CN107096299A - A kind of edible oil processes the material vibrating deslagging filtering filter aid that deoils - Google Patents
A kind of edible oil processes the material vibrating deslagging filtering filter aid that deoils Download PDFInfo
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- CN107096299A CN107096299A CN201710265096.8A CN201710265096A CN107096299A CN 107096299 A CN107096299 A CN 107096299A CN 201710265096 A CN201710265096 A CN 201710265096A CN 107096299 A CN107096299 A CN 107096299A
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- parts
- filter aid
- edible oil
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- filter
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
- B01D37/02—Precoating the filter medium; Addition of filter aids to the liquid being filtered
Abstract
The material vibrating deslagging filtering filter aid that deoils is processed the invention discloses a kind of edible oil, is related to edible oil processing technique field, is made up of the raw material of following parts by weight：10 15 parts of microcrystalline cellulose, 5 10 parts of modified crosslinking PVP, 35 parts of volcanic ash, 23 parts of polyethylene glycol oxide, 23 parts of lotus leaf powder, 23 parts of allyl glycidyl ether, 12 parts of polyvinyl alcohol resin, 12 parts of sepiolite fibre, 12 parts of polydiallyldimethyl ammonium chloride, 0.5 1 parts of ATBC, 0.5 1 parts of sodium gluconate, 0.5 1 parts of nanometer titanium dioxide.The use of filter aid of the present invention significantly improves vibrating, deslagging filter filter efficiency, extends the service life of its filter screen, and will not increase waste discharge intractability, and the filter aid is mixed in filter residue to be filtered to remove.
Description
Technical field：
The present invention relates to edible oil processing technique field, and in particular to a kind of edible oil processes material vibrating deslagging mistake of deoiling
Filter filter aid.
Background technology：
Edible oil makes the required consumer goods of people's life, is to provide human body heat energy and essential fatty acid, promotes fat-soluble dimension
The important living material that raw element absorbs.People squeeze edible oil crude oil by raw material of oilseed, and it is refined will be right in crude oil
The impurity pernicious such as edible, storage are removed, and water content is more in crude oil, and the presence of moisture content easily makes grease hydrolysis acid
Lose rotten.The material that deoils after refined need to be filtered through vibrating, deslagging filter, remove the Solid content in the material that deoils, to meet
Discharging of waste liquid standard.And Solid content present in material of deoiling easily causes the blocking of vibrating, deslagging filter screen, reduction
Filter effect, and shorten the service life of filter screen.
For this problem, our company develops a kind of edible oil and processes the material vibrating deslagging filtering filter aid that deoils,
The filter aid, which is mixed into the material that deoils, to significantly improve the filtering of vibrating, deslagging filter on the basis of filter effect is ensured
Efficiency, extends the service life of filter screen, and will not increase the intractability of waste discharge.
The content of the invention：
The technical problems to be solved by the invention be to provide one kind can significantly improve vibrating, deslagging filter filter efficiency,
Extension filter screen service life and will not increase waste discharge intractability edible oil processing deoil material vibrating deslagging filtering use
Filter aid.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of edible oil processes the material vibrating deslagging filtering filter aid that deoils, and is made up of the raw material of following parts by weight：
10-15 parts of microcrystalline cellulose, 5-10 parts of modified crosslinking PVP, 3-5 parts of volcanic ash, 2-3 parts of polyethylene glycol oxide, lotus
2-3 parts of leaf powder, 2-3 parts of allyl glycidyl ether, 1-2 parts of polyvinyl alcohol resin, 1-2 parts of sepiolite fibre, polydiene diformazan
1-2 parts of ammonium chloride, 0.5-1 parts of ATBC, 0.5-1 parts of sodium gluconate, 0.5-1 parts of nanometer titanium dioxide.
Its preparation method comprises the following steps：
(1) allyl glycidyl ether and nanometer titanium dioxide are added into microcrystalline cellulose, and with 5 DEG C/min heating speed
Degree is warming up to 75-80 DEG C of insulation mixing 15-30min, adds polyvinyl alcohol resin and ATBC, is continuously heating to
105-110 DEG C of insulation mixing 10-15min, produces modified microcrystalline cellulose；
(2) polyethylene glycol oxide and sepiolite fibre are added into volcanic ash, microwave treater microwave is utilized after being sufficiently mixed
5-10min is handled, then adds polydiallyldimethyl ammonium chloride and sodium gluconate while hot, 0-5 DEG C of environment is transferred to after being well mixed
Middle standing 1-2h, produces auxiliary material powder；
(3) modified crosslinking PVP, auxiliary material powder and lotus leaf powder are added into modified microcrystalline cellulose, is passed through after being sufficiently mixed
Vacuum compression is blocking, and micro mist most is made through micronizer afterwards.
The modified crosslinking PVP is modified by PVPP and is made, and its specific method of modifying is：To PVPP
Middle addition pre-gelatinized starch and poloxamer, utilize microwave treater microwave treatment 3-5min, add hydrogenation after being sufficiently mixed
Castor oil and sesbania gum, continue microwave treatment 3-5min after being well mixed, are then cooled to 0-5 with 5 DEG C/min cooling rate
DEG C insulation stand 0.5-1h, and into gained mixture add 35-40 DEG C of water, after being sufficiently mixed send into freeze drier in, warp
After fully drying modified crosslinking PVP is produced through gained solid abrasive into powder.
The PVPP, pre-gelatinized starch, poloxamer, rilanit special, the weight consumption ratio of sesbania gum and water
For 15-20:0.5-1:0.3-0.5:0.3-0.5:0.1-0.3:50-80.
Microwave frequency 2450MHz, the power output 700W of the microwave treater.
The pre-gelatinized starch is made up of plant amylum through pre-gelatinized.
The beneficial effects of the invention are as follows：The present invention strengthens helping for microcrystalline cellulose by the preparation of modified microcrystalline cellulose
Effect is filtered, and is aided with the obtained edible oil of modified crosslinking PVP, volcanic ash and a variety of auxiliary agents and processes material vibrating deslagging mistake of deoiling
Filter filter aid, significantly improves vibrating, deslagging filter filter efficiency by the use of the filter aid, extends the use of its filter screen
Life-span, and waste discharge intractability will not be increased, the filter aid is mixed in filter residue to be filtered to remove.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) 2 parts of allyl glycidyl ethers and 0.5 part of nanometer titanium dioxide are added into 15 parts of microcrystalline celluloses, and with 5
DEG C/min programming rate is warming up to 75-80 DEG C of insulation mixing 15min, adds 1 part of polyvinyl alcohol resin and 0.5 part of citric acid
Tributyl, is continuously heating to 105-110 DEG C of insulation mixing 15min, produces modified microcrystalline cellulose；
(2) 3 parts of polyethylene glycol oxides and 1 part of sepiolite fibre are added into 5 parts of volcanic ash, using at microwave after being sufficiently mixed
Device microwave treatment 5min is managed, then adds 1 part of polydiallyldimethyl ammonium chloride and 0.5 part of sodium gluconate while hot, after being well mixed
It is transferred in 0-5 DEG C of environment and stands 1h, produces auxiliary material powder；
(3) 5 parts of modified crosslinking PVPs, auxiliary material powder and 2 parts of lotus leaf powders are added into modified microcrystalline cellulose, it is fully mixed
It is blocking through vacuum compression after conjunction, micro mist most is made through micronizer afterwards.
The preparation of modified crosslinking PVP：0.5 part of pre-gelatinized soybean starch and 0.5 part are added into 20 parts of PVPPs
Poloxamer, utilizes microwave frequency 2450MHz, power output 700W microwave treater microwave treatment 3min after being sufficiently mixed,
0.5 part of rilanit special and 0.3 part of sesbania gum are added, continues microwave treatment 5min after being well mixed, then with 5 DEG C/min's
Cooling rate is cooled to 0-5 DEG C of insulation and stands 1h, and adds 60 parts of 35-40 DEG C of water into gained mixture, is sent after being sufficiently mixed
Enter in freeze drier, modified crosslinking PVP is produced into powder through gained solid abrasive after fully drying.
Embodiment 2
(1) 3 parts of allyl glycidyl ethers and 0.5 part of nanometer titanium dioxide are added into 15 parts of microcrystalline celluloses, and with 5
DEG C/min programming rate is warming up to 75-80 DEG C of insulation mixing 30min, adds 1 part of polyvinyl alcohol resin and 0.5 part of citric acid
Tributyl, is continuously heating to 105-110 DEG C of insulation mixing 10min, produces modified microcrystalline cellulose；
(2) 2 parts of polyethylene glycol oxides and 1 part of sepiolite fibre are added into 5 parts of volcanic ash, using at microwave after being sufficiently mixed
Device microwave treatment 5min is managed, then adds 1 part of polydiallyldimethyl ammonium chloride and 0.5 part of sodium gluconate while hot, after being well mixed
It is transferred in 0-5 DEG C of environment and stands 2h, produces auxiliary material powder；
(3) 8 parts of modified crosslinking PVPs, auxiliary material powder and 2 parts of lotus leaf powders are added into modified microcrystalline cellulose, it is fully mixed
It is blocking through vacuum compression after conjunction, micro mist most is made through micronizer afterwards.
The preparation of modified crosslinking PVP：1 portion of pre-gelatinized wheaten starch and 0.3 part of pool are added into 20 parts of PVPPs
Luo Shamu, utilizes microwave frequency 2450MHz, power output 700W microwave treater microwave treatment 3min after being sufficiently mixed, then
0.5 part of rilanit special and 0.2 part of sesbania gum are added, continues microwave treatment 5min after being well mixed, then with 5 DEG C/min drop
Warm speed is cooled to 0-5 DEG C of insulation and stands 1h, and adds 60 parts of 35-40 DEG C of water into gained mixture, is sent into after being sufficiently mixed
In freeze drier, modified crosslinking PVP is produced into powder through gained solid abrasive after fully drying.
Embodiment 3
(1) 3 parts of allyl glycidyl ethers and 0.5 part of nanometer titanium dioxide are added into 15 parts of microcrystalline celluloses, and with 5
DEG C/min programming rate is warming up to 75-80 DEG C of insulation mixing 30min, adds 1 part of polyvinyl alcohol resin and 0.5 part of citric acid
Tributyl, is continuously heating to 105-110 DEG C of insulation mixing 10min, produces modified microcrystalline cellulose；
(2) 2 parts of polyethylene glycol oxides and 1 part of sepiolite fibre are added into 5 parts of volcanic ash, using at microwave after being sufficiently mixed
Device microwave treatment 5min is managed, then adds 1 part of polydiallyldimethyl ammonium chloride and 0.5 part of sodium gluconate while hot, after being well mixed
It is transferred in 0-5 DEG C of environment and stands 2h, produces auxiliary material powder；
(3) 8 parts of PVPPs, auxiliary material powder and 2 parts of lotus leaf powders are added into modified microcrystalline cellulose, after being sufficiently mixed
It is blocking through vacuum compression, micro mist most is made through micronizer afterwards.
Embodiment 4
Embodiment 1, embodiment 2 and the processing of the made filter aid of embodiment 3 is utilized respectively to deoil with batch 150L fundamentals
Material, and the insoluble suspension formed in the material that deoils is filtered by vibrating, deslagging filter, its drainage effect is determined, as a result
As shown in table 1.
The filter aid drainage effect of the embodiment of the present invention of table 1
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Filter aid consumption | 100g | 100g | 100g |
| Removal of impurity | 95.34% | 94.26% | 81.05% |
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (6)
- The material vibrating deslagging filtering filter aid 1. a kind of edible oil processing is deoiled, it is characterised in that by following parts by weight Raw material is made：10-15 parts of microcrystalline cellulose, 5-10 parts of modified crosslinking PVP, 3-5 parts of volcanic ash, 2-3 parts of polyethylene glycol oxide, lotus leaf powder 2-3 parts, 2-3 parts of allyl glycidyl ether, 1-2 parts of polyvinyl alcohol resin, 1-2 parts of sepiolite fibre, polydiallyldimethyl chlorine Change 1-2 parts of ammonium, 0.5-1 parts of ATBC, 0.5-1 parts of sodium gluconate, 0.5-1 parts of nanometer titanium dioxide.
- The material vibrating deslagging filtering filter aid 2. edible oil processing according to claim 1 is deoiled, it is characterised in that：Its Preparation method comprises the following steps：(1) allyl glycidyl ether and nanometer titanium dioxide are added into microcrystalline cellulose, and with 5 DEG C/min programming rate liter Temperature adds polyvinyl alcohol resin and ATBC, is continuously heating to 105- to 75-80 DEG C of insulation mixing 15-30min 110 DEG C of insulation mixing 10-15min, produce modified microcrystalline cellulose；(2) polyethylene glycol oxide and sepiolite fibre are added into volcanic ash, microwave treater microwave treatment is utilized after being sufficiently mixed 5-10min, then polydiallyldimethyl ammonium chloride and sodium gluconate are added while hot, it is transferred to after being well mixed quiet in 0-5 DEG C of environment 1-2h is put, auxiliary material powder is produced；(3) modified crosslinking PVP, auxiliary material powder and lotus leaf powder are added into modified microcrystalline cellulose, through vacuum after being sufficiently mixed Compression is blocking, and micro mist most is made through micronizer afterwards.
- The material vibrating deslagging filtering filter aid 3. edible oil processing according to claim 1 is deoiled, it is characterised in that：Institute State modified crosslinking PVP to be made by PVPP modification, its specific method of modifying is：Pre- paste is added into PVPP Change starch and poloxamer, microwave treater microwave treatment 3-5min is utilized after being sufficiently mixed, rilanit special and field is added Cyanines glue, microwave treatment 3-5min is continued after being well mixed, and is then cooled to 0-5 DEG C of insulation standing with 5 DEG C/min cooling rate 0.5-1h, and 35-40 DEG C of water is added into gained mixture, sent into after being sufficiently mixed in freeze drier, after fully drying Through gained solid abrasive into powder, modified crosslinking PVP is produced.
- The material vibrating deslagging filtering filter aid 4. edible oil processing according to claim 3 is deoiled, it is characterised in that：Institute The weight consumption ratio for stating PVPP, pre-gelatinized starch, poloxamer, rilanit special, sesbania gum and water is 15-20: 0.5-1:0.3-0.5:0.3-0.5:0.1-0.3:50-80。
- The material vibrating deslagging filtering filter aid 5. edible oil processing according to claim 3 is deoiled, it is characterised in that：Institute State microwave frequency 2450MHz, the power output 700W of microwave treater.
- The material vibrating deslagging filtering filter aid 6. edible oil processing according to claim 3 is deoiled, it is characterised in that：Institute Pre-gelatinized starch is stated to be made up through pre-gelatinized of plant amylum.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710265096.8A CN107096299B (en) | 2017-04-21 | 2017-04-21 | A kind of processing of edible oil is deoiled material vibrating deslagging filtering filter aid |
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| CN201710265096.8A CN107096299B (en) | 2017-04-21 | 2017-04-21 | A kind of processing of edible oil is deoiled material vibrating deslagging filtering filter aid |
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| CN107096299A true CN107096299A (en) | 2017-08-29 |
| CN107096299B CN107096299B (en) | 2019-07-26 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110922301A (en) * | 2019-11-19 | 2020-03-27 | 山东福田药业有限公司 | Method for extracting sugar alcohol from chewing gum waste |
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| US20110073802A1 (en) * | 2009-04-06 | 2011-03-31 | Anthony P Haag | Slow release tablet composition for treating industrial water systems |
| CN103571166A (en) * | 2012-07-20 | 2014-02-12 | 东北林业大学 | Cellulose-microcrystalline cellulose-polypropylenecarbonate composition and preparation method thereof |
| CN103702754A (en) * | 2011-07-29 | 2014-04-02 | 东丽株式会社 | Method of manufacturing filter aid |
| CN105920654A (en) * | 2016-04-27 | 2016-09-07 | 李明华 | Burn dressing applicable to department of burn and having antibacterial effect |
| CN106396054A (en) * | 2016-10-18 | 2017-02-15 | 马鞍山市金农牧业有限公司 | Primary precipitator for waste water treatment of livestock breeding |
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2017
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US20110073802A1 (en) * | 2009-04-06 | 2011-03-31 | Anthony P Haag | Slow release tablet composition for treating industrial water systems |
| CN103702754A (en) * | 2011-07-29 | 2014-04-02 | 东丽株式会社 | Method of manufacturing filter aid |
| CN103571166A (en) * | 2012-07-20 | 2014-02-12 | 东北林业大学 | Cellulose-microcrystalline cellulose-polypropylenecarbonate composition and preparation method thereof |
| CN105920654A (en) * | 2016-04-27 | 2016-09-07 | 李明华 | Burn dressing applicable to department of burn and having antibacterial effect |
| CN106396054A (en) * | 2016-10-18 | 2017-02-15 | 马鞍山市金农牧业有限公司 | Primary precipitator for waste water treatment of livestock breeding |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110922301A (en) * | 2019-11-19 | 2020-03-27 | 山东福田药业有限公司 | Method for extracting sugar alcohol from chewing gum waste |
| CN110922301B (en) * | 2019-11-19 | 2021-12-17 | 山东福田药业有限公司 | Method for extracting sugar alcohol from chewing gum waste |
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| CN107096299B (en) | 2019-07-26 |
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Denomination of invention: Filtering aid for vibrating, slagging and filtering oil materials in edible oil processing Effective date of registration: 20200629 Granted publication date: 20190726 Pledgee: Revitalize the financing Company limited by guarantee in harmony with County Pledgor: ANHUI JIAYIWEI FOOD Co.,Ltd. Registration number: Y2020980003597 |