CN107125444A - A kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application - Google Patents
A kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application Download PDFInfo
- Publication number
- CN107125444A CN107125444A CN201710173787.5A CN201710173787A CN107125444A CN 107125444 A CN107125444 A CN 107125444A CN 201710173787 A CN201710173787 A CN 201710173787A CN 107125444 A CN107125444 A CN 107125444A
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- China
- Prior art keywords
- chain fatty
- glyceride
- acid
- lactic acid
- short
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/30—Feeding-stuffs specially adapted for particular animals for swines
Abstract
The present invention disclose a kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application, comprising short chain fatty acids 10~90%, medium-chain fatty glyceride 10~50%, and sour 1~20%, preparation method is：First medium-chain fatty glyceride is added in short-chain fat acid glyceride emulsion to be mixed；Again lactic acid is added in mix emulsion fluid to be mixed；Then, it is spray-dried.The compound is applied in animal feed additive, improve the nutritive value of feed, animal gastrointestinal tract is contributed to develop and microbial balance, reduce bacterial diarrhea, mitigate the constipation of pregnancy parent, shorten sow stages of labor, improve lactation parent milk quality, feed intake and reduce the nascent cub death rate and improve weaning weight, a kind of hygienic, efficient method is provided for cultivation, Feed Manufacturing.
Description
Technical field
It is to be related to a kind of brachymedial chain fatty more specifically the invention belongs to animal feed additive production technical field
The compound of acid glyceride and lactic acid.
Background technology
The pig farmer in the whole world 50% concentrates on China, followed by European Union and the U.S.；Show, these areas will be pork
Production and the maximum consumer of pig mixed feed；Feed additives have the trophism for improving feed, improve the utilization rate of feed, promote
Enter growth of animal and prevention disease, nutriment loss during reducing feed storage etc. is made, feed addictive be in feed not
The part that can lack.
But some additives currently on the market add the antibiotic or sulfa drugs of low amounts to prevent and treat livestock and poultry
Or diarrhoea, but the microbial balance that the antibiotic of addition can so destroyed in natural environment, and be enriched in human body, to people
Disease treatment and heredity produce influence.
In addition, the additive component complexity being made mostly using Chinese herbal medicine on the market, unfavorable for the livestock and poultry of feeding
In digesting and assimilating, the waste to nutriment in feed is caused.
Most of all, for shortening poultry stages of labor, improving parent milk quality, the death of less cub in these additives
Rate and raising weaning weight all effects without significant effective.
Inventor is devoted for years in livestock and poultry cultivation industry, for problem above, constantly looks for new more preferable feed addition
The preparation method and application approach of agent.
The content of the invention
Goal of the invention：The purpose of the present invention be for existing feed addictive exist not enough there is provided a kind of brachymedial chain
Fatty glyceride and the compound and preparation method of lactic acid and its application, to improve feed nutritive value, meet gastrointestinal tract of livestock and fowls
Development and the requirement of microbial balance, reach few bacterial diarrhea, the situation of mitigation pregnancy parent constipation, shorten parent stages of labor,
Improve parent milk quality and feed intake, reduce the nascent cub death rate, high weaning weight, high feed digestion utilization rate, raising seat
The purpose of tire rate, enhancing kind fowl power and improvement meat quality.
Technical scheme：In order to realize foregoing invention purpose, the technical solution adopted in the present invention is：A kind of brachymedial chain fatty
The compound of acid glyceride and lactic acid, comprising following material, is combined by weight percentage：Short-chain fat acid glyceride 10~
90%, medium-chain fatty glyceride 10~50%, lactic acid 1~20%.Wherein：Short chain fatty acids refer to propionic acid glyceride or butyric acid
Glyceride；Medium chain fatty acid refers to glycerol caprylate, certain herbaceous plants with big flowers acid glyceride.
A kind of compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid comprises the following steps：
A, in short-chain fat acid glyceride water-in-oil emulsion add medium-chain fatty glyceride mixed, mixed proportion with
Pure substance meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%；
B, in brachymedial chain fatty acid triglyceride mix emulsion fluid add lactic acid mixed, mixed proportion is with pure substance
Meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%, lactic acid 1~20%；
C, spray drying：Spraying is carried out under the conditions of 180 DEG C~220 DEG C of EAT, 70 DEG C~150 DEG C of leaving air temp dry
It is dry；
D, product：The dry powder collected through cyclone separator or vibrations fluid bed is brachymedial chain fatty acid triglyceride and lactic acid
Compound.
Further, the preparation method of brachymedial chain fatty acid triglyceride comprises the following steps：
(A1) esterification：Butyric acid/propionic acid and glycerine are added in the reactor, in high vacuum, control temperature at 180 DEG C,
Without being reacted under the conditions of chemical catalyst, short-chain fat acid glyceride is generated.
(A2) reinforcing esterification, injects reactor, with short-chain fat acid glyceride under the conditions of high vacuum and 220 DEG C by glycerine
Mixing, is made uniform mixture.
Yet further, the compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Fatty glyceride water emulsification
Add medium-chain fatty glyceride in liquid to be mixed, mixed proportion is in terms of pure substance, short-chain fat acid glyceride 10~90%,
Chain fatty acid triglyceride 10~50%.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：The medium-chain fatty glyceride of addition is with pure substance
Meter, first in the reactor by medium chain fatty acid and glycerine reaction formation mixture, then with short-chain fat acid glyceride emulsion one
Rise and mixed.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Lactic acid material is added, lactic acid is first dissolved in water, so
After be then added in brachymedial chain fatty acid triglyceride emulsion and mixed.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Medium-chain fatty glyceride and lactic acid are added short
It is stirred, is well mixed in chain fatty acid triglyceride emulsion, form suspension, is sprayed while stirring into step C
Dry.
Beneficial effect：Beneficial effects of the present invention are：
1st, the constitution of parent and piglet greatly improved to improve the parent feed addictive of piglet survival ratio in the present invention,
Compared to existing feed addictive, it is more easy to absorb, and nutritious, instant effect, injure small.
2nd, pig feed additive of the invention can not only promote swine rationses comprehensive nutrition, improve efficiency of feed utilization and feed
Nutritional ingredient, and animal body resistance can be strengthened, prophylactic treatment Animal diseases promote growth.
3rd, feed addictive of the present invention has antibacterial, regulation gut flora, promotes intestinal growth, improves immunity
Deng effect, can effective prevention of diarrhea in piglets generation, promote piglet to grow, build up health, this feed addictive have noresidue,
Have no drug resistance, safe advantage, can effective substitute antibiotics, effectively improve the survival rate of piglet, reduction piglet is dead
Rate, increases economic efficiency, and meets healthy aquaculture developing direction.
4th, the trend of livestock and poultry meat fiber can be changed by product of the present invention being used for a long time, and be allowed to finer and smoother, more with battalion
Support, the meat of food is fragrant and tender, and smooth in taste, and nutritious, results in the healthy pork of green safety.
5th, the additive for farm animal feed that the present invention is provided improves feed conversion rate, rate of returns and the weightening of pig, improves its drive
Worm, stomach invigorating, growth encourage, the immunologic function for improving body, and raw material are easy to get, and produce conveniently, can promote the use of.
Embodiment
With reference to embodiment, the technical program is described in detail, but the protection domain not office of invention
It is limited to the embodiment.
A kind of compound of brachymedial chain fatty acid triglyceride and lactic acid, its Short-Chain Fatty Acids 60%, fatty glyceride
25%, lactic acid 15%.Its preparation method is as follows：
A, in short-chain fat acid glyceride water-in-oil emulsion add medium-chain fatty glyceride mixed, mixed proportion with
Pure substance meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%；
B, in brachymedial chain fatty acid triglyceride mix emulsion fluid add lactic acid mixed, mixed proportion is with pure substance
Meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%, lactic acid 1~20%；
C, spray drying：Spraying is carried out under the conditions of 180 DEG C~220 DEG C of EAT, 70 DEG C~150 DEG C of leaving air temp dry
It is dry；
D, product：The dry powder collected through cyclone separator or vibrations fluid bed is brachymedial chain fatty acid triglyceride and lactic acid
Compound.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Chain in being added in fatty glyceride water-in-oil emulsion
Fatty glyceride is mixed, and mixed proportion is in terms of pure substance, short-chain fat acid glyceride 10~90%, chain fatty acid glycerine
Ester 10~50%.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：The medium-chain fatty glyceride of addition is with pure substance
Meter, first in the reactor by medium chain fatty acid and glycerine reaction formation mixture, then with short-chain fat acid glyceride emulsion one
Rise and mixed.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Lactic acid material is added, lactic acid is first dissolved in water, so
After be then added in brachymedial chain fatty acid triglyceride emulsion and mixed.
The compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid is：Medium-chain fatty glyceride and lactic acid are added short
It is stirred, is well mixed in chain fatty acid triglyceride emulsion, form suspension, is sprayed while stirring into step C
Dry.
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic.
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention's
Within protection domain.
Claims (8)
1. the compound of a kind of brachymedial chain fatty acid triglyceride and lactic acid, it is characterised in that comprising following material, by 100 percentages
Than metering, each composition percentage is as follows：
Short-chain fat acid glyceride 10~90%；
Medium-chain fatty glyceride 10~50%；
Lactic acid 1~20%,
The short-chain fat acid glyceride, medium-chain fatty glyceride and the combination of the component of lactic acid three obtain 100% compound.
2. a kind of compound of brachymedial chain fatty acid triglyceride and lactic acid according to claim 1, it is characterised in that：Short chain fat
Fat acid refers to propionic acid glyceride or glycerol monobutyralte, and medium chain fatty acid refers to glycerol caprylate, certain herbaceous plants with big flowers acid glyceride.
3. the compound preparation method of a kind of brachymedial chain fatty acid triglyceride and lactic acid, it is characterised in that：Comprise the following steps：
A, in short-chain fat acid glyceride water-in-oil emulsion add medium-chain fatty glyceride mixed, mixed proportion is with pure
Thing meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%；
B, in brachymedial chain fatty acid triglyceride mix emulsion fluid add lactic acid mixed, mixed proportion is short in terms of pure substance
Chain fatty acid triglyceride 10~90%, medium-chain fatty glyceride 10~50%, lactic acid 1~20%；
C, spray drying：It is spray-dried under the conditions of 180 DEG C~220 DEG C of EAT, 70 DEG C~150 DEG C of leaving air temp；
D, product：The dry powder collected through cyclone separator or vibrations fluid bed is answering for brachymedial chain fatty acid triglyceride and lactic acid
Compound.
4. a kind of compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid according to claim 3, it is characterised in that：Institute
A steps are stated, the preparation method of brachymedial chain fatty acid triglyceride comprises the following steps：
A1, esterification：Butyric acid/propionic acid and glycerine are added in the reactor, in high vacuum, control temperature in 180 DEG C, no chemistry
Reacted under catalysts conditions, generate short-chain fat acid glyceride；
A2, reinforcing esterification：Glycerine is injected into reactor, mixed under the conditions of high vacuum and 220 DEG C with short-chain fat acid glyceride,
Uniform mixture is made.
5. a kind of compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid according to claim 3, it is characterised in that：Institute
A steps are stated, medium-chain fatty glyceride is added in short-chain fat acid glyceride water-in-oil emulsion and is mixed, mixed proportion is with pure
Net thing meter, short-chain fat acid glyceride 10~90%, medium-chain fatty glyceride 10~50%；The A steps, the middle chain of addition
Fatty glyceride in terms of pure substance, first in the reactor by medium chain fatty acid and glycerine reaction formation mixture, then with short chain
Fatty glyceride emulsion is mixed together.
6. a kind of compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid according to claim 4, it is characterised in that：Institute
B steps are stated, lactic acid material is added, lactic acid is first dissolved in water, is then then added in brachymedial chain fatty acid triglyceride emulsion
Row mixing.
7. according to a kind of compound preparation method of brachymedial chain fatty acid triglyceride and lactic acid as claimed in claim 4, it is characterised in that：
A, B step, medium-chain fatty glyceride and lactic acid are added and are stirred in short-chain fat acid glyceride emulsion, is mixed
Uniformly, suspension is formed, is spray-dried while stirring into step C.
8. a kind of application of the compound of brachymedial chain fatty acid triglyceride and lactic acid is as follows：
It is used as the feed addictive for improving parent milk quality and feed intake；
As improving, immunity of livestock, the reduction cub death rate and holding animal gastrointestinal tract are developed and the diseases prevention of microbial balance is controlled
Sick class feed addictive；
It is used as the feed addictive for improving feed nutritive value.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710173787.5A CN107125444A (en) | 2017-03-22 | 2017-03-22 | A kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710173787.5A CN107125444A (en) | 2017-03-22 | 2017-03-22 | A kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application |
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| Publication Number | Publication Date |
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| CN107125444A true CN107125444A (en) | 2017-09-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710173787.5A Pending CN107125444A (en) | 2017-03-22 | 2017-03-22 | A kind of brachymedial chain fatty acid triglyceride and the compound and preparation method of lactic acid and its application |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107373212A (en) * | 2017-08-08 | 2017-11-24 | 胡从玉 | A kind of breeding feed for improving freshwater shrimp immunity of organisms |
| CN108208341A (en) * | 2017-12-29 | 2018-06-29 | 湖北浩华生物技术有限公司 | Purposes, feed addictive and feed of the fat or oil composition on pig feed additive for fowls is prepared |
| CN109511811A (en) * | 2019-01-29 | 2019-03-26 | 潍坊加易加生物科技有限公司 | One kind is for anti-Short-Chain Fatty Acids essential oil formulation and preparation method thereof and its application |
| CN110037182A (en) * | 2019-03-08 | 2019-07-23 | 佛山深农饲料有限公司 | A kind of milking sow concentrated feed |
| WO2021191470A1 (en) * | 2020-03-27 | 2021-09-30 | Basf Se | Composition comprising glycerides for the treatment of gastro-intestinal dysfunction and/or associated morbidities thereto |
| CN113632888A (en) * | 2021-08-10 | 2021-11-12 | 广州朴成生物科技有限公司 | Functional additive for reducing weaning stress of piglets and preparation method and application thereof |
| CN114223793A (en) * | 2021-11-01 | 2022-03-25 | 中国农业大学 | Composition and feed for improving reproductive performance of sows |
Citations (2)
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| CN101647517A (en) * | 2009-06-17 | 2010-02-17 | 新奥（厦门）农牧发展有限公司 | Compound of butyrate or glycerol monobutyralte and fructo-oligosaccharide, preparation method of compound and application of compound in feed addictive |
| CN105124326A (en) * | 2015-10-14 | 2015-12-09 | 安徽农业大学 | Early-stage livestock nutritious supplement micro-capsule powder and preparing method and application thereof |
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2017
- 2017-03-22 CN CN201710173787.5A patent/CN107125444A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101647517A (en) * | 2009-06-17 | 2010-02-17 | 新奥（厦门）农牧发展有限公司 | Compound of butyrate or glycerol monobutyralte and fructo-oligosaccharide, preparation method of compound and application of compound in feed addictive |
| CN105124326A (en) * | 2015-10-14 | 2015-12-09 | 安徽农业大学 | Early-stage livestock nutritious supplement micro-capsule powder and preparing method and application thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107373212A (en) * | 2017-08-08 | 2017-11-24 | 胡从玉 | A kind of breeding feed for improving freshwater shrimp immunity of organisms |
| CN108208341A (en) * | 2017-12-29 | 2018-06-29 | 湖北浩华生物技术有限公司 | Purposes, feed addictive and feed of the fat or oil composition on pig feed additive for fowls is prepared |
| CN108208341B (en) * | 2017-12-29 | 2021-11-30 | 湖北浩华生物技术有限公司 | Application of grease composition in preparation of pig and poultry feed additive, feed additive and feed |
| CN109511811A (en) * | 2019-01-29 | 2019-03-26 | 潍坊加易加生物科技有限公司 | One kind is for anti-Short-Chain Fatty Acids essential oil formulation and preparation method thereof and its application |
| CN110037182A (en) * | 2019-03-08 | 2019-07-23 | 佛山深农饲料有限公司 | A kind of milking sow concentrated feed |
| WO2021191470A1 (en) * | 2020-03-27 | 2021-09-30 | Basf Se | Composition comprising glycerides for the treatment of gastro-intestinal dysfunction and/or associated morbidities thereto |
| CN113632888A (en) * | 2021-08-10 | 2021-11-12 | 广州朴成生物科技有限公司 | Functional additive for reducing weaning stress of piglets and preparation method and application thereof |
| CN114223793A (en) * | 2021-11-01 | 2022-03-25 | 中国农业大学 | Composition and feed for improving reproductive performance of sows |
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Application publication date: 20170905 |
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