CN107032712B - Fireproof heated board and preparation method thereof - Google Patents
Fireproof heated board and preparation method thereof Download PDFInfo
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- CN107032712B CN107032712B CN201710189795.9A CN201710189795A CN107032712B CN 107032712 B CN107032712 B CN 107032712B CN 201710189795 A CN201710189795 A CN 201710189795A CN 107032712 B CN107032712 B CN 107032712B
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- heated board
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- fireproof heated
- component
- fireproof
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
- C04B28/065—Calcium aluminosulfate cements, e.g. cements hydrating into ettringite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
The invention discloses fireproof heated board and preparation method thereof, which is made of fireproof and heat-insulating material, and fireproof and heat-insulating material includes component A and B component；By weight, component A includes: 80~120 parts of alumina silicate fibre, 100~140 parts of sepiolite fibre, 40~60 parts of dioctylsulfosuccinat, 2000~2500 parts of water, 40~60 parts of polyvinyl alcohol, 15~30 parts of graphite powder；B component includes: 600~800 parts of sulphate aluminium cement, 5~10 parts of hydrophober.Fireproof heated board provided by the invention, bulk density is in 150-200kg/m3, bulk density and thermal coefficient are low, easy for construction；Exclusive foam cells structure and the fiber wherein added in fireproof heated board, make it have certain elasticity and good mechanical strength, and when construction is not easily broken；Fiber is conducive to dispersion temperature stress, avoids cracking.
Description
Technical field
The present invention relates to energy-saving building materials technical field more particularly to fireproof heated boards and preparation method thereof.
Background technique
A critically important measure of building energy conservation is exactly to establish insulation energy-saving system to wall, at present the wall thermal insulating in China
The main exterior wall internal insulation system of energy conserving system, the sandwich thermal insulated system of wall and external thermal insulation system.External-wall external-insulation energy-saving body
It is the mainstream in the form of its numerous advantage has become wall thermal insulating.Currently, in outer heat preservation system, material used in insulating layer
Presently mainly polystyrene expansion plate (EPS), extruded sheet (XPS), polyurethane sheet, although its thermal coefficient is lower, Ke Yiman
The existing energy-efficient requirement of foot, but there is serious fire safety evaluating hidden danger, it is brought greatly to people's lives and property
It threatens.The production and application for greatly developing especially A grades of fire-type energy-saving building materials of novel energy-saving construction material are to ensure people
The needs of people's safety of life and property, and the emphasis of construction technique development from now on.
The inorganic material such as pearlite insulation plate, rock wool board, foamed cement board and the glass fibre cotton applied at present have
There is certain thermal insulation property, is often used as thermal insulation material.Take perlite as the heat preservation slurry and plate of basic raw material, there is fire prevention
The advantages that performance is good, thermal insulation property is good, low in cost and easy for construction meets current architectural exterior insulation material and is necessary for A grades
The requirement of material.But perlite plate thermal coefficient, generally 0.06 or more, bulk density is in 300kg/m3, to reach same section
It can require, the thickness of perlite plate is approximately twice of organic insulation material thickness, and panel weight used is about organic heat-insulating plate
20~30 times of the weight of material, under this brings all wall constructional difficulties as above and plate easy to the practical application of pearlite insulation plate
Many problems such as pendant.At present with inorganic fireproofing insulation material that perlite is basic raw material there are still heat insulation effects poor, bulk density compared with
Greatly, the disadvantages of the problems such as easily broken, bad mechanical strength, nail-holding ability are poor and difficulty of construction is big.Rock wool has heat insulating ability and fire prevention etc.
The advantages that grade is high, is a kind of A grades of heat preservation plate materials being commonly used, but this kind of plate there is also production energy consumptions big, the easy moisture absorption,
The disadvantages of difficulty of construction is big, intensity is extremely low can generate easily tenesmus, under surface mortar is easy to fall off and thermal insulation property in use
The problems such as serious, drops.Foamed cement has many advantages, such as processing at low cost, easy to produce, and fire protecting performance is A grades, can be used as architecture indoor
Wall is filled, is used in recent years used also as thermal insulation material, but it belongs to fragile material, difficulty of construction is big and weatherability is poor.Cause
This, at present there are some disadvantages for being difficult to overcome when applying on building heat preservation in inorganic heat preservation plate.
Authorization Notice No. is a kind of inorganic fireproofing insulation material of Chinese patent and preparation method thereof of 103214228 B of CN,
Disclose a kind of inorganic fireproofing insulation material, component and part are as follows: 0.5~30 part of reinforcing fiber；Lightweight aggregate 40~65
Part；2~15 parts of bentonite；12~35 parts of adhesive；5~20 parts of inorganic gel materials；2~10 parts of interfacial agents；Expansion polyphenyl
0~10 part of grain；200~260 parts of water；It is with lightweight aggregate thermal insulation material as main component, and condensation hardening is not easy to realize slowly
Industrialized production, and its thermal coefficient is higher.
Summary of the invention
Aiming at the shortcomings existing in the above problems, the present invention provides fireproof heated board and preparation method thereof, mentions significantly
High fire-protection rating, thermal coefficient is low, and heat insulation effect is good, light-weight, is easy to constructing operation.
To achieve the above object, the present invention provides a kind of fireproof heated board, which is by fireproof and heat-insulating material
It is made, the fireproof and heat-insulating material includes component A and B component；
By weight, the component A includes:
By weight, the B component includes:
600~800 parts of sulphate aluminium cement；
5~10 parts of hydrophober.
As a further improvement of the present invention, the model 24-88 of the polyvinyl alcohol.
As a further improvement of the present invention, the graphite powder partial size is 1500~2500 mesh.
As a further improvement of the present invention, the hydrophober is calcium stearate, zinc stearate, one in aluminum stearate
Kind.
As a further improvement of the present invention, the fireproof heated board also needs that dioxygen water foaming agent, the hydrogen peroxide is added
The parts by weight of foaming agent are 35~50 parts.
The present invention also provides a kind of preparation methods of fireproof heated board, comprising:
Step 1 weighs polyvinyl alcohol, alumina silicate fibre, sepiolite fibre, dioctylsulfosuccinat, stone by weight
Ink powder, sulphate aluminium cement, hydrophober, dioxygen water foaming agent and water；
Step 2, stirring that polyvinyl alcohol is added to the water are until the polyvinyl alcohol water solution that concentration is 10% is made in dissolution；
Step 3 sequentially adds dioctylsulfosuccinat, alumina silicate fibre, sepiolite fibre, graphite powder in water,
Mixing speed is uniform stirring in the blender of 800 turns/min, stands for 24 hours, obtains impregnating mixed liquor；
Step 4, take polyvinyl alcohol water solution, impregnate mixed liquor, remaining water, sulphate aluminium cement and hydrophober 120 turns/
It is stirred evenly in the blender of min, blowing enters mold after adding dioxygen water foaming agent stirring 2min；
Step 5, mold is transported to fog room maintenance, after for 24 hours afterwards carry out being cut into plate；
Step 6 will be put in storage after the fireproof heated board packaging after drying.
Compared with prior art, the invention has the benefit that
1, fireproof heated board provided by the invention, bulk density is in 150-200kg/m3, bulk density is low, easy for construction.
2, the fiber added due to foam cells structure exclusive in fireproof heated board provided by the invention and wherein, makes its tool
There are certain elasticity and a good mechanical strength, when construction is not easily broken.
3, the thermal coefficient of fireproof heated board provided by the invention is low.
4, fireproof heated board adding of fiber provided by the invention, is conducive to dispersion temperature stress, avoids cracking.
5, preparation method provided by the present invention is mature, simple and convenient, industrialized production easy to operate and realize.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is of the invention one
Section Example, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not doing
Every other embodiment obtained under the premise of creative work out, shall fall within the protection scope of the present invention.
The present invention provides a kind of fireproof heated board, which is made of fireproof and heat-insulating material, fireproof heat insulating material
Material includes component A and B component；
By weight, component A includes:
By weight, B component includes:
600~800 parts of sulphate aluminium cement；
5~10 parts of hydrophober.
Preferably, the model 24-88 of polyvinyl alcohol.
Preferably, graphite powder partial size is 1500~2500 mesh.
Preferably, hydrophober is one of calcium stearate, zinc stearate, aluminum stearate.
Preferably, fireproof heated board also needs that dioxygen water foaming agent is added, and the parts by weight of dioxygen water foaming agent are 35~50
Part.
The present invention also provides a kind of preparation methods of fireproof heated board, comprising:
Step 1 weighs polyvinyl alcohol, alumina silicate fibre, sepiolite fibre, dioctylsulfosuccinat, stone by weight
Ink powder, sulphate aluminium cement, hydrophober, dioxygen water foaming agent and water；
Step 2, stirring that polyvinyl alcohol is added to the water are until the polyvinyl alcohol water solution that concentration is 10% is made in dissolution；
Step 3 sequentially adds dioctylsulfosuccinat, alumina silicate fibre, sepiolite fibre, graphite powder in water,
Mixing speed is uniform stirring in the blender of 800 turns/min, stands for 24 hours, obtains impregnating mixed liquor；
Step 4, take polyvinyl alcohol water solution, impregnate mixed liquor, remaining water, sulphate aluminium cement and hydrophober 120 turns/
It is stirred evenly in the blender of min, blowing enters mold after adding dioxygen water foaming agent stirring 2min；
Step 5, mold is transported to fog room maintenance, after for 24 hours afterwards carry out being cut into plate；
Step 6 will be put in storage after the fireproof heated board packaging after drying.
The present invention is described in further detail combined with specific embodiments below:
Embodiment 1:
Fireproof heated board of the present invention, including component A and B component, wherein the component and each component that component A includes
Parts by weight are as follows:
The parts by weight of component and each component that B component includes are as follows:
600 parts of sulphate aluminium cement；
5 parts of hydrophober.
Wherein:
The model 24-88 of polyvinyl alcohol；
Graphite powder partial size is 1500 mesh；
Hydrophober is one of calcium stearate, zinc stearate, aluminum stearate, preferably zinc stearate.
Fireproof heated board also needs that dioxygen water foaming agent is added, and the parts by weight of dioxygen water foaming agent are 35.
Embodiment 2:
Fireproof heated board of the present invention, including component A and B component, wherein the component and each component that component A includes
Parts by weight are as follows:
The parts by weight of component and each component that B component includes are as follows:
700 parts of sulphate aluminium cement；
8 parts of hydrophober.
Wherein:
The model 24-88 of polyvinyl alcohol；
Graphite powder partial size is 2000 mesh；
Hydrophober is one of calcium stearate, zinc stearate, aluminum stearate, preferably zinc stearate.
Fireproof heated board also needs that dioxygen water foaming agent is added, and the parts by weight of dioxygen water foaming agent are 40.
Embodiment 3:
Fireproof heated board of the present invention, including component A and B component, wherein the component and each component that component A includes
Parts by weight are as follows:
The parts by weight of component and each component that B component includes are as follows:
800 parts of sulphate aluminium cement；
10 parts of hydrophober.
Wherein:
The model 24-88 of polyvinyl alcohol；
Graphite powder partial size is 2500 mesh；
Hydrophober is one of calcium stearate, zinc stearate, aluminum stearate, preferably zinc stearate.
Fireproof heated board also needs that dioxygen water foaming agent is added, and the parts by weight of dioxygen water foaming agent are 50.
In embodiment 1-3, fireproof heated board the preparation method comprises the following steps:
Step 1 weighs polyvinyl alcohol, alumina silicate fibre, sepiolite fibre, dioctylsulfosuccinat, stone by weight
Ink powder, sulphate aluminium cement, hydrophober, dioxygen water foaming agent and water；
Step 2, stirring that polyvinyl alcohol is added to the water are until the polyvinyl alcohol water solution that concentration is 10% is made in dissolution；
Step 3 sequentially adds dioctylsulfosuccinat, alumina silicate fibre, sepiolite fibre, graphite powder in water,
Mixing speed is uniform stirring in the blender of 800 turns/min, stands for 24 hours, obtains impregnating mixed liquor；
Step 4, take polyvinyl alcohol water solution, impregnate mixed liquor, remaining water, sulphate aluminium cement and hydrophober 120 turns/
It is stirred evenly in the blender of min, blowing enters mold after adding dioxygen water foaming agent stirring 2min；
Step 5, mold is transported to fog room maintenance, after for 24 hours afterwards carry out being cut into plate；
Step 6 will be put in storage after the fireproof heated board packaging after drying.
The performance indicator of fireproof heated board is as shown in table 1 in 1-3 of the embodiment of the present invention；
The performance indicator of 1 specific embodiment of table
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Bulk density kg/m3 | 198 | 180 | 165 |
| Compression strength MPa | 0.35 | 0.28 | 0.25 |
| Tensile strength MPa | 0.23 | 0.18 | 0.15 |
| Volume water absorption rate % | 4.5 | 3.8 | 3.5 |
| Coefficient of softing | 85 | 92 | 94 |
| Thermal coefficient W/mK | 0.039 | 0.036 | 0.035 |
| Combustion rating | A1 | A1 | A1 |
Compared with prior art, the invention has the benefit that
1, fireproof heated board provided by the invention, bulk density is in 150-200kg/m3, bulk density is low, easy for construction.
2, the fiber added due to foam cells structure exclusive in fireproof heated board provided by the invention and wherein, makes its tool
There are certain elasticity and a good mechanical strength, when construction is not easily broken.
3, the thermal coefficient of fireproof heated board provided by the invention is low.
4, fireproof heated board adding of fiber provided by the invention, is conducive to dispersion temperature stress, avoids cracking.
5, preparation method provided by the present invention is mature, simple and convenient, industrialized production easy to operate and realize.
These are only the preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (6)
1. a kind of fireproof heated board, which is characterized in that the fireproof heated board is made of fireproof and heat-insulating material, the fireproof heat insulating
Material includes component A and B component；
By weight, the component A includes:
By weight, the B component includes:
600~800 parts of sulphate aluminium cement；
5~10 parts of hydrophober.
2. fireproof heated board as described in claim 1, which is characterized in that the model 24-88 of the polyvinyl alcohol.
3. fireproof heated board as described in claim 1, which is characterized in that the graphite powder partial size is 1500~2500 mesh.
4. fireproof heated board as described in claim 1, which is characterized in that the hydrophober is calcium stearate, zinc stearate, hard
One of resin acid aluminium.
5. fireproof heated board as described in claim 1, which is characterized in that the fireproof heated board also needs that dioxygen Water blown is added
Agent, the parts by weight of the dioxygen water foaming agent are 35~50 parts.
6. a kind of preparation method of fireproof heated board as claimed in claim 5 characterized by comprising
Step 1, weigh by weight polyvinyl alcohol, alumina silicate fibre, sepiolite fibre, dioctylsulfosuccinat, graphite powder,
Sulphate aluminium cement, hydrophober, dioxygen water foaming agent and water；
Step 2, stirring that polyvinyl alcohol is added to the water are until the polyvinyl alcohol water solution that concentration is 10% is made in dissolution；
Step 3 sequentially adds dioctylsulfosuccinat, alumina silicate fibre, sepiolite fibre, graphite powder in water, is stirring
Speed is uniform stirring in the blender of 800 turns/min, stands for 24 hours, obtains impregnating mixed liquor；
Step 4 takes polyvinyl alcohol water solution, impregnates mixed liquor, remaining water, sulphate aluminium cement and hydrophober in 120 turns/min
Blender in stir evenly, add dioxygen water foaming agent stirring 2min after blowing enter mold；
Step 5, mold is transported to fog room maintenance, after for 24 hours afterwards carry out being cut into plate；
Step 6 will be put in storage after the fireproof heated board packaging after drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710189795.9A CN107032712B (en) | 2017-03-28 | 2017-03-28 | Fireproof heated board and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710189795.9A CN107032712B (en) | 2017-03-28 | 2017-03-28 | Fireproof heated board and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107032712A CN107032712A (en) | 2017-08-11 |
| CN107032712B true CN107032712B (en) | 2019-04-16 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109467372B (en) * | 2018-12-14 | 2021-04-06 | 中北大学 | Sulphoaluminate cement foaming insulation board and preparation method thereof, and assembled integrated insulation wall and preparation method thereof |
| CN116253578B (en) * | 2023-02-08 | 2024-03-22 | 烟台德孚瑞环保节能科技有限公司 | High-temperature-resistant inorganic fiber ceramic heat-insulating material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587607A (en) * | 2012-01-09 | 2012-07-18 | 武汉理工大学 | Fireproof and flame-retarding type composite heat-insulation decorating plate for outer wall and preparation method of fireproof and flame-retarding type composite heat-insulation decorating plate |
| CN104478038A (en) * | 2014-11-20 | 2015-04-01 | 许天浩 | Uninterrupted water treatment device |
| CN105367120A (en) * | 2015-11-24 | 2016-03-02 | 安庆市大成防腐保温材料有限责任公司 | Method for manufacturing hard silicate heat-preservation and heat-insulation board |
-
2017
- 2017-03-28 CN CN201710189795.9A patent/CN107032712B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587607A (en) * | 2012-01-09 | 2012-07-18 | 武汉理工大学 | Fireproof and flame-retarding type composite heat-insulation decorating plate for outer wall and preparation method of fireproof and flame-retarding type composite heat-insulation decorating plate |
| CN104478038A (en) * | 2014-11-20 | 2015-04-01 | 许天浩 | Uninterrupted water treatment device |
| CN105367120A (en) * | 2015-11-24 | 2016-03-02 | 安庆市大成防腐保温材料有限责任公司 | Method for manufacturing hard silicate heat-preservation and heat-insulation board |
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