CN107099996A - A kind of microwave dyeing color fixing process of polyester fabric - Google Patents

A kind of microwave dyeing color fixing process of polyester fabric Download PDF

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Publication number
CN107099996A
CN107099996A CN201710408758.2A CN201710408758A CN107099996A CN 107099996 A CN107099996 A CN 107099996A CN 201710408758 A CN201710408758 A CN 201710408758A CN 107099996 A CN107099996 A CN 107099996A
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Prior art keywords
microwave
dyeing
color fixing
terylene
polyester fabric
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CN201710408758.2A
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Inventor
卫必兵
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Ma'anshan Ever Home Textile Co Ltd
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Ma'anshan Ever Home Textile Co Ltd
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Priority to CN201710408758.2A priority Critical patent/CN107099996A/en
Publication of CN107099996A publication Critical patent/CN107099996A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M10/00Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
    • D06M10/04Physical treatment combined with treatment with chemical compounds or elements
    • D06M10/06Inorganic compounds or elements
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48Derivatives of carbohydrates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/60General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
    • D06P1/613Polyethers without nitrogen
    • D06P1/6131Addition products of hydroxyl groups-containing compounds with oxiranes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642Compounds containing nitrogen
    • D06P1/649Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491(Thio)urea or (cyclic) derivatives
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/653Nitrogen-free carboxylic acids or their salts
    • D06P1/6533Aliphatic, araliphatic or cycloaliphatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/34Material containing ester groups
    • D06P3/52Polyesters
    • D06P3/54Polyesters using dispersed dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02After-treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02After-treatment
    • D06P5/10After-treatment with compounds containing metal
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/20Physical treatments affecting dyeing, e.g. ultrasonic or electric
    • D06P5/2011Application of vibrations, pulses or waves for non-thermic purposes

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of microwave dyeing color fixing process of polyester fabric, it is related to field of printing and dyeing, including terylene pretreatment, dye liquor mixed processing, microwave dyeing flow, microwave color fixing and cleaning process and sizing winding, the present invention has advantages below:Polyester fabric is pre-processed using microwave, later stage dye-uptake and colour fixation is improved;By dye liquor mixing microwave treatment, the solubility of disperse dyes is improved, the dispersion stabilization of disperse dyes is improved, Color is improved;During microwave dyeing, the method for microwave power is increased than keeping the constant colouring method of microwave power to be compared with common steam or heating water bath printing and dyeing using the stage, chemical fiber fabric dyeing firmness after dyeing, color is plentiful and dye uniformity increases;Heated in dyeing terylene laking process using microwave, heating is rapid, uniform, efficient energy-saving.

Description

A kind of microwave dyeing color fixing process of polyester fabric
Technical field
The present invention relates to field of printing and dyeing, and in particular to a kind of microwave dyeing color fixing process of polyester fabric.
Background technology
In recent years, the Chinese dyeing industry output value and yield balanced growth is about 17%, is quickly grown, but average rate of profit is only Have 3% or so.The dyeing for illustrating China still has that product specification is relatively low, added value is not high, process technology innovation is not enough, The problems such as equipment falls behind relatively, energy resource consumption is huge, environmental pollution is serious, clean manufacturing is pushed slowly.
In printing and dyeing enterprise, water, electricity, coal energy cost account for 40% of totle drilling cost or so, are only second to dyestuff.Current water resource Worsening shortages, energy shortage, energy expenditure straight rise increases the production cost of printing and dyeing enterprise, it is necessary to use conservation measures.
At present, printing and dyeing enterprise is in dye fixing flow, and often by steam or heating water bath, the energy disappears during one side Consumption is huge, and heat utilization ratio is low, and another aspect steam or water bath heating fault often occur as a piece of cloth and last block Cloth often uneven dyeing and selvedge uneven color.
Microwave dyeing is exactly the staining technique heated using microwave, and microwave has a fuel factor and non-thermal effect, it is inside and outside simultaneously Heating, allows fabric to reach the inside and outside effect with heat in a short time, and the dyeing uniformity of fabric is greatly improved, dye-uptake High, chromaticity index height and good color fastness.And the energy resource consumption of printing and dyeing enterprise can be greatly reduced.
Application notification number discloses a kind of two kinds of pure cotton fabric microwave color fixings for the A of CN 103276613 Chinese patent Colouring method, including (1) microwave dip method:Configuration dye liquor → addition accelerant → is put into pure cotton bleached cotton fabric → microwave dyeing 1- 8min → addition alkaline agent → microwave color fixing 8min, (2) microwave pad-dyeing method:By High Temperature Type Reactive Dyes, accelerant, alkaline agent in room temperature Lower mixing, stirs;Pure cotton fabric is subjected to microwave pad dyeing in above-mentioned dye liquor.The colouring method of the microwave color fixing is only For pure cotton fabric, we are verified by studying, and change conditional parameter and material auxiliary agent, obtain being adapted to the microwave dye of polyester fabric Color color fixing process.
The content of the invention
(1) technical problem solved
In view of the shortcomings of the prior art, the invention provides a kind of microwave dyeing color fixing process of polyester fabric so that washs The dyeing uniformity of synthetic fibre fabric, dye-uptake, chromaticity index and color fastness are all improved, and reduce the energy of printing and dyeing enterprise Consumption and waste gas discharge, protect environment.
(2) technical scheme
To realize object above, the present invention is achieved by the following technical programs:
A kind of microwave dyeing color fixing process of polyester fabric, comprises the following steps:
(1) pre-process:Terylene is put into sodium hydroxide solution, OP-4 is added, it is 500-700W to control microwave power, 5-15min is radiated, waste liquid of draining, centrifugal dehydration after washing twice, room temperature is dried;
(2) dye liquor mixed processing:By disperse dyes, urea, glacial acetic acid, sodium alginate, levelling agent MCH-315, compounding point Powder is added sequentially in water, microwave radiation stirring, and it is 200-400W to control microwave power, and mixing speed is 40-70r/min, Radiate 3-5min;
(3) dyeing flow:Terylene is added in above-mentioned dye liquor, microwave power 200-400W, microwave dyeing 7min is controlled Afterwards, increase microwave power is to 500-700W, after microwave dyeing 5min, pads dye liquor, controls padding machine rotating speed 2.5m/min, pick-up 30%, then preliminary drying 2-5min, 80 DEG C of preliminary drying temperature;
(4) fixation cleaning process:Xiang Shuizhong adds color fixing agent, sodium sulphate and pre-baked terylene, controls microwave power After 300-800W, microwave heating fixation 5-10min, by terylene successively with after suds and cold water elution, dry;
(5) sizing winding:Terylene after drying is shaped, 170-200 DEG C of setting temperature, speed 20-28m/min, finally Terylene is wound.
Preferably, the mass percent concentration of the sodium hydroxide solution is 10%.
Preferably, the disperse dyes in the step (2) are dispersed ruby SE-GFL, disperse orange SE-RFL, disperse blue SE- One kind in 2R, dispersed ruby H-2GFL, disperse orange S-4RL and disperse blue S-GL.
Preferably, the compounding dispersant in the step (2) is that AEO and sodium lignin sulfonate are compounded Form, and the consumption of the compounding dispersant is the 2-5% of disperse dyes quality used.
Preferably, the color fixing agent in the step (4) is color fixing agent HH-365.
Preferably, the mass percent concentration of the suds in the step (4) is 5%.
(3) beneficial effect
The invention provides a kind of microwave dyeing color fixing process of polyester fabric, with advantages below:
(1) polyester fabric is pre-processed using microwave, thus it is possible to vary the surface texture of terylene, carries out supramolecular structure It is modified, improve later stage dye-uptake and colour fixation.
(2) by dye liquor mixing microwave treatment, the solubility of disperse dyes can be effectively improved, point of disperse dyes is improved Stability is dissipated, Color is improved.The dispersant compounded can greatly improve solubility of the disperse dyes in water, shorten dye Expect jitter time, the dispersion of stable dispersion dyestuff improves the Color of dyestuff.
(3) during microwave dyeing, dye molecule heats up in the presence of microwave because occurring induction, so as to Quick colouring and fixation on terylene, by checking, during microwave dyeing, increase the method ratio of microwave power using the stage The constant colouring method of microwave power is kept to be compared with common steam or heating water bath printing and dyeing, the chemical fiber fabric dyeing jail after dyeing Soundness, color is plentiful and dye uniformity increases.
(4) heated in dyeing terylene laking process using microwave, heating is rapid, uniform, efficient energy-saving, with common steam Compared with heating water bath, save energy more than 60%, reduce the production cost of enterprise, saved the energy, reduce waste gas row Put and protect environment, and there is microwave sterilization to remove mould effect, can kill the bacterium in cloth.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1:
A kind of microwave dyeing color fixing process of polyester fabric, comprises the following steps:
(1) pre-process:Terylene is put into the sodium hydroxide solution that mass percent concentration is 10%, adds OP-4, It is 600W to control microwave power, radiates 12min, and waste liquid of draining, centrifugal dehydration after washing twice, room temperature is dried;
(2) dye liquor mixed processing:By disperse dyes, urea, glacial acetic acid, sodium alginate, levelling agent MCH-315, compounding point Powder is added sequentially in water, microwave radiation stirring, and it is 250W to control microwave power, and mixing speed is 50r/min, radiation 4min;
(3) dyeing flow:Terylene is added in above-mentioned dye liquor, controlled after microwave power 300W, microwave dyeing 7min, is increased Plus microwave power is to 600W, after microwave dyeing 5min, dye liquor is padded, padding machine rotating speed 2.5m/min is controlled, pick-up 30%, then in advance Dry 4min, 80 DEG C of preliminary drying temperature;
(4) fixation cleaning process:Xiang Shuizhong adds color fixing agent HH-365, sodium sulphate and pre-baked terylene, controls microwave After power 600W, microwave heating fixation 7min, by terylene successively with after suds and cold water elution, dry;
(5) sizing winding:By the terylene sizing after drying, 180 DEG C of setting temperature, speed 25m/min finally receives terylene Volume.
Wherein, the disperse dyes in step (2) be dispersed ruby SE-GFL, disperse orange SE-RFL, disperse blue SE-2R, point Dissipate one kind in carbuncle H-2GFL and disperse blue S-GL;It is that AEO and sodium lignin sulfonate are multiple to compound dispersant With into and the consumption of compounding dispersant is the 2% of disperse dyes quality used.
Embodiment 2:
A kind of microwave dyeing color fixing process of polyester fabric, comprises the following steps:
(1) pre-process:Terylene is put into the sodium hydroxide solution that mass percent concentration is 10%, adds OP-4, It is 500W to control microwave power, radiates 10min, and waste liquid of draining, centrifugal dehydration after washing twice, room temperature is dried;
(2) dye liquor mixed processing:By disperse dyes, urea, glacial acetic acid, sodium alginate, levelling agent MCH-315, compounding point Powder is added sequentially in water, microwave radiation stirring, and it is 300W to control microwave power, and mixing speed is 40r/min, radiation 3min;
(3) dyeing flow:Terylene is added in above-mentioned dye liquor, controlled after microwave power 200W, microwave dyeing 7min, is increased Plus microwave power is to 500W, after microwave dyeing 5min, dye liquor is padded, padding machine rotating speed 2.5m/min is controlled, pick-up 30%, then in advance Dry 3min, 80 DEG C of preliminary drying temperature;
(4) fixation cleaning process:Xiang Shuizhong adds color fixing agent HH-365, sodium sulphate and pre-baked terylene, controls microwave After power 500W, microwave heating fixation 5min, by terylene successively with after suds and cold water elution, dry;
(5) sizing winding:By the terylene sizing after drying, 170 DEG C of setting temperature, speed 20m/min finally receives terylene Volume.
Wherein, the disperse dyes in step (2) be dispersed ruby SE-GFL, disperse orange SE-RFL, disperse blue SE-2R, point Dissipate one kind in carbuncle H-2GFL and disperse blue S-GL;It is that AEO and sodium lignin sulfonate are multiple to compound dispersant With into and the consumption of compounding dispersant is the 4% of disperse dyes quality used.
Embodiment 3:
A kind of microwave dyeing color fixing process of polyester fabric, comprises the following steps:
(1) pre-process:Terylene is put into the sodium hydroxide solution that mass percent concentration is 10%, adds OP-4, It is 700W to control microwave power, radiates 15min, and waste liquid of draining, centrifugal dehydration after washing twice, room temperature is dried;
(2) dye liquor mixed processing:By disperse dyes, urea, glacial acetic acid, sodium alginate, levelling agent MCH-315, fatty alcohol APEO and the dispersant of sodium lignin sulfonate compounding are added sequentially in water, and microwave radiation stirring controls microwave Power is 200W, and mixing speed is 60r/min, radiates 5min;
(3) dyeing flow:Terylene is added in above-mentioned dye liquor, controlled after microwave power 400W, microwave dyeing 7min, is increased Plus microwave power is to 700W, after microwave dyeing 5min, dye liquor is padded, padding machine rotating speed 2.5m/min is controlled, pick-up 30%, then in advance Dry 5min, 80 DEG C of preliminary drying temperature;
(4) fixation cleaning process:Xiang Shuizhong adds color fixing agent HH-365, sodium sulphate and pre-baked terylene, controls microwave After power 800W, microwave heating fixation 10min, by terylene successively with after suds and cold water elution, dry;
(5) sizing winding:By the terylene sizing after drying, 200 DEG C of setting temperature, speed 27m/min finally receives terylene Volume.
Wherein, the disperse dyes in step (2) be dispersed ruby SE-GFL, disperse orange SE-RFL, disperse blue SE-2R, point Dissipate one kind in carbuncle H-2GFL and disperse blue S-GL;It is that AEO and sodium lignin sulfonate are multiple to compound dispersant With into and the consumption of compounding dispersant is the 5% of disperse dyes quality used.
Embodiment 4:
The microwave dyeing color fixing process of polyester fabric is substantially the same manner as Example 1 in embodiment 4, and difference is, step (1) Middle microwave power is 600W, and it is the 3% of disperse dyes quality used, microwave to radiate compounding dispersant dosage in 5min, step (2) Power is 400W, and mixing speed is 70r/min, radiates in 4min, step (3) and successively controls microwave power to be 300W and 700W, Microwave power 300W in preliminary drying 2min, step (4), heats 190 DEG C of setting temperature, speed 28m/ in fixation 8min, step (5) min。
Embodiment 5:
The microwave dyeing color fixing process of polyester fabric is substantially the same manner as Example 1 in embodiment 5, and difference is, step (1) Middle microwave power is 500W, and it is the 4% of disperse dyes quality used, microwave to radiate compounding dispersant dosage in 8min, step (2) Power is 250W, and mixing speed is 40r/min, radiates in 3min, step (3) and successively controls microwave power to be 200W and 500W, Microwave power 400W in preliminary drying 4min, step (4), heats 170 DEG C of setting temperature, speed 26m/ in fixation 8min, step (5) min。
Performance test:
The chemical fibre testing result of embodiment 1-5 dyeing, as shown in table 1:
Table 1:Testing result
To sum up, the embodiment of the present invention has good dyefastness and dye uptake.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments The present invention is described in detail, it will be understood by those within the art that:It still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic;And these modification or Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (6)

1. the microwave dyeing color fixing process of a kind of polyester fabric, it is characterised in that comprise the following steps:
(1) pre-process:Terylene is put into sodium hydroxide solution, OP-4 is added, it is 500-700W, radiation to control microwave power 5-15min, waste liquid of draining, centrifugal dehydration after washing twice, room temperature is dried;
(2) dye liquor mixed processing:By disperse dyes, urea, glacial acetic acid, sodium alginate, levelling agent MCH-315, compounding dispersant It is added sequentially in water, microwave radiation stirring, it is 200-400W to control microwave power, and mixing speed is 40-70r/min, radiation Stir 3-5min;
(3) dyeing flow:Terylene is added in above-mentioned dye liquor, controlled after microwave power 200-400W, microwave dyeing 7min, is increased Plus microwave power is to 500-700W, after microwave dyeing 5min, dye liquor is padded, padding machine rotating speed 2.5m/min is controlled, pick-up 30%, Preliminary drying 2-5min, 80 DEG C of preliminary drying temperature again;
(4) fixation cleaning process:Xiang Shuizhong adds color fixing agent, sodium sulphate and pre-baked terylene, control microwave power 300- After 800W, microwave heating fixation 5-10min, by terylene successively with after suds and cold water elution, dry;
(5) sizing winding:By the terylene sizing after drying, 170-200 DEG C of setting temperature, speed 20-28m/min will finally be washed Synthetic fibre is wound.
2. the microwave dyeing color fixing process of polyester fabric as claimed in claim 1, it is characterised in that the sodium hydroxide solution Mass percent concentration be 10%.
3. the microwave dyeing color fixing process of polyester fabric as claimed in claim 1, it is characterised in that in the step (2) Disperse dyes are dispersed ruby SE-GFL, disperse orange SE-RFL, disperse blue SE-2R, dispersed ruby H-2GFL, disperse orange S-4RL With one kind in disperse blue S-GL.
4. the microwave dyeing color fixing process of polyester fabric as claimed in claim 1, it is characterised in that in the step (2) Compounding dispersant is that AEO and sodium lignin sulfonate compounding are formed, and the consumption of the compounding dispersant is institute With the 2-5% of disperse dyes quality.
5. the microwave dyeing color fixing process of polyester fabric as claimed in claim 1, it is characterised in that in the step (4) Color fixing agent is color fixing agent HH-365.
6. the microwave dyeing color fixing process of polyester fabric as claimed in claim 1, it is characterised in that in the step (4) The mass percent concentration of suds is 5%.
CN201710408758.2A 2017-06-02 2017-06-02 A kind of microwave dyeing color fixing process of polyester fabric Pending CN107099996A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
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CN108179643A (en) * 2017-12-28 2018-06-19 嘉兴市庆联纺织印染科技有限公司 Spin production method in four sides elasticity spring Asia
CN108824036A (en) * 2018-05-31 2018-11-16 镇江虎瑞生物科技有限公司 A kind of method of microwave treatment printing and dyeing fixation cloth
CN108930172A (en) * 2018-06-04 2018-12-04 安徽恒益纺织科技有限公司 A method of it improving non-woven fabrics and disperses pad dyeing degree of fixation
CN108951236A (en) * 2018-06-04 2018-12-07 安徽恒益纺织科技有限公司 A method of improving home decoration cotton textiles dye gigging degree of fixation
CN109306585A (en) * 2018-08-15 2019-02-05 青岛即发集团股份有限公司 A kind of fabric dyeing method and dyeing apparatus
CN110863379A (en) * 2019-11-21 2020-03-06 艾绳瑞 Coloring agent for polyester fibers

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1293283A (en) * 1999-10-18 2001-05-02 绍兴市永通印染技术开发中心 Microwave dyeing method for fabric

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1293283A (en) * 1999-10-18 2001-05-02 绍兴市永通印染技术开发中心 Microwave dyeing method for fabric

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
张壮余等: "《染料应用》", 30 September 1958, 高等教育出版社 *
梁治齐等: "《功能性表面活性剂》", 30 April 2002, 中国轻工业出版社 *
赵雪等: "微波在纺织品染色中的应用研究", 《染整技术》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108179643A (en) * 2017-12-28 2018-06-19 嘉兴市庆联纺织印染科技有限公司 Spin production method in four sides elasticity spring Asia
CN108824036A (en) * 2018-05-31 2018-11-16 镇江虎瑞生物科技有限公司 A kind of method of microwave treatment printing and dyeing fixation cloth
CN108930172A (en) * 2018-06-04 2018-12-04 安徽恒益纺织科技有限公司 A method of it improving non-woven fabrics and disperses pad dyeing degree of fixation
CN108951236A (en) * 2018-06-04 2018-12-07 安徽恒益纺织科技有限公司 A method of improving home decoration cotton textiles dye gigging degree of fixation
CN109306585A (en) * 2018-08-15 2019-02-05 青岛即发集团股份有限公司 A kind of fabric dyeing method and dyeing apparatus
CN110863379A (en) * 2019-11-21 2020-03-06 艾绳瑞 Coloring agent for polyester fibers

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Application publication date: 20170829