CN107116641A - A kind of processing method for improving levant cotton exocarp tinctorial property - Google Patents
A kind of processing method for improving levant cotton exocarp tinctorial property Download PDFInfo
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- CN107116641A CN107116641A CN201710226014.9A CN201710226014A CN107116641A CN 107116641 A CN107116641 A CN 107116641A CN 201710226014 A CN201710226014 A CN 201710226014A CN 107116641 A CN107116641 A CN 107116641A
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- levant cotton
- cotton exocarp
- coloring agent
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0005—Cryogenic treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/003—Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
- B27K5/0065—Ultrasonic treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/02—Staining or dyeing wood; Bleaching wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/04—Combined bleaching or impregnating and drying of wood
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Mechanical Engineering (AREA)
- Coloring (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention belongs to dyeing process technical field, especially a kind of processing method for improving levant cotton exocarp tinctorial property, specific method is as follows：（1）Immersion, freezing and microwave drying treatment；（2）Dye and ultrasonically treated；（3）Baking and microwave drying treatment；The present invention not only effectively facilitates coloring agent and enters longtitudinal dispersion passage from cross section and enter horizontal infiltration passage from vertical section, promote infiltration and the even dyeing of coloring agent, so that coloring agent not only equal level dyeing in the surface of levant cotton exocarp, and can uniformly penetrating to inside levant cotton exocarp, after being soaked using soak, coloring agent is effectively facilitated to react with levant cotton exocarp, form Covalent bonding together, improve Color and not fugitive color, effectively improve soaping fastness, and can effectively strengthen the toughness of levant cotton exocarp, make its non-breakable, strengthen its aesthetics and use value.
Description
Technical field
The invention belongs to dyeing process technical field, especially a kind of processing method for improving levant cotton exocarp tinctorial property.
Background technology
Levant cotton exocarp is the exocarp of malvaceae plant cotton etc., controls diaphragm food, diaphragm gas, but uses its processing dyeing at present and add
Perfume (or spice) is fabricated to colored sachet, but the coloring of levant cotton exocarp is difficult, and dyeing rear stability is poor, easily fades；Therefore, invent a kind of
The processing method that levant cotton exocarp tinctorial property can be effectively improved is current urgent problem to be solved.
The content of the invention
In view of the above-mentioned problems, a kind of the present invention is intended to provide processing method for improving levant cotton exocarp tinctorial property.
The present invention is achieved through the following technical solutions：
A kind of processing method for improving levant cotton exocarp tinctorial property, specific method is as follows：
（1）Immersion, freezing and microwave drying treatment
Levant cotton exocarp is broken into flap, constant temperature in soak is immersed in and soaks 480 ~ 490min, take out, it is -19 ~ -18 to insert temperature
DEG C household freezer 115 ~ 120min of cryostat, -4 ~ -3 DEG C, cryostat are warming up to 1.1 ~ 1.2 DEG C/min heating rate
135 ~ 140min, microwave drying to moisture is 4% ~ 5% under conditions of frequency is 350 ~ 360MHz；
Described soak, is made up of the raw material of following parts by weight：4.5 ~ 4.7 parts of silkworm excrement, 7.6 ~ 7.8 parts of resina liquidamberis, Artemisia japonica 3.3
~ 3.5 parts, 4.6 ~ 4.8 parts of ardisia japonica, 5.4 ~ 5.6 parts of Sorrel, 4.9 ~ 5.1 parts of dioscoreae septemlobae,rhizoma, 9.4 ~ 9.6 parts of asarum, water 210 ~
220 parts；
（2）Dye and ultrasonically treated
Will be through step（1）Levant cotton exocarp after processing is immersed in 140 ~ 150min of immersion in coloring agent, and application frequency is 25 ~ 26kHz
Ultrasonic echography handle 16 ~ 17min, continue soak 190 ~ 200min, levant cotton exocarp is taken out from coloring agent；
Described coloring agent, is made up of the raw material of following parts by weight：Reactive brilliant red X-B9.4 ~ 9.8 part, 26 ~ 27 parts of fresh leaf sumac,
0.85 ~ 0.89 part of jumcus bufonius, 0.75 ~ 0.77 part of Medulla Tetrapanacis extract, 33 ~ 35 parts of fresh humid euphorbia blade of grass, fresh-rose petal
21 ~ 23 parts, 6.4 ~ 6.8 parts of sodium citrate, 160 ~ 170 parts of water；
（3）Baking and microwave drying treatment
Will be through step（2）Levant cotton exocarp after processing inserts the baking box that temperature is 55 ~ 57 DEG C and toasts 190 ~ 200s, takes out, in frequency
Rate is that microwave drying to moisture is 7% ~ 8% under conditions of 470 ~ 480MHz.
It is used as the further scheme of invention：Step（1）Described soak, is prepared according to the following steps：By silkworm excrement, maple
Face cream, Artemisia japonica, ardisia japonica, Sorrel, dioscoreae septemlobae,rhizoma and asarum are crushed in 90 ~ 100 mesh, input water, are 120 ~ 130r/ with rotating speed
Min agitator stirs 6 ~ 7min, 12 ~ 13min of homogeneous under conditions of pressure is 2.2 ~ 2.3MPa, is boiled by fire, slow fire is endured
34 ~ 36min is boiled, 220 ~ 230 mesh filter clothes are crossed, filtrate is taken, room temperature naturally cools to temperature for 42 ~ 44 DEG C, obtains soak.
It is used as the further scheme of invention：Step（2）The preparation method of described coloring agent, specifically includes following steps：
A. fresh leaf sumac, fresh humid euphorbia blade of grass and fresh-rose petal are put into rotating speed to crush in 780 ~ 800r/min pulverizer
14 ~ 15min, is taken out, and is boiled by fire in input water, and slow fire 22 ~ 24min of infusion is inserted and sent out in the fermenting case that temperature is 42 ~ 44 DEG C
27 ~ 29h of ferment, takes out, and continues 34 ~ 36min of slow fire infusion and is simultaneously stirred continuously with rotating speed for 64 ~ 66r/min agitator, excessively 230 ~
240 mesh filter clothes, take filtrate, obtain floral leaf liquid；
B. sodium citrate and reactive brilliant red are added in floral leaf liquid, with rotating speed for 95 ~ 100r/min agitator stirring 8 ~
9min, adds jumcus bufonius and Medulla Tetrapanacis extract continues to stir 5 ~ 6min, under conditions of pressure is 5.5 ~ 5.7MPa
23 ~ 25min of matter, obtains coloring agent.
It is used as the further scheme of invention：Silkworm excrement used in the present invention, resina liquidamberis, Artemisia japonica, ardisia japonica, Sorrel, silk floss
Bi Collettii and the content of asarum are in terms of dry weight weight.
Beneficial effects of the present invention：A kind of processing method for raising levant cotton exocarp tinctorial property that the present invention is provided, not only has
Effect promotes coloring agent to enter longtitudinal dispersion passage from cross section and enter horizontal infiltration passage from vertical section, promotes oozing for coloring agent
Thoroughly and even dyeing so that coloring agent not only equal level dyeing in the surface of levant cotton exocarp, and can uniformly penetrating to inside levant cotton exocarp, use
After soak immersion, effectively facilitate coloring agent and reacted with levant cotton exocarp, form Covalent bonding together, improve Color and be difficult
Fade, effectively improve soaping fastness, and can effectively strengthen the toughness of levant cotton exocarp, make its non-breakable, strengthen its aesthetics
And use value；The coloring agent active ingredient of the present invention contains more water soluble group, and simple in construction, molecular weight is small, linear,
Aromatic ring coplanarity is not strong, and aggregation extent is weak in aqueous, readily permeable to inside levant cotton exocarp, and fragrance is pure and fresh persistently, stingless
Property smell is swashed, to human body without any injury.
Embodiment
Illustrate the present invention with specific embodiment below, but be not limitation of the present invention.
Embodiment 1
In the embodiment of the present invention, a kind of processing method for improving levant cotton exocarp tinctorial property, specific method is as follows：
（1）Immersion, freezing and microwave drying treatment
Levant cotton exocarp is broken into flap, constant temperature in soak is immersed in and soaks 480min, take out, insert the freezing that temperature is -19 DEG C
Case cryostat 115min, -4 DEG C are warming up to 1.1 DEG C/min heating rate, and cryostat 135min is in frequency
Microwave drying to moisture is 4% under conditions of 350MHz；
Described soak, is made up of the raw material of following parts by weight：It is 4.5 parts of silkworm excrement, 7.6 parts of resina liquidamberis, 3.3 parts of Artemisia japonica, short
4.6 parts of tea, 5.4 parts of Sorrel, 4.9 parts of dioscoreae septemlobae,rhizoma, 9.4 parts of asarum, 210 parts of water；
（2）Dye and ultrasonically treated
Will be through step（1）Levant cotton exocarp after processing, which is immersed in coloring agent, soaks 140min, applies the ultrasonic wave that frequency is 25kHz
Ultrasonically treated 16min, continues to soak 190min, levant cotton exocarp is taken out from coloring agent；
Described coloring agent, is made up of the raw material of following parts by weight：X-B9.4 parts of reactive brilliant red, 26 parts of fresh leaf sumac, rush
0.85 part of extract, 0.75 part of Medulla Tetrapanacis extract, 33 parts of fresh humid euphorbia blade of grass, 21 parts of fresh-rose petal, 6.4 parts of sodium citrate,
160 parts of water；
（3）Baking and microwave drying treatment
Will be through step（2）Levant cotton exocarp after processing inserts the baking box baking 190s that temperature is 55 DEG C, takes out, is in frequency
Microwave drying to moisture is 7% under conditions of 470MHz.
It is used as the further scheme of invention：Step（1）Described soak, is prepared according to the following steps：By silkworm excrement, maple
Face cream, Artemisia japonica, ardisia japonica, Sorrel, dioscoreae septemlobae,rhizoma and asarum are crushed in 90 mesh, input water, are stirring for 120r/min with rotating speed
Device stirring 6min is mixed, the homogeneous 12min under conditions of pressure is 2.2MPa is boiled by fire, and slow fire infusion 34min crosses the filter of 220 mesh
Cloth, takes filtrate, and room temperature naturally cools to temperature for 42 DEG C, obtains soak.
It is used as the further scheme of invention：Step（2）The preparation method of described coloring agent, specifically includes following steps：
A. fresh leaf sumac, fresh humid euphorbia blade of grass and fresh-rose petal are put into rotating speed to crush in 780r/min pulverizer
14min, takes out, and is boiled by fire in input water, slow fire infusion 22min, inserts fermentation 27h in the fermenting case that temperature is 42 DEG C, takes
Go out, continue slow fire infusion 34min and be 64r/min with rotating speed agitator be stirred continuously, cross 230 mesh filter clothes, take filtrate, obtain flower
Leaf liquid；
B. sodium citrate and reactive brilliant red are added in floral leaf liquid, the agitator for being 95r/min with rotating speed stirring 8min is added
Jumcus bufonius and Medulla Tetrapanacis extract continue to stir 5min, the homogeneous 23min under conditions of pressure is 5.5MPa, must dye
Agent.
The saline solution immersion 80h that temperature in use is 52 DEG C after dyeing, mass fraction is 3.1%, does not occur discoloration.
Embodiment 2
In the embodiment of the present invention, a kind of processing method for improving levant cotton exocarp tinctorial property, specific method is as follows：
（1）Immersion, freezing and microwave drying treatment
Levant cotton exocarp is broken into flap, constant temperature is immersed in soak and soaks 485min, take out, temperature is inserted cold for -18.5 DEG C
Freeze case cryostat 118min, be warming up to -3.5 DEG C with 1.15 DEG C/min heating rate, cryostat 138min is in frequency
Microwave drying to moisture is 4.5% under conditions of 355MHz；
Described soak, is made up of the raw material of following parts by weight：It is 4.6 parts of silkworm excrement, 7.7 parts of resina liquidamberis, 3.4 parts of Artemisia japonica, short
4.7 parts of tea, 5.5 parts of Sorrel, 5 parts of dioscoreae septemlobae,rhizoma, 9.5 parts of asarum, 215 parts of water；
（2）Dye and ultrasonically treated
Will be through step（1）Levant cotton exocarp after processing, which is immersed in coloring agent, soaks 145min, applies the ultrasound that frequency is 25.5kHz
The ultrasonically treated 16.5min of ripple, continues to soak 195min, levant cotton exocarp is taken out from coloring agent；
Described coloring agent, is made up of the raw material of following parts by weight：X-B9.6 parts of reactive brilliant red, 26.5 parts of fresh leaf sumac, lampwick
Careless 0.87 part of extract, 0.76 part of Medulla Tetrapanacis extract, 34 parts of fresh humid euphorbia blade of grass, 22 parts of fresh-rose petal, sodium citrate 6.6
Part, 165 parts of water；
（3）Baking and microwave drying treatment
Will be through step（2）Levant cotton exocarp after processing inserts the baking box baking 195 that temperature is 56 DEG C, takes out, is in frequency
Microwave drying to moisture is 7.5% under conditions of 475MHz.
It is used as the further scheme of invention：Step（1）Described soak, is prepared according to the following steps：By silkworm excrement, maple
Face cream, Artemisia japonica, ardisia japonica, Sorrel, dioscoreae septemlobae,rhizoma and asarum are crushed in 95 mesh, input water, are stirring for 125r/min with rotating speed
Device stirring 6.5min is mixed, the homogeneous 12.5min under conditions of pressure is 2.25MPa is boiled by fire, slow fire infusion 35min, mistake
225 mesh filter clothes, take filtrate, and room temperature naturally cools to temperature for 43 DEG C, obtains soak.
It is used as the further scheme of invention：Step（2）The preparation method of described coloring agent, specifically includes following steps：
A. fresh leaf sumac, fresh humid euphorbia blade of grass and fresh-rose petal are put into rotating speed to crush in 790r/min pulverizer
14.5min, takes out, and is boiled by fire in input water, slow fire infusion 23min, inserts fermentation 28h in the fermenting case that temperature is 43 DEG C,
Taking-up, continuation slow fire infusion 35min and the agitator for being 65r/min with rotating speed are stirred continuously, and are crossed 235 mesh filter clothes, are taken filtrate, obtain
Floral leaf liquid；
B. sodium citrate and reactive brilliant red are added in floral leaf liquid, the agitator for being 98r/min with rotating speed stirring 8.5min, plus
Enter jumcus bufonius and Medulla Tetrapanacis extract continues to stir 5.5min, the homogeneous 24min under conditions of pressure is 5.6MPa must contaminate
Toner.
The saline solution immersion 80h that temperature in use is 52 DEG C after dyeing, mass fraction is 3.1%, does not occur discoloration.
Embodiment 3
In the embodiment of the present invention, a kind of processing method for improving levant cotton exocarp tinctorial property, specific method is as follows：
（1）Immersion, freezing and microwave drying treatment
Levant cotton exocarp is broken into flap, constant temperature in soak is immersed in and soaks 490min, take out, insert the freezing that temperature is -18 DEG C
Case cryostat 120min, -3 DEG C are warming up to 1.2 DEG C/min heating rate, and cryostat 140min is in frequency
Microwave drying to moisture is 5% under conditions of 360MHz；
Described soak, is made up of the raw material of following parts by weight：It is 4.7 parts of silkworm excrement, 7.8 parts of resina liquidamberis, 3.5 parts of Artemisia japonica, short
4.8 parts of tea, 5.6 parts of Sorrel, 5.1 parts of dioscoreae septemlobae,rhizoma, 9.6 parts of asarum, 220 parts of water；
（2）Dye and ultrasonically treated
Will be through step（1）Levant cotton exocarp after processing, which is immersed in coloring agent, soaks 150min, applies the ultrasonic wave that frequency is 26kHz
Ultrasonically treated 17min, continues to soak 200min, levant cotton exocarp is taken out from coloring agent；
Described coloring agent, is made up of the raw material of following parts by weight：X-B9.8 parts of reactive brilliant red, 27 parts of fresh leaf sumac, rush
0.89 part of extract, 0.77 part of Medulla Tetrapanacis extract, 35 parts of fresh humid euphorbia blade of grass, 23 parts of fresh-rose petal, 6.8 parts of sodium citrate,
170 parts of water；
（3）Baking and microwave drying treatment
Will be through step（2）Levant cotton exocarp after processing inserts the baking box baking 200s that temperature is 57 DEG C, takes out, is in frequency
Microwave drying to moisture is 8% under conditions of 480MHz.
It is used as the further scheme of invention：Step（1）Described soak, is prepared according to the following steps：By silkworm excrement, maple
Face cream, Artemisia japonica, ardisia japonica, Sorrel, dioscoreae septemlobae,rhizoma and asarum are crushed in 100 mesh, input water, are stirring for 130r/min with rotating speed
Device stirring 7min is mixed, the homogeneous 13min under conditions of pressure is 2.3MPa is boiled by fire, and slow fire infusion 36min crosses the filter of 230 mesh
Cloth, takes filtrate, and room temperature naturally cools to temperature for 44 DEG C, obtains soak.
It is used as the further scheme of invention：Step（2）The preparation method of described coloring agent, specifically includes following steps：
A. fresh leaf sumac, fresh humid euphorbia blade of grass and fresh-rose petal are put into rotating speed to crush in 800r/min pulverizer
15min, takes out, and is boiled by fire in input water, slow fire infusion 24min, inserts fermentation 29h in the fermenting case that temperature is 44 DEG C, takes
Go out, continue slow fire infusion 36min and be 66r/min with rotating speed agitator be stirred continuously, cross 240 mesh filter clothes, take filtrate, obtain flower
Leaf liquid；
B. sodium citrate and reactive brilliant red are added in floral leaf liquid, the agitator for being 100r/min with rotating speed stirring 9min, plus
Enter jumcus bufonius and Medulla Tetrapanacis extract continues to stir 6min, the homogeneous 25min under conditions of pressure is 5.7MPa must be dyed
Agent.
The saline solution immersion 80h that temperature in use is 52 DEG C after dyeing, mass fraction is 3.1%, does not occur discoloration.
Comparative example
The common staining method of the levant cotton exocarp of prior art
, there is serious discoloration in the saline solution immersion 20h that temperature in use is 52 DEG C after dyeing, mass fraction is 1.2%.
Claims (3)
1. a kind of processing method for improving levant cotton exocarp tinctorial property, it is characterised in that specific method is as follows：
（1）Immersion, freezing and microwave drying treatment
Levant cotton exocarp is broken into flap, constant temperature in soak is immersed in and soaks 480 ~ 490min, take out, it is -19 ~ -18 to insert temperature
DEG C household freezer 115 ~ 120min of cryostat, -4 ~ -3 DEG C, cryostat are warming up to 1.1 ~ 1.2 DEG C/min heating rate
135 ~ 140min, microwave drying to moisture is 4% ~ 5% under conditions of frequency is 350 ~ 360MHz；
Described soak, is made up of the raw material of following parts by weight：4.5 ~ 4.7 parts of silkworm excrement, 7.6 ~ 7.8 parts of resina liquidamberis, Artemisia japonica 3.3
~ 3.5 parts, 4.6 ~ 4.8 parts of ardisia japonica, 5.4 ~ 5.6 parts of Sorrel, 4.9 ~ 5.1 parts of dioscoreae septemlobae,rhizoma, 9.4 ~ 9.6 parts of asarum, water 210 ~
220 parts；
（2）Dye and ultrasonically treated
Will be through step（1）Levant cotton exocarp after processing is immersed in 140 ~ 150min of immersion in coloring agent, and application frequency is 25 ~ 26kHz
Ultrasonic echography handle 16 ~ 17min, continue soak 190 ~ 200min, levant cotton exocarp is taken out from coloring agent；
Described coloring agent, is made up of the raw material of following parts by weight：Reactive brilliant red X-B9.4 ~ 9.8 part, 26 ~ 27 parts of fresh leaf sumac,
0.85 ~ 0.89 part of jumcus bufonius, 0.75 ~ 0.77 part of Medulla Tetrapanacis extract, 33 ~ 35 parts of fresh humid euphorbia blade of grass, fresh-rose petal
21 ~ 23 parts, 6.4 ~ 6.8 parts of sodium citrate, 160 ~ 170 parts of water；
（3）Baking and microwave drying treatment
Will be through step（2）Levant cotton exocarp after processing inserts the baking box that temperature is 55 ~ 57 DEG C and toasts 190 ~ 200s, takes out, in frequency
Rate is that microwave drying to moisture is 7% ~ 8% under conditions of 470 ~ 480MHz.
2. the processing method according to claim 1 for improving levant cotton exocarp tinctorial property, it is characterised in that step（1）It is described
Soak, prepared according to the following steps：Silkworm excrement, resina liquidamberis, Artemisia japonica, ardisia japonica, Sorrel, dioscoreae septemlobae,rhizoma and asarum are crushed
To 90 ~ 100 mesh, put into water, 6 ~ 7min is stirred for 120 ~ 130r/min agitator with rotating speed, be 2.2 ~ 2.3MPa in pressure
Under conditions of 12 ~ 13min of homogeneous, be boiled by fire, slow fire 34 ~ 36min of infusion crosses 220 ~ 230 mesh filter clothes, takes filtrate, room temperature from
Temperature is so cooled to for 42 ~ 44 DEG C, soak is obtained.
3. the processing method according to claim 1 for improving levant cotton exocarp tinctorial property, it is characterised in that step（2）It is described
Coloring agent preparation method, specifically include following steps：
A. fresh leaf sumac, fresh humid euphorbia blade of grass and fresh-rose petal are put into rotating speed to crush in 780 ~ 800r/min pulverizer
14 ~ 15min, is taken out, and is boiled by fire in input water, and slow fire 22 ~ 24min of infusion is inserted and sent out in the fermenting case that temperature is 42 ~ 44 DEG C
27 ~ 29h of ferment, takes out, and continues 34 ~ 36min of slow fire infusion and is simultaneously stirred continuously with rotating speed for 64 ~ 66r/min agitator, excessively 230 ~
240 mesh filter clothes, take filtrate, obtain floral leaf liquid；
B. sodium citrate and reactive brilliant red are added in floral leaf liquid, with rotating speed for 95 ~ 100r/min agitator stirring 8 ~
9min, adds jumcus bufonius and Medulla Tetrapanacis extract continues to stir 5 ~ 6min, under conditions of pressure is 5.5 ~ 5.7MPa
23 ~ 25min of matter, obtains coloring agent.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108748532A (en) * | 2018-06-08 | 2018-11-06 | 阜南县永盛工艺品有限公司 | A kind of dyeing treatment of levant cotton exocarp |
| CN108908606A (en) * | 2018-05-17 | 2018-11-30 | 阜南县铭钰柳木工艺品有限公司 | A kind of toughening dyeing treatment of wheat stalk |
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| CN108748532A (en) * | 2018-06-08 | 2018-11-06 | 阜南县永盛工艺品有限公司 | A kind of dyeing treatment of levant cotton exocarp |
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