CN107189752A - A kind of novel ceramic tile gap filler and preparation method thereof - Google Patents
A kind of novel ceramic tile gap filler and preparation method thereof Download PDFInfo
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- CN107189752A CN107189752A CN201710536312.8A CN201710536312A CN107189752A CN 107189752 A CN107189752 A CN 107189752A CN 201710536312 A CN201710536312 A CN 201710536312A CN 107189752 A CN107189752 A CN 107189752A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J183/00—Adhesives based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Adhesives based on derivatives of such polymers
- C09J183/04—Polysiloxanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0806—Silver
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of novel ceramic tile gap filler, include the raw material of following parts by weight：1.3~1.8 parts of 15~28 parts of organic silicon emulsion, 10~30 parts of modification infusorial earth, 12~23 parts of acrylate synthetic resin, 5~10 parts of dicalcium powder, 8~16 parts of calcite in powder, 2~5 parts of redispersible latex powder, 3~7 parts of titanium dioxide, 2~3 parts of curing agent, 1~2 part of cellulose, 1.3~2.1 parts of anti-crack water-proof agent, 0.7~1.5 part of defoamer, 1~2 part of bactericide and ultra-violet absorber.Novel ceramic tile gap filler shrinkage of the present invention is good, and thermal adaptability is strong, is not susceptible to be cracked, no accumulation of salt in the surface soil phenomenon, and will not turn to be yellow mouldy blackening, with good water-fast, decay resistance.
Description
Technical field
The invention belongs to gap filler technical field, and in particular to a kind of novel ceramic tile gap filler and preparation method thereof.
Background technology
At present, ceramic tile has become one of principal item of China ground and wall decorative material.At present, between ceramic tile
Gap is mainly filled using the cement mortar or net slurry of Portland cement, white cement and coloured cement as pointing,
This easy drying shrinkage of pointing produces crack, causes rain leakage.Meanwhile, this pointing deformability is poor, and heat expansion is cold
Contracting produces stress concentration, causes ceramic tile to come off.
The content of the invention
The invention provides a kind of novel ceramic tile gap filler and preparation method thereof, efficiently solve traditional pointing and easily open
Split, the problem of water proofing property is poor.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of novel ceramic tile gap filler, includes the raw material of following parts by weight：15~28 parts of organic silicon emulsion, modification infusorial earth 10~
30 parts, 12~23 parts of acrylate synthetic resin, 5~10 parts of dicalcium powder, 8~16 parts of calcite in powder, redispersible latex powder 2
~5 parts, 3~7 parts of titanium dioxide, 2~3 parts of curing agent, 1~2 part of cellulose, 1.3~2.1 parts of anti-crack water-proof agent, defoamer 0.7~
1.3~1.8 parts of 1.5 parts, 1~2 part of bactericide and ultra-violet absorber.
It is preferred that, the novel ceramic tile gap filler includes the raw material of following parts by weight：22 parts of organic silicon emulsion, modified silicon
28 parts of diatomaceous earth, 17 parts of acrylate synthetic resin, 7 parts of dicalcium powder, 13 parts of calcite in powder, 4 parts of redispersible latex powder, titanium white
5 parts of powder, 2.8 parts of curing agent, 1.4 parts of cellulose, 1.9 parts of anti-crack water-proof agent, 1.2 parts of defoamer, 1.3 parts of bactericide and ultraviolet
1.5 parts of absorbent.
It is preferred that, the modification infusorial earth has following methods to be made：
（1）Diatomite is put into concentration to soak after 2~5h for 8~13% sodium hydroxide solutions, then adjusts pH to neutrality；
（2）The diatomite after above-mentioned processing is taken out, is dried at a temperature of 45~55 DEG C to water content 3~5%, colophony powder is added and mixes
Close uniform；
（3）Add carboxymethyl cellulose to be well mixed, material is ground to form into 8.0~10.0 μm of powder, modification infusorial earth is obtained.
It is preferred that, the cellulose selects free hydroxy ethyl cellulose, hydroxyethylmethylcellulose, hydroxypropyl methyl cellulose
At least one of.
It is preferred that, the antiseptic is nano-TiO2, silver nano material or carry Ag titanium dioxide.
It is preferred that, the curing agent is watersoluble modified fatty amine and/or alicyclic ring amine epoxy curing agent.
It is preferred that, the ultra-violet absorber is salicylic acid esters, benzophenone class, benzotriazole, group-substituted acrylonitrile, three
One kind and/or more than one mixture in piperazine class.
A kind of method for preparing the novel ceramic tile gap filler, comprises the following steps：
（1）Weigh organic silicon emulsion by above-mentioned formula, it is modification infusorial earth, acrylate synthetic resin, calcite in powder, redispersible
Property latex powder, titanium dioxide, curing agent, cellulose, anti-crack water-proof agent, defoamer, bactericide and ultra-violet absorber, it is standby；
（2）Modification infusorial earth and calcite in powder, titanium dioxide are put into mixer and be uniformly mixed, wet-milling in ball mill is placed in
20~30 minutes, obtain mixed slurry；
（3）Organic silicon emulsion is placed in reactor, 50~55 DEG C are heated to, 20~30 minutes are incubated, redispersible is put into
Latex powder, it is scattered 5~10 minutes at a high speed, 72~78 DEG C are heated to, is vacuumized, input acrylate synthetic resin and cellulose,
It is uniformly mixed, is incubated 20~30 minutes；
（4）By step（2）Obtained mixed slurry and step（3）Obtained product is well mixed, scattered 12~18 minutes at a high speed,
Put into curing agent, anti-crack water-proof agent, bactericide, ultra-violet absorber and defoamer successively again, stirring is mixed, until bubble-free,
Produce the novel ceramic tile gap filler.
It is preferred that, the step（2）The weight ratio of middle mixed slurry material and water is 1:0.5.
It is preferred that, the step（3）The scattered speed of high speed is 3000~4000r/min.
Compared with prior art, it has the advantages that the present invention：
Novel ceramic tile gap filler shrinkage of the present invention is good, and thermal adaptability is strong, is not susceptible to cracking, and no accumulation of salt in the surface soil shows
As will not turn to be yellow mouldy blackening, specific as follows with good water-fast, decay resistance：
（1）Novel ceramic tile gap filler of the present invention using modification infusorial earth as raw material, modified diatomite have compared with
High impact strength, tensile strength and tearing strength, the soft wearability of light weight is good, and compression strength is good, preferably water-fast and corrosion-resistant
The advantages of performance, it can reduce and cause flexible because humidity changes, significantly improve the performance of gap filler；
（2）Novel ceramic tile gap filler of the present invention is by the combination of inorganic material and organic material, when temperature changes
When causing stress changes, it is not easy to cause crawling phenomenon；Adhesive property is good, acrylate synthetic resin and organosilicon breast
Liquid, with good cementitiousness, can form transparent glossiness film, improve the caking property of gap filler, acrylate synthesis tree
Fat then possesses good elasticity, and the addition of synthetic resin improves the elastic tensile modulus of the present invention, makes the present invention will not be because outer
The displacement of wall ceramic tile and produce crack；
（3）Novel ceramic tile gap filler of the present invention also added the additives such as bactericide, waterproofing agent, ultra-violet absorber,
Sterilizing ability, water resistance and the anti-uv-ray of gap filler are significantly improved, extends its service life.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of novel ceramic tile gap filler, includes the raw material of following parts by weight：15 parts of organic silicon emulsion, modified silicon
10 parts of diatomaceous earth, 12 parts of acrylate synthetic resin, 5 parts of dicalcium powder, 8 parts of calcite in powder, 2 parts of redispersible latex powder, titanium white
3 parts of powder, 2 parts of curing agent, 1 part of cellulose, 1.3 parts of anti-crack water-proof agent, 0.7 part of defoamer, 1 part of bactericide and ultra-violet absorber
1.3 part.
Wherein, the modification infusorial earth has following methods to be made：
（1）After diatomite is put into concentration for 8 sodium hydroxide solutions immersion 2h, then pH is adjusted to neutrality；
（2）The diatomite after above-mentioned processing is taken out, is dried at a temperature of 45 DEG C to water content 3%, colophony powder is added and is well mixed；
（3）Add carboxymethyl cellulose to be well mixed, material is ground to form into 8.0~10.0 μm of powder, modification infusorial earth is obtained.
Wherein, the cellulose is hydroxyethyl cellulose.
Wherein, the antiseptic is nano-TiO2。
Wherein, the curing agent is watersoluble modified fatty amine curing agent.
Wherein, the ultra-violet absorber is salicylate ultraviolet absorbent.
A kind of method for preparing the novel ceramic tile gap filler, comprises the following steps：
（1）Weigh organic silicon emulsion by above-mentioned formula, it is modification infusorial earth, acrylate synthetic resin, calcite in powder, redispersible
Property latex powder, titanium dioxide, curing agent, cellulose, anti-crack water-proof agent, defoamer, bactericide and ultra-violet absorber, it is standby；
（2）Modification infusorial earth and calcite in powder, titanium dioxide are put into mixer and be uniformly mixed, wet-milling in ball mill is placed in
20 minutes, the weight ratio for obtaining material and water in mixed slurry, mixed slurry was 1:0.5；
（3）Organic silicon emulsion is placed in reactor, 50 DEG C are heated to, 20 minutes are incubated, redispersible latex powder is put into, it is high
Speed is scattered 5 minutes, and scattered speed is 3000r/min at a high speed, is heated to 72 DEG C, vacuumizes, and puts into acrylate synthetic resin
And cellulose, it is uniformly mixed, is incubated 20 minutes；
（4）By step（2）Obtained mixed slurry and step（3）Obtained product is well mixed, scattered 12 minutes at a high speed, then according to
Secondary input curing agent, anti-crack water-proof agent, bactericide, ultra-violet absorber and defoamer, stirring mixing, until bubble-free, is produced
The novel ceramic tile gap filler.
Embodiment 2
The present embodiment is related to a kind of novel ceramic tile gap filler, includes the raw material of following parts by weight：28 parts of organic silicon emulsion, modified silicon
30 parts of diatomaceous earth, 23 parts of acrylate synthetic resin, 10 parts of dicalcium powder, 16 parts of calcite in powder, 5 parts of redispersible latex powder, titanium
7 parts of white powder, 3 parts of curing agent, 2 parts of cellulose, 2.1 parts of anti-crack water-proof agent, 1.5 parts of defoamer, 2 parts of bactericide and ultraviolet radiation absorption
1.8 parts of agent.
Wherein, the modification infusorial earth has following methods to be made：
（1）After diatomite is put into concentration for 13% sodium hydroxide solution immersion 5h, then pH is adjusted to neutrality；
（2）The diatomite after above-mentioned processing is taken out, is dried at a temperature of 55 DEG C to water content 5%, colophony powder is added and is well mixed；
（3）Add carboxymethyl cellulose to be well mixed, material is ground to form into 8.0~10.0 μm of powder, modification infusorial earth is obtained.
Wherein, the cellulose is hydroxyethylmethylcellulose.
Wherein, the antiseptic is silver nano material.
Wherein, the curing agent is alicyclic ring amine epoxy curing agent.
Wherein, the ultra-violet absorber is benzophenone class ultra-violet absorber.
A kind of method for preparing the novel ceramic tile gap filler, comprises the following steps：
（1）Weigh organic silicon emulsion by above-mentioned formula, it is modification infusorial earth, acrylate synthetic resin, calcite in powder, redispersible
Property latex powder, titanium dioxide, curing agent, cellulose, anti-crack water-proof agent, defoamer, bactericide and ultra-violet absorber, it is standby；
（2）Modification infusorial earth and calcite in powder, titanium dioxide are put into mixer and be uniformly mixed, wet-milling in ball mill is placed in
20~30 minutes, the weight ratio for obtaining material and water in mixed slurry, mixed slurry was 1:0.5；
（3）Organic silicon emulsion is placed in reactor, 55 DEG C are heated to, 30 minutes are incubated, redispersible latex powder is put into, it is high
The speed that speed is disperseed at a high speed for scattered 10 minutes is 4000r/min, is heated to 78 DEG C, vacuumizes, and puts into acrylate synthetic resin
And cellulose, it is uniformly mixed, is incubated 30 minutes；
（4）By step（2）Obtained mixed slurry and step（3）Obtained product is well mixed, scattered 18 minutes at a high speed, then according to
Secondary input curing agent, anti-crack water-proof agent, bactericide, ultra-violet absorber and defoamer, stirring mixing, until bubble-free, is produced
The novel ceramic tile gap filler.
Embodiment 3
The present embodiment is related to a kind of novel ceramic tile gap filler, includes the raw material of following parts by weight：22 parts of organic silicon emulsion, modified silicon
28 parts of diatomaceous earth, 17 parts of acrylate synthetic resin, 7 parts of dicalcium powder, 13 parts of calcite in powder, 4 parts of redispersible latex powder, titanium white
5 parts of powder, 2.8 parts of curing agent, 1.4 parts of cellulose, 1.9 parts of anti-crack water-proof agent, 1.2 parts of defoamer, 1.3 parts of bactericide and ultraviolet
1.5 parts of absorbent.
Wherein, the modification infusorial earth has following methods to be made：
（1）After diatomite is put into concentration for 10% sodium hydroxide solution immersion 3h, then pH is adjusted to neutrality；
（2）The diatomite after above-mentioned processing is taken out, is dried at a temperature of 50 DEG C to water content 4%, colophony powder is added and is well mixed；
（3）Add carboxymethyl cellulose to be well mixed, material is ground to form into 8.0~10.0 μm of powder, modification infusorial earth is obtained.
Wherein, the cellulose is hydroxypropyl methyl cellulose.
Wherein, the antiseptic is load Ag titanium dioxide.
Wherein, the curing agent is the mixture of watersoluble modified fatty amine and alicyclic ring amine epoxy curing agent.
Wherein, the ultra-violet absorber is the mixture of benzotriazole and group-substituted acrylonitrile.
A kind of method for preparing the novel ceramic tile gap filler, comprises the following steps：
（1）Weigh organic silicon emulsion by above-mentioned formula, it is modification infusorial earth, acrylate synthetic resin, calcite in powder, redispersible
Property latex powder, titanium dioxide, curing agent, cellulose, anti-crack water-proof agent, defoamer, bactericide and ultra-violet absorber, it is standby；
（2）Modification infusorial earth and calcite in powder, titanium dioxide are put into mixer and be uniformly mixed, wet-milling in ball mill is placed in
25 minutes, the weight ratio for obtaining material and water in mixed slurry, mixed slurry was 1:0.5；
（3）Organic silicon emulsion is placed in reactor, 52 DEG C are heated to, 25 minutes are incubated, redispersible latex powder is put into, it is high
Speed is scattered 7 minutes, and scattered speed is 3500r/min at a high speed, is heated to 75 DEG C, vacuumizes, and puts into acrylate synthetic resin
And cellulose, it is uniformly mixed, is incubated 27 minutes；
（4）By step（2）Obtained mixed slurry and step（3）Obtained product is well mixed, scattered 16 minutes at a high speed, then according to
Secondary input curing agent, anti-crack water-proof agent, bactericide, ultra-violet absorber and defoamer, stirring mixing, until bubble-free, is produced
The novel ceramic tile gap filler.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of novel ceramic tile gap filler, it is characterised in that include the raw material of following parts by weight：15~28 parts of organic silicon emulsion,
10~30 parts of modification infusorial earth, 12~23 parts of acrylate synthetic resin, 5~10 parts of dicalcium powder, 8~16 parts of calcite in powder, can
2~5 parts of redispersibility latex powder, 3~7 parts of titanium dioxide, 2~3 parts of curing agent, 1~2 part of cellulose, anti-crack water-proof agent 1.3~
1.3~1.8 parts of 2.1 parts, 0.7~1.5 part of defoamer, 1~2 part of bactericide and ultra-violet absorber.
2. novel ceramic tile gap filler according to claim 1, it is characterised in that include the raw material of following parts by weight：It is organic
22 parts of silicon emulsion, 28 parts of modification infusorial earth, 17 parts of acrylate synthetic resin, 7 parts of dicalcium powder, 13 parts of calcite in powder, it can divide again
Dissipate 4 parts of property latex powder, 5 parts of titanium dioxide, 2.8 parts of curing agent, 1.4 parts of cellulose, 1.9 parts of anti-crack water-proof agent, 1.2 parts of defoamer,
1.5 parts of 1.3 parts of bactericide and ultra-violet absorber.
3. novel ceramic tile gap filler according to claim 1, it is characterised in that the modification infusorial earth has following methods system
：
（1）Diatomite is put into concentration to soak after 2~5h for 8~13% sodium hydroxide solutions, then adjusts pH to neutrality；
（2）The diatomite after above-mentioned processing is taken out, is dried at a temperature of 45~55 DEG C to water content 3~5%, colophony powder is added and mixes
Close uniform；
（3）Add carboxymethyl cellulose to be well mixed, material is ground to form into 8.0~10.0 μm of powder, modification infusorial earth is obtained.
4. novel ceramic tile gap filler according to claim 1, it is characterised in that the cellulose is selected from by hydroxy ethyl fiber
At least one of element, hydroxyethylmethylcellulose, hydroxypropyl methyl cellulose.
5. novel ceramic tile gap filler according to claim 1, it is characterised in that the antiseptic is nano-TiO2, silver nanoparticle
Material carries Ag titanium dioxide.
6. novel ceramic tile gap filler according to claim 1, it is characterised in that the curing agent is watersoluble modified fatty amine
And/or alicyclic ring amine epoxy curing agent.
7. novel ceramic tile gap filler according to claim 1, it is characterised in that the ultra-violet absorber is salicylate
Class, benzophenone class, benzotriazole, group-substituted acrylonitrile, one kind in triazines and/or more than one mixture.
8. a kind of method for preparing any one of the claim 1~7 novel ceramic tile gap filler, it is characterised in that including as follows
Step：
（1）Weigh organic silicon emulsion by above-mentioned formula, it is modification infusorial earth, acrylate synthetic resin, calcite in powder, redispersible
Property latex powder, titanium dioxide, curing agent, cellulose, anti-crack water-proof agent, defoamer, bactericide and ultra-violet absorber, it is standby；
（2）Modification infusorial earth and calcite in powder, titanium dioxide are put into mixer and be uniformly mixed, wet-milling in ball mill is placed in
20~30 minutes, obtain mixed slurry；
（3）Organic silicon emulsion is placed in reactor, 50~55 DEG C are heated to, 20~30 minutes are incubated, redispersible is put into
Latex powder, it is scattered 5~10 minutes at a high speed, 72~78 DEG C are heated to, is vacuumized, input acrylate synthetic resin and cellulose,
It is uniformly mixed, is incubated 20~30 minutes；
（4）By step（2）Obtained mixed slurry and step（3）Obtained product is well mixed, scattered 12~18 minutes at a high speed,
Put into curing agent, anti-crack water-proof agent, bactericide, ultra-violet absorber and defoamer successively again, stirring is mixed, until bubble-free,
Produce the novel ceramic tile gap filler.
9. preparation method according to claim 8, it is characterised in that the step（2）Middle mixed slurry material and water
Weight ratio is 1:0.5.
10. preparation method according to claim 8, it is characterised in that the step（3）The scattered speed of high speed is
3000~4000r/min.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107603521A (en) * | 2017-10-27 | 2018-01-19 | 桂林市漓江机电制造有限公司 | A kind of non-cement-based tile adhesives of anti-formaldehyde |
| CN107858036A (en) * | 2017-11-02 | 2018-03-30 | 陈谓清 | A kind of gap filler and preparation method thereof |
| CN108102585A (en) * | 2018-01-24 | 2018-06-01 | 合肥市大卓电力有限责任公司 | A kind of environment friendly mildew resistant ceramic wall and floor tile gap filler and preparation method thereof |
| CN108275929A (en) * | 2018-05-04 | 2018-07-13 | 合肥天沃能源科技有限公司 | A kind of energy-saving brick for building and preparation method thereof |
| CN112142363A (en) * | 2020-10-10 | 2020-12-29 | 杭州瑞鼎建材有限公司 | Automatic shrinkage compensation efflorescence resistant concrete |
| CN114368959A (en) * | 2022-02-08 | 2022-04-19 | 邓晶晶 | Anti-impact corrosion-resistant ceramic tile and preparation method thereof |
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| CN112142363A (en) * | 2020-10-10 | 2020-12-29 | 杭州瑞鼎建材有限公司 | Automatic shrinkage compensation efflorescence resistant concrete |
| CN112142363B (en) * | 2020-10-10 | 2021-12-28 | 杭州瑞鼎建材有限公司 | Automatic shrinkage compensation efflorescence resistant concrete |
| CN114368959A (en) * | 2022-02-08 | 2022-04-19 | 邓晶晶 | Anti-impact corrosion-resistant ceramic tile and preparation method thereof |
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