CN104651061A - Snowflake candle and preparation method thereof - Google Patents
Snowflake candle and preparation method thereof Download PDFInfo
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- CN104651061A CN104651061A CN201510052918.5A CN201510052918A CN104651061A CN 104651061 A CN104651061 A CN 104651061A CN 201510052918 A CN201510052918 A CN 201510052918A CN 104651061 A CN104651061 A CN 104651061A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/008—Candles characterised by their form; Composite candles, e.g. candles containing zones of different composition, inclusions, or the like
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- Chemical Kinetics & Catalysis (AREA)
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- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to snowflake candle and a preparation method thereof, and belongs to the field of fine chemical engineering. The snowflake candle comprises a lampwick and a candle body which is mainly made of wax, wherein the wax of the candle body mainly consists of the following raw materials (in percentage by mass): 5-8% of soft wax, 2-5% of a plant additive, 1-3% of fragrance, 0.3-0.8% of pigment, 0.3-0.6% of an antioxidant, 0.4-0.8% of a lubricant and the balance of paraffin. The invention further provides the preparation method of the snowflake candle. The preparation method comprises the following steps: uniformly mixing the raw materials, heating to melt the raw materials, casting, cooling and forming, thereby obtaining a finished product. The snowflake candle provided by the invention is simple in preparation method, relatively low in production cost, good in comprehensive property such as the overall hardness, the surface smoothness, thermal resistance and the like, long-lasting in color and fragrance, good in snowflake effect, attractive in appearance, convenient to use and relatively good in market competiveness, and the raw materials are environmentally friendly and easily available.
Description
Technical field
The present invention relates to a kind of snowflake candle and preparation method thereof, belong to field of fine chemical.
Background technology
The use of candle is with a long history, and in ancient times, candle is simple illuminations mostly.But in the modern times, candle has turned to gradually from single illuminations possesses artistry, appreciating and the several functions such as ornamental.At present, the production kind of candle has a lot, generally can be divided into common making candle for domestic illumination and craftwork candle, and wherein craftwork candle can be divided into again jelly artistic taper and candle and stacte artistic taper and candle.
Snowflake candle utilizes essence crystallization and a kind of surface effect candle formed in the process of cooling of paraffin.Chinese invention patent application file (publication number: CN1616623A) discloses a kind of method for making water cooling snow flake candle adding high molecular polymer.The method for raw material, obtains snowflake candle through melting, the processes such as wax, cooling, benefit wax and the slotting wick of finishing of filling with paraffin, alpha-olefin superpolymer, snuff wax, essence and oxidation inhibitor.Although the snowflake candle obtained by this formula and complete processing overcomes little, many, the close and defect that oil impregnate is serious of the snowflake of the snowflake candle that traditional diamond-making technique obtains, but the complete processing of snowflake candle is relatively loaded down with trivial details, and be not well positioned to meet modern Man's Demands in appearance yet.
In prior art, the main raw material of conventional candle candle body is generally paraffin, spices, colorant etc., and the candle body of snowflake candle of the present invention on the basis of existing technology, with the addition of appropriate plant additive, soft wax, oxidation inhibitor and lubricant.Soft wax add the combustion time the saturation ratio increasing colorant that effectively can improve candle, soft wax add-on is very few, and the color and luster of candle is bright not, and combustion time is short, and soft wax add-on too much can reduce the hardness etc. of candle on the contrary.In addition, oxidation inhibitor plays antioxygenation and keeps candle fragrance and fast in colour, lubricant lubricate increase surface of candle glossiness in the course of processing.Therefore, the present invention by the reasonable compatibility between candle candle body each composition, obtain color and luster better, the good snowflake candle of lasting fragrance, snowflower effect.
Plant additive described in the present invention is one or more in vegetable wax, and vegetable wax can present special crystal habit when high temperature cooling crystallization, and then improves the snowflower effect of snowflake candle.
As preferably, vegetable wax is one or more in carnauba wax, gama wax, rice bran wax, sugar-cane wax, laurel wax, Pseudotsuga menziesii (Mirbel) Franco wax.
Further preferably, the plant additive adopted in the present invention is the mixture of carnauba wax and gama wax, wherein carnauba wax: the mass ratio of gama wax is 5-8:3.Carnauba wax and gama wax are biodegradable, reproducible natural environmental-protective vegetable wax.Especially, carnauba wax is smokeless when burning, and has the features such as natural, health environment-friendly, can also be compatible admirably with essence, colorant etc.In the prior art, the candle ubiquity hardness that single paraffin is made is low, the easy defect such as softening, the present invention is composite use gama wax on the basis of carnauba wax, not only effectively overcome these defects, significantly improve the integral hardness of candle, the thermotolerance of candle and the transparency, surface smoothness etc. of outward appearance thereof can also be improved, meet environmental requirement simultaneously.
The candle body of snowflake candle of the present invention spices used is one or more in rose compound, Mint Essence, Syringa oblata Lindl. essence, lavender oil, jacinthe essence, cream jasmin france.Adding of these essence can make candle in the process of burning, gives out fragrance, invigorating.
In order to prevent candle oxidized and keep the fragrance of candle and color and luster more lasting, add appropriate oxidation inhibitor in snowflake wax of the present invention, described oxidation inhibitor can be in oxidation inhibitor sp, antioxidant 264, antioxidant 1010, antioxidant 300, antioxidant 2246-s one or more.These oxidation inhibitor are low volatilization, nontoxic, excellent property, free of contamination environment-friendly type oxidation inhibitor, make the snowflake candle obtained have more the market competitiveness.
And adding of lubricant, lubrication can be played on the one hand in the course of processing, then can improve the softening temperature of candle on the other hand, increase its intensity, hardness and surface gloss.As preferably, lubricant used in the candle body of snowflake candle of the present invention is one or more in polyethylene wax, Poly Propylene Wax and hydrogenated vegetable oil.
Another object of the present invention is to provide a kind of preparation method of above-mentioned snowflake candle, and this preparation method comprises the steps:
S1, each raw material of above-mentioned snowflake candle candle body to be mixed (by percentage to the quality), reheat melting and obtain wax liquid;
S2, then above-mentioned wax liquid to be poured into a mould fixing for wick in a mold, then at constant temperature 10-18 DEG C cooling forming, the demoulding obtains snowflake candle finished product.
In the preparation method of above-mentioned a kind of snowflake candle, in order to enable each raw material of the candle body of snowflake candle fully melting obtain the wax liquid that is uniformly dissolved, as preferably, the temperature of the heating and melting described in step S1 is 90-100 DEG C, heat-up time is 0.5-1h.And in casting process, the viscosity influence of wax liquid the quality of final candle finished product.In casting process, the viscosity of wax liquid is excessive or too small, and the excessive mould phenomenon of generation in casting process or candle finished product can be caused to occur the defects such as crackle space.Therefore in the casting process of snowflake candle of the present invention, need the viscosity of wax liquid to remain on 0.4-0.6Pa.s.In addition, before wax liquid is poured into a mould, by mould and die preheating to 100-120 DEG C, to prevent mould severe attrition, thus the mold use life-span need be extended.
In the preparation method of above-mentioned a kind of snowflake candle, the time of the demoulding described in step S2 is 1.0-1.5h.In addition, in the preparation method of snowflake candle of the present invention, as preferably, mould used is the mould of plastics of anti-essence corrosion.Compared with common metal die, mould therefor of the present invention not only cost is low, and good corrosion resistance, can effectively prevent essence to the corrosion of mould, extends the mold use life-span further.
Compared with prior art, the present invention has following advantage:
The formula of snowflake candle candle body of the present invention is on the basis of paraffin, add appropriate soft wax, plant additive, oxidation inhibitor, lubricant etc., especially plant additive adopts the composite use of mixture of carnauba wax and gama wax two kinds of natural phant waxes, raw material environmental protection is easy to get, then make further by simple working method, not only increase integral hardness and the thermotolerance of snowflake candle, also can improve the transparency, surface smoothness etc. of candle outward appearance, and the snowflower effect of snowflake candle is good, color and luster and lasting fragrance, have more the market competitiveness.
Summary of the invention
The object of the invention is for the above-mentioned problems in the prior art, propose the snowflake candle that a kind of complete processing is simple, snowflower effect good, outward appearance has more appreciating.
Object of the present invention realizes by following technical proposal: a kind of snowflake candle, comprise wick and the candle body primarily of wax composition, the raw material of the wax of described candle body is become to be grouped into (by percentage to the quality) by following: soft wax: 5-8%, plant additive: 2-5%, spices: 1-3%, colorant: 0.3-0.8%, oxidation inhibitor: 0.3-0.6%, lubricant: 0.4-0.8%, surplus is paraffin.
Embodiment
Be below specific embodiments of the invention, technical scheme of the present invention is further described, but the present invention is not limited to these embodiments.
Table 1: the main moiety of embodiment of the present invention 1-5 snowflake candle and mass percent
Embodiment 1
Mixed by each raw material of snowflake candle candle body described in table 1 embodiment 1, then heat 0.5h at 90 DEG C, melting obtains wax liquid; Wherein carnauba wax: the mass ratio of gama wax is 6:3.
By mould and die preheating to 100 DEG C, and afterwards above-mentioned wax liquid is poured into a mould fixing for textile wick in a mold, then at constant temperature 12 DEG C after cooling forming the demoulding obtain snowflake candle finished product; Wherein mould adopts the mould of plastics that anti-essence corrodes, and in casting process, keep the viscosity of wax liquid to be 0.4Pa.s, demould time is 1.2h.
Embodiment 2
Mixed by each raw material of snowflake candle candle body described in table 1 embodiment 2, then heat 1h at 100 DEG C, melting obtains wax liquid; Wherein carnauba wax: the mass ratio of gama wax is 5:3.
By mould and die preheating to 105 DEG C, and afterwards above-mentioned wax liquid is poured into a mould fixing for textile wick in a mold, then at constant temperature 12 DEG C after cooling forming the demoulding obtain snowflake candle finished product; Wherein mould adopts the mould of plastics that anti-essence corrodes, and in casting process, keep the viscosity of wax liquid to be 0.6Pa.s, demould time is 1.0h.
Embodiment 3
Mixed by each raw material of snowflake candle candle body described in table 1 embodiment 3, then heat 0.8h at 95 DEG C, melting obtains wax liquid; Wherein carnauba wax: the mass ratio of gama wax is 7:3.
By mould and die preheating to 110 DEG C, and afterwards above-mentioned wax liquid is poured into a mould fixing for textile wick in a mold, then at constant temperature 15 DEG C after cooling forming the demoulding obtain snowflake candle finished product; Wherein mould adopts the mould of plastics that anti-essence corrodes, and in casting process, keep the viscosity of wax liquid to be 0.5Pa.s, demould time is 1.3h.
Embodiment 4
Mixed by each raw material of snowflake candle candle body described in table 1 embodiment 4, then heat 1h at 98 DEG C, melting obtains wax liquid; Wherein carnauba wax: the mass ratio of gama wax is 8:3.
By mould and die preheating to 120 DEG C, and afterwards above-mentioned wax liquid is poured into a mould fixing for textile wick in a mold, then at constant temperature 18 DEG C after cooling forming the demoulding obtain snowflake candle finished product; Wherein mould adopts the mould of plastics that anti-essence corrodes, and in casting process, keep the viscosity of wax liquid to be 0.5Pa.s, demould time is 1.5h.
Embodiment 5
Mixed by each raw material of snowflake candle candle body described in table 1 embodiment 5, then heat 0.7h at 100 DEG C, melting obtains wax liquid; Wherein carnauba wax: the mass ratio of gama wax is 7:3.
By mould and die preheating to 115 DEG C, and afterwards above-mentioned wax liquid is poured into a mould fixing for textile wick in a mold, then at constant temperature 14 DEG C after cooling forming the demoulding obtain snowflake candle finished product; Wherein mould adopts the mould of plastics that anti-essence corrodes, and in casting process, keep the viscosity of wax liquid to be 0.55Pa.s, demould time is 1.5h.
The snowflake candle obtained by embodiment of the present invention 1-5 and the snowflake candle of comparative example carry out performance test, and test result is as shown in table 2.
The performance test results of the snowflake candle of table 2: embodiment of the present invention 1-5 and comparative example
Comparative example is commercially available common snowflake candle.
In sum, the raw material of snowflake candle of the present invention candle body is by the composite use of vegetable wax of paraffin and natural environmental-protective, and add soft wax, oxidation inhibitor, lubricant etc., and adopt simple preparation method to prepare snowflake candle, compared with common snowflake candle, its hardness is good, snowflower effect is good, burning is good without black smoke, outward appearance, and has more the market competitiveness.
Specific embodiment described herein is only to the explanation for example of the present invention's spirit.Those skilled in the art can make various amendment or supplement or adopt similar mode to substitute to described specific embodiment, but can't depart from spirit of the present invention or surmount the scope that appended claims defines.
Although made a detailed description the present invention and quoted some specific embodiments as proof, to those skilled in the art, only otherwise it is obvious for leaving that the spirit and scope of the present invention can make various changes or revise.
Claims (10)
1. a snowflake candle, comprise wick and the candle body primarily of wax composition, it is characterized in that, the raw material of the wax of described candle body is become to be grouped into (by percentage to the quality) by following: soft wax: 5-8%, plant additive: 2-5%, spices: 1-3%, colorant: 0.3-0.8%, oxidation inhibitor: 0.3-0.6%, lubricant: 0.4-0.8%, surplus is paraffin.
2. snowflake candle according to claim 1, is characterized in that, described plant additive is one or more in vegetable wax.
3. snowflake candle according to claim 2, is characterized in that, described vegetable wax is one or more in carnauba wax, gama wax, rice bran wax, sugar-cane wax, laurel wax, Pseudotsuga menziesii (Mirbel) Franco wax.
4. snowflake candle according to claim 1 and 2, is characterized in that, described plant additive is the mixture of carnauba wax and gama wax, wherein carnauba wax: the mass ratio of gama wax is 5-8:3.
5. snowflake candle according to claim 1, is characterized in that, described oxidation inhibitor is one or more in oxidation inhibitor sp, antioxidant 264, antioxidant 1010, antioxidant 300, antioxidant 2246-s.
6. snowflake candle according to claim 1, is characterized in that, described lubricant is one or more in polyethylene wax, Poly Propylene Wax and hydrogenated vegetable oil.
7. a preparation method for snowflake candle, is characterized in that, described preparation method comprises the steps:
S1, by described in claim 1 snowflake candle candle body each raw material mix (by percentage to the quality), reheat melting and obtain wax liquid;
S2, then above-mentioned wax liquid to be poured into a mould fixing for wick in a mold, then at constant temperature 10-18 DEG C cooling forming, the demoulding obtains snowflake candle finished product.
8. the preparation method of snowflake candle according to claim 7, is characterized in that, the temperature of heating and melting described in step S1 is 90-100 DEG C, heat-up time is 0.5-1h.
9. the preparation method of snowflake candle according to claim 7, is characterized in that, in casting process described in step S2, the viscosity of wax liquid remains on 0.4-0.6Pa.s.
10. the preparation method of snowflake candle according to claim 7, is characterized in that, the time of the demoulding described in step S2 is 1.0-1.5h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510052918.5A CN104651061B (en) | 2015-02-02 | 2015-02-02 | A kind of snowflake candle and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510052918.5A CN104651061B (en) | 2015-02-02 | 2015-02-02 | A kind of snowflake candle and preparation method thereof |
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| CN104651061A true CN104651061A (en) | 2015-05-27 |
| CN104651061B CN104651061B (en) | 2018-10-30 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106916632A (en) * | 2017-02-21 | 2017-07-04 | 大连达伦特工艺品有限公司 | A kind of rice bran candle and preparation method thereof |
| CN107011999A (en) * | 2017-05-05 | 2017-08-04 | 青岛金王应用化学股份有限公司 | A kind of cottonseed plays caul-fat and the candle that rockets |
| CN109370784A (en) * | 2018-11-12 | 2019-02-22 | 颍上邢氏实业科技有限公司 | A kind of production method of color lacquer candle |
| CN109880697A (en) * | 2019-03-13 | 2019-06-14 | 东莞理工学院 | A kind of special type candle wax material and special type candle |
| CN110305739A (en) * | 2019-08-02 | 2019-10-08 | 南通职业大学 | A kind of candle that can be recycled, formula and initial candle preparation method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616622A (en) * | 2004-09-23 | 2005-05-18 | 青岛金王应用化学股份有限公司 | Recipe for making candle without dewalling using palm wax |
| CN102517158A (en) * | 2011-11-18 | 2012-06-27 | 宁波旷世居家用品有限公司 | Snowflake candle with alpha-olefin polymer and preparation method thereof |
-
2015
- 2015-02-02 CN CN201510052918.5A patent/CN104651061B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616622A (en) * | 2004-09-23 | 2005-05-18 | 青岛金王应用化学股份有限公司 | Recipe for making candle without dewalling using palm wax |
| CN102517158A (en) * | 2011-11-18 | 2012-06-27 | 宁波旷世居家用品有限公司 | Snowflake candle with alpha-olefin polymer and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106916632A (en) * | 2017-02-21 | 2017-07-04 | 大连达伦特工艺品有限公司 | A kind of rice bran candle and preparation method thereof |
| CN107011999A (en) * | 2017-05-05 | 2017-08-04 | 青岛金王应用化学股份有限公司 | A kind of cottonseed plays caul-fat and the candle that rockets |
| CN107011999B (en) * | 2017-05-05 | 2020-11-03 | 青岛金王应用化学股份有限公司 | Cottonseed flower oil and flower candle |
| CN109370784A (en) * | 2018-11-12 | 2019-02-22 | 颍上邢氏实业科技有限公司 | A kind of production method of color lacquer candle |
| CN109880697A (en) * | 2019-03-13 | 2019-06-14 | 东莞理工学院 | A kind of special type candle wax material and special type candle |
| CN110305739A (en) * | 2019-08-02 | 2019-10-08 | 南通职业大学 | A kind of candle that can be recycled, formula and initial candle preparation method |
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| Publication number | Publication date |
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| CN104651061B (en) | 2018-10-30 |
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Address after: 315000 Xuejia Village, Gulin Town, Haishu District, Ningbo City, Zhejiang Province Patentee after: Ningbo Kuanshi Zhiyuan Technology Design Co., Ltd. Address before: 315176 Xuejia Village, Gulin Town, Yinzhou District, Ningbo City, Zhejiang Province Patentee before: Ningbo Kwung's Gift Co., Ltd. |
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