CN107090244B - A kind of colour water writing cloth and production method - Google Patents
A kind of colour water writing cloth and production method Download PDFInfo
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- CN107090244B CN107090244B CN201710255751.1A CN201710255751A CN107090244B CN 107090244 B CN107090244 B CN 107090244B CN 201710255751 A CN201710255751 A CN 201710255751A CN 107090244 B CN107090244 B CN 107090244B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B43—WRITING OR DRAWING IMPLEMENTS; BUREAU ACCESSORIES
- B43L—ARTICLES FOR WRITING OR DRAWING UPON; WRITING OR DRAWING AIDS; ACCESSORIES FOR WRITING OR DRAWING
- B43L1/00—Repeatedly-usable boards or tablets for writing or drawing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to a kind of colored water writing cloth and production methods.A kind of colour water writing cloth, including base and coating, the coating include coloured substrate and development surface layer, and the coloured substrate painting is imprinted in the base, and the development surface layer painting is imprinted on the coloured substrate；The coloured substrate is prepared from the following raw materials: mill base coating, waterborne polyurethane resin, aqueous acrylic emulsion, silica, Cornstarch, calcium carbonate, propylene glycol, defoaming agent, levelling agent.The invention has the benefit that formula is simple, and product can achieve excellent excellent water suction and quick-drying effect without being modified processing；With color abundant, the appearance of water writing cloth product is enriched；It realizes that the ingredient of color bottom is roughly the same with the ingredient of developing layer, not only saves ingredient, construction is easy, and color bottom can be merged preferably with developing layer, and it is bright-colored, and prolonged not fugitive color.
Description
Technical field
The invention belongs to stationery fields, and in particular to a kind of colour water writing cloth and production method.
Background technique
Water writing cloth be it is a kind of dipped in after clear water writes on its surface with writing brush, show black ink marks at once, can be again after water is dry
It writes, for practicing the painting and calligraphy artistic drawing set for writing Writing brush calligraphy, painting and calligraphy and allowing child daubing drawing.Water writing cloth is mainly using cloth as material
Matter；The transparent principle of water is met according to coating to make；Using calico as medium, its surface add one layer through special process handle
Environment-friendlywhite white coating, which, which has, meets the transparent effect of water.
Water writing cloth has the advantages that the aobvious ink of 1, clear water, and ten thousand writings are economical and practical, saves paper ink, clean hygiene, ring
It protects efficiently, first to use, wonderful such as rice paper, long use is more fresh, and effect is marvellous；2, the service life it is long, it is resistance to write, be washable, not tympanites (institute on the market
It says and thickeies water writing cloth, it is most of made for thick paper jam, wallpaper, plastic paper, nonwoven cloth material, it cannot reach washing, resistance to write ten thousand
Secondary standard)；3, low-carbon environment-friendly will not make clothes, elbow and indoor environment dirty, a large amount of to save drills to improve one's handwriting paper, reduce by hand
Serious pollution of the papermaking to environment；4, it is easy to use, using preceding without preparing ink, standby paper, felt etc.；After use without wash pen,
It tidies up and practices useless paper.
Patent CN 106192409A discloses water writing cloth coating adhesive and processing method, uses diphenyl methane two is different
Cyanate, ethylene glycol polyethers, polybutadiene dihydric alcohol, adipic dihydrazide, diethylene glycol dimethacrylate, metering system
The reagents such as sour isobornyl thiocyanoacetate, triethylamine, are deployed at different temperature, obtain acrylic acid modified polyurethane lotion；Again will
This acrylic acid modified polyurethane lotion is mixed with reagents such as advection agent, silica, has obtained water writing cloth coating adhesive.The water suction of this glue
Property it is good, can dry rapidly, anti-liquid is stain, still, use in the invention is up to 8 kinds or more modified, more using reagent, and
And modified technique is relative complex.
Summary of the invention
Of the existing technology modified complicated in order to solve the problems, such as, the present invention provides colored water writing cloth and production sides
Method has the characteristics that easy to process, multiple color, clear, water stain quick-drying of writing.
The technical scheme adopted by the invention is as follows:
A kind of colour water writing cloth, including base and coating, the coating include coloured substrate and development surface layer, the colour
Bottom painting is imprinted in the base, and the development surface layer painting is imprinted on the coloured substrate；The coloured substrate is by following raw material
Be made: mill base coating, aqueous acrylic emulsion, silica, Cornstarch, calcium carbonate, propylene glycol, disappears at waterborne polyurethane resin
Infusion, levelling agent.
Further, the coloured substrate is made of raw material from the following weight: 0.1~0.5 part of mill base coating, aqueous poly-
30~40 parts of urethane resin, 10~15 parts of aqueous acrylic emulsion, 20~25 parts of silica, 5~10 parts of Cornstarch, calcium carbonate
10~15 parts, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, 0.1~0.5 part of levelling agent.
Further, the development surface layer is prepared from the following raw materials: waterborne polyurethane resin, aqueous acrylic emulsion, two
Silica, Cornstarch, calcium carbonate, propylene glycol, defoaming agent, levelling agent.
Further, the development surface layer is made of following raw material: 30~40 parts of waterborne polyurethane resin, aqueous
10~15 parts of acrylic emulsion, 20~25 parts of silica, 5~10 parts of Cornstarch, 10~15 parts of calcium carbonate, propylene glycol 3~8
Part, 0.1~0.5 part of defoaming agent, 0.1~0.5 part of levelling agent.
Further, the base is colored non-woven fabrics.
Further, the colored non-woven fabrics is added color slurry by white polyester fiber and prints and dyes.
A kind of production method of colour water writing cloth, comprising the following steps:
(1) 0.1~0.5 part of mill base coating, 30~40 parts of waterborne polyurethane resin, aqueous acrylic emulsion 10~15 are taken
Part, 20~25 parts of silica, 5~10 parts of Cornstarch, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, defoaming agent 0.1~0.5
Part, 0.1~0.5 part of levelling agent be uniformly mixed, coloured substrate coating is made；
(2) first road color layer: the coloured substrate coating is sprayed in base, and controls 110~150 DEG C of temperature progress
Drying；
(3) two color layers: the coloured substrate coating is sprayed again, and is controlled 110~150 DEG C of temperature and dried
It is dry；
(4) 30~40 parts of aqueous polyurethane resin, 10~15 parts of aqueous acrylic emulsion, 20~25 parts of silica,
5~10 parts of Cornstarch, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, 0.1~0.5 part of levelling agent,
Development investment precoat is made, is then sprayed.
Further, in step (4), the spraying including surface layer of developing twice controls after the completion of the spraying of first development surface layer
110~150 DEG C of temperature processed are dried, then carry out the spraying of second development surface layer.
Further, the colored non-woven fabrics is added color slurry by white polyester fiber and prints and dyes.
Further, the weight ratio of the color slurry and the white polyester fiber is 1:300~320.
The invention has the benefit that
1. existing water writing cloth is that white water writes surface, the present invention has water writing cloth abundant by using mill base coating
Color, the water that can be dyeing into multiple color write face, and can also print and dye multiple color in one piece of water writing cloth, when writing, at once
Show black ink marks, colored or polychrome word or figureThe appearance of water writing cloth product is not only enriched, and enhances user's
Writing experience；
2. cooperating using mill base coating and waterborne polyurethane resin, aqueous acrylic emulsion, not only mill base can be made secured, it is resistance to
Rubber cement migration is good, and without being modified processing, product can achieve excellent water suction and quick-drying effect；
3. color layer of the invention is printed and dyed using Shou Dao and two is compound, it can not only make color fast, and can be with
Improve the brightness of color, the amalgamation of enhancing and development surface layer；
4. adjusting the material rate of color bottom and surface layer of developing, the ingredient of the ingredient and developing layer of realizing color bottom is big
It causes identical, not only saves ingredient, construction is easy, and color bottom can be merged preferably with developing layer, bright-colored and prolonged
Not fugitive color.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1
The production method of colored water writing cloth:
(1) preparation of coloured substrate coating: take mill base coating D-102 1 kilogram red, 300 kilograms of waterborne polyurethane resin,
100 kilograms of aqueous acrylic emulsion, 200 kilograms of silica, 50 parts of Cornstarch, 100 kilograms of calcium carbonate, 30 kilograms of propylene glycol,
1 kilogram of defoaming agent, 1 kilogram of levelling agent are uniformly mixed, coloured substrate coating are made；
(2) first road color layer: the coloured substrate coating is sprayed on non-woven fabrics, and controls 115 DEG C of temperature and is dried
It is dry；
(3) two color layers: the coloured substrate coating is sprayed again, and is controlled 120 DEG C of temperature and dried；
(4) preparation of development coating: 300 kilograms of aqueous polyurethane resin, 100 kilograms of aqueous acrylic emulsion, two
200 kilograms of silica, 50 kilograms of Cornstarch, 100 kilograms of calcium carbonate, 30 kilograms of propylene glycol, 1 kilogram of defoaming agent, levelling agent 1 are public
Jin, is made development investment precoat.
(5) one of developing layer: spray development investment precoat, 110 DEG C of temperature processed of control are dried.
Embodiment 2
The production method of colored water writing cloth:
(1) preparation of coloured substrate coating: take 3 kilograms of mill base coating (blue FB), 400 kilograms of waterborne polyurethane resin,
Aqueous acrylic emulsion 120 kg, 220 kilograms of silica, 70 kilograms of Cornstarch, calcium carbonate 120 kg, propylene glycol 50 are public
Jin, 3 kilograms of defoaming agent, 3 kilograms of levelling agent are uniformly mixed, coloured substrate coating are made；
(2) first road color layer: the coloured substrate coating is sprayed on non-woven fabrics, and controls 130 DEG C of temperature and is dried
It is dry；
(3) two color layers: the coloured substrate coating is sprayed again, and is controlled 135 DEG C of temperature and dried；
(4) preparation of development coating: 400 kilograms of aqueous polyurethane resin, aqueous acrylic emulsion 120 kg, two
220 kilograms of silica, 70 kilograms of Cornstarch, calcium carbonate 120 kg, 50 kilograms of propylene glycol, 3 kilograms of defoaming agent, levelling agent 3 are public
Jin, is made development investment precoat；
(5) one of developing layer: spray development investment precoat, 120 DEG C of temperature processed of control are dried
(6) two developing layers: spray development investment precoat, 120 DEG C of temperature processed of control are dried.
Embodiment 3
The production method of colored water writing cloth:
(1) production of multicolored base layer: the weight ratio of color slurry (green slurry FG) and the white polyester fiber is 1:
300。
(1) 5 kilograms of mill base coating, 400 kilograms of waterborne polyurethane resin, aqueous acrylamide the preparation of coloured substrate coating: are taken
150 kilograms of yogurt liquid, 250 kilograms of silica, 100 kilograms of Cornstarch, 150 kilograms of calcium carbonate, 80 kilograms of propylene glycol, defoaming agent
5 kilograms, 5 kilograms of levelling agent are uniformly mixed, coloured substrate coating are made；
(2) first road color layer: the coloured substrate coating is sprayed on non-woven fabrics, and controls 140 DEG C of temperature and is dried
It is dry；
(3) two color layers: on the basis of color bottom coating, add into 10 kilograms of aqueous acrylic emulsion, aqueous
30 kilograms of polyurethane resin, two colour-washes are made, are sprayed again, and controls 180 DEG C of temperature and dried；
(4) 5 kilograms of mill base coating, 400 kilograms of waterborne polyurethane resin, water soluble acrylic acid the preparation of development coating: are taken
150 kilograms of lotion, 250 kilograms of silica, 100 kilograms of Cornstarch, 150 kilograms of calcium carbonate, 80 kilograms of propylene glycol, defoaming agent 5
Kilogram, 5 kilograms of levelling agent, development investment precoat is made；
(5) one of developing layer: spray development investment precoat, 130 DEG C of temperature processed of control are dried；
(6) two developing layers: spray development investment precoat, 135 DEG C of temperature processed of control are dried.
Embodiment 4
The production method of colored water writing cloth:
(1) production of multicolored base layer: the weight ratio of color slurry (brown slurry FRG) and the white polyester fiber is 1:
320；
(1) 2.5 kilograms of mill base coating, 380 kilograms of waterborne polyurethane resin, aqueous third preparation of coloured substrate coating: are taken
Olefin(e) acid lotion 120 kg, 220 kilograms of silica, 70 kilograms of Cornstarch, 110 kilograms of calcium carbonate, 50 kilograms of propylene glycol, defoaming
3 kilograms of agent, 7 kilograms of levelling agent are uniformly mixed, coloured substrate coating are made；
(2) first road color layer: the coloured substrate coating is sprayed on non-woven fabrics, and control 110~150 DEG C of temperature into
Row drying；
(3) two color layers: on the basis of color bottom coating, add into 0.5 kilogram of brown slurry, water soluble acrylic acid
15 kilograms of lotion, 20 kilograms of waterborne polyurethane resin, are made two colour-washes, spray again, and control temperature 110~150
It DEG C is dried；
(4) preparation of development coating: 380 kilograms of aqueous polyurethane resin, aqueous acrylic emulsion 120 kg, two
220 kilograms of silica, 70 kilograms of Cornstarch, 110 kilograms of calcium carbonate, 50 kilograms of propylene glycol, 3 kilograms of defoaming agent, levelling agent 7 are public
Jin, is made development investment precoat；
(5) one of developing layer: spray development investment precoat, 175 DEG C of temperature processed of control are dried
(6) two developing layers: development investment precoat is adjusted to 350 kilograms of waterborne polyurethane resin, aqueous acrylamide yogurt
130 kilograms of liquid, other compositions are constant, carry out coating again, and 170 DEG C of temperature processed of control is dried.
The basic property of the product of 1 Examples 1 to 4 of table
In table, comparative example 2 is the achromaticity water writing cloth of commercially available modification.
Indices detection method in above table:
Water absorption rate evaluation criteria: GB/T 21655.1-2008；Vapor transfer rate evaluation criteria: GB/T 21655.1-2008；Drop
Water diffusion time evaluation criteria: GB/T 21655.1-2008；Evaporation rate evaluation criteria: GB/T 21655.1-2008.
The above experiment shows that the present invention without modified situation, can also get preferable performance, water absorption rate drips
Diffusion time and evaporation rate and modified product are essentially identical, even better than modified product.Therefore, the present invention can change numerous
For letter, the prejudice (the modified effect that could have been obtained of coating adhesive) in the field of breakthrough makes pretreated without complexity
Mill base coating and other components cooperate, and have played huge unexpected effect.
The product coloring performance of 2 Examples 1 to 4 of table
Indices detection method in above table:
Fast light firmness executes standard: GB/T8427-1998 uses instrument Q-Panel Lab products xenon lamp aging
Tester；
Resistance to pressing securely executes standard, and: GB/T6152-1997 uses instrument hot press；
Washability executes standard: GB/T8629-2001 is washed 30 times by 5A program.
Above data shows colored water writing cloth of the invention, not only has color abundant, and has after printing and dyeing certain
Fast light firmness, resistance to pressing fastness and washability, even when being applied between it is permanent, color keep is good.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (8)
1. a kind of colour water writing cloth, it is characterised in that: including base and coating, the coating includes coloured substrate and development face
Layer, the coloured substrate painting are imprinted in the base, and the development surface layer painting is imprinted on the coloured substrate；The coloured substrate
Be prepared from the following raw materials: mill base coating, waterborne polyurethane resin, aqueous acrylic emulsion, silica, titanium dioxide, calcium carbonate,
Propylene glycol, defoaming agent, levelling agent；
The production method of the colour water writing cloth, comprising the following steps:
(1) 0.1~0.5 part of mill base coating, 30~40 parts of waterborne polyurethane resin, 10~15 parts of aqueous acrylic emulsion, two are taken
20~25 parts of silica, 5~10 parts of titanium dioxide, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, stream
0.1~0.5 part of flat agent is uniformly mixed, and coloured substrate coating is made；
(2) first road color layer: the coloured substrate coating is sprayed in base, and controls 110~150 DEG C of temperature and is dried
It is dry；
(3) two color layers: the coloured substrate coating is sprayed again, and is controlled 110~150 DEG C of temperature and dried；
(4) 30~40 parts of aqueous polyurethane resin, 10~15 parts of aqueous acrylic emulsion, 20~25 parts of silica, titanium white
5~10 parts of powder, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, 0.1~0.5 part of levelling agent, are made
Develop investment precoat, is then sprayed.
2. it is according to claim 1 colour water writing cloth, it is characterised in that: the coloured substrate by following parts by weight raw material
It is made: 0.1~0.5 part of mill base coating, 30~40 parts of waterborne polyurethane resin, 10~15 parts of aqueous acrylic emulsion, titanium dioxide
20~25 parts of silicon, 5~10 parts of titanium dioxide, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, levelling agent
0.1~0.5 part.
3. colour water writing cloth according to claim 1, it is characterised in that: the development surface layer is prepared from the following raw materials: water
Property polyurethane resin, aqueous acrylic emulsion, silica, titanium dioxide, calcium carbonate, propylene glycol, defoaming agent, levelling agent.
4. colour water writing cloth according to claim 3, it is characterised in that: the development surface layer is by following raw material system
At: 30~40 parts of waterborne polyurethane resin, 10~15 parts of aqueous acrylic emulsion, 20~25 parts of silica, titanium dioxide 5~10
Part, 10~15 parts of calcium carbonate, 3~8 parts of propylene glycol, 0.1~0.5 part of defoaming agent, 0.1~0.5 part of levelling agent.
5. colour water writing cloth according to any one of claims 1 to 4, it is characterised in that: the base is colored non-woven fabrics.
6. colour water writing cloth according to claim 5, it is characterised in that: the colour non-woven fabrics is added by white polyester fiber
Enter color slurry to print and dye.
7. colour water writing cloth according to claim 6, it is characterised in that: the color slurry and the white polyester fiber
Weight ratio be 1:300~320.
8. colour water writing cloth according to claim 1, it is characterised in that: in step (4), the spray including surface layer of developing twice
It applies, is dried after the completion of the spraying of first development surface layer at 110~150 DEG C of temperature, then carry out the spraying of second development surface layer.
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