CN107184407A - A kind of soft and smooth moisturizing granulates clean face powder and preparation method thereof - Google Patents
A kind of soft and smooth moisturizing granulates clean face powder and preparation method thereof Download PDFInfo
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- CN107184407A CN107184407A CN201710372872.4A CN201710372872A CN107184407A CN 107184407 A CN107184407 A CN 107184407A CN 201710372872 A CN201710372872 A CN 201710372872A CN 107184407 A CN107184407 A CN 107184407A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
Clean face powder is granulated the invention discloses a kind of soft and smooth moisturizing, is made up of the material of following parts by weight：10 60 parts of mannitol, 2 20 parts of sodium cocoyl glutamate, 2 20 parts of sodium lauroyl glutamate, 2 20 parts of myristoyl glutamate sodium, 3 20 parts of cocounut oil acyl isethionic acid ester sodium, 2 20 parts of cornstarch, 0.5 3 parts of tapioca, 0.3 3 parts of sodium chloride, 0.1 2 parts of hydroxypropyl methyl cellulose, 0.1 1 parts of dipotassium glycyrrhizinate, 0.05 0.3 parts of allantoin, 0.05 0.5 parts of polylysine, 0.02 0.2 parts of Sodium Hyaluronate, 0.05 0.3 parts of poly methyl silsesquioxane, 0.5 5 parts of purslane extract.The soft and smooth moisturizing of the present invention granulates clean face powder, using gentle amino acid surfactant as main cleaning agent, not powder spreading during use, particle water disintegration speed is fast, it is soft and smooth when using, gently skin and eyes are not stimulated, the function with cleaning and moisturizing, and the problem of solve clean face powder the moisture absorption is lumpd in placement process.The invention provides the preparation method that a kind of above-mentioned soft and smooth moisturizing granulates clean face powder simultaneously.
Description
Technical field
The present invention relates to personal care articles preparing technical field, and in particular to a kind of soft and smooth moisturizing granulates clean face powder and its system
Preparation Method.
Background technology
Clean skin always is a mostly important link of skin care.The skin of people, especially skin of face, the moment all with
External environment is in contact.The dust that is suspended in air, smog, microorganism, are all easily absorbing on our skins；Sebaceous glands point
The sebum secreted easily is decomposed after retaining for a long time by air oxidation and bacterium, is harmful to skin；Sweat evaporation can secrete solids
Thing etc. remains in skin surface, stimulates skin；The sebum of dead cell meeting that cuticula metabolism comes off and secretion, sweat with
And external dust is together, is attached on skin and generates dirt, the secretion of sebum and sweat, breed bacteria are hindered；To often cosmetic
People for, be coated in foundation cream, kermes, eye shadow, lipstick on the face etc. and be easily absorbing on skin.If skin cleaning is not thorough enough
Bottom, it is easy to trigger clogging of pores, skin water oil is unbalance, sensitiveness skin, skin ageing the problems such as.
Popular face cleaning product, is divided into soap base, table work, soap table compound system in the market, not special according to respective skin
Point differentiation is used, and easily makes cuticula thinning in the course of time, or even destruction skin barrier, becomes sensitive skin.Clean face powder is mesh
Product the gentleest in preceding cleaning class skin care item, while skin cleaning is helped, moreover it is possible to reduce the allergy rate of skin, by
Numerous women's pursues.Beauty market make rapid progress today, clean face powder be increasingly becoming irreplaceable clean skin product it
One.But clean face powder manufacturing technology in the market is to be uniformly mixed that (what is disclosed shows by powder material is fine ground mostly
There is technology to include CN104825376A, CN102475662A, CN103230350A, CN103446038A) or it is well mixed after mistake
Mesh sieve (prior art disclosed include CN105687054A, CN105596248A, CN105769729A) and be made, deposit
The problem of being settled between different solid powders because of density difference, the shortcomings of easily causing powder spreading when using.Amino acid
Face cleaning product is current more pro-skin, gentle face cleaning product, and not tight with rear skin, moisture-retaining capacity is strong, is that sensitive flesh is adapted to make
Cleaning products (existing prior art is CN105769729A, CN106309198A, CN106466235A).But amino acid
Surfactant foaminess and cleaning capacity are general.
The content of the invention
The invention aims to overcome the deficiencies in the prior art there is provided a kind of soft and smooth moisturizing to granulate clean face powder, with
Gentle amino acid surfactant is main cleaning agent, and not powder spreading during use, particle water disintegration speed is fast, soft when using
It is sliding, do not stimulate skin and eyes gently, the function with cleaning and moisturizing, and solve clean face powder moisture absorption knot in placement process
The problem of block.
Another object of the present invention is to provide the preparation method that a kind of above-mentioned soft and smooth moisturizing granulates clean face powder.
Realizing a kind of technical scheme of above-mentioned purpose is：A kind of soft and smooth moisturizing granulates clean face powder, includes the group of following parts by weight
Point：
A kind of above-mentioned soft and smooth moisturizing granulates clean face powder, wherein, the polylysine has bacteriostasis efficacy but being not belonging to
Cosmetic preservative.
A kind of above-mentioned soft and smooth moisturizing granulates clean face powder, wherein, the sodium cocoyl glutamate, sodium lauroyl glutamate and
Myristoyl glutamate sodium constitutes primary surfactant, and the primary surfactant is amino acid surfactant, the cocounut oil
Acyl isethionic acid ester sodium is cosurfactant, and the ratio of the primary surfactant and cosurfactant is 2:1.
Present invention also offers the preparation method that a kind of soft and smooth moisturizing granulates clean face powder, comprise the following steps：
A, preparation process：Formula according to claim 1 weighs each component material, and wherein solid material uses xeraphium
Last shape material, liquid material is added in binder solution after weighing and is well mixed；
B, dispersion steps：All powder shape material is put into fluid bed, powder material is blown out into fluidisation using air intake
State, room temperature air intake, fluidization dispersions 20min；
C, granulation step：The EAT of fluid bed is set as 60 DEG C, intake velocity is controlled in 700-1000m3/ h, is used
Top spray technique is blended with the binder solution of liquid material and is atomized and is sprayed onto with 1 part/min sample introduction speed to be in fluidisation shape
On powder material under state；
D, drying steps：It is mixed with after the binder solution of liquid material sprayed, continuation is entered under 60 DEG C of EAT
Distinguished and admirableization 30min, dried material；
E, sifting step：Dried material is sieved, soft and smooth moisturizing is produced and granulates clean face powder.
Above-mentioned soft and smooth moisturizing is granulated in the preparation method of clean face powder, step A, and described adhesive solution is adopted as 0.1%
The cornstarch aqueous solution of mass fraction, binder solution is used for the growth and shaping of particle during fluidization granulation；
In step C, the binder solution for being mixed with liquid material is divided into 30 parts, and liquids are blended with top spray technique
The binder solution of material is atomized and is sprayed onto on the powder material being under fluidized state with 1 part/min sample introduction speed, is glued
Moisture in mixture solution is finally removed by drying and volatilizing.
Above-mentioned soft and smooth moisturizing is granulated in the preparation method of clean face powder, step E, and the soft and smooth moisturizing after sieving granulates clean face powder
Grain diameter be the mesh of 20 mesh -100, and apparent density be 0.41 ± 0.05g/ml.
A kind of soft and smooth moisturizing for employing the present invention granulates the technical scheme of clean face powder, compared with prior art, and existing
Technology is compared, and is had the advantages that：
(1) soft and smooth moisturizing of the invention granulates clean face powder, and particle is uniform, and not stratified, not powder spreading during use, particle is met
Water disintegration is fast；
(2) soft and smooth moisturizing of the invention granulates clean face powder, no soap base, no sensitization preservative, the sensitization such as without essence, pigment into
Point, by acute skin irritation test and acute eye irritation test, releive gentle；
(3) soft and smooth moisturizing of the invention granulates clean face powder, and cleaning capacity is good, and moistening effect is good, is moistened with rear skin, soft
It is sliding, not tight, non-scale.
(4) soft and smooth moisturizing of the invention granulates clean face powder, and moisture absorption caking is difficult during the storage behind Kaifeng, constant
Color, solves moisture absorption caking phenomenon during most clean face powder uses on the market.
(5) soft and smooth moisturizing of the invention granulates clean face powder, controls product apparent density, it is ensured that in various packing specifications
In versatility.
(6) soft and smooth moisturizing of the invention granulates clean face powder, by the ratio of primary surfactant and cosurfactant,
The problem of solving general amino acid surfactant foaminess and not enough cleaning capacity, without as needing to coordinate soap base to carry in the past
The safety risks for rising foam effect and cleaning capacity and bringing.
The technical scheme of the preparation method of clean face powder is granulated using a kind of soft and smooth moisturizing of the present invention, is overcome in the market
Clean face powder manufacturing technology shortcoming, be not susceptible to settlement issues, and be not easy to cause powder spreading when using.
Brief description of the drawings
Fig. 1 granulates clean face powder and the moisture absorption test result figure of commercially available prod for the soft and smooth moisturizing of the present invention；
Fig. 2 granulates clean face powder and the foam performance test result figure of commercially available prod for the soft and smooth moisturizing of the present invention；
Fig. 3 granulates the Analyses Methods for Sensory Evaluation Results figure of clean face powder for the soft and smooth moisturizing of embodiment 1；
Fig. 4 granulates the Analyses Methods for Sensory Evaluation Results figure of clean face powder for the soft and smooth moisturizing of embodiment 2.
Embodiment
The present inventor is in order to be able to preferably understand technical scheme, below by specifically real
Apply example and be described in detail with reference to accompanying drawing：
Table 1
The soft and smooth moisturizing that raw material proportioning according to table 1 prepares embodiment 1-3 granulates clean face powder.
In above-mentioned raw materials：Mannitol trade name mannitol, producer Luo Gaite Lianyun Harbour Co., Ltd；Cocounut oil acyl paddy
Propylhomoserin sodium trade name Eversoft UCS-100S, Nanjing Huashi Chemical Co., Ltd. of producer；Sodium lauroyl glutamate trade name
For AMISOFT LS-11, Ajincomoto Co., Inc of producer；Myristoyl glutamate sodium trade name AMISOFT MS-11, producer
Ajincomoto Co., Inc；Cocounut oil acyl isethionic acid ester sodium trade name Elfan AT 84, producer Akzo Nobel；Corn forms sediment
Powder trade name PURITY 21C PURE, producer Akzo Nobel；Tapioca and poly methyl silsesquioxane trade name
DRY-FLO TS PURE, producer Akzo Nobel；Sodium chloride trade name sodium chloride, the prosperous and powerful functionalized chemical share in producer Jiangsu
Co., Ltd；Hydroxypropyl methyl cellulose trade name METHOCEL 40-0202, Dow Chemical of producer；Dipotassium glycyrrhizinate
Trade name dipotassium glycyrrhizinate, producer Beijing and Zheng Tang bio tech ltd；Allantoin trade name ALLANTOIN, factory
Clariant Chemical Group company of family；Polylysine trade name Everguard PL, Nanjing Huashi Chemical Co., Ltd. of producer；Thoroughly
The sour sodium trade name HA-TLM20-40 of bright matter, Fu Ruida Pharmaceutical Groups company of producer；Purslane extract (liquid), Kunming shellfish
Prepared by Tai Ni bio tech ltd research and development laboratory extracts.
The soft and smooth moisturizing that the present invention is provided granulates clean face powder and prepared by following steps：
A, preparation process：Each component material is weighed according to formula, wherein solid material uses dry powdered material, liquid
Add in binder solution and be well mixed after body material weighing is good；The corn that binder solution is adopted as 0.1% mass fraction forms sediment
Amidin, the binder solution for being mixed with liquid material is divided into 30 parts；
B, dispersion steps：All powder shape material is put into fluid bed, powder material is blown out into fluidisation using air intake
State, room temperature air intake, fluidization dispersions 20min；
C, granulation step：The EAT of fluid bed is set as 60 DEG C, intake velocity is controlled in 700-1000m3/ h, is used
Top spray technique is blended with the binder solution of liquid material and is atomized and is sprayed onto with 1 part/min sample introduction speed to be in fluidisation shape
On powder material under state；
D, drying steps：It is mixed with after the binder solution of liquid material sprayed, continuation is entered under 60 DEG C of EAT
Distinguished and admirableization 30min, dried material；
E, sifting step：Dried material is sieved, soft and smooth moisturizing is produced and granulates clean face powder.Soft and smooth moisturizing granulation after sieving
The grain diameter of clean face powder is the mesh of 20 mesh -100, and apparent density is 0.41 ± 0.05g/ml.
Binder solution is used for the growth and shaping of particle during fluidization granulation, the final quilt of the moisture in binder solution
Drying and volatilizing and remove.
When the soft and smooth moisturizing for preparing embodiment 1 granulates clean face powder, the intake velocity in step C is controlled in 700m3/h；Prepare
When the soft and smooth moisturizing of embodiment 2 granulates clean face powder, the intake velocity in step C is controlled in 1000m3/h；Prepare the soft of embodiment 3
When sliding moisturizing granulates clean face powder, the intake velocity in step C is controlled in 800m3/h。
Security test：
Soft and smooth moisturizing to the above-mentioned embodiment 1-3 prepared granulates clean face powder progress security test, including acute skin
Skin irritant test and acute eye irritation test, tested material：Embodiment 1, is tested after being uniformly dispersed with the pure water of 50% mass fraction；
Embodiment 2, is tested after being uniformly dispersed with the pure water of 50% mass fraction；Embodiment 3, it is scattered equal with the pure water of 50% mass fraction
Tested after even：
(1) acute skin irritation test：
Soft and smooth moisturizing to embodiment 1, embodiment 2, embodiment 3 granulates clean face powder progress acute skin irritation test, often
Individual embodiment selects 4 albino guinea-pigs to be tested, and tests room temperature：20-24 DEG C, relative humidity：60-70%.Before experiment
About 24h, experimental animal back backbone both sides hair is cut, and unhairing scope is respectively 2cm × 3cm, and application area 2.5cm ×
2.5cm.Tested material about 0.5mL is taken to be applied on the skin of side, when tested material is prepared using nonirritant solvent, opposite side is applied
Solvent is smeared 1 time daily as control, continuous to smear 14 days.Since second day, cropping is answered before smearing every time, with water or nothing
Excitant solvent cleaning remains tested material, and result is observed after one hour.Reference《Cosmetics safety technical specification》(version in 2015)
Regulation carries out stimulate the reaction scoring.Acute skin irritation test result is as shown in table 2：
Table 2
From the acute skin irritation test result of table 2, embodiment 1, embodiment 2, the clean face powder pair of granulation of embodiment 3
The acute skin irritation test of cavy, is showed no irritative response.Therefore a kind of soft and smooth moisturizing of the present invention granulates clean face powder, anxious
Property Skin Irritation Test result shows no skin irritation.
(2) acute eye irritation test
Soft and smooth moisturizing to embodiment 1, embodiment 2, embodiment 3 granulates clean face powder progress acute eye irritation test, each
Embodiment selects 3 healthy adult white rabbits to be tested, and tests room temperature：20-24 DEG C, relative humidity：60-70%.
Animal will at least adapt to 3 day time in experimental animal room environment before experiment.A palpebra inferior for hairy rat side eyes is gently pulled open,
Tested material 0.1mL (100mg) is instilled in (or being painted into) conjunctival sac, upper and lower eyelid is passively closed 1s, to prevent tested material from losing
Lose.Opposite side eyes, which are not handled, makees own control.After instilling tested material eyes are not rinsed in 24 hours.If thinking necessary, in 24h
When can be rinsed.If above-mentioned result of the test shows that tested material is irritant, it need to select else and effect examination is rinsed with 3 rabbit
Test, i.e., to rabbit eyes instill after tested material 30s with enough, flow velocity it is very fast but will not cause the current of animal eye injury rinse to
Few 30s.1 after tested material is instilled, 24,48,72 hours and the 4th drop and the 7th drop checked animal eyes.If 72 is small
When do not occur stimulate the reaction, you can termination test.If it find that involving cornea or there are other Eye irritations to act on, do not recover in 7 days
Person, to determine that the invertibity or irreversibility of the infringement need to extend observing time, is usually no more than 21 days.Reference《Cosmetics are defended
Raw specification (2007 editions)》Regulation carries out stimulate the reaction scoring.Acute eye irritation test result is as shown in table 3：
Table 3
From the acute ocular stimulation test result of table 3, embodiment 1, embodiment 2, embodiment 3 soft and smooth moisturizing granulation it is clean
Eye irritation experiment of the face powder to rabbit has no irritative response.Therefore a kind of soft and smooth moisturizing of the present invention granulates clean face powder, anxious
Property eye irritant test show without acute eye irritation.
The moisture absorption is tested：
The soft and smooth moisturizing of embodiment 1, embodiment 2, embodiment 3 is granulated into clean face powder and commercially available prod 1 (not granulating), it is commercially available
Product 2 (not granulating) each 3.00g is put into 50g clean medical PET bottle, without bottle cap, and room temperature lower open mouth is placed 2 weeks records and inhaled
Water rate (%).Water absorption rate (%)=(example weight-sample original weight)/sample original weight * 100%.
Commercially available prod 1 is does not granulate the clean face powder of amino acid soap base, and commercially available prod 2 is does not granulate the clean face powder of soap base, and the moisture absorption is surveyed
Test result is as shown in Figure 1：
By Fig. 1 moisture absorption test result, embodiment 1, embodiment 2, the soft and smooth moisturizing of embodiment 3 granulate clean face powder, room temperature
The lower moisture absorption situation placed of opening wide is substantially better than the commercially available prod not granulated.
Agglomeration resistance is tested：
The soft and smooth moisturizing of embodiment 1, embodiment 2, embodiment 3 is granulated into clean face powder and commercially available prod 1, commercially available prod 2 each
20.0g is put into 80g clean medical PET bottle, screws bottle cap, 90 days observation caking situations is deposited at room temperature, commercially available prod 1 is
The clean face powder of amino acid soap base is not granulated, and commercially available prod 2 is does not granulate the clean face powder of soap base, and test result is as shown in table 4：
Table 4
As shown in Table 4, embodiment 1, embodiment 2, the soft and smooth moisturizing of embodiment 3 granulate clean face powder, after depositing 90 days, no knot
Block phenomenon, commercially available non-granulation product 1 and 2 has obvious caking phenomenon.
Foam performance is tested：
The soft and smooth moisturizing of embodiment 1, embodiment 2, embodiment 3 is granulated into clean face powder and commercially available prod 1, commercially available prod 2, ginseng
Examine《Surfactant detergent test method》(GB/T 13173-2008) carries out foam performance test, and commercially available prod 1 is not make
The grain clean face powder of amino acid soap base, commercially available prod 2 is does not granulate the clean face powder of soap base, and foam performance test result is as shown in Figure 2.
As shown in Figure 2：The foam height of embodiment 1 is 135.5mm, and the foam height of embodiment 2 is 148.5mm, and embodiment 3 is steeped
Foam is highly 143.0mm, and the foam height of commercially available prod 1 is 89.0mm, and the foam height of commercially available prod 2 is 163.0mm.Embodiment 1,
Embodiment 2, the soft and smooth moisturizing of embodiment 3, which granulate clean face powder, good foam performance, and embodiment 2 is better than embodiment 1 and in fact
Apply example 3.
Sense organ investigation test and appraisal：
The soft and smooth moisturizing of embodiment 1 and embodiment 2 is granulated into clean face powder, by special sensory evaluation survey team personnel's group
Sense organ investigation test and appraisal are knitted, 38 crowds on probation with certain sensory evaluation experience are chosen, the range of age is between 18-50 Sui.
Application method：Face first is soaked with clear water, this product 0.2-0.4g is taken in the centre of the palm, plus a little clear water is looped and rubs molten with the hands, is rubbed abundant
After foam, face is massaged in the way of softly looping, is finally cleaned with clear water.Sooner or later it is each daily to use 1 time, use 1 week
Post analysis investigation result.Evaluation result uses marking system, and full marks are 15 points.
The soft and smooth moisturizing of embodiment 1 granulates the Analyses Methods for Sensory Evaluation Results of clean face powder as shown in figure 3, from the figure 3, it may be seen that embodiment 1
Soft and smooth moisturizing granulate clean face powder, gentle to moisten, feel is soft and smooth in use, easily rinses, and foaming characteristic and foam volume are good, use rear flesh
Skin is soft and smooth, and no tight feeling, moisturizing sense is good.
The soft and smooth moisturizing of embodiment 2 granulates the Analyses Methods for Sensory Evaluation Results of clean face powder as shown in figure 4, as shown in Figure 4, embodiment 2
Soft and smooth moisturizing granulate clean face powder, cleaning capacity is good, and foaming characteristic is good in use, foaming abundancy, salubrious easily to rinse, and uses rear skin
Soft and smooth high resilience, no tight feeling, moisturizing sense is preferable.
From above test result, soft and smooth moisturizing of the invention granulates clean face powder, and product is stable, with gentle amino acid
Surfactant is main cleaning agent, and not powder spreading during use, particle water disintegration speed is fast, soft and smooth when using, and does not pierce gently
Swash skin and eyes, the function with cleaning and moisturizing, and the problem of solve clean face powder the moisture absorption is lumpd in placement process.
The soft and smooth moisturizing of the present invention granulates the preparation method of clean face powder, overcomes lacking for clean face powder manufacturing technology in the market
Point, is not susceptible to settlement issues, and is not easy to cause powder spreading when using.
Those of ordinary skill in the art it should be appreciated that the embodiment of the above be intended merely to explanation the present invention,
And be not used as limitation of the invention, as long as in the spirit of the present invention, the change to embodiment described above
Change, modification will all fall in the range of claims of the present invention.
Claims (6)
1. a kind of soft and smooth moisturizing granulates clean face powder, it is characterised in that include the component of following parts by weight：
2. a kind of soft and smooth moisturizing as claimed in claim 1 granulates clean face powder, it is characterised in that the polylysine has antibacterial
Effect but it is not belonging to cosmetics preservative.
3. a kind of soft and smooth moisturizing as claimed in claim 1 granulates clean face powder, it is characterised in that the sodium cocoyl glutamate,
Sodium lauroyl glutamate and myristoyl glutamate sodium constitute primary surfactant, and the primary surfactant is amino acid surface
Activating agent, the cocounut oil acyl isethionic acid ester sodium is cosurfactant, the primary surfactant and cosurfactant
The ratio of agent is 2:1.
4. a kind of soft and smooth moisturizing as claimed in claim 1 granulates the preparation method of clean face powder, it is characterised in that including following step
Suddenly：
A, preparation process：Formula according to claim 1 weighs each component material, and wherein solid material is using dry powdered
Material, liquid material is added in binder solution after weighing and is well mixed；
B, dispersion steps：All powder shape material is put into fluid bed, powder material is blown out into fluidized state using air intake,
Room temperature air intake, fluidization dispersions 20min；
C, granulation step：The EAT of fluid bed is set as 60 DEG C, intake velocity is controlled in 700-1000m3/ h, uses top spray
Technique is blended with the binder solution of liquid material and is atomized and is sprayed onto with 1 part/min sample introduction speed to be under fluidized state
Powder material on；
D, drying steps：It is mixed with after the binder solution of liquid material sprayed, continues the air intake under 60 DEG C of EAT
Change 30min, dried material；
E, sifting step：Dried material is sieved, soft and smooth moisturizing is produced and granulates clean face powder.
5. soft and smooth moisturizing as claimed in claim 4 granulates the preparation method of clean face powder, it is characterised in that in step A, described viscous
Mixture solution is adopted as the cornstarch aqueous solution of 0.1% mass fraction, and binder solution is used for particle during fluidization granulation
Growth and shaping；
In step C, the binder solution for being mixed with liquid material is divided into 30 parts, and liquid material is blended with top spray technique
Binder solution is atomized and is sprayed onto on the powder material being under fluidized state, adhesive with 1 part/min sample introduction speed
Moisture in solution is finally removed by drying and volatilizing.
6. soft and smooth moisturizing as claimed in claim 4 granulates the preparation method of clean face powder, it is characterised in that in step E, after sieving
Soft and smooth moisturizing to granulate the grain diameter of clean face powder be the mesh of 20 mesh -100, and apparent density is 0.41 ± 0.05g/ml.
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| CN112274467A (en) * | 2020-10-30 | 2021-01-29 | 广东丸美生物技术股份有限公司 | Mild moisturizing face cleansing powder and preparation method thereof |
| CN113081886A (en) * | 2021-04-15 | 2021-07-09 | 南京泛成生物科技有限公司 | Alkyl polyglycoside solid preparation, preparation method and application |
| CN113318027A (en) * | 2021-06-15 | 2021-08-31 | 何平蓉 | Mild oil-control acne-removing facial cleansing composition and preparation method thereof |
| CN115804742A (en) * | 2022-12-22 | 2023-03-17 | 花安堂生物科技集团有限公司 | Face cleaning powder and preparation method thereof |
| WO2024112980A1 (en) * | 2022-11-28 | 2024-06-06 | Dendra Gmbh | Cleaning agent with granulate particles |
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| CN108486855B (en) * | 2018-03-20 | 2020-07-31 | 石狮市万峰盛漂染织造有限公司 | Composition for woven fabric de-dyeing one-bath process and preparation method thereof |
| CN112274467A (en) * | 2020-10-30 | 2021-01-29 | 广东丸美生物技术股份有限公司 | Mild moisturizing face cleansing powder and preparation method thereof |
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