CN107142067A - A kind of measurement of algae under water cable fluid sealant and preparation method thereof - Google Patents
A kind of measurement of algae under water cable fluid sealant and preparation method thereof Download PDFInfo
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- CN107142067A CN107142067A CN201710317695.XA CN201710317695A CN107142067A CN 107142067 A CN107142067 A CN 107142067A CN 201710317695 A CN201710317695 A CN 201710317695A CN 107142067 A CN107142067 A CN 107142067A
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- under water
- fluid sealant
- algae
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2296—Oxides; Hydroxides of metals of zinc
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2312/00—Crosslinking
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
- C09K2003/1034—Materials or components characterised by specific properties
- C09K2003/1068—Crosslinkable materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
Abstract
The invention discloses a kind of measurement of algae under water cable fluid sealant, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, 23 parts of bamboo vinegar, 25 parts of silicone oil, 12 parts of white oil, 15 20 parts of coumarone indene resin, 36 parts of zinc oxide, 13 parts of auxiliary agent, 25 parts of activated Calcium carbonate, 58 parts of filler, 15 25 parts of polydimethylsiloxanes institute, 60 80 parts of polyvinyl alcohol;The invention also discloses the preparation method that a kind of algae under water measures cable fluid sealant.The waterproof and decay resistance of product greatly improved in the present invention, extends the service life of cable, it is ensured that algae measuring accuracy under water, and preparation is simple, is easy to industrialization.
Description
Technical field
The present invention relates to cable sealing glue technical field, more particularly to a kind of measurement cable fluid sealant of algae under water and its
Preparation method.
Background technology
The measurement of algae under water is one of key areas in the research work of deep-sea, and subaqueous survey be unable to do without making for watertight cable
With its sealing performance to CABLE MATERIALS has strict requirements.Fluid sealant be often used to be filled in sealant and oversheath,
Between insulating barrier and sealant and screen layer and insulating barrier, play important viscous glutinous effect, and fluid sealant water resistance often
Determine the overall waterproof sealing effect of the cable.The common cable fluid sealant that current subaqueous survey is used mostly, its waterproof
Performance can not fully meet deepwater work environment and height water resistance.
The content of the invention
The present invention proposes cable fluid sealant of algae measurement under water and preparation method thereof, and the waterproof of product greatly improved
And decay resistance, extend the service life of cable, it is ensured that algae measuring accuracy under water
A kind of measurement of algae under water cable fluid sealant proposed by the present invention, its raw material includes by weight:Polyurethane is pre-
100 parts of aggressiveness, 2-3 parts of bamboo vinegar, 2-5 parts of silicone oil, 1-2 parts of white oil, 15-20 parts of coumarone indene resin, 3-6 parts of zinc oxide, auxiliary agent
1-3 parts, 2-5 parts of activated Calcium carbonate, 5-8 parts of filler, 15-25 parts of polydimethylsiloxanes institute, 60-80 parts of polyvinyl alcohol.
Preferably, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, 2.2-2.8 parts of bamboo vinegar, silicone oil 3-4
Part, 1.2-1.8 parts of white oil, 16-18 parts of coumarone indene resin, 4-5 parts of zinc oxide, 1.5-2.5 parts of age resistor, activated Calcium carbonate 3-4
Part, 6-7 parts of filler, 65-75 parts of polyvinyl alcohol.
Preferably, its raw material includes by weight:It is 100 parts of base polyurethane prepolymer for use as, 2.5 parts of bamboo vinegar, 3.5 parts of silicone oil, white
1.5 parts of oil, 17 parts of coumarone indene resin, 4.5 parts of zinc oxide, 2 parts of age resistor, 3.5 parts of activated Calcium carbonate, 6.5 parts of filler, polyethylene
70 parts of alcohol.
Preferably, filler is one or more mixtures with carbon fiber in white carbon, diatomite, talcum powder.
Preferably, auxiliary agent is one or both of age resistor, antioxidant, stabilizer, lubricant thing mixed above.
The present invention proposes the preparation method that a kind of algae under water measures cable fluid sealant, comprises the following steps:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, mixed at 100-150 DEG C
1-2h is refined, mixed material 1 is obtained;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 120-180 DEG C,
Insulation 2-3h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, are mixed at 180-200 DEG C
Refining, degassing obtains the cable fluid sealant of algae measurement under water.
The present invention coordinates using base polyurethane prepolymer for use as and coumarone indene resin as major ingredient and adds silicone oil, white oil, zinc oxide, rationally
The control system degree of cross linking, refines structure, reduces the generation in space, improve the water resistance of product, while improving colloid
Bonding force between CABLE MATERIALS, polydimethylsiloxanes institute, polyvinyl alcohol mating reaction form water-repellent layer in system, further
Water resistance is improved, in addition, polyvinyl alcohol coordinates filler to be interacted with resin Composition, the mechanical property of product is improved, it is ensured that
Excellent mechanical strength and impact flexibility, produce buffering effect at cable connection, are formed and mutually slided, it is to avoid CABLE MATERIALS is broken
Phenomenon is split, cable service life is extended;Bamboo vinegar and activated Calcium carbonate mating reaction have good bacteria mildew-proof effect, right
Algal grown has certain inhibitory action, it is ensured that cable product for a long time be used under water algae measure when will not produce go mouldy or
Surface grows algae influence measuring accuracy, improves decay resistance;Activated Calcium carbonate, zinc oxide and filler synergy,
Reinforcement and filler effect is enhanced, the impact flexibility and water resistance of product is improved, meets application request;It is prepared by the present invention
Method is simple and easy to control, beneficial to industrialization production.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of measurement of algae under water cable fluid sealant, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, bamboo
2 parts of vinegar liquid, 5 parts of silicone oil, 2 parts of white oil, 15 parts of coumarone indene resin, 6 parts of zinc oxide, 1 part of auxiliary agent, 5 parts of activated Calcium carbonate, filler 5
Part, 25 parts of polydimethylsiloxanes institute, 60 parts of polyvinyl alcohol;
The cable fluid sealant of algae measurement under water has the following steps obtained:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, kneaded at 100 DEG C
2h, obtains mixed material 1;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 180 DEG C, is incubated
2h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, knead at 200 DEG C, take off
It is so incensed that the cable fluid sealant of algae measurement under water.
Embodiment 2
A kind of measurement of algae under water cable fluid sealant, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, bamboo
3 parts of vinegar liquid, 2 parts of silicone oil, 1 part of white oil, 20 parts of coumarone indene resin, 3 parts of zinc oxide, 3 parts of auxiliary agent, 2 parts of activated Calcium carbonate, filler 8
Part, 15 parts of polydimethylsiloxanes institute, 80 parts of polyvinyl alcohol;
Wherein, filler is the mixture of white carbon and carbon fiber;Auxiliary agent is age resistor, antioxidant, stabilizer, lubricant;
The cable fluid sealant of algae measurement under water has the following steps obtained:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, kneaded at 110 DEG C
1h, obtains mixed material 1;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 120 DEG C, is incubated
3h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, knead at 180 DEG C, take off
It is so incensed that the cable fluid sealant of algae measurement under water.
Embodiment 3
A kind of measurement of algae under water cable fluid sealant, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, bamboo
2.5 parts of vinegar liquid, 3.5 parts of silicone oil, 1.5 parts of white oil, 17 parts of coumarone indene resin, 4.5 parts of zinc oxide, 2 parts of age resistor, activated Calcium carbonate
3.5 parts, 6.5 parts of filler, 70 parts of polyvinyl alcohol;
Wherein, filler is the mixture of white carbon, diatomite and carbon fiber;Auxiliary agent be age resistor, antioxidant, stabilizer,
Lubricant;
The cable fluid sealant of algae measurement under water has the following steps obtained:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, kneaded at 130 DEG C
1.5h, obtains mixed material 1;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 160 DEG C, is incubated
2.5h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, knead at 190 DEG C, take off
It is so incensed that the cable fluid sealant of algae measurement under water.
Embodiment 4
A kind of measurement of algae under water cable fluid sealant, its raw material includes by weight:100 parts of base polyurethane prepolymer for use as, bamboo
2.2 parts of vinegar liquid, 4 parts of silicone oil, 1.2 parts of white oil, 18 parts of coumarone indene resin, 4 parts of zinc oxide, 2.5 parts of age resistor, activated Calcium carbonate 3
Part, 7 parts of filler, 65 parts of polyvinyl alcohol;
Wherein, filler is the mixture of white carbon, diatomite, talcum powder and carbon fiber;Auxiliary agent be age resistor, antioxidant,
Stabilizer, lubricant;
The cable fluid sealant of algae measurement under water has the following steps obtained:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, kneaded at 120 DEG C
1.5h, obtains mixed material 1;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 150 DEG C, is incubated
2.5h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, knead at 190 DEG C, take off
It is so incensed that the cable fluid sealant of algae measurement under water.
The cable of algae measurement under water is made in embodiment 1-4 and carries out performance test with fluid sealant, test result is as follows:
Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 3 | Embodiment 4 |
Drippage experiment | Pass through | Pass through | Pass through | Pass through | Pass through |
Axial pressure-resistant 1.0Mpa | 6h | 6h | 6h | 6h | 6h |
Displacement/mm | 43 | 42 | 39 | 35 | 37 |
Total seepage water volume/ml | 2.8 | 3.2 | 3.0 | 2.4 | 3.3 |
From test data as can be seen that the present invention has good water resistance, compressive property is good, meets algae under water
Class measures performance requirement of the cable to fluid sealant.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (6)
1. a kind of measurement of algae under water cable fluid sealant, it is characterised in that its raw material includes by weight:Base polyurethane prepolymer for use as
100 parts, 2-3 parts of bamboo vinegar, 2-5 parts of silicone oil, 1-2 parts of white oil, 15-20 parts of coumarone indene resin, 3-6 parts of zinc oxide, auxiliary agent 1-3
Part, 2-5 parts of activated Calcium carbonate, 5-8 parts of filler, 15-25 parts of polydimethylsiloxanes institute, 60-80 parts of polyvinyl alcohol.
2. algae under water according to claim 1 measures cable fluid sealant, it is characterised in that its raw material is wrapped by weight
Include:100 parts of base polyurethane prepolymer for use as, 2.2-2.8 parts of bamboo vinegar, 3-4 parts of silicone oil, 1.2-1.8 parts of white oil, coumarone indene resin 16-18
Part, 4-5 parts of zinc oxide, 1.5-2.5 parts of age resistor, 3-4 parts of activated Calcium carbonate, 6-7 parts of filler, 65-75 parts of polyvinyl alcohol.
3. algae under water according to claim 1 measures cable fluid sealant, it is characterised in that its raw material is wrapped by weight
Include:100 parts of base polyurethane prepolymer for use as, 2.5 parts of bamboo vinegar, 3.5 parts of silicone oil, 1.5 parts of white oil, 17 parts of coumarone indene resin, zinc oxide 4.5
Part, 2 parts of age resistor, 3.5 parts of activated Calcium carbonate, 6.5 parts of filler, 70 parts of polyvinyl alcohol.
4. the measurement cable fluid sealant of algae under water according to claim any one of 1-3, it is characterised in that filler is white
One or more and the mixture of carbon fiber in carbon black, diatomite, talcum powder.
5. the measurement cable fluid sealant of algae under water according to claim any one of 1-3, it is characterised in that auxiliary agent is anti-
One or both of old agent, antioxidant, stabilizer, lubricant thing mixed above.
6. a kind of algae under water according to claim any one of 1-5 measures the preparation method of cable fluid sealant, it is special
Levy and be, comprise the following steps:
S1, base polyurethane prepolymer for use as, silicone oil, white oil, coumarone indene resin, zinc oxide is well mixed, 1- is kneaded at 100-150 DEG C
2h, obtains mixed material 1;
S2, to add into mixed material polydimethylsiloxanes institutes, polyvinyl alcohol uniform, is warming up at 120-180 DEG C, is incubated
2-3h obtains mixed material 2;
S3, addition bamboo vinegar, activated Calcium carbonate, filler, auxiliary agent mixing into mixed material 2, knead at 180-200 DEG C, take off
It is so incensed that the cable fluid sealant of algae measurement under water.
Priority Applications (1)
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CN201710317695.XA CN107142067A (en) | 2017-05-08 | 2017-05-08 | A kind of measurement of algae under water cable fluid sealant and preparation method thereof |
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CN201710317695.XA CN107142067A (en) | 2017-05-08 | 2017-05-08 | A kind of measurement of algae under water cable fluid sealant and preparation method thereof |
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CN107142067A true CN107142067A (en) | 2017-09-08 |
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CN201710317695.XA Withdrawn CN107142067A (en) | 2017-05-08 | 2017-05-08 | A kind of measurement of algae under water cable fluid sealant and preparation method thereof |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104725860A (en) * | 2013-12-24 | 2015-06-24 | 李茜茜 | Sealant for cables |
CN105038685A (en) * | 2015-08-14 | 2015-11-11 | 上海应用技术学院 | Non-tar cable connector polyurethane waterproof sealant and preparation method thereof |
-
2017
- 2017-05-08 CN CN201710317695.XA patent/CN107142067A/en not_active Withdrawn
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104725860A (en) * | 2013-12-24 | 2015-06-24 | 李茜茜 | Sealant for cables |
CN105038685A (en) * | 2015-08-14 | 2015-11-11 | 上海应用技术学院 | Non-tar cable connector polyurethane waterproof sealant and preparation method thereof |
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Application publication date: 20170908 |
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