CN107114652A - A kind of golden elder berry extract Compositional antiseptic agent - Google Patents
A kind of golden elder berry extract Compositional antiseptic agent Download PDFInfo
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- CN107114652A CN107114652A CN201710406464.6A CN201710406464A CN107114652A CN 107114652 A CN107114652 A CN 107114652A CN 201710406464 A CN201710406464 A CN 201710406464A CN 107114652 A CN107114652 A CN 107114652A
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- 239000000284 extract Substances 0.000 title claims abstract description 166
- 235000007440 Sambucus pubens f xanthocarpa Nutrition 0.000 title claims abstract description 80
- 244000007821 Sambucus pubens f. xanthocarpa Species 0.000 title claims abstract description 80
- 239000004599 antimicrobial Substances 0.000 title claims abstract description 36
- 241000972672 Phellodendron Species 0.000 claims abstract description 42
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims abstract description 40
- 235000010241 potassium sorbate Nutrition 0.000 claims abstract description 40
- 239000004302 potassium sorbate Substances 0.000 claims abstract description 40
- 229940069338 potassium sorbate Drugs 0.000 claims abstract description 40
- 238000002360 preparation method Methods 0.000 claims abstract description 22
- 239000001509 sodium citrate Substances 0.000 claims abstract description 22
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims description 56
- 238000010992 reflux Methods 0.000 claims description 52
- 230000001476 alcoholic effect Effects 0.000 claims description 49
- 238000000605 extraction Methods 0.000 claims description 44
- 239000002893 slag Substances 0.000 claims description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 238000002137 ultrasound extraction Methods 0.000 claims description 28
- 239000011812 mixed powder Substances 0.000 claims description 27
- 241000218691 Cupressaceae Species 0.000 claims description 24
- 239000012141 concentrate Substances 0.000 claims description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 21
- 238000001914 filtration Methods 0.000 claims description 21
- 238000000967 suction filtration Methods 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 15
- 239000000706 filtrate Substances 0.000 claims description 14
- 238000000227 grinding Methods 0.000 claims description 14
- 230000002829 reductive effect Effects 0.000 claims description 14
- 239000002002 slurry Substances 0.000 claims description 14
- 239000000779 smoke Substances 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 7
- 238000013329 compounding Methods 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 235000013399 edible fruits Nutrition 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 4
- 235000021028 berry Nutrition 0.000 claims description 3
- 238000005260 corrosion Methods 0.000 claims description 2
- 230000002421 anti-septic effect Effects 0.000 abstract description 13
- 239000000243 solution Substances 0.000 description 69
- 230000000052 comparative effect Effects 0.000 description 7
- 235000008429 bread Nutrition 0.000 description 6
- 239000003755 preservative agent Substances 0.000 description 6
- 235000013305 food Nutrition 0.000 description 5
- 235000019249 food preservative Nutrition 0.000 description 5
- 239000005452 food preservative Substances 0.000 description 5
- 230000002335 preservative effect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 244000005700 microbiome Species 0.000 description 4
- 230000001988 toxicity Effects 0.000 description 4
- 231100000419 toxicity Toxicity 0.000 description 4
- 241000233866 Fungi Species 0.000 description 3
- 241000208829 Sambucus Species 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 235000008995 european elder Nutrition 0.000 description 3
- 235000005979 Citrus limon Nutrition 0.000 description 2
- 244000131522 Citrus pyriformis Species 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000003899 bactericide agent Substances 0.000 description 2
- 239000000022 bacteriostatic agent Substances 0.000 description 2
- 238000009395 breeding Methods 0.000 description 2
- 230000001488 breeding effect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 2
- 235000010234 sodium benzoate Nutrition 0.000 description 2
- 239000004299 sodium benzoate Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 235000018735 Sambucus canadensis Nutrition 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 229940064004 antiseptic throat preparations Drugs 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000007123 blue elder Nutrition 0.000 description 1
- 235000007124 elderberry Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000006916 nutrient agar Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of golden elder berry extract Compositional antiseptic agent, it is made up of the raw material below according to parts by weight：20 24 parts of potassium sorbate, 12 16 parts of golden elder berry extract, 23 parts of sodium citrate, 58 parts of phellodendron extract.The invention also discloses the preparation method of the golden elder berry extract Compositional antiseptic agent.Compositional antiseptic agent prepared by the present invention has good antiseptic property, compounded by golden elder berry extract, sodium citrate, phellodendron extract and potassium sorbate, on the basis of security is ensured, strengthen antiseptic effect, with important market value and social value.
Description
Technical field
The present invention relates to preservative technology field, specifically a kind of golden elder berry extract Compositional antiseptic agent.
Background technology
Food preservative is to prevent putrid and deteriorated, extension effective period of food quality the additive as caused by microorganism.Because simultaneous
Prevent microbial reproduction from causing food poisoning, also known as antimicrobial.Its main function is to suppress micro- in food
Biological breeding.It is important that it can suppress the generation of most easy putrefaction in varied situations, particularly make in general sterilizing
With it is insufficient when still have continuation effect.
Conventional food preservative can be divided into bactericide and the class of bacteriostatic agent two by effect.With the food for killing microbial action
Product additive is referred to as bactericide, can suppress growth of microorganism the additive referred to as bacteriostatic agent of breeding.Preservative presses component and source
It is broadly divided into chemical classes food preservative and natural class food preservative.Food preservative species is various, and China is up to the present
Food antiseptics that 32 kinds of approved is used, most common of which has sodium benzoate, potassium sorbate etc..The toxicity of sodium benzoate
It is stronger than potassium sorbate, and inhibitory effect is only the 1/3 of potassium sorbate under identical acidity value, therefore many countries gradually use
Potassium sorbate.Potassium sorbate is to generally acknowledge one of safest chemical preservative in the world at present, main to suppress mould and yeast.But
It is that effect is not played in the case where microorganism is excessive, therefore it is applied to have good hygiene condition and micro organism quantity less
Food in.If a kind of Compositional antiseptic agent can be researched and developed based on potassium sorbate, on the basis of security is ensured, enhancing anti-corrosion effect
Really, by with important market value and social value.
The content of the invention
It is an object of the invention to provide a kind of golden elder berry extract Compositional antiseptic agent, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
20-24 parts, 12-16 parts of golden elder berry extract, 2-3 parts of sodium citrate, 5-8 parts of phellodendron extract.
It is used as further scheme of the invention：It is made up of the raw material below according to parts by weight：21-23 parts of potassium sorbate, west
13-15 parts of Sambucus hi Rra L berry extract, 2.3-2.7 parts of sodium citrate, 6-7 parts of phellodendron extract.
It is used as further scheme of the invention：It is made up of the raw material below according to parts by weight：22 parts of potassium sorbate, the West
14 parts of elderberry extract, 2.5 parts of sodium citrate, 6.5 parts of phellodendron extract.
It is used as further scheme of the invention：The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 1-2 times of weight, slurries are polished into using beater, to slurry
Liquid carries out suction filtration processing, obtains smoke filtrate and suction filtration slag；
A2) suction filtration slag is put into container, the alcoholic solution of 6-8 times of weight is added, after being uniformly mixed, 3- is stood
5h, heating and refluxing extraction 1-2h, filtering obtain a reflux extracting liquid and a refluxing extraction slag, by a refluxing extraction slag
The alcoholic solution of 3-4 times of weight is added again, after being uniformly mixed, stands 1-2h, heating and refluxing extraction 40-50min, mistake
Filter, obtains secondary back extract solution and secondary back extracts slag, and a reflux extracting liquid and secondary back extract solution are merged, obtained
Obtain the total liquid of refluxing extraction；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, it is that relative density is 1.10-1.12 at 60 DEG C that concentration, which is evaporated under reduced pressure,
Concentrate, concentrate is spray-dried, golden elder berry extract is produced.
It is used as further scheme of the invention：Step a2) in, the alcoholic solution is the alcohol water of volumetric concentration 80%
Solution.
It is used as further scheme of the invention：The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 50-80 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 12-15 times of weight, obtain percolate and
The diacolation dregs of a decoction；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 2-3 times of weight, ultrasonic wave extraction 40-45min, mistake is added
Filter, obtains ultrasonic extraction liquid and ultrasonic extraction residue, and ultrasonic extraction residue is added to the water of 6-8 times of weight, soaks 3-4h, decocts
50-60min, filtering obtains to decoct extract solution and decoct and extracts residue；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.10-1.12 concentrate, concentrate is spray-dried, and produces phellodendron extract.
It is used as further scheme of the invention：Step b2) in, the alcoholic solution is the alcohol water of volumetric concentration 75%
Solution.
It is used as further scheme of the invention：Step b3) in, the alcoholic solution is the alcohol water of volumetric concentration 60%
Solution.
The preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 80-100 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 50-60 mesh sieves, obtains second and mixes
Close powder；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Compared with prior art, the beneficial effects of the invention are as follows：
Compositional antiseptic agent prepared by the present invention has good antiseptic property, passes through golden elder berry extract, lemon
Sour sodium, phellodendron extract and potassium sorbate are compounded, on the basis of security is ensured, strengthen antiseptic effect, with important
Market value and social value.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
20 parts, 12 parts of golden elder berry extract, 2 parts of sodium citrate, 5 parts of phellodendron extract.
The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 1 times of weight, slurries are polished into using beater, to slurries
Suction filtration processing is carried out, smoke filtrate and suction filtration slag is obtained；
A2) suction filtration slag is put into container, the alcoholic solution of 6 times of weight is added, after being uniformly mixed, 3h is stood, plus
Circumfluence distillation 1h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, a refluxing extraction slag is added again
The alcoholic solution of 3 times of weight, after being uniformly mixed, stands 1h, heating and refluxing extraction 40min, filtering obtains secondary back and carried
Take liquid and secondary back to extract slag, a reflux extracting liquid and secondary back extract solution are merged, the total liquid of refluxing extraction is obtained, its
In, the alcoholic solution is the alcohol water blend of volumetric concentration 80%；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, be evaporated under reduced pressure concentration be at 60 DEG C relative density be 1.10 it is dense
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 50 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 12 times of weight, percolate and diacolation is obtained
The dregs of a decoction, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 75%；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 2 times of weight is added, ultrasonic wave extraction 40min, filtering is obtained
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 6 times of weight, 3h is soaked, 50min, mistake is decocted
Filter, obtains to decoct extract solution and decoct and extracts residue, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 60%；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.10 concentrate, concentrate is spray-dried, and produces phellodendron extract.
In the present embodiment, the preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 80 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 50 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Embodiment 2
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
21 parts, 13 parts of golden elder berry extract, 2.7 parts of sodium citrate, 7 parts of phellodendron extract.
The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 1 times of weight, slurries are polished into using beater, to slurries
Suction filtration processing is carried out, smoke filtrate and suction filtration slag is obtained；
A2) suction filtration slag is put into container, the alcoholic solution of 7 times of weight is added, after being uniformly mixed, 3.5h is stood,
Heating and refluxing extraction 1h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, a refluxing extraction slag is added again
Enter the alcoholic solution of 3 times of weight, after being uniformly mixed, stand 1.5h, heating and refluxing extraction 42min, filtering obtains secondary returning
Flow extract solution and secondary back extracts slag, a reflux extracting liquid and secondary back extract solution are merged, refluxing extraction is obtained total
Liquid, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 80%；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, be evaporated under reduced pressure concentration be at 60 DEG C relative density be 1.10 it is dense
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 60 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 13 times of weight, percolate and diacolation is obtained
The dregs of a decoction, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 75%；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 2 times of weight is added, ultrasonic wave extraction 41min, filtering is obtained
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 7 times of weight, 3.5h is soaked, 50min is decocted,
Filtering, obtains to decoct extract solution and decoct and extracts residue, wherein, the alcoholic solution is water-soluble for the alcohol of volumetric concentration 60%
Liquid；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.10 concentrate, concentrate is spray-dried, and produces phellodendron extract.
In the present embodiment, the preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 90 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 50 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Embodiment 3
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
22 parts, 14 parts of golden elder berry extract, 2.5 parts of sodium citrate, 6.5 parts of phellodendron extract.
The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 1.5 times of weight, slurries are polished into using beater, to slurry
Liquid carries out suction filtration processing, obtains smoke filtrate and suction filtration slag；
A2) suction filtration slag is put into container, the alcoholic solution of 7 times of weight is added, after being uniformly mixed, 4h is stood, plus
Circumfluence distillation 1.5h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, a refluxing extraction slag is added again
Enter the alcoholic solution of 3.5 times of weight, after being uniformly mixed, stand 1.5h, heating and refluxing extraction 45min, filtering is obtained secondary
Reflux extracting liquid and secondary back extract slag, and a reflux extracting liquid and secondary back extract solution are merged, refluxing extraction is obtained
Total liquid, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 80%；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, be evaporated under reduced pressure concentration be at 60 DEG C relative density be 1.11 it is dense
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 70 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 14 times of weight, percolate and diacolation is obtained
The dregs of a decoction, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 75%；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 2.5 times of weight is added, ultrasonic wave extraction 43min is filtered,
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 7 times of weight, 3.5h is soaked, decocted
55min, filtering obtains to decoct extract solution and decoct and extracts residue, wherein, the alcoholic solution is the alcohol of volumetric concentration 60%
The aqueous solution；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.11 concentrate, concentrate is spray-dried, and produces phellodendron extract.
In the present embodiment, the preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 90 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 60 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Embodiment 4
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
23 parts, 15 parts of golden elder berry extract, 2.3 parts of sodium citrate, 6 parts of phellodendron extract.
The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 2 times of weight, slurries are polished into using beater, to slurries
Suction filtration processing is carried out, smoke filtrate and suction filtration slag is obtained；
A2) suction filtration slag is put into container, the alcoholic solution of 7 times of weight is added, after being uniformly mixed, 4.5h is stood,
Heating and refluxing extraction 1.5h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, by a refluxing extraction slag again
The alcoholic solution of 4 times of weight is added, after being uniformly mixed, 2h, heating and refluxing extraction 48min is stood, filtering obtains secondary returning
Flow extract solution and secondary back extracts slag, a reflux extracting liquid and secondary back extract solution are merged, refluxing extraction is obtained total
Liquid, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 80%；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, be evaporated under reduced pressure concentration be at 60 DEG C relative density be 1.12 it is dense
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 70 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 14 times of weight, percolate and diacolation is obtained
The dregs of a decoction, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 75%；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 3 times of weight is added, ultrasonic wave extraction 44min, filtering is obtained
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 7 times of weight, 3.5h is soaked, 60min is decocted,
Filtering, obtains to decoct extract solution and decoct and extracts residue, wherein, the alcoholic solution is water-soluble for the alcohol of volumetric concentration 60%
Liquid；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.12 concentrate, concentrate is spray-dried, and produces phellodendron extract.
In the present embodiment, the preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 90 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 60 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Embodiment 5
A kind of golden elder berry extract Compositional antiseptic agent, is made up of the raw material below according to parts by weight：Potassium sorbate
24 parts, 16 parts of golden elder berry extract, 3 parts of sodium citrate, 8 parts of phellodendron extract.
The preparation method of the golden elder berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 2 times of weight, slurries are polished into using beater, to slurries
Suction filtration processing is carried out, smoke filtrate and suction filtration slag is obtained；
A2) suction filtration slag is put into container, the alcoholic solution of 8 times of weight is added, after being uniformly mixed, 5h is stood, plus
Circumfluence distillation 2h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, a refluxing extraction slag is added again
The alcoholic solution of 4 times of weight, after being uniformly mixed, stands 2h, heating and refluxing extraction 50min, filtering obtains secondary back and carried
Take liquid and secondary back to extract slag, a reflux extracting liquid and secondary back extract solution are merged, the total liquid of refluxing extraction is obtained, its
In, the alcoholic solution is the alcohol water blend of volumetric concentration 80%；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, be evaporated under reduced pressure concentration be at 60 DEG C relative density be 1.12 it is dense
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
The preparation method of the phellodendron extract is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 80 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 15 times of weight, percolate and diacolation is obtained
The dregs of a decoction, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 75%；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 3 times of weight is added, ultrasonic wave extraction 45min, filtering is obtained
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 8 times of weight, 4h is soaked, 60min, mistake is decocted
Filter, obtains to decoct extract solution and decoct and extracts residue, wherein, the alcoholic solution is the alcohol water blend of volumetric concentration 60%；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.12 concentrate, concentrate is spray-dried, and produces phellodendron extract.
In the present embodiment, the preparation method of the golden elder berry extract Compositional antiseptic agent, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 100 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 60 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding is produced anti-
Rotten agent.
Comparative example 1
Preservative is used as using potassium sorbate.
Comparative example 2
Compared with Example 3, without potassium sorbate, other are same as Example 3.
Comparative example 3
Compared with Example 3, without golden elder berry extract and potassium sorbate, other are same as Example 3.
Antiseptic property is tested
Preservative prepared by embodiment 3 and comparative example 1-3 is configured to the antiseptic solution that concentration is 5mg/mL, will be dried
Baked bread is divided into five groups, the antiseptic solution that first group of sprinkling embodiment 3 is configured, and second group to the 4th group is sprayed respectively
The antiseptic solution that embodiment 3 and comparative example 1-3 are configured, it is molten that fountain height uniformly sprays 1mL preservatives for every bread surface
Liquid, the 5th group of bread surface sprays the pure water of equal volume.Then this five groups of bread are used into freshness protection package packaging, is put into 25
DEG C insulating box in store, record once a day the total plate count and fungi count on bread, continuous record ten days.Result of the test is such as
Shown in table 1.
Counting method is poured into using flat board.Total plate count detection uses nutrient agar, 37 DEG C of culture 48h；Fungi count
Detection uses glucose agar medium, 28 DEG C of culture 5d.Aforesaid operations are carried out in gnotobasis.
The result of the test statistical form of table 1
Note：Cake bread sanitary standard GB7099-2003, it is desirable to total number of bacteria ＜ 1500CFU/g, fungi count ＜
100CFU/g。
As can be seen from the above table, first group of shelf-life is most long, and the 5th group worst, and second group and the 3rd group is superior to the 4th
Group.
Due to comparative example 1 compared with Example 3, without golden elder berry extract, other are same as Example 3.It is right
Compared with Example 3, without potassium sorbate, other are same as Example 3 for ratio 2.Comparative example 3 compared with Example 3, without west
Sambucus hi Rra L berry extract and potassium sorbate, other are same as Example 3.Therefore as can be seen that the present invention from result above
Compositional antiseptic agent is by adding golden elder berry extract and potassium sorbate, golden elder berry extract and potassium sorbate phase
Mutually coordinate, and with other components compatibility, it is possible to increase the antiseptic effect of the Compositional antiseptic agent.
Compositional antiseptic agent prepared by the present invention uses potassium sorbate, golden elder berry extract, sodium citrate and golden cypress
Extract is formulated, and potassium sorbate toxicity is relatively low, and golden elder berry extract, sodium citrate and phellodendron extract are nontoxic
Property, so as to " dilute " toxicity of potassium sorbate to a certain extent, the Compositional antiseptic agent that this four components are constituted is weighed on an equal basis
The lower toxicity of amount is less than pure potassium sorbate, in addition, the antiseptic effect of Compositional antiseptic agent prepared by the present invention, better than pure potassium sorbate.
Compositional antiseptic agent prepared by the present invention has good antiseptic property, passes through golden elder berry extract, lemon
Sour sodium, phellodendron extract and potassium sorbate are compounded, on the basis of security is ensured, strengthen antiseptic effect, with important
Market value and social value.
The better embodiment to the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
, can also be on the premise of present inventive concept not be departed from formula, the knowledge that one skilled in the relevant art possesses
Various changes can be made.
Claims (9)
1. a kind of golden elder berry extract Compositional antiseptic agent, it is characterised in that be made up of the raw material below according to parts by weight：
20-24 parts of potassium sorbate, 12-16 parts of golden elder berry extract, 2-3 parts of sodium citrate, 5-8 parts of phellodendron extract.
2. golden elder berry extract Compositional antiseptic agent according to claim 1, it is characterised in that by below according to weight
The raw material of amount part is made：21-23 parts of potassium sorbate, 13-15 parts of golden elder berry extract, 2.3-2.7 parts of sodium citrate, Huang
6-7 parts of cypress extract.
3. golden elder berry extract Compositional antiseptic agent according to claim 2, it is characterised in that by below according to weight
The raw material of amount part is made：22 parts of potassium sorbate, 14 parts of golden elder berry extract, 2.5 parts of sodium citrate, phellodendron extract
6.5 part.
4. golden elder berry extract Compositional antiseptic agent according to claim 1, it is characterised in that the Western synthetism
The preparation method of wooden berry extract is as follows：
A1) take golden elder fruit, after cleaning, add the water of 1-2 times of weight, be polished into slurries using beater, enter to slurries
The processing of row suction filtration, obtains smoke filtrate and suction filtration slag；
A2) suction filtration slag is put into container, the alcoholic solution of 6-8 times of weight is added, after being uniformly mixed, 3-5h is stood, plus
Circumfluence distillation 1-2h, filtering obtains a reflux extracting liquid and a refluxing extraction slag, a refluxing extraction slag is added again
Enter the alcoholic solution of 3-4 times of weight, after being uniformly mixed, stand 1-2h, heating and refluxing extraction 40-50min, filter, obtain
Secondary back extract solution and secondary back extract slag, and a reflux extracting liquid and secondary back extract solution are merged, flowed back
Extract total liquid；
A3) the total liquid of refluxing extraction and smoke filtrate are merged, it is that relative density is the dense of 1.10-1.12 at 60 DEG C that concentration, which is evaporated under reduced pressure,
Contracting liquid, concentrate is spray-dried, and produces golden elder berry extract.
5. golden elder berry extract Compositional antiseptic agent according to claim 4, it is characterised in that step a2) in, institute
State the alcohol water blend that alcoholic solution is volumetric concentration 80%.
6. golden elder berry extract Compositional antiseptic agent according to claim 1, it is characterised in that the golden cypress is extracted
The preparation method of thing is as follows：
B1 golden cypress) is taken, is cleaned, drying is ground, and crosses 50-80 mesh sieves, obtains golden cypress powder；
B2) golden cypress powder is put into percolator, diacolation is carried out with the alcoholic solution of 12-15 times of weight, percolate and diacolation is obtained
The dregs of a decoction；
B3) the diacolation dregs of a decoction are put into container, the alcoholic solution of 2-3 times of weight is added, ultrasonic wave extraction 40-45min is filtered,
Ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is added to the water of 6-8 times of weight, 3-4h is soaked, 50- is decocted
60min, filtering obtains to decoct extract solution and decoct and extracts residue；
B4) by percolate, ultrasonic extraction liquid and decoct extract solution and merge, it is that relative density is at 60 DEG C that concentration, which is evaporated under reduced pressure,
1.10-1.12 concentrate, concentrate is spray-dried, and produces phellodendron extract.
7. golden elder berry extract Compositional antiseptic agent according to claim 6, it is characterised in that step b2) in, institute
State the alcohol water blend that alcoholic solution is volumetric concentration 75%.
8. golden elder berry extract Compositional antiseptic agent according to claim 6, it is characterised in that step b3) in, institute
State the alcohol water blend that alcoholic solution is volumetric concentration 60%.
9. a kind of preparation method of golden elder berry extract Compositional antiseptic agent as described in claim 1-8 is any, it is special
Levy and be, step is as follows：
1) golden elder berry extract and phellodendron extract are prepared, it is standby；
2) potassium sorbate and sodium citrate are weighed, mixed grinding crosses 80-100 mesh sieves, obtains the first mixed-powder；
3) golden elder berry extract and phellodendron extract are weighed, mixed grinding crosses 50-60 mesh sieves, obtains the second mixed powder
End；
4) after being well mixed the first mixed-powder and the second mixed-powder, golden elder berry extract compounding anti-corrosion is produced
Agent.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055244A (en) * | 2015-08-24 | 2015-11-18 | 上海东晟源日化有限公司 | Organic natural plant preservative |
| CN106038398A (en) * | 2016-06-30 | 2016-10-26 | 广州市禾基生物科技有限公司 | Method for preparing cortex phellodendri extract and application of cortex phellodendri extract composition prepared from cortex phellodendri extract in bacteriostatic agent |
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2017
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105055244A (en) * | 2015-08-24 | 2015-11-18 | 上海东晟源日化有限公司 | Organic natural plant preservative |
| CN106038398A (en) * | 2016-06-30 | 2016-10-26 | 广州市禾基生物科技有限公司 | Method for preparing cortex phellodendri extract and application of cortex phellodendri extract composition prepared from cortex phellodendri extract in bacteriostatic agent |
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