CN107189874A - A kind of preparation method of glass detergent - Google Patents

A kind of preparation method of glass detergent Download PDF

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Publication number
CN107189874A
CN107189874A CN201710444531.3A CN201710444531A CN107189874A CN 107189874 A CN107189874 A CN 107189874A CN 201710444531 A CN201710444531 A CN 201710444531A CN 107189874 A CN107189874 A CN 107189874A
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China
Prior art keywords
parts
glass detergent
mixture
glass
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710444531.3A
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Chinese (zh)
Inventor
朱明静
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Hefei Steel Glass Products Co Ltd
Original Assignee
Hefei Steel Glass Products Co Ltd
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Filing date
Publication date
Application filed by Hefei Steel Glass Products Co Ltd filed Critical Hefei Steel Glass Products Co Ltd
Priority to CN201710444531.3A priority Critical patent/CN107189874A/en
Publication of CN107189874A publication Critical patent/CN107189874A/en
Withdrawn legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/83—Mixtures of non-ionic with anionic compounds
    • C11D1/831—Mixtures of non-ionic with anionic compounds of sulfonates with ethers of polyoxyalkylenes without phosphates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2006—Monohydric alcohols
    • C11D3/201—Monohydric alcohols linear
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2041—Dihydric alcohols
    • C11D3/2044—Dihydric alcohols linear
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2079—Monocarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/34—Organic compounds containing sulfur
    • C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)

Abstract

A kind of preparation method of glass detergent, comprises the following steps：First, deionization ethanol, propane diols and deionized water are mixed, stirs and obtain mixture one after heating；2nd, AEO, sodium citrate and neopelex are sequentially added into mixture one to be stirred, mixture two is obtained after stirring；3rd, after addition sodium stearate and glycerine are stirred into mixture two, carry out cooling treatment and obtain mixture three；4th, glycerine is added into mixture three, homogenization is carried out using homogenizer after heating, obtains glass detergent crude product；5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.The present invention does not produce corrosion to glass surface, while layer protecting film is left in its surface, with soil resistance, it is possible to reduce cleaning frequency, and preparation technology of the present invention is simple, and step is simple to operation, it is adaptable to industrialization large-scale production.

Description

A kind of preparation method of glass detergent
Technical field
The invention belongs to glass detergent manufacture technology field, and in particular to a kind of preparation method of glass detergent.
Background technology
Because glass has the characteristic of glossy clear, the light transmittance and decorative effect that can have been reached, therefore be widely used In building, automobile and other industries.But glass is easy to contamination dust, particularly high buildings and large mansions building exterior wall glass and automobile gear Easily dirty on wind glass, the dirt of these glass is mainly：Dust, silicone glass glue stain, cement mortar exudate, glass Weathering oxide and insect form the obstinate dirt impurity being difficult to clean off after being hit with glass surface.If long-term is not right Glass is cleaned, glass will burnt hair it is dimmed, its transparency and unsightly is influenceed, so need to enter at regular intervals to glass Row cleaning, keeps good transparency and definition.At present, an emerging industry is turned into glass cleaning and maintenance, but It is that current glass cleaner is bad using rear clean effect, some glue stains, dust are easily remained, and easily etching glass table Face, reduces the smoothness of glass, makes glass be easier to be infected with dust, is also easy to be formed after mist layer, the permeability for reducing glass Reflectance.
The content of the invention
It is an object of the invention to provide a kind of preparation method of glass detergent, raw material of the invention is with ethanol and deionization Water is that major ingredient and a variety of surfactants, auxiliary agent are composited, and foam is few when the present invention is used, water-soluble strong, nontoxic, non-stimulated Property, dust, oxide etc. can be dispelled, washmarking is not stayed after volatilization, light does not produce corrosion to glass surface, while on its surface On leave layer protecting film, reduce the contamination of dust, with soil resistance, it is possible to reduce cleaning frequency, and the present invention prepares work Skill is simple, and step is simple to operation, it is adaptable to industrialization large-scale production.
The invention provides following technical scheme：
A kind of preparation method of glass detergent, comprises the following steps：
First, deionization ethanol, propane diols and deionized water are mixed, 50-60 DEG C is heated to after stirring, heat 20-30min After obtain mixture one；
2nd, AEO, sodium citrate and neopelex is sequentially added into mixture one to be stirred Mix, mixing speed is 300-500r/min, mixing time is to obtain mixture two after 30-40min, stirring；
3rd, add sodium stearate into mixture two and glycerine be stirred, after stirring 20-30min, carry out cooling treatment, Obtain mixture three；
4th, glycerine is added into mixture three, is heated at 120-150 DEG C after 5-10min, carried out using homogenizer at homogeneous Reason, obtains glass detergent crude product；
5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.
It is preferred that, the glass detergent includes the raw material of following parts by weight：12-15 parts of deionization ethanol, propane diols 8- 13 parts, 10-15 parts of deionized water, 8-12 parts of AEO, 11-15 parts of sodium citrate, neopelex 10-16 parts of 12-16 parts, 9-14 parts of sodium stearate, 8-10 parts of glycerine and glycerine.
It is preferred that, the glass detergent includes the raw material of following parts by weight：15 parts of deionization ethanol, 8 parts of propane diols, go 15 parts of ionized water, 8 parts of AEO, 11 parts of sodium citrate, 16 parts of neopelex, 9 parts of sodium stearate, 11 parts of 10 parts of glycerine and glycerine.
It is preferred that, the step 3 is cooled to after less than 10 DEG C, stands 2-3h.
It is preferred that, after the step 4 homogenization, add chelating agent, preservative and lubricant and be stirred.
It is preferred that, the gross mass of the chelating agent, preservative and lubricant three accounts for the 5- of glass detergent crude product quality 10%。
It is preferred that, the chelating agent is sodium gluconate, and preservative is BIT or poly- six methylene Base guanidine.
It is preferred that, the step 5 exhaust uses vacuum pressed degassing method, and evacuation time is in 20-30min.
The beneficial effects of the invention are as follows：
The raw material of the present invention is that major ingredient and a variety of surfactants, auxiliary agent are composited using ethanol and deionized water, and the present invention makes Used time foam is few, water-soluble strong, nontoxic, nonirritant, can dispel dust, oxide etc., washmarking is not stayed after volatilization, and light is right Glass surface does not produce corrosion, while leaving layer protecting film in its surface, reduces the contamination of dust, can with soil resistance To reduce cleaning frequency.
And preparation technology of the present invention is simple, and step is simple to operation, low raw-material cost, it is easy to obtain, it is adaptable to work Industryization is mass produced.
Embodiment
Embodiment 1
A kind of preparation method of glass detergent, comprises the following steps：
First, deionization ethanol, propane diols and deionized water are mixed, obtained after 60 DEG C, heating 20min are heated to after stirring Mixture one；
2nd, AEO, sodium citrate and neopelex is sequentially added into mixture one to be stirred Mix, mixing speed is 500r/min, mixing time is to obtain mixture two after 30min, stirring；
3rd, add sodium stearate into mixture two and glycerine is stirred, after stirring 30min, carry out cooling treatment, obtain Mixture three；
4th, glycerine is added into mixture three, is heated at 150 DEG C after 5min, carried out homogenization using homogenizer, obtain glass Glass detergent crude product；
5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.
Glass detergent includes the raw material of following parts by weight：15 parts of deionization ethanol, 8 parts of propane diols, 15 parts of deionized water, 8 parts of AEO, 11 parts of sodium citrate, 16 parts of neopelex, 9 parts of sodium stearate, 10 parts of glycerine With 11 parts of glycerine.
Step 3 is cooled to after less than 10 DEG C, stands 2h.
After step 4 homogenization, add chelating agent, preservative and lubricant and be stirred.
The gross mass of chelating agent, preservative and lubricant three accounts for the 10% of glass detergent crude product quality.
Chelating agent is sodium gluconate, and preservative is BIT.
Step 5 exhaust uses vacuum pressed degassing method, and evacuation time is in 30min.
Embodiment 2
A kind of preparation method of glass detergent, comprises the following steps：
First, deionization ethanol, propane diols and deionized water are mixed, obtained after 50 DEG C, heating 20min are heated to after stirring Mixture one；
2nd, AEO, sodium citrate and neopelex is sequentially added into mixture one to be stirred Mix, mixing speed is 300r/min, mixing time is to obtain mixture two after 30min, stirring；
3rd, add sodium stearate into mixture two and glycerine is stirred, after stirring 20min, carry out cooling treatment, obtain Mixture three；
4th, glycerine is added into mixture three, is heated at 120 DEG C after 5min, carried out homogenization using homogenizer, obtain glass Glass detergent crude product；
5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.
Glass detergent includes the raw material of following parts by weight：12 parts of deionization ethanol, 13 parts of propane diols, deionized water 15 Part, 8 parts of AEO, 15 parts of sodium citrate, 12 parts of neopelex, 14 parts of sodium stearate, glycerine 8 10 parts of part and glycerine.
Step 3 is cooled to after less than 10 DEG C, stands 2h.
After step 4 homogenization, add chelating agent, preservative and lubricant and be stirred.
The gross mass of chelating agent, preservative and lubricant three accounts for the 5% of glass detergent crude product quality.
Chelating agent is sodium gluconate, and preservative is polyhexamethylene guanide.
Step 5 exhaust uses vacuum pressed degassing method, and evacuation time is in 20min.
Embodiment 3
A kind of preparation method of glass detergent, comprises the following steps：
First, deionization ethanol, propane diols and deionized water are mixed, obtained after 60 DEG C, heating 30min are heated to after stirring Mixture one；
2nd, AEO, sodium citrate and neopelex is sequentially added into mixture one to be stirred Mix, mixing speed is 500r/min, mixing time is to obtain mixture two after 40min, stirring；
3rd, add sodium stearate into mixture two and glycerine is stirred, after stirring 30min, carry out cooling treatment, obtain Mixture three；
4th, glycerine is added into mixture three, is heated at 150 DEG C after 10min, carried out homogenization using homogenizer, obtain Glass detergent crude product；
5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.
Glass detergent includes the raw material of following parts by weight：15 parts of deionization ethanol, 8 parts of propane diols, 15 parts of deionized water, 8 parts of AEO, 11 parts of sodium citrate, 16 parts of neopelex, 9 parts of sodium stearate, 10 parts of glycerine With 11 parts of glycerine.
Step 3 is cooled to after less than 10 DEG C, stands 3h.
After step 4 homogenization, add chelating agent, preservative and lubricant and be stirred.
The gross mass of chelating agent, preservative and lubricant three accounts for the 10% of glass detergent crude product quality.
Chelating agent is sodium gluconate, and preservative is BIT.
Step 5 exhaust uses vacuum pressed degassing method, and evacuation time is in 30min.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.

Claims (8)

1. a kind of preparation method of glass detergent, it is characterised in that comprise the following steps：
First, deionization ethanol, propane diols and deionized water are mixed, 50-60 DEG C is heated to after stirring, heat 20-30min After obtain mixture one；
2nd, AEO, sodium citrate and neopelex is sequentially added into mixture one to be stirred Mix, mixing speed is 300-500r/min, mixing time is to obtain mixture two after 30-40min, stirring；
3rd, add sodium stearate into mixture two and glycerine be stirred, after stirring 20-30min, carry out cooling treatment, Obtain mixture three；
4th, glycerine is added into mixture three, is heated at 120-150 DEG C after 5-10min, carried out using homogenizer at homogeneous Reason, obtains glass detergent crude product；
5th, after glass detergent crude product being cooled down, be vented and filtered, you can obtain finished product.
2. a kind of preparation method of glass detergent according to claim 1, it is characterised in that the glass detergent bag Include the raw material of following parts by weight：12-15 parts of deionization ethanol, 8-13 parts of propane diols, 10-15 parts of deionized water, fatty alcohol polyoxy 8-12 parts of vinethene, 11-15 parts of sodium citrate, 12-16 parts of neopelex, 9-14 parts of sodium stearate, glycerine 8- 10 parts and 10-16 parts of glycerine.
3. a kind of preparation method of glass detergent according to claim 1, it is characterised in that the glass detergent bag Include the raw material of following parts by weight：15 parts of deionization ethanol, 8 parts of propane diols, 15 parts of deionized water, 8 parts of AEO, 11 parts of 11 parts of sodium citrate, 16 parts of neopelex, 9 parts of sodium stearate, 10 parts of glycerine and glycerine.
4. the preparation method of a kind of glass detergent according to claim 1, it is characterised in that the step 3 is cooled to After less than 10 DEG C, 2-3h is stood.
5. the preparation method of a kind of glass detergent according to claim 1, it is characterised in that at the step 4 homogeneous After reason, add chelating agent, preservative and lubricant and be stirred.
6. the preparation method of a kind of glass detergent according to claim 5, it is characterised in that the chelating agent, anti-corrosion The gross mass of agent and lubricant three account for the 5-10% of glass detergent crude product quality.
7. the preparation method of a kind of glass detergent according to claim 5, it is characterised in that the chelating agent is grape Sodium saccharate, preservative is BIT or polyhexamethylene guanide.
8. the preparation method of a kind of glass detergent according to claim 5, it is characterised in that the step 5 exhaust is adopted Vacuum pressed degassing method is used, evacuation time is in 20-30min.
CN201710444531.3A 2017-06-13 2017-06-13 A kind of preparation method of glass detergent Withdrawn CN107189874A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710444531.3A CN107189874A (en) 2017-06-13 2017-06-13 A kind of preparation method of glass detergent

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Application Number Priority Date Filing Date Title
CN201710444531.3A CN107189874A (en) 2017-06-13 2017-06-13 A kind of preparation method of glass detergent

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CN107189874A true CN107189874A (en) 2017-09-22

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108641831A (en) * 2018-05-24 2018-10-12 安徽省凤阳县前力玻璃制品有限公司 A kind of tempered glass rapid cleaning liquid
CN108949368A (en) * 2018-07-02 2018-12-07 滁州亿扬零部件制造有限公司 A kind of low freezing point automobile windscreen cleaning agent

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102911819A (en) * 2012-09-28 2013-02-06 上海群乐船舶附件启东有限公司 Detergent for glass
CN103897854A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Preparation method of glass detergent
CN103966030A (en) * 2014-05-23 2014-08-06 江苏紫石化工科技有限公司 Glass detergent
CN105647680A (en) * 2016-02-25 2016-06-08 陈俊俊 Glass detergent and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102911819A (en) * 2012-09-28 2013-02-06 上海群乐船舶附件启东有限公司 Detergent for glass
CN103897854A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Preparation method of glass detergent
CN103966030A (en) * 2014-05-23 2014-08-06 江苏紫石化工科技有限公司 Glass detergent
CN105647680A (en) * 2016-02-25 2016-06-08 陈俊俊 Glass detergent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108641831A (en) * 2018-05-24 2018-10-12 安徽省凤阳县前力玻璃制品有限公司 A kind of tempered glass rapid cleaning liquid
CN108949368A (en) * 2018-07-02 2018-12-07 滁州亿扬零部件制造有限公司 A kind of low freezing point automobile windscreen cleaning agent

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Application publication date: 20170922

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