CN107094759A - A kind of granular pesticide using attapulgite as auxiliary material carrier - Google Patents

A kind of granular pesticide using attapulgite as auxiliary material carrier Download PDF

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Publication number
CN107094759A
CN107094759A CN201710507366.1A CN201710507366A CN107094759A CN 107094759 A CN107094759 A CN 107094759A CN 201710507366 A CN201710507366 A CN 201710507366A CN 107094759 A CN107094759 A CN 107094759A
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CN
China
Prior art keywords
parts
attapulgite
auxiliary material
leek
granular pesticide
Prior art date
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Pending
Application number
CN201710507366.1A
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Chinese (zh)
Inventor
何峰
韩继英
滕振远
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Shandong Danong Pharmaceutical Co Ltd
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Shandong Danong Pharmaceutical Co Ltd
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Priority to CN201710507366.1A priority Critical patent/CN107094759A/en
Publication of CN107094759A publication Critical patent/CN107094759A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12—Powders or granules
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/08—Amines; Quaternary ammonium compounds containing oxygen or sulfur
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing heterocyclic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A01N59/20—Copper
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D5/00—Fertilisers containing magnesium
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00—Soil-conditioning materials or soil-stabilising materials
    • C09K17/02—Soil-conditioning materials or soil-stabilising materials containing inorganic compounds only
    • C09K17/04—Soil-conditioning materials or soil-stabilising materials containing inorganic compounds only applied in a physical form other than a solution or a grout, e.g. as granules or gases
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2101/00—Agricultural use

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Dentistry (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Soil Sciences (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a kind of medicine for being used to kill fragrant-flowered garlic maggot in leek ground, more particularly to a kind of granular pesticide using attapulgite as auxiliary material carrier, it is made of following methods, takes 30 50 parts of 50% phoxim emulsifiable concentrate, 2.5% 30 50 parts of deltamethrin milk oil, 48% 30 50 parts of Le Siben missible oil, 4.5% 10 20 parts of permethrin milk oil, 10 20 parts of ephedrine, 10 20 parts of copper sulphate, 30 50 parts of gelatine, 35 30 50 parts of Baume degrees waterglass；Dissolved in the water that above-mentioned raw materials are added to 500 parts, obtain decoction；The attapulgite of 200 300 parts by weight is taken, above-mentioned decoction is uniformly sprayed on attapulgite, mixes, is dried to granule.The granule that the present invention is made has slow release effect, reaches the long-term effect for putting fragrant-flowered garlic maggot in advance, and leek meet the requirement of environmental protection effectively mitigates soil hardening, beneficial to chesson.

Description

A kind of granular pesticide using attapulgite as auxiliary material carrier
Technical field
The present invention relates to a kind of medicine for being used to kill fragrant-flowered garlic maggot in leek ground, more particularly to one kind is using attapulgite as auxiliary material The granular pesticide of carrier.
Background technology
Fragrant-flowered garlic maggot, scientific name Bradysia odoriphaga belongs to Diptera, Nematocera, to the greatest extent eye Sciaridae, eye Sciara, fragrant-flowered garlic maggot adult The long 3.3-4.8mm of male worm body, average 4.3mm, dark brown, the female long 4-5mm of polypide, average 4.6mm, the two is similar, but female adult Feeler is shorter and thin.It is that one of China's Major Pests, particularly leek are aggrieved most heavy.
The gregarious life of fragrant-flowered garlic maggot larva hidden.It is gathered at underground part leek bulb, root and false stem and causes harm, from outer and interior Moth food, causes plant leaf from outer and interior flavescence, then dries up.Larva can continue to cause harm downwards, moth food bulb and root, make life Long point is damaged, it is impossible to produce young leaves and whole strain is withered.The happiness of fragrant-flowered garlic maggot larva is moist, and soil moisture is most suitable with 20% -24.7%.
The generation of fragrant-flowered garlic maggot is different and different according to each department and cultivation mode.Occur 4-6 generations within 1 year in North China, Spring and autumn occur it is serious, it is native in leek bulb or rhizome and its nearby more with larva in survive the winter.
The plot of breed selection, phase of causing harm in spring is shorter, the button canopy phase in winter cause harm it is most heavy, mainly by cultivation management mode Influence.Wen Peng fields are gone up in button canopy phase temperature of shed, and the larva survived the winter slowly recovers, moved up, along with soil moisture is big in canopy, Easily cause the big generation of fragrant-flowered garlic maggot.Spring is lifted after canopy, and some plot leek drought, soil moisture content declines, the normal development of larva by To influence, spring causes harm gently, and the phase of going through of causing harm shortens.
At present, plantation leek quantity is more and more in China's warmhouse booth, and the preventing and treating for fragrant-flowered garlic maggot is more and more important.
Now, the main still medical treatment of the method for preventing and treating fragrant-flowered garlic maggot, needs according to the multiple dispenser of epidemic situation, with cost every year Height, labor intensity is big, and prevention effect is undesirable.
The content of the invention
The present invention provides a kind of granular pesticide using attapulgite as auxiliary material carrier, mainly for leek in warmhouse booth Fragrant-flowered garlic maggot prevention, low with cost, prevention effect is good, be often only need a dispenser.
The present invention is realized by following measures
The present invention relates to a kind of granular pesticide using attapulgite as auxiliary material carrier, it is characterised in that uses following methods system Into,
（1）Choose the raw material of following parts by weight, 50% 30-50 parts of phoxim emulsifiable concentrate, 2.5% 30-50 parts of deltamethrin milk oil, 48% 30-50 parts of Le Siben missible oil, 4.5% 10-20 parts of permethrin milk oil, 10-20 parts of ephedrine, copper sulphate 10-20 Part, 30-50 parts of gelatine, 35 30-50 parts of Baume degrees waterglass；Dissolved in the water that above-mentioned raw materials are added to 500 parts, obtain decoction；
（2）The attapulgite of 200-300 parts by weight is taken, above-mentioned decoction is uniformly sprayed on attapulgite, mixes, is dried to Granula.
The granular pesticide using attapulgite as auxiliary material carrier of the invention described above, it is preferred that 50% phoxim emulsifiable concentrate 40 Part, 2.5% 40 parts of deltamethrin milk oil, 48% 40 parts of Le Siben missible oil, 4.5% 20 parts of permethrin milk oil, ephedrine 10 Part, 10 parts of copper sulphate, 40 parts of gelatine, 35 40 parts of Baume degrees waterglass, 250 parts of attapulgite.
The granular pesticide using attapulgite as auxiliary material carrier of the present invention, its usage and consumption：Spring is together with base fertilizer Apply in soil layer 20-30 centimeters, it is about 20-30KG that addition, which is every mu,.Once a year.
It is mainly used in warmhouse booth leek preventing and treating fragrant-flowered garlic maggot and other underground pests.
Packaging：Every bag of 50KG, is packed, moistureproof.
The innovative point of the present invention is essentially consisted in, and first, the granule being made has slow release effect, and spring applies together with base fertilizer In soil layer 20-30 centimeters, it is about 20-30KG that addition, which is every mu,.Due to viscous between gelatine, waterglass and attapulgite Cooperation is used, and granule is had certain intensity, meanwhile, the medicine of absorption is slowly discharged, reach the long-term effect for putting fragrant-flowered garlic maggot in advance Really.
Second, the present invention, as main adsorbent, by specifically matching, makes granule in soil using attapulgite In, final resolving time control resolved into the fertilizer that powdered attapulgite may act as leek, together at 6-10 months When, can be to greatest extent in the property of medicine of release agricultural chemicals., can be with more efficient because warmhouse booth belongs to the larva high-incidence season in winter Ground controls the growth of larva.
3rd, the medicinal raw material that the present invention is used is low toxicity medicine, and is slow release, and leek reaches that environmental protection will Ask.
4th, the granule of the present invention is used for a long time,, can be effective after decomposition due to containing a certain amount of attapulgite Mitigate soil hardening, beneficial to chesson.
Embodiment
Embodiment
It is made the present invention relates to a kind of using attapulgite as the granular pesticide of auxiliary material carrier of following methods,
Weigh the raw material of following parts by weight, 50% phoxim emulsifiable concentrate 400KG, 2.5% deltamethrin milk oil 400KG, 48% pleasure This this missible oil 400KG, 4.5% permethrin milk oil 200KG, ephedrine 100KG, copper sulphate 100KG, gelatine 400KG, 35 Baume degrees waterglass 400KG；Dissolved in the water that above-mentioned raw materials are added to 5000KG, obtain decoction；
2500KG attapulgite is taken, above-mentioned decoction is uniformly sprayed on attapulgite, mixes, is dried to granule.
Packaging：Every bag of 50KG, is packed, moistureproof.
In warmhouse booth leek on the ground, applied in spring together with base fertilizer in soil layer 20-30 centimeters, addition is every mu big About 25KG.
During leek is planted, end, which is seen, has obvious fragrant-flowered garlic maggot to occur.
Finished product leek is taken to detect, it is as a result as follows
By four seasons of spring, summer, autumn and winter, take four batch leek to be detected respectively, be that 10 portions of leek carry out residues of pesticides per batch Detection.
Experiment purpose：Detect whether agriculture is residual exceeded for leek
According to national standard《Organophosphorus and carbamate pesticides pesticide residue amount is quick in GB/T5009.199-2003 vegetables Detection》, fast inspection residual to leek agriculture respectively weighs 1 gram of sample, sequentially adds reagent, finally show the inhibiting rate number of each sample According to.
National Specification, the residual inhibiting rate of agriculture《50% is feminine gender, and it is qualified to represent.
The residual inhibiting rate of agriculture be a kind of judgement sample whether the computational methods containing high dose agricultural chemicals, under certain condition, have Machine phosphorus and carbamate chemicals for agriculture have inhibitory action to cholinesterase normal function, and the concentration of its inhibiting rate and agricultural chemicals is in positive Close, inhibiting rate is qualified, illustrates that agriculture is not residual exceeded.
Experimental result is shown in Table 1.
As shown in Table 1, using the medicine of the present invention, leek qualification rate 100%, all samples are in national standard inhibiting rate In the range of, persticide residue is in safe range.
Table 1, leek Pesticide Residues inhibiting rate
Spring Summer Autumn Winter
The residual inhibiting rate of agriculture 38 42 42 43
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to be said using the present invention Equivalent structure or equivalent flow conversion that bright book content is made, or other related technical fields are directly or indirectly used in, Similarly it is included within the scope of the present invention.

Claims (3)

1. a kind of granular pesticide using attapulgite as auxiliary material carrier, it is characterised in that include following percentage by weight Raw material,
Choose the raw material of following parts by weight, 50% 30-50 parts of phoxim emulsifiable concentrate, 2.5% 30-50 parts of deltamethrin milk oil, 48% 30-50 parts of Le Siben missible oil, 4.5% 10-20 parts of permethrin milk oil, 10-20 parts of ephedrine, copper sulphate 10-20 Part, 30-50 parts of gelatine, 35 30-50 parts of Baume degrees waterglass；Dissolved in the water that above-mentioned raw materials are added to 500 parts, obtain decoction；
The attapulgite of 200-300 parts by weight is taken, above-mentioned decoction is uniformly sprayed on attapulgite, mixes, is dried to particle Agent.
2. the granular pesticide according to claim 1 using attapulgite as auxiliary material carrier, it is characterised in that the raw material Parts by weight be, 50% 40 parts of phoxim emulsifiable concentrate, 2.5% 40 parts of deltamethrin milk oil, 48% 40 parts of Le Siben missible oil, 4.5% 20 parts of permethrin milk oil, 10 parts of ephedrine, 10 parts of copper sulphate, 40 parts of gelatine, 35 40 parts of Baume degrees waterglass are recessed Convex 250 parts of rod soil.
3. a kind of granular pesticide according to claim 1 or 2 using attapulgite as auxiliary material carrier is on preventing and treating fragrant-flowered garlic maggot Application.
CN201710507366.1A 2017-06-28 2017-06-28 A kind of granular pesticide using attapulgite as auxiliary material carrier Pending CN107094759A (en)

Priority Applications (1)

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CN201710507366.1A CN107094759A (en) 2017-06-28 2017-06-28 A kind of granular pesticide using attapulgite as auxiliary material carrier

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Application Number Priority Date Filing Date Title
CN201710507366.1A CN107094759A (en) 2017-06-28 2017-06-28 A kind of granular pesticide using attapulgite as auxiliary material carrier

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002037964A1 (en) * 2000-11-10 2002-05-16 Syngenta Participations Ag Synergistic pesticidal compositions comprising n-cyanomethyl-4-(trifluoromethyl)nicotinamide
CN102125049A (en) * 2010-10-30 2011-07-20 孙雪梅 Pesticide composition of phoxim and chlorpyrifos

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002037964A1 (en) * 2000-11-10 2002-05-16 Syngenta Participations Ag Synergistic pesticidal compositions comprising n-cyanomethyl-4-(trifluoromethyl)nicotinamide
CN102125049A (en) * 2010-10-30 2011-07-20 孙雪梅 Pesticide composition of phoxim and chlorpyrifos

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
刘程，等: "《表面活性剂性质理论与应用》", 30 June 2003, 北京：北京工业大学出版社 *
胡涛，等: "凹凸棒土的应用研究", 《中国矿业》 *

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Application publication date: 20170829

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