CN107011999A - A kind of cottonseed plays caul-fat and the candle that rockets - Google Patents
A kind of cottonseed plays caul-fat and the candle that rockets Download PDFInfo
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- CN107011999A CN107011999A CN201710310065.XA CN201710310065A CN107011999A CN 107011999 A CN107011999 A CN 107011999A CN 201710310065 A CN201710310065 A CN 201710310065A CN 107011999 A CN107011999 A CN 107011999A
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- caul
- fat
- oil
- cottonseed
- candle
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
Caul-fat and the candle that rockets are played the invention provides a kind of cottonseed, be 5~5 DEG C for melting range based on the present invention, the discovery for the cottonseed oil new application that iodine number scope is 105~120, caul-fat is played there is provided a kind of cottonseed, composition includes cottonseed oil, essential oil, mineral oil and side chain alpha-olefin polymers composition, and the percentage by weight that wherein cottonseed oil has accounted for caul-fat is 1%~100%.Caul-fat is played provided by the present invention for the cottonseed for the candle that rockets, with the excellent effect that rockets, a variety of snowflake shapes can be made：Point, piece, group, nebula etc.；Suitable for plurality of raw materials system candle, including paraffinic base candle, plant cerul candle, animal aliphatic radical candle and mixed base candle.And it is easy to use, the technique for making the candle that rockets is simple, cost-effective.
Description
Technical field
The present invention relates to artistic taper and candle technical field, particularly one kind candle can be made to produce flakes, nebulous etc. outer
The cottonseed of sight plays caul-fat and adds the snowflake candle of composition preparation.
Background technology
The candle that rockets is a kind of candle with flakes, lenticular, snowflake shape or nebulous outward appearance, is also snowflake wax,
Liked extensively by people, formed larger market.The snowflake wax used at present, preparation method includes two kinds.
A kind of is that precipitation is crystallized in the cooling procedure of paraffin using essence and is formed, and snowflake is hot snowflower effect.Specifically
Manufacturing process is first to prepare post wax, is stained with paraffin refined wax liquid on surface, the wax liquor that re-melting is made up of paraffin, snuff wax and essence,
High temperature is poured into the mould for having installed post wax, cooling and mould unloading, finishing.The candle snowflake that this mode is produced is small, many, close, and oozes
It is oily serious.
In order to improve such case, derived second method, i.e., using the combination of paraffin-snuff wax-perfume ingredient and
Appropriate cooling means produces snowflake.Water cooling and constant temperature cooling side is respectively adopted in such as patent CN1616623A, CN1616620A
Formula controls the precipitation of snowflake, both modes enable to snowflake it is big, less, dredge, effect is true to nature.But this method is only applicable to one
Material system (paraffin-snuff wax-essence) is planted, with raw material limitation.
Cottonseed oil is the large resource of China one, and abundance ranks first in the world throughout the year.It will be China's industry to make good use of cottonseed oil
A big advantage.But current cottonseed oil usage amount is less, it is mainly used in making the edible oils such as frying oil, shortening, or be used for
The general industry product such as soap, ink, pesticide solvent are produced, technology content is relatively low, and under-capacity operation, serious waste of resources.
The content of the invention
It is applied to a variety of candle raw material systems there is provided one kind to solve above mentioned problem of the prior art, wax can be made
The multiple patterns such as good snowflake, crystal, snowflake or nebulous, an effect caul-fat true to nature are presented in candle surface.
It is a further object to provide the candle that rockets with These characteristics.
To achieve these goals, the present invention provides following technical scheme：
The invention provides the application that plays caul-fat raw material of the cottonseed oil as the candle that rockets, the cottonseed oil melting range
For -5~5 DEG C, iodine number scope is 105~120.
The research of the present invention finds that cottonseed oil is used for making the candle that rockets as caul-fat is played, and can present and rocket well
Effect.Flowering mechanism：Candle body crystallizes to form crystal boundary, and causes crystal boundary to shrink in recrystallization process, formed grain boundary gaps or
Crack, the anaclasis occurred in plane of crystal will be generated with mottled pattern.Certain many crystal boundaries and grain boundary gaps
It will form snowflake, and the addition for the cottonseed oil that melting range is -5~5 DEG C, iodine number scope is 105~120 can then reduce crystal
Between cohesive force, produce more crystal boundaries and gap, it is filled therebetween as liquid phase, through anaclasis, will result in mottled shape
Looks increase, snowflower effect enhancing.
Caul-fat is played the invention provides a kind of cottonseed, composition is by cottonseed oil, essential oil, mineral oil and side chain alpha-olefin polymerization
Thing is constituted, and the percentage by weight that wherein cottonseed oil has accounted for caul-fat is 1%~100%.
Side chain alpha-olefin polymers are the hydro carbons that alpha-olefin aggregates into appropriate relative molecular mass under catalyst action, and
Obtained by techniques such as hydrofinishing, vacuum distillations.Straightαolefin polymeric lock oil ability is then poor, side chain alpha-olefin polymerization
Thing structure is more unordered, more network structure, with more the oily ability of lock, the lock of the invention by using side chain alpha-olefin polymers
Oily ability fully assembles the essential oil and mineral oil of cottonseed oil and auxiliary, will not excessively disperse in wax liquor, and then produce
Preferably rocket effect.It is at room temperature liquid that this, which plays caul-fat, and the dress of different shape can be formed by being added in basic wax
Decoration line, when using low melting point cottonseed oil (- 5 DEG C~0 DEG C) or mineral oil, can be made point-like or small size snowflake plays caul-fat；
During using high-melting-point cottonseed oil (be more than 0 DEG C and be less than or equal to 5 DEG C) or mineral oil, sheet can be made or large scale snowflake plays caul-fat；
When the side chain alhpa olefin using macromolecule (1000~2000), high usage ratio (accounted for caul-fat gross weight 20%~40%)
During polymer, it can be made and play caul-fat with what seepage-proof oil was acted on；Use small-molecular-weight (100 less than 1000), low ratio
During the side chain alpha-olefin polymers of (more than 5% is less than 20%), then seepage-proof oil declines, but do not impacted to normal rocket.
During without essence oil addition, the effect that rockets of caul-fat is played without significant change.Also there is such rule in addition：It is fragrant in candle raw material
Smart ratio (accounts for total wax and weighs more than 5%) when more, and playing caul-fat can less plus (accounting for total wax weight ratio 0.1%~3%).
Preferably, above-mentioned cottonseed is risen in caul-fat, and the C atoms number of the side chain alpha-olefin polymers is 14~20.
It is highly preferred that above-mentioned cottonseed is risen in caul-fat, the side chain alpha-olefin polymers molecular weight is 100~2000, and viscosity is
500~1500cps under the conditions of 20 DEG C.
Above-mentioned cottonseed plays caul-fat, cottonseed oil, essential oil, the part by weight of mineral oil and side chain alpha-olefin polymers for 40~
80:10~40:10~20:10~40.
Preferably, above-mentioned cottonseed plays caul-fat, and the cottonseed oil fusing point is -1~5 DEG C, and iodine number is 105~110.This fusing point,
The cottonseed oil of iodine number scope can facilitate the snowflake pattern of large-size, and sparse, uniform.Preferred melting range is -3~
5℃。
Preferably, above-mentioned cottonseed plays caul-fat, the essential oil is the essential oil of plant extract, animal is extracted essential oil,
Synthetic fragrance oil, or any two or more mixture；The mineral oil is liquid refining petroleum or liquid paraffin oil.
Rocketed candle present invention also offers one kind, its raw material includes basic wax and the cottonseed described in any of the above rockets
Oil, plays caul-fat and accounts for the 0.1~5% of whole candle raw material gross weight；The basic wax is paraffin, vegetable wax, animal wax, Huo Zheqi
In any two or more blended wax.
Preferably, the above-mentioned candle that rockets, raw material also includes one kind in essence, dyestuff, ultraviolet screener and antioxidant
Or it is several.Preferably to improve the universality energy for the candle that rockets.
Present invention also offers the preparation method of the above-mentioned candle that rockets, it is that will play caul-fat to mix with basic wax liquor, is filling wax
Cooled down, be then stripped with the speed that room temperature is cooled in 1~2h times afterwards.Preparation method very simple.
The present invention has the advantages that：
It is many-sided applications expanding scope of cottonseed oil the invention provides a kind of new application of cottonseed oil.The present invention
The cottonseed for the candle that rockets provided plays caul-fat, with the excellent effect that rockets, can make a variety of snowflake shapes：Point, piece,
Group, nebula etc.；Suitable for plurality of raw materials system candle, including paraffinic base candle, plant cerul candle, animal aliphatic radical candle and mixed
Close base candle.And it is easy to use, the technique for making the candle that rockets is simple, cost-effective.
Embodiment
In order that those skilled in the art more fully understand the present invention program, with reference to embodiment to this hair
It is bright to be described in further detail.
Embodiment one：
Cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is -3 DEG C, iodine number is 115 or so；Essential oil uses the essential oil of plant extract；
Mineral oil uses liquid refining petroleum；Side chain alpha-olefin polymers carbon number is (14~18), molecular weight (100~1000), viscous
Spend (500~1000,20 DEG C).
By above-mentioned cottonseed oil, essential oil, mineral oil, side chain alpha-olefin polymers with 80:5:5:10 ratios are well mixed, system
Into a caul-fat.It is liquid at room temperature to meet this and play caul-fat.
Embodiment two：
A kind of cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is 5 DEG C, iodine number is 105 or so, essential oil uses the essential oil that animal is extracted；Ore deposit
Thing oil uses liquid paraffin oil；Side chain alpha-olefin polymers carbon number is (14~18), molecular weight (100~1000), viscosity
(500~1000,20 DEG C).
By cottonseed oil, essential oil, mineral oil, side chain alpha-olefin polymers with 80:5:5:10 ratios are well mixed, and have been made
Caul-fat.It is liquid at room temperature to meet this and play caul-fat.
Embodiment three：
A kind of cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is 2 DEG C, iodine number is 108 or so；Essential oil uses the essence extracted from plant
Oil；Mineral oil uses liquid refining petroleum；Increase：Side chain alpha-olefin polymers carbon number is (16~18), molecular weight (1000
~1800), viscosity (700~1200,20 DEG C).
By cottonseed oil, essential oil, mineral oil, side chain alpha-olefin polymers with 40:10:10:40 ratios are well mixed, and are made
Play caul-fat.It is liquid at room temperature to meet this and play caul-fat.
Example IV：
A kind of cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is 2 DEG C, iodine number is 108 or so；Essential oil uses the essence extracted from plant
Oil；Mineral oil uses liquid refining petroleum；Side chain alpha-olefin polymers carbon number be (14~18), molecular weight (100~
1000), viscosity (500~1000,20 DEG C).
By cottonseed oil, essential oil, mineral oil, side chain alpha-olefin polymers with 40:10:10:40 ratios are well mixed, and are made
Play caul-fat.It is liquid at room temperature to meet this and play caul-fat.
Embodiment five：
A kind of cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is 2 DEG C, iodine number is 108 or so；Essential oil uses the essential oil extracted from plant；
Mineral oil uses liquid paraffin oil；Side chain alpha-olefin polymers carbon number is (16~18) molecular weight (1000~1800), viscosity
(700~1200,20 DEG C).
By cottonseed oil, essential oil, mineral oil, side chain alpha-olefin polymers with 75:10:10:5 ratios are well mixed, and have been made
Caul-fat.It is liquid at room temperature to meet this and play caul-fat.
Embodiment six：
A kind of cottonseed for candle plays the preparation of caul-fat, comprises the following steps：
(1) by environment temperature control at 5~30 DEG C；
(2) raw material：The cottonseed oil that fusing point is 2 DEG C, iodine number is 108 or so, mineral oil uses liquid paraffin oil, side chain α alkene
Hydrocarbon polymer carbon number is (16~18) molecular weight (1000~1800), viscosity (700~1200,20 DEG C).
By cottonseed oil, mineral oil, side chain alpha-olefin polymers with 50:10:40 ratios are well mixed, and caul-fat has been made.Meet
It is liquid at room temperature that this, which plays caul-fat,.
The gained of embodiment one to six plays caul-fat, mix respectively with paraffin (caul-fat can both have been added before melted paraffin wax or
Can be individually added into, will not have an impact to product after melted paraffin wax), fill after wax to be cooled to the speed of room temperature in the 1-2h times
Cooling, obtains the candle that rockets.
The gained of embodiment one to six can certainly be played caul-fat, be mixed respectively with vegetable wax, animal wax or blended wax,
Acquisition rockets candle.
Table 1, each embodiment rocket performance and permeability situation contrast
Caul-fat making embodiment is more played no longer to describe, but it is general with such rule：Use low melting point cottonseed oil
Or during mineral oil, point-like can be made or small size snowflake plays caul-fat；During using high-melting-point cottonseed oil or mineral oil, sheet can be made
Or large scale snowflake plays caul-fat；Using macromolecule, at high proportion side chain alpha-olefin polymers when, can be made with seepage-proof oil effect
Rise caul-fat；During using small-molecular-weight, low ratio side chain alpha-olefin polymers, then and without seepage-proof oil effect, but risen to normal
Flower is not impacted；During without essence oil addition, the effect that rockets of caul-fat is played without significant change.Also there is such rule in addition：
When essence is more in candle raw material, playing caul-fat can add less.
Specific case used herein is set forth to the principle and embodiment of the present invention, and above example is said
The bright core concept for being only intended to help to understand the present invention.It should be pointed out that for those skilled in the art,
Under the premise without departing from the principles of the invention, some improvement and modification can also be carried out to the present invention, these improve and modified
Fall into the protection domain of the claims in the present invention.
Claims (10)
1. cottonseed oil is as the application for playing caul-fat raw material for the candle that rockets, the cottonseed oil melting range is -5~5 DEG C, iodine number model
Enclose for 105~120.
2. a kind of cottonseed plays caul-fat, it is characterised in that composition is by cottonseed oil, essential oil, mineral oil and side chain alpha-olefin polymers group
Into the percentage by weight that wherein cottonseed oil has accounted for caul-fat is 1%~100%.
3. cottonseed according to claim 2 plays caul-fat, it is characterised in that the C atom numbers of the side chain alpha-olefin polymers
For 14~20.
4. cottonseed according to claim 3 plays caul-fat, it is characterised in that the side chain alpha-olefin polymers molecular weight is 100
~2000, viscosity is 500~1500cps under the conditions of 20 DEG C.
5. cottonseed according to claim 2 plays caul-fat, it is characterised in that cottonseed oil, essential oil, mineral oil and side chain α alkene
The part by weight of hydrocarbon polymer is 1~100:0~40:0~20:0~40.
6. cottonseed according to claim 2 plays caul-fat, it is characterised in that the cottonseed oil fusing point is -1~5 DEG C, iodine number is
105~120.
7. cottonseed according to claim 2 rise caul-fat, it is characterised in that the essential oil for plant extract essential oil,
Essential oil, the synthetic fragrance oil of animal extraction, or any two or more mixture；The mineral oil is that liquid refines stone
Oil or liquid paraffin oil.
The candle 8. one kind rockets, it is characterised in that raw material includes basic wax and any described cottonseed of claim 2~7 rockets
Oil, plays caul-fat and accounts for the 0.1%~5% of whole candle raw material gross weight；The basic wax be paraffin, vegetable wax, animal wax, or
Wherein any two or more blended wax.
9. the candle according to claim 8 that rockets, it is characterised in that raw material also include essence, dyestuff, ultraviolet screener and
One or more in antioxidant.
10. the preparation method of the candle that rockets described in claim 8, it is characterised in that be that will play caul-fat to mix with basic wax liquor,
Fill wax after with 1~2 hour in be cooled to room temperature speed cooling, be then stripped.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710310065.XA CN107011999B (en) | 2017-05-05 | 2017-05-05 | Cottonseed flower oil and flower candle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710310065.XA CN107011999B (en) | 2017-05-05 | 2017-05-05 | Cottonseed flower oil and flower candle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107011999A true CN107011999A (en) | 2017-08-04 |
| CN107011999B CN107011999B (en) | 2020-11-03 |
Family
ID=59448812
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710310065.XA Active CN107011999B (en) | 2017-05-05 | 2017-05-05 | Cottonseed flower oil and flower candle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107011999B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030046860A1 (en) * | 2001-08-02 | 2003-03-13 | Archer Daniels Midland Co. | Vegetable fat-based candles |
| CN102517158A (en) * | 2011-11-18 | 2012-06-27 | 宁波旷世居家用品有限公司 | Snowflake candle with alpha-olefin polymer and preparation method thereof |
| CN104651061A (en) * | 2015-02-02 | 2015-05-27 | 宁波旷世智源工艺设计股份有限公司 | Snowflake candle and preparation method thereof |
-
2017
- 2017-05-05 CN CN201710310065.XA patent/CN107011999B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030046860A1 (en) * | 2001-08-02 | 2003-03-13 | Archer Daniels Midland Co. | Vegetable fat-based candles |
| CN102517158A (en) * | 2011-11-18 | 2012-06-27 | 宁波旷世居家用品有限公司 | Snowflake candle with alpha-olefin polymer and preparation method thereof |
| CN104651061A (en) * | 2015-02-02 | 2015-05-27 | 宁波旷世智源工艺设计股份有限公司 | Snowflake candle and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN107011999B (en) | 2020-11-03 |
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