CN110438828A - A kind of organic pigment coating dyeing method of blended fabric - Google Patents
A kind of organic pigment coating dyeing method of blended fabric Download PDFInfo
- Publication number
- CN110438828A CN110438828A CN201810420402.5A CN201810420402A CN110438828A CN 110438828 A CN110438828 A CN 110438828A CN 201810420402 A CN201810420402 A CN 201810420402A CN 110438828 A CN110438828 A CN 110438828A
- Authority
- CN
- China
- Prior art keywords
- organic pigment
- pigment coating
- blended fabric
- agent
- dyeing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/6426—Heterocyclic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
Abstract
The invention discloses a kind of organic pigment coating dyeing methods of blended fabric, compound organic pigment coating fine latex of the preparation for the characteristic of blended fabric, fine latex, which is used, to be mixed containing certain inorganic pigment coating with organic pigment coating, use N- (4- propanoic acid tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid as solvent simultaneously, under the action of other auxiliary agents, the cladding ability and adhesion of further organic pigment coating fine latex, furthermore the fabric treating before being dyed using Low Temperature Plasma Treating technique, to improve the glossiness and mellow and full property of blend fibre, make naturally to distort and disappear, the more fluffy adhesive force to increase dyeing, secondary color fixing process increases colour fixation；Mixed fiber fabric dyeing effect after the dyeing is uniform, not fugitive color, especially increases its uvioresistant ageing resistance, has efficient sun-resistant water scrub function, and color fastness is strong, and dyeing effect color is clearly demarcated, and industrialization degree is high.
Description
Technical field
The present invention relates to the processing method of fabric more particularly to a kind of organic pigment pigment dyeing sides of blended fabric
Method.
Background technique
Fiber type at present on the market is more and more abundant, and knitted fabric, at coil, is mutually established rules according to one by yarn bends
Rule string set is coupled, and is the important family of textile and woven, supatex fabric are classified as three main kind of, In of textile
Meet domestic market demand, foreign exchange earning aspect has played great function.
Knitted fabric it is various in style, by raw material can be divided into cotton fabrics, woollen jersey, silk knitted fabric, chemical fibre be knitted
Object and blended fabric etc., wherein blended fabric as its using two or more different fibers carry out it is blended made of, In
It is particularly susceptible during dyeing and finishing and the problems such as dyeing is uneven, and fixation is difficult, fugitive color, intolerant to washing solarization occurs.
Organic pigment pigment dyeing has many advantages, such as compared with conventional dyes dye: organic coating dyeing has process
It is short, the simple process and advantage not selective to fiber is contaminated suitable for the dyeing of various fibers especially for conventional dyes
The blend fibre of color difficulty, the advantage of organic pigment pigment dyeing are especially apparent, and have superior color fastness after the completion of dyeing；
But for blended fabric, the usual adhesion strength of organic pigment pigment dyeing is poor, is easy when carrying out textile dyeing
The problem for hardly possible of now painting.
A kind of worth research of the organic pigment coating dyeing method suitable for blended fabric can solve the above problem.
Summary of the invention
Goal of the invention: in order to solve the problems of prior art, the present invention provides a kind of easy to operate, colourings
Fastly, dyeing effect is uniform, not fugitive color, the organic pigment coating dyeing method of the strong blended fabric of sun-resistant water scrub function.
Technical solution: in order to achieve the above objectives, the invention adopts the following technical scheme: a kind of organic face of blended fabric
Expect coating dyeing method, comprising the following steps:
(1) preparation of compound organic pigment coating fine latex: first by inorganic pigment coating and organic pigment with 1:10
Mass ratio mixed, be added in 30-50 times of volumes of deionized water, while the N- (4- of solvent volume one third is added
Propanoic acid tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid, assistant for emulsifying agent, dispersing agent, in 500W ultrasound 120s in Vltrasonic device
After obtain dispersion liquid；It is first cooled to room temperature after placing 1h after being warming up to 65 DEG C of heating and thermal insulation 10min and carries out high-speed stirred 5min；Side
It stirs side and emulsifier is added, continue to be placed in 300W in Vltrasonic device and be ultrasonically treated 100s, 90 DEG C of copolyreaction after initiator are added
It is overnight to obtain compound organic pigment coating fine latex；
(2) pre-treatment is dyed: preparation blended fabric fabric, bath raio 1:28, addition enzyme refining agent, dosage 1-2g/L,
Immersion treatment is carried out after being warming up to 48-55 DEG C, is naturally cooling to room temperature after heat preservation 20min and is washed；Bath raio 1:28 when washing,
Be added the neutral detergent that mass fraction is 1%-2% carry out multiple washing dehydration to 8 one-tenth it is dry；
(3) Low Temperature Plasma Treating technique: processing gas is the mixed gas of helium and nitrogen, processing power 220-
250W, specific using plasma processing 3min, hot water wash 5min, corona treatment 3min, cold water wash the processing side of 5min
Formula；
(4) presetting technology: will be placed on job platform, built-in edge region by the blended fabric of ultrasonic treatment,
Make fabric nature spread apart；Pre-setting heat treatment is carried out to its surface, makes corrugationless on fabric, it is naturally smooth；
(5) organic pigment pigment dyeing treatment process: carrying out dyeing 25min for the blended fabric after presetting technology,
The dye composite of bath raio 1:8, investment include following components in mass: 30-55 parts of compound organic pigment coating fine latex,
5 parts of dispersing agent, 12 parts of reserve salt, 6 parts of chitosan, 15 parts of wetting agent, 6 parts of levelling agent, 7 parts of surfactant, 280 parts of water；
(6) two secondary color fixing process: are carried out after the blended fabric after organic pigment pigment dyeing is taken out washing
Secondary fixation treatment, dehydration to eighty per cant it is dry after continue put into fixation container, be added fabric weight 6% compound organic pigment coating
Fine latex, color fixing agent, linolenic mixture first carry out low-temperature solid color 18min, then carry out medium temperature fixation 8min, finally carry out
Low temperature fixation 12min；
(7) reduction cleaning: the blended fabric after step (6) fixation is subjected to reduction cleaning, removes staining and loose colour；
(8) it dries: blended fabric being placed in ventilating and cooling place and is dried, temperature is 25-35 DEG C；
(9) it presses whole: the blended fabric after drying being pressed into integer using flatiron.
More preferably, inorganic pigment coating described in step (1) is titania/silica composite inorganic coating.
More preferably, in the titania/silica composite inorganic coating titanium dioxide and silica matter
Amount is than being 1:3.
More preferably, the mixing that assistant for emulsifying agent is sodium alginate and sodium acrylate mass ratio is 3:1 in the step (1)
Object.
More preferably, dispersing agent is macromolecule dispersing agent in the step (1).
More preferably, initiator described in step (1) is sodium hydrogensulfite.
More preferably, the mixed gas volume ratio of helium and nitrogen is 1:4 in step (3).
More preferably, the mixing that wetting agent described in step (5) is soybean lecithin and polyalcohols mass ratio is 2:3
Object.
More preferably, surfactant described in step (5) is nonionic surface active agent.
More preferably, color fixing agent described in step (6) is acrylate and the poly- ammonium salt mass ratio of chitosan is the mixed of 2:3
Close object.
The utility model has the advantages that a kind of organic pigment coating dyeing method of blended fabric provided by the present invention, preparation are directed to
The compound organic pigment coating fine latex of the characteristic of blended fabric, fine latex use containing certain inorganic pigment coating with
The mixing of organic pigment coating, while using N- (4- propanoic acid tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid is as solvent, at it
Under the action of his auxiliary agent, furthermore the cladding ability and adhesion of further organic pigment coating fine latex use low-temperature plasma
Fabric treating before body treatment process is dyed makes naturally distortion disappear to improve the glossiness and mellow and full property of blend fibre
It loses, the more fluffy adhesive force to increase dyeing, secondary color fixing process increases colour fixation；Blend fibre after the dyeing
Textile dyeing uniform in effect, fugitive color, does not increase its uvioresistant ageing resistance especially, has efficient sun-resistant washing function
Can, color fastness is strong, and dyeing effect color is clearly demarcated, and industrialization degree is high.
Specific embodiment
Invention is further explained combined with specific embodiments below:
Embodiment 1:
A kind of organic pigment coating dyeing method of blended fabric, comprising the following steps:
(1) preparation of compound organic pigment coating fine latex: first by inorganic pigment coating and organic pigment with 1:10
Mass ratio mixed, be added in 30 times of volumes of deionized water, while N- (the 4- propionic acid of solvent volume one third is added
The tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid, assistant for emulsifying agent, dispersing agent, in Vltrasonic device after 500W ultrasound 120s
To dispersion liquid；It is first cooled to room temperature after placing 1h after being warming up to 65 DEG C of heating and thermal insulation 10min and carries out high-speed stirred 5min；Side stirring
Emulsifier is added in side, continues to be placed in 300W in Vltrasonic device and is ultrasonically treated 100s, 90 DEG C of copolyreaction are overnight after initiator is added
Obtain compound organic pigment coating fine latex；The inorganic pigment coating is that the titania/silica that mass ratio is 1:3 is multiple
Close inorganic coating；The mixture that assistant for emulsifying agent is sodium alginate and sodium acrylate mass ratio is 3:1；Dispersing agent is macromolecule dispersion
Agent；The initiator is sodium hydrogensulfite；
(2) it dyes pre-treatment: preparing blended fabric fabric, enzyme refining agent is added in bath raio 1:28, and dosage 1g/L rises
Temperature keeps the temperature to immersion treatment is carried out after 48 DEG C and is naturally cooling to room temperature after 20min and is washed；Bath raio 1:28 when washing is added
The neutral detergent that mass fraction is 1% carry out multiple washing dehydration to 8 one-tenth it is dry；
(3) Low Temperature Plasma Treating technique: processing gas is the mixed gas of the helium that volume ratio is 1:4 and nitrogen,
Processing power is 220W, and specific using plasma processing 3min, hot water wash 5min, corona treatment 3min, cold water are washed
The processing mode of 5min；
(4) presetting technology: will be placed on job platform, built-in edge region by the blended fabric of ultrasonic treatment,
Make fabric nature spread apart；Pre-setting heat treatment is carried out to its surface, makes corrugationless on fabric, it is naturally smooth；
(5) organic pigment pigment dyeing treatment process: carrying out dyeing 25min for the blended fabric after presetting technology,
The dye composite of bath raio 1:8, investment include following components in mass: compound organic pigment coating fine latex 30 part, point
5 parts of powder, 12 parts of reserve salt, 6 parts of chitosan, 15 parts of wetting agent, 6 parts of levelling agent, 7 parts of surfactant, 280 parts of water；It is described
The mixture that wetting agent is soybean lecithin and polyalcohols mass ratio is 2:3；The surfactant is non-ionic surface
Activating agent；
(6) two secondary color fixing process: are carried out after the blended fabric after organic pigment pigment dyeing is taken out washing
Secondary fixation treatment, dehydration to eighty per cant it is dry after continue put into fixation container, be added fabric weight 6% compound organic pigment coating
Fine latex, color fixing agent, linolenic mixture first carry out low-temperature solid color 18min, then carry out medium temperature fixation 8min, finally carry out
Low temperature fixation 12min；The mixture that the color fixing agent is acrylate and the poly- ammonium salt mass ratio of chitosan is 2:3；
(7) reduction cleaning: the blended fabric after step (6) fixation is subjected to reduction cleaning, removes staining and loose colour；
(8) it dries: blended fabric being placed in ventilating and cooling place and is dried, temperature is 25 DEG C；
(9) it presses whole: the blended fabric after drying being pressed into integer using flatiron.
Embodiment 2:
A kind of organic pigment coating dyeing method of blended fabric, comprising the following steps:
(1) preparation of compound organic pigment coating fine latex: first by inorganic pigment coating and organic pigment with 1:10
Mass ratio mixed, be added in 50 times of volumes of deionized water, while N- (the 4- propionic acid of solvent volume one third is added
The tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid, assistant for emulsifying agent, dispersing agent, in Vltrasonic device after 500W ultrasound 120s
To dispersion liquid；It is first cooled to room temperature after placing 1h after being warming up to 65 DEG C of heating and thermal insulation 10min and carries out high-speed stirred 5min；Side stirring
Emulsifier is added in side, continues to be placed in 300W in Vltrasonic device and is ultrasonically treated 100s, 90 DEG C of copolyreaction are overnight after initiator is added
Obtain compound organic pigment coating fine latex；The inorganic pigment coating is that the titania/silica that mass ratio is 1:3 is multiple
Close inorganic coating；The mixture that assistant for emulsifying agent is sodium alginate and sodium acrylate mass ratio is 3:1；Dispersing agent is macromolecule dispersion
Agent；The initiator is sodium hydrogensulfite；
(2) it dyes pre-treatment: preparing blended fabric fabric, enzyme refining agent is added in bath raio 1:28, and dosage 2g/L rises
Temperature keeps the temperature to immersion treatment is carried out after 55 DEG C and is naturally cooling to room temperature after 20min and is washed；Bath raio 1:28 when washing is added
The neutral detergent that mass fraction is 2% carry out multiple washing dehydration to 8 one-tenth it is dry；
(3) Low Temperature Plasma Treating technique: processing gas is the mixed gas of the helium that volume ratio is 1:4 and nitrogen,
Processing power is 250W, and specific using plasma processing 3min, hot water wash 5min, corona treatment 3min, cold water are washed
The processing mode of 5min；
(4) presetting technology: will be placed on job platform, built-in edge region by the blended fabric of ultrasonic treatment,
Make fabric nature spread apart；Pre-setting heat treatment is carried out to its surface, makes corrugationless on fabric, it is naturally smooth；
(5) organic pigment pigment dyeing treatment process: carrying out dyeing 25min for the blended fabric after presetting technology,
The dye composite of bath raio 1:8, investment include following components in mass: compound organic pigment coating fine latex 55 part, point
5 parts of powder, 12 parts of reserve salt, 6 parts of chitosan, 15 parts of wetting agent, 6 parts of levelling agent, 7 parts of surfactant, 280 parts of water；It is described
The mixture that wetting agent is soybean lecithin and polyalcohols mass ratio is 2:3；The surfactant is non-ionic surface
Activating agent；
(6) two secondary color fixing process: are carried out after the blended fabric after organic pigment pigment dyeing is taken out washing
Secondary fixation treatment, dehydration to eighty per cant it is dry after continue put into fixation container, be added fabric weight 6% compound organic pigment coating
Fine latex, color fixing agent, linolenic mixture first carry out low-temperature solid color 18min, then carry out medium temperature fixation 8min, finally carry out
Low temperature fixation 12min；The mixture that the color fixing agent is acrylate and the poly- ammonium salt mass ratio of chitosan is 2:3；
(7) reduction cleaning: the blended fabric after step (6) fixation is subjected to reduction cleaning, removes staining and loose colour；
(8) it dries: blended fabric being placed in ventilating and cooling place and is dried, temperature is 35 DEG C；
(9) it presses whole: the blended fabric after drying being pressed into integer using flatiron.
Embodiment 3:
A kind of organic pigment coating dyeing method of blended fabric, comprising the following steps:
(1) preparation of compound organic pigment coating fine latex: first by inorganic pigment coating and organic pigment with 1:10
Mass ratio mixed, be added in 40 times of volumes of deionized water, while N- (the 4- propionic acid of solvent volume one third is added
The tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid, assistant for emulsifying agent, dispersing agent, in Vltrasonic device after 500W ultrasound 120s
To dispersion liquid；It is first cooled to room temperature after placing 1h after being warming up to 65 DEG C of heating and thermal insulation 10min and carries out high-speed stirred 5min；Side stirring
Emulsifier is added in side, continues to be placed in 300W in Vltrasonic device and is ultrasonically treated 100s, 90 DEG C of copolyreaction are overnight after initiator is added
Obtain compound organic pigment coating fine latex；The inorganic pigment coating is that the titania/silica that mass ratio is 1:3 is multiple
Close inorganic coating；The mixture that assistant for emulsifying agent is sodium alginate and sodium acrylate mass ratio is 3:1；Dispersing agent is macromolecule dispersion
Agent；The initiator is sodium hydrogensulfite；
(2) pre-treatment is dyed: preparation blended fabric fabric, bath raio 1:28, addition enzyme refining agent, dosage 1.5g/L,
Immersion treatment is carried out after being warming up to 52 DEG C, is naturally cooling to room temperature after heat preservation 20min and is washed；Bath raio 1:28 when washing, adds
Enter the neutral detergent that mass fraction is 1.5% carry out multiple washing dehydration to 8 one-tenth it is dry；
(3) Low Temperature Plasma Treating technique: processing gas is the mixed gas of the helium that volume ratio is 1:4 and nitrogen,
Processing power is 240W, and specific using plasma processing 3min, hot water wash 5min, corona treatment 3min, cold water are washed
The processing mode of 5min；
(4) presetting technology: will be placed on job platform, built-in edge region by the blended fabric of ultrasonic treatment,
Make fabric nature spread apart；Pre-setting heat treatment is carried out to its surface, makes corrugationless on fabric, it is naturally smooth；
(5) organic pigment pigment dyeing treatment process: carrying out dyeing 25min for the blended fabric after presetting technology,
The dye composite of bath raio 1:8, investment include following components in mass: compound organic pigment coating fine latex 45 part, point
5 parts of powder, 12 parts of reserve salt, 6 parts of chitosan, 15 parts of wetting agent, 6 parts of levelling agent, 7 parts of surfactant, 280 parts of water；It is described
The mixture that wetting agent is soybean lecithin and polyalcohols mass ratio is 2:3；The surfactant is non-ionic surface
Activating agent；
(6) two secondary color fixing process: are carried out after the blended fabric after organic pigment pigment dyeing is taken out washing
Secondary fixation treatment, dehydration to eighty per cant it is dry after continue put into fixation container, be added fabric weight 6% compound organic pigment coating
Fine latex, color fixing agent, linolenic mixture first carry out low-temperature solid color 18min, then carry out medium temperature fixation 8min, finally carry out
Low temperature fixation 12min；The mixture that the color fixing agent is acrylate and the poly- ammonium salt mass ratio of chitosan is 2:3；
(7) reduction cleaning: the blended fabric after step (6) fixation is subjected to reduction cleaning, removes staining and loose colour；
(8) it dries: blended fabric being placed in ventilating and cooling place and is dried, temperature is 25-35 DEG C；
(9) it presses whole: the blended fabric after drying being pressed into integer using flatiron.
By the embodiment 1-3 same blended fabric fabric for carrying out treated fabric and traditional handicraft dyeing and finishing be comparative example into
The test of row anti-uv-ray, the results are shown in Table 1:
1 embodiment 1-3 of table and comparative example uvioresistant absorbability compare
Use a kind of organic pigment coating dyeing method of blended fabric of above-described embodiment 1-3, hence it is evident that improve mixed
The various problems occurred in dyeing knitted fabric are spun, dyeing and finishing technology yields improves 35%, and the fabric uniform in color after dyeing and finishing,
Not colour contamination, wrong color, coloring effect is good, beautiful and generous, bright in colour, does not fade, uvioresistant of the finished product to each wavelength period ultraviolet light
Line absorption ability is good, to impart its superior sun-resistant water scrub function.
It should be pointed out that the above specific embodiment is only illustrative of the invention and is not intended to limit the scope of the invention, In
After having read the present invention, those skilled in the art fall within power appended by the application to the modification of various equivalent forms of the invention
Benefit requires limited range.
Claims (10)
1. a kind of organic pigment coating dyeing method of blended fabric, it is characterised in that the following steps are included:
(1) preparation of compound organic pigment coating fine latex: first by inorganic pigment coating and organic pigment with the matter of 1:10
Amount ratio is mixed, and is added in 30-50 times of volumes of deionized water, while N- (the 4- propionic acid of solvent volume one third is added
The tert-butyl ester-phenyl) -5- oxo-pyrrolidine -2- carboxylic acid, assistant for emulsifying agent, dispersing agent, in Vltrasonic device after 500W ultrasound 120s
To dispersion liquid；It is first cooled to room temperature after placing 1h after being warming up to 65 DEG C of heating and thermal insulation 10min and carries out high-speed stirred 5min；Side stirring
Emulsifier is added in side, continues to be placed in 300W in Vltrasonic device and is ultrasonically treated 100s, 90 DEG C of copolyreaction are overnight after initiator is added
Obtain compound organic pigment coating fine latex；
(2) it dyes pre-treatment: preparing blended fabric fabric, enzyme refining agent, dosage 1-2g/L, heating is added in bath raio 1:28
Immersion treatment is carried out after to 48-55 DEG C, is naturally cooling to room temperature after heat preservation 20min and is washed；Bath raio 1:28 when washing is added
The neutral detergent that mass fraction is 1%-2% carry out multiple washing dehydration to 8 one-tenth it is dry；
(3) Low Temperature Plasma Treating technique: processing gas is the mixed gas of helium and nitrogen, processing power 220-
250W, specific using plasma processing 3min, hot water wash 5min, corona treatment 3min, cold water wash the processing side of 5min
Formula；
(4) it presetting technology: will be placed on job platform by the blended fabric of ultrasonic treatment, built-in edge region makes to knit
Object nature spread apart；Pre-setting heat treatment is carried out to its surface, makes corrugationless on fabric, it is naturally smooth；
(5) blended fabric after presetting technology organic pigment pigment dyeing treatment process: is subjected to dyeing 25min, bath raio
The dye composite of 1:8, investment include following components in mass: 30-55 parts of compound organic pigment coating fine latex, dispersion
5 parts of agent, 12 parts of reserve salt, 6 parts of chitosan, 15 parts of wetting agent, 6 parts of levelling agent, 7 parts of surfactant, 280 parts of water；
(6) it secondary color fixing process: will be carried out after the blended fabric taking-up washing after organic pigment pigment dyeing secondary solid
Color processing, dehydration to eighty per cant it is dry after continue put into fixation container, be added fabric weight 6% the compound micro- glue of organic pigment coating
Cream, color fixing agent, linolenic mixture first carry out low-temperature solid color 18min, then carry out medium temperature fixation 8min, finally carry out low temperature
Fixation 12min；
(7) reduction cleaning: the blended fabric after step (6) fixation is subjected to reduction cleaning, removes staining and loose colour；
(8) it dries: blended fabric being placed in ventilating and cooling place and is dried, temperature is 25-35 DEG C；
(9) it presses whole: the blended fabric after drying being pressed into integer using flatiron.
2. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
(1) inorganic pigment coating described in is titania/silica composite inorganic coating.
3. a kind of organic pigment coating dyeing method of blended fabric according to claim 2, it is characterised in that: described
The mass ratio of titanium dioxide and silica is 1:3 in titania/silica composite inorganic coating.
4. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: described
The mixture that assistant for emulsifying agent is sodium alginate and sodium acrylate mass ratio is 3:1 in step (1).
5. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: described
Dispersing agent is macromolecule dispersing agent in step (1).
6. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
(1) initiator described in is sodium hydrogensulfite.
7. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
(3) the mixed gas volume ratio of helium and nitrogen is 1:4 in.
8. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
(5) mixture that wetting agent described in is soybean lecithin and polyalcohols mass ratio is 2:3.
9. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
(5) surfactant described in is nonionic surface active agent.
10. a kind of organic pigment coating dyeing method of blended fabric according to claim 1, it is characterised in that: step
Suddenly the mixture that color fixing agent described in (6) is acrylate and the poly- ammonium salt mass ratio of chitosan is 2:3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420402.5A CN110438828A (en) | 2018-05-04 | 2018-05-04 | A kind of organic pigment coating dyeing method of blended fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420402.5A CN110438828A (en) | 2018-05-04 | 2018-05-04 | A kind of organic pigment coating dyeing method of blended fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110438828A true CN110438828A (en) | 2019-11-12 |
Family
ID=68428149
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810420402.5A Withdrawn CN110438828A (en) | 2018-05-04 | 2018-05-04 | A kind of organic pigment coating dyeing method of blended fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110438828A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111535049A (en) * | 2020-06-08 | 2020-08-14 | 武汉纺织大学 | Inorganic pigment dyeing method for cotton textiles |
| CN114855474A (en) * | 2022-06-25 | 2022-08-05 | 江苏鼎新印染有限公司 | Dyeing process of blended fabric |
| CN115322589A (en) * | 2022-08-25 | 2022-11-11 | 杭州萧山环保化工有限公司 | Pigment not easy to fade and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616554A (en) * | 2003-09-25 | 2005-05-18 | 默克专利股份有限公司 | Encapsulated pigments |
| CN105002761A (en) * | 2015-08-17 | 2015-10-28 | 青岛大学 | Preparation and application method of separable micro latex for pigment dyeing |
| CN106436359A (en) * | 2016-08-23 | 2017-02-22 | 苏州市恒信针织印染有限责任公司 | Ecological dyeing and finishing process of polyester fiber fabric |
-
2018
- 2018-05-04 CN CN201810420402.5A patent/CN110438828A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616554A (en) * | 2003-09-25 | 2005-05-18 | 默克专利股份有限公司 | Encapsulated pigments |
| CN105002761A (en) * | 2015-08-17 | 2015-10-28 | 青岛大学 | Preparation and application method of separable micro latex for pigment dyeing |
| CN106436359A (en) * | 2016-08-23 | 2017-02-22 | 苏州市恒信针织印染有限责任公司 | Ecological dyeing and finishing process of polyester fiber fabric |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111535049A (en) * | 2020-06-08 | 2020-08-14 | 武汉纺织大学 | Inorganic pigment dyeing method for cotton textiles |
| CN111535049B (en) * | 2020-06-08 | 2022-05-17 | 武汉纺织大学 | Inorganic pigment dyeing method for cotton textiles |
| CN114855474A (en) * | 2022-06-25 | 2022-08-05 | 江苏鼎新印染有限公司 | Dyeing process of blended fabric |
| CN115322589A (en) * | 2022-08-25 | 2022-11-11 | 杭州萧山环保化工有限公司 | Pigment not easy to fade and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106223076B (en) | A kind of two step exhaust dyeing methods of bath of dispersion reactive dye one of polyester-cotton fabric | |
| CN105200817B (en) | A kind of bright and beautiful cotton reactive dye one-bath process method | |
| CN110438828A (en) | A kind of organic pigment coating dyeing method of blended fabric | |
| CN109371721A (en) | Complete cotton knitted fabric dyeing production technology | |
| CN109680514A (en) | A kind of dyeing for washing ammonia four sides elasticity fabric | |
| CN105908534B (en) | A kind of viscose cheese dyeing | |
| CN105803824B (en) | A kind of Non-water washing reactive dye non-aqueous solvent dyeing method | |
| CN108166241A (en) | Cotton knitwear short route dyeing and finishing technology method | |
| CN109233337B (en) | Black dye composition and dye product | |
| CN104018369A (en) | Process for dyeing silk interwoven jacquard fabric | |
| CN108708190A (en) | A kind of dyeing of Cationic Dyeable Pet | |
| CN100500981C (en) | Gemini type positive ion colloidal and method for improving fabric dyeing fastness | |
| CN108193517A (en) | Terylen cotton knitting cloth directly/dispersion single bath process short route dyeing and finishing technology | |
| CN107287933A (en) | A kind of colouring method of polyimide fiber or polyimides fabric | |
| CN107268300B (en) | A kind of colour bar colouring method of tencel interwoven fabric | |
| CN1635213A (en) | Soybean fiber loose-stock dyeing and processing method | |
| CN110438824A (en) | A kind of coating dyeing and finishing technology of silk fiber fabric | |
| CN108532060A (en) | A kind of spinning process of the good mixed yarn of dyeability | |
| CN109403069A (en) | A kind of dyeing of TR looped fabric | |
| CN104358139A (en) | Dyeing method for improving color fastness of wool and chemical fiber blended fabric | |
| CN101649563A (en) | Room temperature wool pad dyeing microwave color fixing method | |
| JPS6225793B2 (en) | ||
| CN111778735A (en) | Acid rapid pad dyeing method for chinlon 56 fiber and fabric thereof | |
| CN105040471A (en) | Dyeing process of polyester fiber fabric | |
| CN109505160A (en) | A kind of textile dyeing and printing technique |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20191112 |
|
| WW01 | Invention patent application withdrawn after publication |