CN107142550B - A kind of preparation method of the fiber of thread sliding underwear fabric - Google Patents

A kind of preparation method of the fiber of thread sliding underwear fabric Download PDF

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Publication number
CN107142550B
CN107142550B CN201710435285.5A CN201710435285A CN107142550B CN 107142550 B CN107142550 B CN 107142550B CN 201710435285 A CN201710435285 A CN 201710435285A CN 107142550 B CN107142550 B CN 107142550B
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fiber
composite fibre
preparation
underwear fabric
sliding
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CN201710435285.5A
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CN107142550A (en
Inventor
唐卫兵
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Foshan Fuda Asset Investment Co ltd
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Chongqing Admiration Garment Co Ltd
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/12Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00Chemical after-treatment of artificial filaments or the like during manufacture
    • D01F11/04Chemical after-treatment of artificial filaments or the like during manufacture of synthetic polymers
    • D01F11/08Chemical after-treatment of artificial filaments or the like during manufacture of synthetic polymers of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/14Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The preparation method of the fiber of a kind of proposed by the present invention sliding underwear fabric, the following steps are included: S1: by polyamide and polyester heating fusing, obtain mixed molten liquid, keep temperature, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder are added into mixed molten liquid, is uniformly mixed up to composite fibre melt;S2: composite fibre melt is subjected to spinning in spinning machine, then cured, cooling to get nascent composite fibre;S3: nascent composite fibre is immersed in flexibility agent, and ultrasonic in Ultrasound Instrument, then the nascent composite fibre after ultrasound is placed in ethanol solution and is impregnated, then through drip liquid, program drying to get finished product.Preparation method proposed by the present invention, production process is simple, and fibrous raw material easily mixes, and softening effect is good, and drying rate is fast, and harmless to fiber, and manufactured fiber is not easy to break, soft, cunning is glutinous, not wrinkled.

Description

A kind of preparation method of the fiber of thread sliding underwear fabric
Technical field
The present invention relates to dress materials technical field more particularly to the preparation methods of the fiber of a kind of sliding underwear fabric.
Background technique
Underwear refers to the personal clothing worn, including vest, undershirt, shorts, brassiere etc., usually directly contacts skin, It is indispensable one of the dress ornament of modern.With the improvement of people's life quality, requirement of the people to clothes comfort level is also more next Higher, especially underwear, in direct contact with the skin, wearer feels most sensitive to underwear comfort level.
The underwear fabric of commercial type is mainly cotton, nylon and spandex, and wherein the stability of cotton is preferable, but pliability and Feel is poor compared with nylon and spandex, and creases easily, and the comfort level of nylon and Lycra is more excellent, but nylon and Lycra fabric are to the stabilization of light Property is poor, and the long-term irradiation through sunlight is easily turned to be yellow discoloration in use, and the heat resistance of nylon and Lycra fabric is equal It is bad.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of sliding underwear fabric proposed The preparation method of fiber.
A kind of preparation method of the fiber of thread sliding underwear fabric, comprising the following steps:
S1: polyamide and polyester slice are placed in melting machine and heat fusing, obtained mixed by the preparation of composite fibre melt Melt is closed, the temperature of melting machine is kept, sequentially adds septichen phenyl ester, micro- into mixed molten liquid under stirring conditions Spar wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and superfine silicon dioxide Powder is uniformly mixed up to composite fibre melt;
S2: composite fibre melt prepared by S1 step is placed in spinning machine and carries out spinning by the preparation of nascent composite fibre, Cured again, 30 DEG C of 20~40min of vacuum cooled, and vacuum pressure in 4MPa hereinafter, up to nascent composite fibre;
S3: the post-processing of nascent composite fibre, nascent composite fibre prepared by S2 step are immersed in flexibility agent, and 10~20min of ultrasound in Ultrasound Instrument, then the nascent composite fibre after ultrasound is placed in 5~10min of immersion in ethanol solution, then pass through Drip liquid, the fiber of underwear fabric is slided in program drying to get silk.
Preferably, the spinning speed in the spinning is 1500~2000m/min, and spinneret hole count is 500~800 holes.
Preferably, the polyamide, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, tristearin Sour magnesium, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder weight part ratio be 38~46:42~ 58:3~8:1~3:0.5~1.5:1.5~3:1.5~3:1.2~2.8:2~4:0.2~0.6:4.8~6.8.
Preferably, the polyamide, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, tristearin Sour magnesium, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder weight part ratio be 42:50:5:2:1: 2:2:2.2:3:0.4:5.6.
Preferably, the solid content of the polyamide is 80% or more, and the solid content of the polyester is 85% or more.
Preferably, cured temperature is 100~120 DEG C in the S2 step, and curing time is 60~120min.
Preferably, the program that program is dried in the S3 step are as follows: 0~5min, 30~45 DEG C, 5~10min, 50~65 DEG C, 10~20min, 70~90 DEG C, 20~60min, 70~90 DEG C.
Preferably, flexibility agent is epoxy silicones oil, methylol silicone oil and stearic acid polyethylene glycol in the S3 step The mixture of ester, and the weight percent of epoxy group silicone oil, methylol silicone oil and stearic acid macrogol ester is 30%~45%: 40%~50%:5%~30%.
The preparation method of fiber proposed by the present invention, production process is simple, and fibrous raw material easily mixes, manufactured composite fibre Performance uniformity, it is not easy to break, soft, sliding glutinous, it is not wrinkled, and resistance to mild fast light effect is good, with polyamide and gathers Ester makes fiber with having excellent pliability collectively as the primary raw material of fiber, while adding o-hydroxy in the feed Phenyl formate can reduce fiber destruction of the sunlight middle-ultraviolet lamp to fiber in use, prolong the service life of fiber It is long, and generation the phenomenon that avoid yellowing of fibers, add microcrystalline wax, calcium stearate and magnesium stearate in the feed, three can be with Synergistic effect is played, the workability of raw material is improved, and assists the dispersion of superfine silicon dioxide in raw material, and then make the ratio of fiber Surface area increases, and improves the tensile strength of fiber, keeps fiber not easy to break;It will be immersed in flexibility agent during the preparation process Fiber is placed in ultrasound in Ultrasound Instrument, and the softening effect of flexibility agent can be improved, then is carried out by the way of temperature programming to fiber Drying, not only can be to avoid the damage being rapidly heated to fiber, but also can accelerate the drying rate of fiber.
Specific embodiment
The present invention is further explained in the light of specific embodiments.
Embodiment one
The preparation method of the fiber of a kind of proposed by the present invention sliding underwear fabric, comprising the following steps:
S1: polyamide and polyester slice are placed in melting machine and heat fusing, obtained mixed by the preparation of composite fibre melt Melt is closed, the temperature of melting machine is kept, sequentially adds septichen phenyl ester, micro- into mixed molten liquid under stirring conditions Spar wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and superfine silicon dioxide Powder is uniformly mixed up to composite fibre melt;
S2: composite fibre melt prepared by S1 step is placed in spinning machine and carries out spinning by the preparation of nascent composite fibre, Spinning speed is 2000m/min, and spinneret hole count is 500 holes, then through 110 DEG C of solidification 90min, 30 DEG C of vacuum cooled 30min, and true Pneumatics power is in 4MPa hereinafter, up to nascent composite fibre;
S3: the post-processing of nascent composite fibre, nascent composite fibre prepared by S2 step are immersed in flexibility agent, and Ultrasound 20min in Ultrasound Instrument, then the nascent composite fibre after ultrasound is placed in ethanol solution and impregnates 10min, then through dripping liquid, journey Fiber of the sequence drying to get the sliding underwear fabric of silk, the program of described program drying are as follows: temperature rises to 40 DEG C when 5min, the Temperature rises to 60 DEG C when 10min, and temperature rises to 80 DEG C when 20min, and temperature is still 80 DEG C when 60min.
It is the polyamide, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, hard in the present invention Fatty acid magnesium, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder weight part ratio be 46:58:8:1: 1:3:2:2:2~4:0.5:6;The flexibility agent is epoxy silicones oil, methylol silicone oil and stearic acid macrogol ester Mixture, and the weight percent of epoxy group silicone oil, methylol silicone oil and stearic acid macrogol ester is described in 45%:50%:5% The solid content of polyamide is 80% or more, and the solid content of the polyester is 85% or more.
Embodiment two
The preparation method of the fiber of a kind of proposed by the present invention sliding underwear fabric, comprising the following steps:
S1: polyamide and polyester slice are placed in melting machine and heat fusing, obtained mixed by the preparation of composite fibre melt Melt is closed, the temperature of melting machine is kept, sequentially adds septichen phenyl ester, micro- into mixed molten liquid under stirring conditions Spar wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and superfine silicon dioxide Powder is uniformly mixed up to composite fibre melt;
S2: composite fibre melt prepared by S1 step is placed in spinning machine and carries out spinning by the preparation of nascent composite fibre, Spinning speed is 1500m/min, and spinneret hole count is 800 holes, then through 100 DEG C of solidification 120min, 30 DEG C of vacuum cooled 20min, and Vacuum pressure is in 4MPa hereinafter, up to nascent composite fibre;
S3: the post-processing of nascent composite fibre, nascent composite fibre prepared by S2 step are immersed in flexibility agent, and Ultrasound 20min in Ultrasound Instrument, then the nascent composite fibre after ultrasound is placed in ethanol solution and impregnates 5min, then through dripping liquid, journey Fiber of the sequence drying to get the sliding underwear fabric of silk, the program of described program drying are as follows: temperature rises to 30 DEG C when 5min, the Temperature rises to 50 DEG C when 10min, and temperature rises to 70 DEG C when 20min, and temperature is still 70 DEG C when 60min.
It is the polyamide, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, hard in the present invention Fatty acid magnesium, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder weight part ratio be 46:42:8:2: 1.5:1.5:3:2.8:3:0.2:5;The flexibility agent is epoxy silicones oil, methylol silicone oil and stearic acid macrogol ester Mixture, and the weight percent of epoxy group silicone oil, methylol silicone oil and stearic acid macrogol ester is 30%:50%:20% institute The solid content for stating polyamide is 80% or more, and the solid content of the polyester is 85% or more.
Embodiment three
The preparation method of the fiber of a kind of proposed by the present invention sliding underwear fabric, comprising the following steps:
S1: polyamide and polyester slice are placed in melting machine and heat fusing, obtained mixed by the preparation of composite fibre melt Melt is closed, the temperature of melting machine is kept, sequentially adds septichen phenyl ester, micro- into mixed molten liquid under stirring conditions Spar wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and superfine silicon dioxide Powder is uniformly mixed up to composite fibre melt;
S2: composite fibre melt prepared by S1 step is placed in spinning machine and carries out spinning by the preparation of nascent composite fibre, Spinning speed is 2000m/min, and spinneret hole count is 800 holes, then through 120 DEG C of solidification 90min, 30 DEG C of vacuum cooled 40min, and true Pneumatics power is in 4MPa hereinafter, up to nascent composite fibre;
S3: the post-processing of nascent composite fibre, nascent composite fibre prepared by S2 step are immersed in flexibility agent, and 10~20min of ultrasound in Ultrasound Instrument, then the nascent composite fibre after ultrasound is placed in 5~10min of immersion in ethanol solution, then pass through Drip the fiber of liquid, program drying to get the sliding underwear fabric of silk, the program of described program drying are as follows: temperature rises to 45 when 5min DEG C, temperature rises to 65 DEG C when 10min, and temperature rises to 90 DEG C when 20min, and temperature is still 90 DEG C when 60min.
It is the polyamide, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, hard in the present invention Fatty acid magnesium, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder weight part ratio be 40:52:5:2: 1:2:2:2.5:3:0.4:5.8;The flexibility agent is epoxy silicones oil, methylol silicone oil and stearic acid macrogol ester Mixture, and the weight percent of epoxy group silicone oil, methylol silicone oil and stearic acid macrogol ester is described in 40%:45%:15% The solid content of polyamide is 80% or more, and the solid content of the polyester is 85% or more.
The fiber and commercially available fiber prepare to above-described embodiment one~tri- carries out performance detection, and testing result is as follows:
Performance test results show that the heat resistance of fiber prepared by embodiment one~tri- is good, in 100 DEG C of at a temperature of 4h On fiber without influence, and commercial articles obviously wrinkle, and fabric hand prepared by embodiment one~tri- is also superior to commercial articles; The tensile strength of the tensile strength fiber that as the result is shown prepared by embodiment one~tri- is high, not easy to break;Ultraviolet light irradiation is surveyed The fiber light fastness that test result shows prepared by embodiment one~tri- is good.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (8)

1. the preparation method of the fiber of a kind of sliding underwear fabric, which comprises the following steps:
S1: polyamide and polyester slice are placed in melting machine and heat fusing by the preparation of composite fibre melt, must be mixed molten Liquid keeps the temperature of melting machine, sequentially adds septichen phenyl ester, microlite into mixed molten liquid under stirring conditions Wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index regulator, light stabilizer and microfine silica powder, It is uniformly mixed up to composite fibre melt;
S2: composite fibre melt prepared by S1 step is placed in spinning machine and carries out spinning, then passes through by the preparation of nascent composite fibre Solidification, 30 DEG C of 20~40min of vacuum cooled, and vacuum pressure in 4MPa hereinafter, up to nascent composite fibre;
S3: the post-processing of nascent composite fibre, nascent composite fibre prepared by S2 step are immersed in flexibility agent, and in ultrasound 10~20min of ultrasound in instrument, then the nascent composite fibre after ultrasound is placed in 5~10min of immersion in ethanol solution, then through dripping Liquid, program drying slide the fiber of underwear fabric to get silk.
2. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the spinning In spinning speed be 1500~2000m/min, spinneret hole count be 500~800 holes.
3. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the polyamides Amine, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index tune The weight part ratio for saving agent, light stabilizer and microfine silica powder is 38~46:42~58:3~8:1~3:0.5~1.5: 1.5~3:1.5~3:1.2~2.8:2~4:0.2~0.6:4.8~6.8.
4. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the polyamides Amine, polyester, septichen phenyl ester, microcrystalline wax, anti-aging agent, calcium stearate, magnesium stearate, crosslinking agent, melt index tune The weight part ratio for saving agent, light stabilizer and microfine silica powder is 42:50:5:2:1:2:2:2.2:3:0.4:5.6.
5. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the polyamides The solid content of amine is 80% or more, and the solid content of the polyester is 85% or more.
6. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the S2 step Cured temperature is 100~120 DEG C in rapid, and curing time is 60~120min.
7. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the S3 step The program of program drying in rapid are as follows: 0~5min, 30~45 DEG C, 5~10min, 50~65 DEG C, 10~20min, 70~90 DEG C, 20 ~60min, 70~90 DEG C.
8. the preparation method of the fiber of a kind of according to claim 1 sliding underwear fabric, which is characterized in that the step In S3 flexibility agent be epoxy silicones oil, methylol silicone oil and stearic acid macrogol ester mixture, and epoxy group silicone oil, The weight percent of methylol silicone oil and stearic acid macrogol ester is 30%~45%:40%~50%:5%~30%.
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CN110983484A (en) * 2019-12-06 2020-04-10 浙江升丽纺织有限公司 High-wear-resistance flame-retardant fabric and preparation method thereof
CN113529209B (en) * 2021-07-15 2023-01-03 杭州逸腾新材料有限公司 Superfine denier porous polyester yarn and preparation method thereof

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CN1126832C (en) * 2000-07-18 2003-11-05 上海杰事杰新材料股份有限公司 Silk-like material and its preparing process
CN103275390B (en) * 2013-05-10 2017-02-08 神华集团有限责任公司 Polypropylene-containing composition and preparation method thereof
CN103757745B (en) * 2014-01-21 2015-07-22 中国纺织科学研究院 Polyester blended fiber and preparation method thereof
CN104558839A (en) * 2014-12-29 2015-04-29 广州合成材料研究院有限公司 Ageing resisting master batche for spinning polypropylene material and products and preparation method for ageing resisting master batche

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