CN107142468B - 一种硫化镉化学水浴镀膜反应器 - Google Patents
一种硫化镉化学水浴镀膜反应器 Download PDFInfo
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- WUPHOULIZUERAE-UHFFFAOYSA-N 3-(oxolan-2-yl)propanoic acid Chemical compound OC(=O)CCC1CCCO1 WUPHOULIZUERAE-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 229910052980 cadmium sulfide Inorganic materials 0.000 title claims abstract description 18
- 239000000126 substance Substances 0.000 title claims abstract description 17
- 239000012528 membrane Substances 0.000 title claims abstract description 16
- 238000007747 plating Methods 0.000 title abstract description 7
- 239000011521 glass Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000005086 pumping Methods 0.000 claims abstract description 9
- 238000007789 sealing Methods 0.000 claims description 15
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 239000000243 solution Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
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- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/1601—Process or apparatus
- C23C18/1619—Apparatus for electroless plating
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/1601—Process or apparatus
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- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/1601—Process or apparatus
- C23C18/1633—Process of electroless plating
- C23C18/1675—Process conditions
- C23C18/168—Control of temperature, e.g. temperature of bath, substrate
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Abstract
本发明公开了一种硫化镉化学水浴镀膜反应器,包括基座、真空注排机、电机、底架、真空玻璃外壳和导热板,所述基座上方安装有底架,且基座左侧上方安装有真空注排机,所述电机右侧安装有温度计,所述底架上方安装有真空玻璃外壳,且底架下方安装有加热器,所述真空玻璃外壳底部上方安装有导热板,且真空玻璃外壳右侧安装有抽排水管,所述导热板上方安装有反应器,且导热板左侧安装有水循环叶轮。本发明中,通过使用该硫化镉化学水浴镀膜反应器进行观察,本产品还可以在密闭空间里完成一个完整的水循环系统,操作起来简单方便,通过导热板的间接加热,并非是直接加热,也可以使水温调节更为平缓。
Description
技术领域
本发明涉及化学化工技术领域,尤其涉及一种硫化镉化学水浴镀膜反应器。
背景技术
随着现代工业发展,许多化学原料被开发制造成对人们生活有利的产品,硫化镉在工业生产及人们的生活上也起到了很广泛的应用,对于硫化镉的深度研究则需要反复实验及更透彻的研究。
现有的硫化镉化学水浴镀膜反应器虽然在原理上达到了要求,但是对于细节和观察性并不完善,不能够准确的掌握反应时温度的控制,以及各种温度状态下反应的变化。
发明内容
本发明的目的是为了解决现有技术中存在的缺点,而提出的一种硫化镉化学水浴镀膜反应器。
为了实现上述目的,本发明采用了如下技术方案:
一种硫化镉化学水浴镀膜反应器,包括基座、真空注排机、电机、底架、真空玻璃外壳和导热板,所述基座上方安装有底架,且基座左侧上方安装有真空注排机,所述真空注排机左侧安装有插头,且真空注排机右侧上方安装有电机,所述电机右侧安装有温度计,所述底架上方安装有真空玻璃外壳,且底架下方安装有加热器,所述真空玻璃外壳底部上方安装有导热板,且真空玻璃外壳右侧安装有抽排水管,所述导热板上方安装有反应器,且导热板左侧安装有水循环叶轮。
优选的,所述反应器下方安装有下封闭板,且反应器上方安装有上封闭板,所述上封闭板上方表面安装有密封圈,所述注液管通过密封圈安装在上封闭板的左侧上方,所述排液管通过密封圈安装在上封闭板的右侧上方。
优选的,所述密封圈共设置有两个,且两个密封圈并排安装在上封闭板上方表面。
优选的,所述真空注排机、电机和加热器均与插头电性连接。
优选的,所述抽排水管上方安装有水管阀。
本发明中,通过使用该硫化镉化学水浴镀膜反应器进行观察,真空玻璃外壳可以对一定温度的恒温控制更好掌握,可以长时间的保持恒温状态,还有自带的温度计,也可以更精确的掌握观察数据,本产品还可以在密闭空间里完成一个完整的水循环系统,并且具有抽排一体的放排水系统以及真空注排溶液系统,操作起来简单方便,通过导热板的间接加热,并非是直接加热,也可以使水温调节更为平缓。
附图说明
图1为本发明提出的一种硫化镉化学水浴镀膜反应器的结构示意图;
图2为本发明提出的一种硫化镉化学水浴镀膜反应器的反应器结构示意图。
图中:1插头、2基座、3真空注排机、4电机、5温度计、6底架、7水循环叶轮、8反应器、801下封闭板、802注液管、803上封闭板、804密封圈、805排液管、9真空玻璃外壳、10导热板、11加热器、12水管阀、13抽排水管。
具体实施方式
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。
参照图1-2,一种硫化镉化学水浴镀膜反应器,包括基座2、真空注排机3、电机4、底架6、真空玻璃外壳9和导热板10,基座2 上方安装有底架6,且基座2左侧上方安装有真空注排机3,真空注排机3左侧安装有插头1,且真空注排机3右侧上方安装有电机4,电机4右侧安装有温度计5,底架6上方安装有真空玻璃外壳9,且底架6下方安装有加热器11,真空玻璃外壳9底部上方安装有导热板10,且真空玻璃外壳9右侧安装有抽排水管13,导热板10上方安装有反应器8,且导热板10左侧安装有水循环叶轮7、反应器8下方安装有下封闭板801,且反应器8上方安装有上封闭板803,上封闭板803上方表面安装有密封圈804,注液管802通过密封圈804安装在上封闭板803的左侧上方,排液管805通过密封圈804)安装在上封闭板803的右侧上方、密封圈804共设置有两个,且两个密封圈 804并排安装在上封闭板(803)上方表面、真空注排机3、电机4和加热器11均与插头1电性连接、抽排水管13上方安装有水管阀12。
工作原理:当使用硫化镉化学水浴镀膜反应器时,先用真空注排机3向反应器8中注入溶剂,再通过抽排水管13向真空玻璃外壳9 形成的密闭空间里注满水,开启加热器11,由导热板10传输温度至水中,并开启电机4,使水循环叶轮7工作,形成一个水循环系统,观察温度计5的温度变化,待达到需要温度时停止加热即可。
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本实用新型揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。
Claims (3)
1.一种硫化镉化学水浴镀膜反应器,包括基座(2)、真空注排机(3)、电机(4)、底架(6)、真空玻璃外壳(9)和导热板(10),其特征在于,所述基座(2)上方安装有底架(6),且基座(2)左侧上方安装有真空注排机(3),所述真空注排机(3)左侧安装有插头(1),且真空注排机(3)右侧上方安装有电机(4),所述电机(4)右侧安装有温度计(5),所述底架(6)上方安装有真空玻璃外壳(9),且底架(6)下方安装有加热器(11),所述真空玻璃外壳(9)底部上方安装有导热板(10),且真空玻璃外壳(9)右侧安装有抽排水管(13),所述导热板(10)上方安装有反应器(8),且导热板(10)左侧安装有水循环叶轮(7);所述反应器(8)下方安装有下封闭板(801),且反应器(8)上方安装有上封闭板(803),所述上封闭板(803)上方表面安装有密封圈(804),所述注液管(802)通过密封圈(804)安装在上封闭板(803)的左侧上方,所述排液管(805)通过密封圈(804)安装在上封闭板(803)的右侧上方;所述抽排水管(13)上方安装有水管阀(12)。
2.根据权利要求1所述的一种硫化镉化学水浴镀膜反应器,其特征在于,所述密封圈(804)共设置有两个,且两个密封圈(804)并排安装在上封闭板(803)上方表面。
3.根据权利要求1所述的一种硫化镉化学水浴镀膜反应器,其特征在于,所述真空注排机(3)、电机(4)和加热器(11)均与插头(1)电性连接。
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