina silicate are well mixed, are heated to
75-85 DEG C, 1.5-3.5h is incubated, room temperature is cooled to and obtains material B；Material A and material B are well mixed, in 650-850r/
Min rotating speeds stir 15-25min, make its emulsification uniform, are cooled to room temperature and produce sustained release agent tackifier.
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation of the present invention, and its raw material includes chicken manure, rape cake, life dirt
Mud, lignin, stalk, mica powder, urea, urea phosphate, borax, ammonium chloride, potassium chloride, Diammonium phosphate (DAP), potassium nitrate, humic acid
Calcium, humic acid magnesium, boric acid, ammonium nitrate, potassium nitrate, ammonium molybdate, zinc carbonate, ferrous sulfate, sodium humate, manganese chloride, citric acid
Slag, oil shale, gangue, weathered coal, ferment bacterium, polyacrylamide, modified sustained release agent and sustained release agent tackifier.Wherein, it is modified
Sustained release agent obtains material a by the way that Tween-80, n-hexane and deionized water are well mixed, by polyvinylpyrrolidone and carbonic acid
Sodium is well mixed to obtain material b, is then well mixed material a and material b, stirs, and is subsequently added into calcium chloride solution mixing equal
It is even, stir, dry, be cooled to room temperature and obtain material c；Then it is well mixed to material c and water, it is placed in thermostat water bath and adds
Heat, then adds disodium phosphate soln and is well mixed, and then adjusts pH with sodium hydroxide, and ageing after separation, is washed, dried,
It is cooled to room temperature and obtains material d；Polyvinyl alcohol and distilled water are well mixed, heating and heat preservation, then add material d and anhydrous second
Alcohol is well mixed, ultrasonic disperse, is stood, is cooled to room temperature, then adds chitosan and aqueous acetic acid is well mixed, stirring,
It is cooled to room temperature to obtain being modified sustained release agent, in the organic slow-release fertilizer for applying to the present invention, the present invention can be effectively improved organic slow
Release the sustained release performance of fertilizer so that the more efficient uniform of the nutriment release of organic slow-release fertilizer of the invention, can effectively carry
The yield and quality of high elm mushroom.Wherein, sustained release agent tackifier are by the way that rice bran wax and paraffin are well mixed, heating and thermal insulation, so
Palm wax, gleditsia sinensis liquid, mineral oil, methyl-silicone oil, cocinic acid alkanolamide, coconut oil fat acyl diethanol amine, three second are added afterwards
Hydramine, laurel alcohol ether phosphate, oleic acid, ethylene glycol and empgen BB are well mixed, heat up, and insulation is cooled to room temperature
Obtain material A；Water and alumina silicate are well mixed, heated, insulation is cooled to room temperature and obtains material B；Material A and material B are mixed
Close uniform, stirring makes its emulsification uniform, is cooled to room temperature and produces sustained release agent tackifier, applies to the organic slow-release fertilizer of the present invention
In, and the modification sustained release agent cooperation added with the present invention, the grain forming rate of organic slow-release fertilizer of the present invention is effectively increased, is obtained
Organic fertilizer be difficult bulk cargo so that sustained release performance is effectively guaranteed so that the release of nutriment more uniform high-efficiency, has
Effect improves the yield and quality of elm mushroom.The organic slow-release fertilizer grain forming rate of the present invention is high, bulk cargo is difficult, with excellent
Sustained release performance, disclosure satisfy that the nutritional need in the whole growth course of elm mushroom, efficiently high texture can be released by nutriment
Put, effectively improve the yield and quality of elm mushroom.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair
It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair
In bright protection domain.
In embodiment, the parts by weight of chicken manure can for 80 parts, 85 parts, 90 parts, 95 parts, 100 parts, 105 parts, 110
Part, 115 parts, 120 parts；The parts by weight of rape cake can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts；The weight of domestic sludge
Part can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts；The parts by weight of lignin can be with
For 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts；The parts by weight of stalk can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts；Mica powder
Parts by weight can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of urea can for 20 parts, 25 parts, 30
Part, 35 parts, 40 parts；The parts by weight of urea phosphate can for 2 parts, 2.1 parts, 2.2 parts, 2.3 parts, 2.4 parts, 2.5 parts, 2.6 parts, 2.7
Part, 2.8 parts, 2.9 parts, 3 parts；The parts by weight of borax can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；Ammonium chloride
Parts by weight can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of potassium chloride can for 3 parts, 4 parts, 5
Part, 6 parts, 7 parts, 8 parts, 9 parts；The parts by weight of Diammonium phosphate (DAP) can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；Nitre
The parts by weight of sour potassium can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts；The parts by weight of calcium humate can for 2 parts, 2.5 parts, 3
Part, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of humic acid magnesium can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6
Part；The parts by weight of boric acid can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts；The parts by weight of ammonium nitrate can for 1 part, 1.5 parts, 2 parts,
2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of potassium nitrate can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts；The parts by weight of ammonium molybdate can
Think 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of zinc carbonate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；Sulfuric acid
Ferrous parts by weight can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of sodium humate can for 2 parts, 2.5 parts, 3
Part, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of manganese chloride can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；Citric acid waste
Parts by weight can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of oil shale can for 1 part, 1.5 parts, 2
Part, 2.5 parts, 3 parts, 3.5 parts, 4 parts；The parts by weight of gangue can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts；The parts by weight of weathered coal
It can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts；The parts by weight of ferment bacterium can for 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5
Part, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts；The parts by weight of polyacrylamide can for 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts,
8.5 parts, 9 parts；The parts by weight of modified sustained release agent can for 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23
Part, 24 parts, 25 parts；The parts by weight of sustained release agent tackifier can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts.
Embodiment 1
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 100
Part, 6 parts of rape cake, 10 parts of domestic sludge, 5 parts of lignin, 3 parts of stalk, 3.5 parts of mica powder, 30 parts of urea, 2.5 parts of urea phosphate,
3.5 parts of borax, 2.5 parts of ammonium chloride, 6 parts of potassium chloride, 3.5 parts of Diammonium phosphate (DAP), 2 parts of potassium nitrate, 3.5 parts of calcium humate, humic acid
4.5 parts of magnesium, 3 parts of boric acid, 2.5 parts of ammonium nitrate, 4 parts of potassium nitrate, 4 parts of ammonium molybdate, 3 parts of zinc carbonate, 4 parts of ferrous sulfate, humic acid
3.5 parts of sodium, 3 parts of manganese chloride, 2.5 parts of citric acid waste, 2.5 parts of oil shale, 4 parts of gangue, 4 parts of weathered coal, 3.5 parts of ferment bacterium,
7.5 parts of polyacrylamide, modified 20 parts of sustained release agent, 4.5 parts of sustained release agent tackifier.
Modified sustained release agent is prepared by following technique：By weight by 10 parts of Tween-80s, 5 parts of n-hexanes and deionization
Water is well mixed to obtain material a, is well mixed and obtains material b 4.5 parts of polyvinylpyrrolidones and 2.5 parts of sodium carbonate, then
Material a and material b are well mixed, 30min is stirred in 750r/min rotating speeds, being subsequently added into 3.5 parts of substance withdrawl syndromes is
2.5mol/L calcium chloride solution is well mixed, and 30min is stirred in 1150r/min rotating speeds, then in 80 DEG C of dry 12h, cooling
Material c is obtained to room temperature；Then it is well mixed to material c and water, it is placed in 75 DEG C of thermostat water baths and heats 25min, Ran Houjia
Enter the disodium phosphate soln that 4.5 parts of substance withdrawl syndromes are 0.03mol/L to be well mixed, 2h stirred in 750r/min rotating speeds,
Then pH to 11.0 is adjusted with sodium hydroxide, is aged 1d, after separation, washing, in 80 DEG C of dry 12h, is cooled to room temperature and obtains thing
Expect d；2.5 parts of polyvinyl alcohol and distilled water are well mixed, 90 DEG C of insulation 2h is warming up to, then adds material d and absolute ethyl alcohol
Well mixed, ultrasonic disperse 10min stands 2h, is cooled to room temperature, then adds 3.5 parts of chitosans and 4 parts of substance withdrawl syndromes
It is well mixed for 0.02mol/L aqueous acetic acid, 30min is stirred in 500r/min rotating speeds, is cooled to room temperature and obtains modified slow
Release agent.
Sustained release agent tackifier are prepared by following technique：6 parts of rice bran waxs and 3.5 parts of paraffin are mixed equal by weight
It is even, 100 DEG C are heated to, 1h is incubated, 3 parts of palm waxs, 4.5 parts of gleditsia sinensis extract solutions, 3.5 parts of mineral oil, 4.5 parts of methyl are then added
Silicone oil, 3.5 parts of cocinic acid alkanolamides, 4.5 parts of coconut oil fat acyl diethanol amine, 2.5 parts of triethanolamines, 3.5 parts of laruyl alcohols
Ether phosphate, 4.5 parts of oleic acid, 2.5 parts of ethylene glycol and 3.5 parts of empgen BBs are well mixed, and are warming up to 80 DEG C, insulation
2h, is cooled to room temperature and obtains material A；6 parts of water and 6 parts of alumina silicate are well mixed, 80 DEG C are heated to, 2.5h is incubated, is cooled to
Room temperature obtains material B；Material A and material B are well mixed, 20min is stirred in 750r/min rotating speeds, makes its emulsification uniform, it is cold
But sustained release agent tackifier are produced to room temperature.
Embodiment 2
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 80
Part, 9 parts of rape cake, 5 parts of domestic sludge, 8 parts of lignin, 1 part of stalk, 5 parts of mica powder, 20 parts of urea, 3 parts of urea phosphate, borax 2
Part, 4 parts of ammonium chloride, 3 parts of potassium chloride, 5 parts of Diammonium phosphate (DAP), 1 part of potassium nitrate, 5 parts of calcium humate, 3 parts of humic acid magnesium, 5 parts of boric acid,
1 part of ammonium nitrate, 6 parts of potassium nitrate, 3 parts of ammonium molybdate, 4 parts of zinc carbonate, 3 parts of ferrous sulfate, 5 parts of sodium humate, 2 parts of manganese chloride, lemon
4 parts of lemon acid sludge, 1 part of oil shale, 6 parts of gangue, 3 parts of weathered coal, 6 parts of ferment bacterium, 6 parts of polyacrylamide, modified sustained release agent 25
Part, 3 parts of sustained release agent tackifier.
Modified sustained release agent is prepared by following technique：By weight by 5 parts of Tween-80s, 8 parts of n-hexanes and deionized water
It is well mixed to obtain material a, 3 parts of polyvinylpyrrolidones and 4 parts of sodium carbonate are well mixed and obtain material b, then by material a
It is well mixed with material b, 40min is stirred in 650r/min rotating speeds, the chlorine that 2 parts of substance withdrawl syndromes are 3.5mol/L is subsequently added into
Change calcium solution to be well mixed, stir 40min in 1050r/min rotating speeds, then in 70 DEG C of dry 14h, be cooled to room temperature and obtain thing
Expect c；Then it is well mixed to material c and water, it is placed in 70 DEG C of thermostat water baths and heats 40min, then adds the amount of 3 parts of materials
Concentration is well mixed for 0.04mol/L disodium phosphate soln, stirs 3h in 650r/min rotating speeds, is then adjusted with sodium hydroxide
PH to 10.5 is saved, 2d is aged, after separation, washing, in 75 DEG C of dry 14h, is cooled to room temperature and obtains material d；By 1 part of polyvinyl alcohol
It is well mixed with distilled water, 95 DEG C of insulation 1h are warming up to, material d is then added and absolute ethyl alcohol is well mixed, ultrasonic disperse
15min, stands 1h, is cooled to room temperature, then adds the acetic acid water that 5 parts of chitosans and 3 parts of substance withdrawl syndromes are 0.03mol/L
Solution is well mixed, and is stirred 40min in 450r/min rotating speeds, is cooled to room temperature and obtains being modified sustained release agent.
Sustained release agent tackifier are prepared by following technique：3 parts of rice bran waxs and 5 parts of paraffin are well mixed by weight,
Be heated to 95 DEG C, be incubated 1.5h, then add 1 part of palm wax, 6 parts of gleditsia sinensis extract solutions, 2 parts of mineral oil, 5 parts of methyl-silicone oils, 2 parts
Cocinic acid alkanolamide, 6 parts of coconut oil fat acyl diethanol amine, 1 part of triethanolamine, 5 parts of laurel alcohol ether phosphates, 3 parts of oleic acid,
4 parts of ethylene glycol and 2 parts of empgen BBs are well mixed, and are warming up to 85 DEG C, are incubated 1h, are cooled to room temperature and obtain material A；Will
8 parts of water and 3 parts of alumina silicate are well mixed, and are heated to 85 DEG C, are incubated 1.5h, are cooled to room temperature and obtain material B；By material A and thing
Expect that B is well mixed, 15min is stirred in 850r/min rotating speeds, make its emulsification uniform, be cooled to room temperature and produce sustained release agent tackifier.
Embodiment 3
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 120
Part, 3 parts of rape cake, 15 parts of domestic sludge, 2 parts of lignin, 5 parts of stalk, 2 parts of mica powder, 40 parts of urea, 2 parts of urea phosphate, borax
5 parts, 1 part of ammonium chloride, 9 parts of potassium chloride, 2 parts of Diammonium phosphate (DAP), 3 parts of potassium nitrate, 2 parts of calcium humate, 6 parts of humic acid magnesium, boric acid 1
Part, 4 parts of ammonium nitrate, 2 parts of potassium nitrate, 5 parts of ammonium molybdate, 2 parts of zinc carbonate, 5 parts of ferrous sulfate, 2 parts of sodium humate, 4 parts of manganese chloride,
1 part of citric acid waste, 4 parts of oil shale, 2 parts of gangue, 5 parts of weathered coal, 1 part of ferment bacterium, 9 parts of polyacrylamide, modified sustained release agent
15 parts, 6 parts of sustained release agent tackifier.
Modified sustained release agent is prepared by following technique：By weight by 15 parts of Tween-80s, 2 parts of n-hexanes and deionization
Water is well mixed to obtain material a, is well mixed and obtains material b 6 parts of polyvinylpyrrolidones and 1 part of sodium carbonate, then by thing
Expect that a and material b is well mixed, 20min is stirred in 850r/min rotating speeds, be subsequently added into 5 parts of substance withdrawl syndromes for 1.5mol/L
Calcium chloride solution be well mixed, in 1250r/min rotating speeds stir 20min, then in 90 DEG C of dry 10h, be cooled to room temperature and obtain
To material c；Then it is well mixed to material c and water, it is placed in 80 DEG C of thermostat water baths and heats 20min, then adds 6 parts of materials
Amount concentration for 0.02mol/L disodium phosphate soln be well mixed, in 850r/min rotating speeds stir 1h, then use hydroxide
Sodium adjusts pH to 11.5, is aged 1d, after separation, and washing, in 85 DEG C of dry 10h, is cooled to room temperature and obtains material d；By 4 parts of poly- second
Enol and distilled water are well mixed, are warming up to 85 DEG C of insulation 3h, then add material d and absolute ethyl alcohol is well mixed, ultrasound point
5min is dissipated, 3h is stood, is cooled to room temperature, the acetic acid that 2 parts of chitosans and 5 parts of substance withdrawl syndromes are 0.01mol/L is then added
The aqueous solution is well mixed, and is stirred 20min in 550r/min rotating speeds, is cooled to room temperature and obtains being modified sustained release agent.
Sustained release agent tackifier are prepared by following technique：9 parts of rice bran waxs and 2 parts of paraffin are well mixed by weight,
105 DEG C are heated to, 0.5h is incubated, 5 parts of palm waxs, 3 parts of gleditsia sinensis extract solutions, 5 parts of mineral oil, 4 parts of methyl-silicone oils, 5 are then added
Part cocinic acid alkanolamide, 3 parts of coconut oil fat acyl diethanol amine, 4 parts of triethanolamines, 2 parts of laurel alcohol ether phosphates, 6 parts of oil
Acid, 1 part of ethylene glycol and 5 parts of empgen BBs are well mixed, and are warming up to 75 DEG C, are incubated 3h, are cooled to room temperature and obtain material
A；4 parts of water and 9 parts of alumina silicate are well mixed, 75 DEG C are heated to, 3.5h is incubated, is cooled to room temperature and obtains material B；By material A
It is well mixed with material B, 25min is stirred in 650r/min rotating speeds, makes its emulsification uniform, room temperature is cooled to and produces sustained release agent thickening
Agent.
Embodiment 4
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 85
Part, 8 parts of rape cake, 8 parts of domestic sludge, 7 parts of lignin, 2 parts of stalk, 4 parts of mica powder, 25 parts of urea, 2.8 parts of urea phosphate, boron
3 parts of sand, 3 parts of ammonium chloride, 4 parts of potassium chloride, 4 parts of Diammonium phosphate (DAP), 1.5 parts of potassium nitrate, 4 parts of calcium humate, 4 parts of humic acid magnesium, boron
Acid 4 parts, 2 parts of ammonium nitrate, 5 parts of potassium nitrate, 3.5 parts of ammonium molybdate, 3.5 parts of zinc carbonate, 3.5 parts of ferrous sulfate, 4 parts of sodium humate,
2.5 parts of manganese chloride, 3 parts of citric acid waste, 2 parts of oil shale, 5 parts of gangue, 3.5 parts of weathered coal, 5 parts of ferment bacterium, polyacrylamide 7
Part, modified 22 parts of sustained release agent, 4 parts of sustained release agent tackifier.
Modified sustained release agent is prepared by following technique：By weight by 8 parts of Tween-80s, 7 parts of n-hexanes and deionized water
It is well mixed to obtain material a, 4 parts of polyvinylpyrrolidones and 3 parts of sodium carbonate are well mixed and obtain material b, then by material a
It is well mixed with material b, 35min is stirred in 680r/min rotating speeds, the chlorine that 3 parts of substance withdrawl syndromes are 3.2mol/L is subsequently added into
Change calcium solution to be well mixed, stir 35min in 1080r/min rotating speeds, then in 75 DEG C of dry 13h, be cooled to room temperature and obtain thing
Expect c；Then it is well mixed to material c and water, it is placed in 72 DEG C of thermostat water baths and heats 35min, then adds the amount of 4 parts of materials
Concentration is well mixed for 0.035mol/L disodium phosphate soln, stirs 2.5h in 680r/min rotating speeds, then uses hydroxide
Sodium adjusts pH to 10.8, is aged 2d, after separation, and washing, in 78 DEG C of dry 13h, is cooled to room temperature and obtains material d；By 2 parts of poly- second
Enol and distilled water are well mixed, are warming up to 92 DEG C of insulation 1.5h, then add material d and absolute ethyl alcohol is well mixed, ultrasound
Scattered 12min, stands 1.5h, is cooled to room temperature, and it is 0.025mol/ then to add 4 parts of chitosans and 3.5 parts of substance withdrawl syndromes
L aqueous acetic acid is well mixed, and is stirred 35min in 480r/min rotating speeds, is cooled to room temperature and obtains being modified sustained release agent.
Sustained release agent tackifier are prepared by following technique：4 parts of rice bran waxs and 4 parts of paraffin are well mixed by weight,
98 DEG C are heated to, 1.2h is incubated, 2 parts of palm waxs, 5 parts of gleditsia sinensis extract solutions, 3 parts of mineral oil, 4.8 parts of methyl-silicone oils, 3 are then added
Part cocinic acid alkanolamide, 5 parts of coconut oil fat acyl diethanol amine, 2 parts of triethanolamines, 4 parts of laurel alcohol ether phosphates, 4 parts of oil
Acid, 3 parts of ethylene glycol and 3 parts of empgen BBs are well mixed, and are warming up to 82 DEG C, are incubated 1.5h, are cooled to room temperature and obtain thing
Expect A；7 parts of water and 4 parts of alumina silicate are well mixed, 82 DEG C are heated to, 1.8h is incubated, is cooled to room temperature and obtains material B；By material
A and material B is well mixed, and 18min is stirred in 820r/min rotating speeds, makes its emulsification uniform, is cooled to room temperature and is produced sustained release agent increasing
Stick.
Embodiment 5
High yield organic slow-release fertilizer is used in a kind of elm mushroom plantation proposed by the present invention, and its raw material includes by weight：Chicken manure 115
Part, 4 parts of rape cake, 12 parts of domestic sludge, 3 parts of lignin, 4 parts of stalk, 3 parts of mica powder, 35 parts of urea, 2.2 parts of urea phosphate, boron
4 parts of sand, 2 parts of ammonium chloride, 8 parts of potassium chloride, 3 parts of Diammonium phosphate (DAP), 2.5 parts of potassium nitrate, 3 parts of calcium humate, 5 parts of humic acid magnesium, boron
Acid 2 parts, 3 parts of ammonium nitrate, 3 parts of potassium nitrate, 4.5 parts of ammonium molybdate, 2.5 parts of zinc carbonate, 4.5 parts of ferrous sulfate, 3 parts of sodium humate,
3.5 parts of manganese chloride, 2 parts of citric acid waste, 3 parts of oil shale, 3 parts of gangue, 4.5 parts of weathered coal, 2 parts of ferment bacterium, polyacrylamide 8
Part, modified 18 parts of sustained release agent, 5 parts of sustained release agent tackifier.
Modified sustained release agent is prepared by following technique：By weight by 12 parts of Tween-80s, 3 parts of n-hexanes and deionization
Water is well mixed to obtain material a, is well mixed and obtains material b 5 parts of polyvinylpyrrolidones and 2 parts of sodium carbonate, then by thing
Expect that a and material b is well mixed, 25min is stirred in 820r/min rotating speeds, be subsequently added into 4 parts of substance withdrawl syndromes for 1.8mol/L
Calcium chloride solution be well mixed, in 1220r/min rotating speeds stir 25min, then in 85 DEG C of dry 11h, be cooled to room temperature and obtain
To material c；Then it is well mixed to material c and water, it is placed in 78 DEG C of thermostat water baths and heats 25min, then adds 5 parts of materials
Amount concentration for 0.025mol/L disodium phosphate soln be well mixed, in 820r/min rotating speeds stir 1.5h, then use hydrogen
Sodium oxide molybdena adjusts pH to 11.2, is aged 1d, after separation, and washing, in 82 DEG C of dry 11h, is cooled to room temperature and obtains material d；By 3 parts
Polyvinyl alcohol and distilled water are well mixed, are warming up to 88 DEG C of insulation 2.5h, then add material d and absolute ethyl alcohol is well mixed,
Ultrasonic disperse 8min, stands 2.5h, is cooled to room temperature, then adds 3 parts of chitosans and 4.5 parts of substance withdrawl syndromes are
0.015mol/L aqueous acetic acid is well mixed, and is stirred 25min in 520r/min rotating speeds, is cooled to room temperature and obtains being modified sustained release
Agent.
Sustained release agent tackifier are prepared by following technique：8 parts of rice bran waxs and 3 parts of paraffin are well mixed by weight,
Be heated to 102 DEG C, be incubated 0.8h, then add 4 parts of palm waxs, 4 parts of gleditsia sinensis extract solutions, 4 parts of mineral oil, 4.2 parts of methyl-silicone oils,
4 parts of cocinic acid alkanolamides, 4 parts of coconut oil fat acyl diethanol amine, 3 parts of triethanolamines, 3 parts of laurel alcohol ether phosphates, 5 parts of oil
Acid, 2 parts of ethylene glycol and 4 parts of empgen BBs are well mixed, and are warming up to 78 DEG C, are incubated 2.5h, are cooled to room temperature and obtain thing
Expect A；5 parts of water and 8 parts of alumina silicate are well mixed, 78 DEG C are heated to, 3.2h is incubated, is cooled to room temperature and obtains material B；By material
A and material B is well mixed, and 22min is stirred in 680r/min rotating speeds, makes its emulsification uniform, is cooled to room temperature and is produced sustained release agent increasing
Stick.
Elm mushroom plantation in 1- of embodiment of the present invention embodiments 5 is applied to the reality of elm mushroom with high yield organic slow-release fertilizer
In the plantation of border, and blank control group is set, blank control group is to apply the elm mushroom that common fertilizer is planted, obtained data such as table
Shown in 1.
Table 1：
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (8)
1. high yield organic slow-release fertilizer is used in a kind of elm mushroom plantation, it is characterised in that its raw material includes by weight：Chicken manure 80-120
Part, 3-9 parts of rape cake, 5-15 parts of domestic sludge, 2-8 parts of lignin, 1-5 parts of stalk, 2-5 parts of mica powder, 20-40 parts of urea,
2-3 parts of urea phosphate, 2-5 parts of borax, 1-4 parts of ammonium chloride, 3-9 parts of potassium chloride, 2-5 parts of Diammonium phosphate (DAP), 1-3 parts of potassium nitrate, rotten plant
Sour calcium 2-5 parts, 3-6 parts of humic acid magnesium, 1-5 parts of boric acid, 1-4 parts of ammonium nitrate, 2-6 parts of potassium nitrate, 3-5 parts of ammonium molybdate, zinc carbonate
2-4 parts, 3-5 parts of ferrous sulfate, 2-5 parts of sodium humate, 2-4 parts of manganese chloride, 1-4 parts of citric acid waste, 1-4 parts of oil shale, bastard coal
2-6 parts of stone, 3-5 parts of weathered coal, 1-6 parts of ferment bacterium, 6-9 parts of polyacrylamide, modified 15-25 parts of sustained release agent, sustained release agent thickening
3-6 parts of agent.
2. high yield organic slow-release fertilizer is used in elm mushroom plantation according to claim 1, it is characterised in that the original of modified sustained release agent
Material includes by weight：5-15 parts of Tween-80,2-8 parts of n-hexane, 3-6 parts of polyvinylpyrrolidone, 1-4 parts of sodium carbonate, chlorine
Change 2-5 parts of calcium solution, 3-6 parts of disodium phosphate soln, 1-4 parts of polyvinyl alcohol, 2-5 parts of chitosan, 3-5 parts of aqueous acetic acid.
3. high yield organic slow-release fertilizer is used in elm mushroom plantation according to claim 1 or 2, it is characterised in that modified sustained release agent
Raw material in, the substance withdrawl syndrome of calcium chloride solution is 1.5-3.5mol/L, the substance withdrawl syndrome of disodium bicarbonate solution
For 0.02-0.04mol/L, the substance withdrawl syndrome of aqueous acetic acid is 0.01-0.03mol/L.
4. the elm mushroom plantation high yield organic slow-release fertilizer according to claim any one of 1-3, it is characterised in that modified slow
Agent is released to be prepared by following technique：Tween-80, n-hexane and deionized water are well mixed and obtain material a, by polyethylene pyrrole
Pyrrolidone and sodium carbonate, which are well mixed, obtains material b, is then well mixed material a and material b, stirs, be subsequently added into chlorination
Calcium solution is well mixed, and is stirred, and is dried, is cooled to room temperature and obtains material c；Then it is well mixed to material c and water, it is placed in constant temperature
Heated in water-bath, then add disodium phosphate soln and be well mixed, then adjust pH with sodium hydroxide, be aged, after separation,
Washing, dries, is cooled to room temperature and obtains material d；Polyvinyl alcohol and distilled water are well mixed, heating and heat preservation, then admixture
Expect that d and absolute ethyl alcohol are well mixed, ultrasonic disperse stands, is cooled to room temperature, then add chitosan and aqueous acetic acid mixing
Uniformly, stir, be cooled to room temperature and obtain being modified sustained release agent.
5. the elm mushroom plantation high yield organic slow-release fertilizer according to claim any one of 1-4, it is characterised in that modified slow
Agent is released to be prepared by following technique：Tween-80, n-hexane and deionized water are well mixed and obtain material a, by polyethylene pyrrole
Pyrrolidone and sodium carbonate, which are well mixed, obtains material b, is then well mixed material a and material b, in 650-850r/min rotating speeds
20-40min is stirred, calcium chloride solution is subsequently added into and is well mixed, stir 20-40min in 1050-1250r/min rotating speeds, then
In 70-90 DEG C of dry 10-14h, it is cooled to room temperature and obtains material c；Then it is well mixed to material c and water, it is placed in 70-80 DEG C of perseverance
20-40min is heated in warm water bath, disodium phosphate soln is then added and is well mixed, in the stirring of 650-850r/min rotating speeds
1-3h, then adjusts pH to 10.5-11.5 with sodium hydroxide, is aged 1-2d, after separation, washing, in 75-85 DEG C of dry 10-
14h, is cooled to room temperature and obtains material d；Polyvinyl alcohol and distilled water are well mixed, 85-95 DEG C of insulation 1-3h is warming up to, then
Add material d and absolute ethyl alcohol is well mixed, ultrasonic disperse 5-15min, stand 1-3h, be cooled to room temperature, then add shell and gather
Sugar and aqueous acetic acid are well mixed, and are stirred 20-40min in 450-550r/min rotating speeds, are cooled to room temperature and obtain being modified sustained release
Agent.
6. the elm mushroom plantation high yield organic slow-release fertilizer according to claim any one of 1-5, it is characterised in that sustained release agent
The raw material of tackifier includes by weight：3-9 parts of rice bran wax, 2-5 parts of paraffin, 1-5 parts of palm wax, 3-6 parts of gleditsia sinensis liquid, mineral oil
2-5 parts, 4-5 parts of methyl-silicone oil, 2-5 parts of cocinic acid alkanolamide, 3-6 parts of coconut oil fat acyl diethanol amine, triethanolamine 1-4
Part, 2-5 parts of laurel alcohol ether phosphate, 3-6 parts of oleic acid, 1-4 parts of ethylene glycol, 2-5 parts of empgen BB, 4-8 parts of water, silicic acid
3-9 parts of aluminium.
7. the elm mushroom plantation high yield organic slow-release fertilizer according to claim any one of 1-6, it is characterised in that sustained release agent
Tackifier are prepared by following technique：Rice bran wax and paraffin are well mixed, heating and thermal insulation, then add palm wax, gleditsia sinensis
Liquid, mineral oil, methyl-silicone oil, cocinic acid alkanolamide, coconut oil fat acyl diethanol amine, triethanolamine, lauryl alcohol phosphoric acid
Ester, oleic acid, ethylene glycol and empgen BB are well mixed, heat up, and insulation is cooled to room temperature and obtains material A；By water and silicon
Sour aluminium is well mixed, and is heated, and insulation is cooled to room temperature and obtains material B；Material A and material B are well mixed, stirred, makes its breast
Change uniformly, be cooled to room temperature and produce sustained release agent tackifier.
8. the elm mushroom plantation high yield organic slow-release fertilizer according to claim any one of 1-7, it is characterised in that sustained release agent
Tackifier are prepared by following technique：Rice bran wax and paraffin are well mixed, 95-105 DEG C is heated to, 0.5-1.5h is incubated,
Then palm wax, gleditsia sinensis extract solution, mineral oil, methyl-silicone oil, cocinic acid alkanolamide, coconut oil fat acyl diethanol are added
Amine, triethanolamine, laurel alcohol ether phosphate, oleic acid, ethylene glycol and empgen BB are well mixed, are warming up to 75-85 DEG C,
1-3h is incubated, room temperature is cooled to and obtains material A；Water and alumina silicate are well mixed, 75-85 DEG C is heated to, 1.5-3.5h is incubated,
It is cooled to room temperature and obtains material B；Material A and material B are well mixed, 15-25min is stirred in 650-850r/min rotating speeds, makes
It is emulsified uniformly, is cooled to room temperature and is produced sustained release agent tackifier.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108409444A (en) * | 2018-05-11 | 2018-08-17 | 南通市白龙有机肥科技有限公司 | A kind of universal organic fertilizer |
| CN108440204A (en) * | 2018-05-11 | 2018-08-24 | 南通市白龙有机肥科技有限公司 | A kind of vegetables and fruits fertilizer special for organic |
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| CN106366944A (en) * | 2016-08-27 | 2017-02-01 | 安徽天瞳智能科技有限公司 | High-adhesiveness anti-cracking composite material and preparation method thereof |
| CN106396982A (en) * | 2016-11-29 | 2017-02-15 | 袁家和 | Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer |
| CN106588285A (en) * | 2016-11-29 | 2017-04-26 | 袁家和 | Slow release fertilizer used for rice planting and preparing method thereof |
| CN106588454A (en) * | 2016-12-03 | 2017-04-26 | 滁州市剑春园林园艺工程有限公司 | Planting method of prunus mume |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106366944A (en) * | 2016-08-27 | 2017-02-01 | 安徽天瞳智能科技有限公司 | High-adhesiveness anti-cracking composite material and preparation method thereof |
| CN106396982A (en) * | 2016-11-29 | 2017-02-15 | 袁家和 | Compound fertilizer having growth promotion and high slow-release properties and used for rice planting as well as preparation method of compound fertilizer |
| CN106588285A (en) * | 2016-11-29 | 2017-04-26 | 袁家和 | Slow release fertilizer used for rice planting and preparing method thereof |
| CN106588454A (en) * | 2016-12-03 | 2017-04-26 | 滁州市剑春园林园艺工程有限公司 | Planting method of prunus mume |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108409444A (en) * | 2018-05-11 | 2018-08-17 | 南通市白龙有机肥科技有限公司 | A kind of universal organic fertilizer |
| CN108440204A (en) * | 2018-05-11 | 2018-08-24 | 南通市白龙有机肥科技有限公司 | A kind of vegetables and fruits fertilizer special for organic |
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Application publication date: 20170926 |