CN107189595A - A kind of environment-friendly type road gage mark coating and preparation method thereof - Google Patents
A kind of environment-friendly type road gage mark coating and preparation method thereof Download PDFInfo
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- CN107189595A CN107189595A CN201710598658.0A CN201710598658A CN107189595A CN 107189595 A CN107189595 A CN 107189595A CN 201710598658 A CN201710598658 A CN 201710598658A CN 107189595 A CN107189595 A CN 107189595A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/346—Clay
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/101—Esters; Ether-esters of monocarboxylic acids
- C08K5/103—Esters; Ether-esters of monocarboxylic acids with polyalcohols
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/16—Solid spheres
- C08K7/18—Solid spheres inorganic
- C08K7/20—Glass
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
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Abstract
The present invention provides a kind of environment-friendly type road gage mark coating and preparation method thereof, and the coating is according to the composition of ratio of weight and number：35~53 parts of water-based acrylic resin, 0.02~0.05 part of bactericide, 0.7~0.9 part of defoamer, 0.6~0.7 part of dispersant, thicken 0.02~0.03 part of dispersant, 1~2 part of distilled water, 2~10 parts of titanium dioxide, 33~47 parts of inorganic filler, 0.01~0.02 part of wetting agent, 18~21 parts of glass microballoon, 4~5 parts of volatile solvent, 2~3 parts of film forming agent.Preparation method includes：Dispensing；It is in dispersion machine that water-based acrylic resin and part volatile solvent is uniform；Sequentially add bactericide, defoamer, dispersant, thickening dispersant and wetting agent well mixed；It is well mixed that titanium dioxide, inorganic filler and glass microballoon are added in batches；Sequentially add distilled water, remaining volatile solvent, film forming agent；After all raw materials are added, stir.
Description
Technical field
The present invention relates to chemistry painting industry field, and in particular to a kind of environment-friendly type road gage mark coating and preparation method thereof.
Background technology
One of Scientific And Technical development strategy during Modern Traffic infrastructure is national " 13 ", thus in lifting highway
Construction quality and maintenance level aspect are most important.Wherein, the major function of road traffic marking is guiding control vehicle in road
Safely travelled on road, roadmarking is the safety label of road traffic, be the important measures tightened traffic management；Reach raising
The purpose of road transport capacity, reduction accident and beautifying city road, the round-the-clock visibility of roadmarking, skid resistance are to weigh
The important indicator of road mark paint performance.China's expressway construction was in the period of developing rapidly in recent years.Draw road
The coating consumption of traffic marking surges, so the need for the high-performance gage mark coating of the suitable China's actual conditions of exploitation is reality.
Current road mark paint was divided into heat molten type and normal temperature type, mainly based on heat molten type, with 2014 years Chinese roads
Gage mark coating demand statistics shows that hot-melting road mark paint demand is 28.3 ten thousand tons, wherein being mainly used at a high speed
Highway, Class I highway and urban road；Normal temperature type gage mark coating demand is 4.6 ten thousand tons, wherein being mainly used in Class II highway.
Roadmarking material usage will keep continuous ascendant trend.But have to be mentioned that, hot melt type gage mark coating：Include oil tree
Fat, the chemical substance such as chromium class pigment, melting to 180~220 DEG C using liquefied natural gas heating could construct, and in melting process
The middle many toxic gases of discharge and carbon dioxide.The construction of heat molten type material is complicated, environment is unfriendly, driving comfort is poor.Normal temperature
Type gage mark coating：The organic solvent used can directly destroy nervous system, hematopoietic function, reproductive function and the hepatic injury of human body
At all it is not less than heavy metal Deng, its harmfulness.Therefore, the demand in terms of this invention combination present road gage mark coating, to sum up
Described, from the angle for showing loving care for road user, exploitation is very wide based on environment-friendly road mark paint application prospect.
The content of the invention
The problem of existing for prior art, the present invention provides a kind of environment-friendly type road gage mark coating and preparation method thereof,
The adhesive force of the road mark paint is strong, fast drying, have with glass microballoon that good adhesiveness, hardness be high, resistance to weather resistance is excellent
It is different, while bright in luster, nonpoisonous and tasteless, environmental protection, low-carbon energy-saving, weatherability, wear-resisting antiskid.Technical scheme
For：
A kind of environment-friendly type road gage mark coating, be according to the composition of ratio of weight and number：35~53 parts of water-based acrylic resin,
0.02~0.05 part of bactericide, 0.7~0.9 part of defoamer, 0.6~0.7 part of dispersant thickens 0.02~0.03 part of dispersant,
1~2 part of distilled water, 2~10 parts of titanium dioxide, 33~47 parts of inorganic filler, 0.01~0.02 part of wetting agent, glass microballoon 18~21
Part, 4~5 parts of volatile solvent, 2~3 parts of film forming agent.
Further, the water-based acrylic resin solid content is more than 40%.
Further, the dispersant uses polycarboxylate sodium's type dispersant.
Further, the inorganic filler be selected from kaolin, dicalcium powder, light calcium carbonate powder, talcum powder, without chlorine calcium carbonate, sulfuric acid
One or more in barium.
Further, the glass microballoon is the one or more in 40 mesh, 50 mesh, 60 mesh selected from mesh number.
Further, one or more of the volatile solvent in ammoniacal liquor, methanol, ethanol.
The preparation method of the environment-friendly type road gage mark coating, comprises the following steps：
(1) according to the ratio of weight and number dispensing of above-mentioned environment-friendly type road gage mark coating constituent；
(2) water-based acrylic resin and part volatile solvent are uniformly mixed in dispersion machine, wherein stirring speed
Spend for 400~600r/s；
(3) bactericide, defoamer, dispersant, thickening dispersant and wetting agent are sequentially added in dispersion machine, by stirring speed
Degree is promoted to 1000~1500r/s, is well mixed；
(4) titanium dioxide, inorganic filler and glass microballoon is added in batches in dispersion machine to be uniformly mixed；
(5) reduction mixing speed is to 700~900r/s, sequentially added in dispersion machine distilled water, remaining volatile solvent,
Film forming agent；
(6) after all raw materials are added, mixing speed is promoted to 1000~1100r/s, 15~30min is stirred.
Beneficial effects of the present invention are：The environment-friendly type road gage mark coating of the present invention is resistance to compared with hot-melting road mark
Wait property improve more than 1 times, abrasion resistance properties improve more than 50%, paint film will not become fragile, with bead adhesion improve 1 times with
On, with good nighttime visibility；While the adhesiveness of the environment-friendly type road gage mark coating of the present invention and oiliness bituminous paving
It is suitable with hot-melting road mark paint.In addition, the inventive method process is simple, using Multi-stage stirring mixed mode, prepare
The gage mark coating application prospect come is huge, is worth with stronger promotion and application.
Embodiment
In the description of the invention, it is necessary to explanation, unreceipted actual conditions person in embodiment, according to normal condition or
The condition of manufacturer's suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, are that can be obtained by commercially available purchase
Conventional products.
As long as in addition, technical characteristic involved in invention described below different embodiments non-structure each other
It can just be combined with each other into conflict.
The present invention is described in further details with reference to specific embodiment, it is described be explanation of the invention without
It is to limit.
Embodiment 1
The present embodiment provides a kind of environment-friendly type road gage mark coating, is according to the composition of ratio of weight and number：Solid content exists
35 parts of 45% water-based acrylic resin, 0.04 part of SJ-110 types bactericide, 0.9 part of organic silicon defoamer, OT-75 type dispersants
0.6 part, UH-450 types 0.03 part of dispersant of thickening, 2 parts of distilled water, 2 parts of rutile type titanium white, no 33 parts of chlorine calcium carbonate, ZX-
105 0.02 part of type wetting agents, 21 parts of glass microballoon, 4 parts of industrial grade benzenemethanol, 12 parts of film forming agent alcohol ester；Wherein glass microballoon
Mesh number is two kinds of 40 mesh and 50 mesh, is mixed by 4: 6 mass ratio.
The preparation method of the road mark paint, including：
(1) 35 parts and 2 parts methanol of acrylic emulsion are added into dispersion machine, start stirring, mixing speed is 500r/s,
It is well mixed；
(2) sequentially add 0.04 part of SJ-110 types bactericide, 0.9 part of organic silicon defoamer, 0.6 part of OT-75 types dispersant,
0.02 part of 0.03 part of UH-450 types thickening dispersant and ZX-105 types wetting agent, are promoted to 1500r/s by mixing speed, stir
20min, is well mixed；
(3) added in batches by 2 parts of rutile type titanium white, without 21 parts of 33 parts of chlorine calcium carbonate and glass microballoon, side edged
Keep 1500r/s rotating speed to stir, prevent caking；
(4) reduction rotating speed is slowly added to 2 parts of distilled water, remaining methanol, alcohol ester 12 according to this to 800r/s in dispersant
3 parts；
(5) after all material are added, mixing speed is promoted to 1000r/s, stirred 20 minutes.
Embodiment 2
The present embodiment provides a kind of environment-friendly type road gage mark coating, is according to the composition of ratio of weight and number：Solid content exists
52 parts of 40% water-based acrylic resin, 0.04 part of SJ-110 types bactericide, 0.9 part of organic silicon defoamer, 7423 type dispersants
0.7 part, RM-8W types 0.03 part of dispersant of thickening, 2 parts of distilled water, 2 parts of rutile type titanium white, 35 parts of dicalcium powder, cf-10 types
0.02 part of wetting agent, 21 parts of glass microballoon, 4 parts of technical grade ethanol, 12 parts of film forming agent alcohol ester；The wherein mesh number of glass microballoon
For two kinds of 40 mesh and 60 mesh, mixed by 4: 6 mass ratioes.
The preparation method of the road mark paint, including：
(1) 52 parts and 2 parts ethanol of acrylic emulsion are added into dispersion machine, start stirring, mixing speed is 500r/s,
It is well mixed；
(2) sequentially add 0.4 part of SJ-110 types bactericide, 0.9 part of organic silicon defoamer, 0.4 part of OT-75 types dispersant,
0.02 part of 0.03 part of UH-450 types thickening dispersant and ZX-105 types wetting agent, are promoted to 1500r/s by mixing speed, stir
20min, is well mixed；
(3) added in batches by 2 parts of rutile type titanium white, without 21 parts of 33 parts of chlorine calcium carbonate and glass microballoon, side edged
Keep 1500r/s rotating speed to stir, prevent caking；
(4) reduction rotating speed is slowly added to 2 parts of distilled water, remaining ethanol, alcohol ester 12 according to this to 800r/s in dispersant
3 parts；
(5) after all material are added, mixing speed is promoted to 1000r/s, stirred 20 minutes.
Embodiment 3
The present embodiment provides a kind of environment-friendly type road gage mark coating, is according to the composition of ratio of weight and number：Solid content exists
40 parts of 40% water-based acrylic resin, 1,277 0.03 part of type bactericide, 0.9 part of B-0224 types defoamer, 7423 type dispersants
0.7 part, RM-8W types 0.02 part of dispersant of thickening, 2 parts of distilled water, 10 parts of rutile type titanium white, 45 parts of talcum powder, ot-75 types
0.01 part of wetting agent, 21 parts of glass microballoon, 5 parts of technical grade ethanol, 12 parts of film forming agent alcohol ester；The wherein mesh number of glass microballoon
It is two kinds of 40 mesh and 60 mesh for the mesh number of wherein glass microballoon, is mixed by 4: 6 mass ratioes.
The preparation method of the environment-friendly type road gage mark coating, comprises the following steps：
(1) according to the ratio of weight and number dispensing of above-mentioned environment-friendly type road gage mark coating constituent；
(2) 2 parts of 40 parts of water-based acrylic resin and ethanol are uniformly mixed in dispersion machine, wherein mixing speed is
600r/s；
(3) 0.03 part of 1277 type bactericide, 0.9 part of B-0224 types defoamer, 7423 types point are sequentially added in dispersion machine
0.01 part of 0.7 part of powder, RM-8W types 0.02 part of dispersant of thickening and ot-75 types wetting agent, 1500r/ is promoted to by mixing speed
S, is well mixed；
(4) 10 parts of rutile type titanium white, 45 parts of talcum powder are added in batches in dispersion machine；
(5) reduction mixing speed sequentially adds 2 parts of distilled water, remaining ethanol, alcohol ester 12 to 900r/s in dispersion machine
3 parts；
(6) after all raw materials are added, mixing speed is promoted to 1100r/s, 30min is stirred.
Embodiment 4
The present embodiment provides a kind of environment-friendly type road gage mark coating, is according to the composition of ratio of weight and number：Solid content exists
42 parts of 55% water-based acrylic resin, 0.05 part of SJ-110 types bactericide, 0.8 part of ZX-X1011 types defoamer, FMA-15 types
0.6 part of dispersant, RM-8W types 0.02 part of dispersant of thickening, 2 parts of distilled water, 3 parts of rutile type titanium white, 40 parts of kaolin,
0.01 part of cf-10 types wetting agent, 20 parts of glass microballoon, 5 parts of technical grade ammoniacal liquor, 12 parts of film forming agent alcohol ester；Wherein glass microballoon
Mesh number be two kinds of 50 mesh and 60 mesh, by being spread outside 4: 6 mass fractions.
The preparation method of the environment-friendly type road gage mark coating, comprises the following steps：
(1) according to the ratio of weight and number dispensing of above-mentioned environment-friendly type road gage mark coating constituent；
(2) 2 parts of 42 parts of water-based acrylic resin and ammoniacal liquor are uniformly mixed in dispersion machine, wherein mixing speed is
400r/s；
(3) 0.05 part of SJ-110 types bactericide, 0.8 part of ZX-X1011 types defoamer, FMA- are sequentially added in dispersion machine
0.01 part of 15 0.6 part of type dispersants, RM-8W types 0.02 part of dispersant of thickening and cf-10 types wetting agent, mixing speed is promoted to
1300r/s, is well mixed；
(4) 3 parts of rutile type titanium white, 40 parts of kaolin are added in batches in dispersion machine；
(5) reduction mixing speed sequentially adds 2 parts of distilled water, remained ammonia, alcohol ester 12 to 800r/s in dispersion machine
3 parts；
(6) after all raw materials are added, mixing speed is promoted to 1100r/s, 30min is stirred.
Detection project is with result of the test with reference to shown in table one.
The detection project of table one and experimental result
Although embodiments of the invention have been shown and described above, it is to be understood that above-described embodiment is example
Property, it is impossible to limitation of the present invention is interpreted as, one of ordinary skill in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, changed, replacing and modification.
Claims (7)
1. a kind of environment-friendly type road gage mark coating, it is characterised in that the coating is according to the composition of ratio of weight and number：Aqueous third
35~53 parts of olefin(e) acid resin, 0.02~0.05 part of bactericide, 0.7~0.9 part of defoamer, 0.6~0.7 part of dispersant, thickening point
0.02~0.03 part of powder, 1~2 part of distilled water, 2~10 parts of titanium dioxide, 33~47 parts of inorganic filler, wetting agent 0.01~0.02
Part, 18~21 parts of glass microballoon, 4~5 parts of volatile solvent, 2~3 parts of film forming agent.
2. a kind of environment-friendly type road gage mark coating according to claim 1, it is characterised in that the water-based acrylic resin
Solid content is more than 40%.
3. a kind of environment-friendly type road gage mark coating according to claim 1, it is characterised in that the dispersant uses poly- carboxylic
Acid sodium-salt type dispersant.
4. a kind of environment-friendly type road gage mark coating according to claim 1, it is characterised in that the inorganic filler is selected from height
Ridge soil, dicalcium powder, light calcium carbonate powder, talcum powder, without the one or more in chlorine calcium carbonate, barium sulfate.
5. a kind of environment-friendly type road gage mark coating according to claim 1, it is characterised in that the glass microballoon is selected from mesh
Number is the one or more in 40 mesh, 50 mesh, 60 mesh.
6. a kind of environment-friendly type road gage mark coating according to claim 1, it is characterised in that the volatile solvent is selected from
One or more in ammoniacal liquor, methanol, ethanol.
7. a kind of preparation method of environment-friendly type road gage mark coating described in claim 1, it is characterised in that the preparation method
Comprise the following steps：
(1) according to the ratio of weight and number dispensing of above-mentioned environment-friendly type road gage mark coating constituent；
(2) water-based acrylic resin and part volatile solvent are uniformly mixed in dispersion machine, wherein mixing speed is
400~600r/s；
(3) bactericide, defoamer, dispersant, thickening dispersant and wetting agent are sequentially added in dispersion machine, mixing speed is carried
1000~1500r/s is risen to, is well mixed；
(4) titanium dioxide, inorganic filler and glass microballoon is added in batches in dispersion machine to be uniformly mixed；
(5) reduction mixing speed sequentially adds distilled water, remaining volatile solvent, film forming to 700~900r/s in dispersion machine
Agent；
(6) after all raw materials are added, mixing speed is promoted to 1000~1100r/s, 15~30min is stirred.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108192441A (en) * | 2018-01-08 | 2018-06-22 | 福建省康发高新科技有限公司 | A kind of environment-friendly type aqueous road mark paint and preparation method thereof |
| CN110157264A (en) * | 2019-05-06 | 2019-08-23 | 洛阳双瑞防腐工程技术有限公司 | A kind of environment-friendly type high abrasion waterborne road line paint and preparation method thereof |
| CN111349346A (en) * | 2020-04-26 | 2020-06-30 | 辽宁省交通科学研究院有限责任公司 | Multifunctional modified asphalt and preparation method thereof |
| CN112778863A (en) * | 2021-01-07 | 2021-05-11 | 辽宁省交通科学研究院有限责任公司 | Environment-friendly energy-storage self-luminous road marking paint and preparation method thereof |
| CN116445048A (en) * | 2022-01-07 | 2023-07-18 | 万华化学集团股份有限公司 | Preparation of single-component and quick-drying color anti-slip water-based paint and application of single-component and quick-drying color anti-slip water-based paint in slow running system |
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Application publication date: 20170922 |