CN107007479A - A kind of four layers of low-viscosity (mobile) liquid class cosmetics - Google Patents
A kind of four layers of low-viscosity (mobile) liquid class cosmetics Download PDFInfo
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- CN107007479A CN107007479A CN201710145201.4A CN201710145201A CN107007479A CN 107007479 A CN107007479 A CN 107007479A CN 201710145201 A CN201710145201 A CN 201710145201A CN 107007479 A CN107007479 A CN 107007479A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/03—Liquid compositions with two or more distinct layers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/69—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing fluorine
- A61K8/70—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing fluorine containing perfluoro groups, e.g. perfluoroethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention relates to a kind of four layers of low-viscosity (mobile) liquid class cosmetics, it is characterised in that includes following components：Mass percent for 10% 35% dimethyl silicone polymer, mass percent for 10% 30% carbochain alkane solvents, mass percent for 10% 40% water alcohols solvent, mass percent is 10% 35% perfluoro organic compound solvent, and mass percent is that 0.01% 0.5% polyquaternium 78 or the succinates of cetyl triethyl ammonium dimethyl silicone polymer PEG 8 or any of them compare mixture.The invention provides in the middle of one kind without physical separation, but layer still has four layers of low-viscosity (mobile) liquid class cosmetics of clear layering interfaces with layer, multilayer is mixed after shake, four layers of clear stratification state can be reverted to rapidly again after static, and continue to keep stable clear interface, four layers of low-viscosity (mobile) liquid class cosmetics without oil droplet wall built-up phenomenon after layering.
Description
Technical field
It is more particularly to a kind of middle without physical separation the present invention relates to cosmetic technical field, but layer and layer are still with clear
Four layers of low-viscosity (mobile) liquid class cosmetics of clear layering interfaces, original four layers clear layering can be recovered rapidly again by shaking after multilayer mixing
State, and continue to keep stable clear interface, and four layers of low-viscosity (mobile) liquid class cosmetics without oil droplet wall built-up phenomenon.
Background technology
Popular low-viscosity (mobile) liquid class cosmetics, are typically uniform one in the market, only least a portion of low viscous
It is two layers to spend liquid type cosmetics, there is also three layers of low-viscosity (mobile) liquid class cosmetics of only a few, but from without four layers of low viscosity
Liquid type cosmetics.
Presently commercially available two layers or three layers of stratified liquid class cosmetics, generally wherein one layer is water, and one is selected in addition
Plant or two kinds of immiscible and different greases of proportion, the effect being layered after shaking up is utilized to reach.Because such usual product is all
It is to use Transparent plastic pack, and plastics are all the non-polar materials of oleophylic, therefore during shake, a small amount of oil droplet can be obstinate
Cause on the inwall for sticking to transparent plastic packaging material after multilayer water class cosmetics shake up, the plastics bottle wall for the part that water layer is occupied
Still have a little oil droplet and there is wall built-up phenomenon, so that the clear of product layering is influenceed, and every layer will not seem so transparent.
Chinese patent CN201110264247《A kind of three layers of water class toner class cosmetics》Three layers are respectively that water alcohols is molten
Oxidant layer, carbochain alkanes or esters solvent layer and perfluoro organic compound solvent layer, because carbochain alkane solvents therein layer
There is the adhesiveness of similar blind date for oleophilic layer and transparent plastic bottle wall, there are carbochain alkane solvents after there is separation and formed
Tiny oil droplets stick to water layer plastics bottle wall, it is opaque to cause to shake up bottle wall after separation, feels the halfway situation of layering.
The content of the invention
The technical problem to be solved in the present invention is to provide in the middle of one kind without physical separation, but layer still has clear point with layer
Four layers of low-viscosity (mobile) liquid class cosmetics of bed boundary, original four layers clear layering shape can be recovered rapidly again by shaking after multilayer mixing
State, and continue to keep stable clear interface, and four layers of low-viscosity (mobile) liquid class cosmetics without oil droplet wall built-up phenomenon.Institute of the present invention
Low viscosity is stated, after referring to that four layers of liquid shake up, overall viscosity is not more than 100cps mobile liquid.
Testing herein viscosity data is used uniformly Brookfield viscosity apparatus, and test condition is 25 DEG C, S02 rotors,
Test rotating speed is 100rpm.
In order to solve the above technical problems, the present invention uses following technical scheme：
A kind of four layers of low-viscosity (mobile) liquid class cosmetics, it is characterised in that include following components：Mass percent is 10%-35%'s
Dimethyl silicone polymer, mass percent is 10%-30% carbochain alkane solvents, and mass percent is 10%-40%'s
Water alcohols solvent, mass percent is 10%-35% perfluoro organic compound solvent, and mass percent is 0.1%-0.5%
Polyquaternium -78 or cetyl triethyl ammonium dimethyl silicone polymer PEG-8 succinates or theirs is any than mixing
Thing.
Four layers of described low-viscosity (mobile) liquid class cosmetics, it is characterised in that：The viscosity of the dimethyl silicone polymer is
0.65-200cps。
Four layers of described low-viscosity (mobile) liquid class cosmetics, it is characterised in that：The carbochain alkane solvents are the hydrogenation poly- last of the ten Heavenly stems
One kind or their mixture in alkene, Parleam, isoparaffin, saualane.The Nexbase 2004, hydrogenation is poly- different
The range of viscosities of butylene is 5.0-100cps；The isoparaffin be Permethyl 99A, isohexadecane, Isoeicosane one of which or
Its mixture.
Four layers of described low-viscosity (mobile) liquid class cosmetics, it is characterised in that：The water alcohols solvent is water, propane diols, two
The polyethylene glycol that polyglycereol that propane diols, glycerine, butanediol, pentanediol, hexylene glycol, the degree of polymerization are 2-10, the degree of polymerization are 4-32
In one kind or their mixture.
Four layers of described low-viscosity (mobile) liquid class cosmetics, it is characterised in that：The perfluoro organic compound is perfluor perhydro
Change phenanthrene, PF 5070, one kind in perfluor hexane or their mixture.
Polyquaternium -78 of the present invention can be the product of COLONIAL CHEMCIAL companies of the U.S., trade name
POLYSUGAQUAT L-1010P。
The cetyl triethyl ammonium dimethyl silicone polymer PEG-8 succinates can be the U.S.
The product of BIOSILTECHNOLOGIES companies, trade name BIOPLEX CETYLSIL S.
The perfluor perhydrophenanthrene, PF 5070, perfluor hexane can be Minnesota Mining and Manufacturing Company's product, and range of commercial products is entitled
NOVEC。
The present invention is in Chinese invention patent CN201110264247《A kind of three layers of water class toner class cosmetics》Water alcohol
On the basis of class solvent layer, carbochain alkanes or esters solvent layer and perfluoro organic compound solvent layer, poly dimethyl silicon is added
Oxygen alkane forms it into the low-viscosity (mobile) liquid class cosmetics of four-layer structure, while adding polyquaternium -78 and cetyl triethyl ammonium
Any one or they of dimethyl silicone polymer PEG-8 succinates it is any than mixture, solve shake up it is rear quiet
The oil droplet wall built-up phenomenon occurred during only so that four layers of low-viscosity (mobile) liquid class cosmetics prepared by the present invention can be quiet after shaking up
Only 10-60min, can quickly be divided into the obvious four layers of liquid of boundary.
Investigate influence of the different type surfactant to four layers of liquid type cosmetics to test, match somebody with somebody on the basis of embodiment 1
Variety classes surfactant is added in side respectively, its influence being layered to four layers of liquid type cosmetics is investigated, experimental result is such as
Shown in table 1：
The different type surfactant of table 1 influences on the layered effect of four layers of liquid type cosmetics
Addition conventional nonionic surfactant, anion surfactant, amphoteric surface are can be seen that from above-mentioned experimental result
Four layers of liquid type cosmetics of activating agent and common cation surfactant can not all fully achieve four layers points of clear interface
From and only adding the cation by especially selecting, i.e. polyquaternium -78 and cetyl triethyl ammonium dimethyl silicone polymer
Four layers of quickly clear interface can be achieved in a kind of or their any formula than mixture in PEG-8 succinates
Separation.
As shown in Figure 1 and Figure 2, not compositions comprising cationic surfactants polyquaternium -78 or cetyl triethyl ammonium poly dimethyl
Four layers of water class cosmetics of siloxanes PEG-8 succinates（Basic components be the same as Example 1）, oil phase is attached on glass after layering
Bottle wall, wall built-up phenomenon is obvious.
As shown in figure 3, four layers of water class cosmetics of addition other types surfactant（Basic components be the same as Example 1）, shake up
It is layered slowly afterwards, and four layers can not be divided into.
As shown in figure 4, the cationic surfactant polyquaternium of addition mass fraction 0.05% prepared by embodiment 1-
78 four layers of water class cosmetics, it can be seen that four layers of liquid layered it is obvious and it is transparent clarification without wall built-up phenomenon.
In summary, the invention provides without physical separation, but layer and layer are still with clear layering interfaces in the middle of one kind
Four layers of low-viscosity (mobile) liquid class cosmetics, multilayer is mixed after shake, static to revert to four layers of clear stratification state rapidly again afterwards, and
It is lasting to keep stable clear interface, four layers of low-viscosity (mobile) liquid class cosmetics without oil droplet wall built-up phenomenon after layering.
The present invention also has exquisite appearance novel, and property is stable, and the oxygen dissolved in perfluoro organic compound solvent is quiet
Only do not allow volatile under state, be skin while keeping the skin wet, the beneficial effect such as oil.
Brief description of the drawings
Fig. 1 is without 0.01-0.50% polyquaterniums -78 and cetyl triethyl ammonium dimethyl silicone polymer PEG-8 ambers
A kind of or their any four layers of low-viscosity (mobile) liquid class cosmetics than mixture in amber acid esters；
Fig. 2 is Figure 1A portions partial enlarged drawing；
Fig. 3 is four layers of water class cosmetics of addition other types surfactant（Except：Addition 0.01-0.50% polyquaterniums-
78 and cetyl triethyl ammonium dimethyl silicone polymer PEG-8 succinates in a kind of or they any than mixing
Thing）；
Fig. 4 is the four layers of water class cosmetics that with the addition of the polyquaternium -78 of mass fraction 0.05% prepared by embodiment 1.
Embodiment
It is described further below by embodiment, the scope of but do not limit the invention in any way.
Embodiment 1：
A kind of four layers of liquid moisture retention water, weigh following components by mass percentage：
Preparation method：
1. above A phase liquid is well mixed, A phases liquid viscosity is measured for 4 cps；
2. above B phase liquid is well mixed, B phases liquid viscosity is measured for 10 cps；
3. above C phase liquid is well mixed, C phases liquid viscosity is measured for 10cps；
4. above D phase liquid is well mixed, D phases liquid viscosity is measured for 195 cps；
5. above-mentioned four kinds of liquid As, B, C and D are well mixed, score layer clearly four layers of low-viscosity (mobile) liquid class is stood completely
Cosmetic, after the cosmetics shake up, overall viscosity is 30cps, can be used as four layers of liquid moisture retention water.
Embodiment 2：
A kind of four layers of liquid cleansing liquid, weigh following components by mass percentage：
Preparation method：
1. above A phase liquid is well mixed, A phases liquid viscosity is measured for 200 cps；
2. above B phase liquid is well mixed, B phases liquid viscosity is measured for 90 cps；
3. above C phase liquid is well mixed, C phases liquid viscosity is measured for 25 cps；
4. above D phase liquid is well mixed, D phases liquid viscosity is measured for 15 cps；
5. above-mentioned four kinds of liquid As, B, C and D are well mixed, score layer clearly four layers of low-viscosity (mobile) liquid class is stood completely
Cosmetic, after the cosmetics shake up, overall viscosity is 60cps, can be used as make up remover.
Embodiment 3：
A kind of four layers of liquid Essence, weigh following components by mass percentage：
Preparation method：
1. above A phase liquid is well mixed, A phases liquid viscosity is measured for 40 cps；
2. above B phase liquid is well mixed, B phases liquid viscosity is measured for 6 cps；
3. above C phase liquid is well mixed, C phases liquid viscosity is measured for 255 cps；
4. above D phase liquid is well mixed, D phases liquid viscosity is measured for 75 cps；
5. above-mentioned four kinds of liquid As, B, C and D are well mixed, score layer clearly four layers of low-viscosity (mobile) liquid class is stood completely
Cosmetic, after the cosmetics shake up, overall viscosity is 200cps, can be used as Essence, is provided simultaneously with moisturizing, repairing effect.
Claims (6)
1. a kind of four layers of low-viscosity (mobile) liquid class cosmetics, it is characterised in that include following components：Mass percent is 10%-35%
Dimethyl silicone polymer, mass percent be 10%-30% carbochain alkane solvents, mass percent is 10%-40%
Water alcohols solvent, mass percent be 10%-35% perfluoro organic compound solvent, mass percent is 0.01%-
0.5% polyquaternium -78 or cetyl triethyl ammonium dimethyl silicone polymer PEG-8 succinates or theirs is any
Compare mixture.
2. four layers of low-viscosity (mobile) liquid class cosmetics according to claim 1, it is characterised in that：The dimethyl silicone polymer
Viscosity be 0.65-200cps.
3. four layers of low-viscosity (mobile) liquid class cosmetics according to claim 1, it is characterised in that：The carbochain alkane solvents
It is one kind or their mixture in Nexbase 2004, Parleam, isoparaffin, saualane.
4. described in Nexbase 2004, the range of viscosities of Parleam is 5.0-100cps；The isoparaffin is different 12
Alkane, isohexadecane, Isoeicosane one of which or its mixture.
5. four layers of low-viscosity (mobile) liquid class cosmetics according to claim 1, it is characterised in that：The water alcohols solvent is
Polyglycereol that water, propane diols, DPG, glycerine, butanediol, pentanediol, hexylene glycol, the degree of polymerization are 2-10, the degree of polymerization are 4-
One kind or their mixture in 32 polyethylene glycol.
6. four layers of low-viscosity (mobile) liquid class cosmetics according to claim 1, it is characterised in that：The perfluoro organic compound
For one kind or their mixture in perfluor perhydrophenanthrene, PF 5070, perfluor hexane.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710145201.4A CN107007479B (en) | 2017-03-13 | 2017-03-13 | A kind of four layers of low-viscosity (mobile) liquid class cosmetics |
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| CN201710145201.4A CN107007479B (en) | 2017-03-13 | 2017-03-13 | A kind of four layers of low-viscosity (mobile) liquid class cosmetics |
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| CN107007479A true CN107007479A (en) | 2017-08-04 |
| CN107007479B CN107007479B (en) | 2019-08-20 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107951749A (en) * | 2017-12-08 | 2018-04-24 | 广东芭薇生物科技股份有限公司 | A kind of four layers of liquid cleansing product |
| CN112006943A (en) * | 2020-08-10 | 2020-12-01 | 广州星业科技股份有限公司 | Multi-cleaning cleansing oil and preparation method thereof |
| CN112022743A (en) * | 2020-09-11 | 2020-12-04 | 广州简灿生物科技有限公司 | Liquid layered perfume and preparation method thereof |
| CN112336639A (en) * | 2020-11-03 | 2021-02-09 | 前研化妆品科技(上海)有限公司 | Four-layer low-viscosity liquid cosmetic without perfluorinated compounds |
| CN112969506A (en) * | 2019-02-27 | 2021-06-15 | 株式会社高丝 | Multi-layer cosmetic protective cosmetic |
| CN114795979A (en) * | 2022-04-15 | 2022-07-29 | 王涛 | Multiphase cosmetic and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102309418A (en) * | 2011-09-05 | 2012-01-11 | 珀莱雅(湖州)化妆品有限公司 | Three-layer water-based cosmetic |
| CN105832576A (en) * | 2016-05-03 | 2016-08-10 | 珠海伊斯佳科技股份有限公司 | Three-layer cleansing lotion and preparing method thereof |
-
2017
- 2017-03-13 CN CN201710145201.4A patent/CN107007479B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102309418A (en) * | 2011-09-05 | 2012-01-11 | 珀莱雅(湖州)化妆品有限公司 | Three-layer water-based cosmetic |
| CN105832576A (en) * | 2016-05-03 | 2016-08-10 | 珠海伊斯佳科技股份有限公司 | Three-layer cleansing lotion and preparing method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107951749A (en) * | 2017-12-08 | 2018-04-24 | 广东芭薇生物科技股份有限公司 | A kind of four layers of liquid cleansing product |
| CN112969506A (en) * | 2019-02-27 | 2021-06-15 | 株式会社高丝 | Multi-layer cosmetic protective cosmetic |
| CN112006943A (en) * | 2020-08-10 | 2020-12-01 | 广州星业科技股份有限公司 | Multi-cleaning cleansing oil and preparation method thereof |
| CN112022743A (en) * | 2020-09-11 | 2020-12-04 | 广州简灿生物科技有限公司 | Liquid layered perfume and preparation method thereof |
| CN112336639A (en) * | 2020-11-03 | 2021-02-09 | 前研化妆品科技(上海)有限公司 | Four-layer low-viscosity liquid cosmetic without perfluorinated compounds |
| CN114795979A (en) * | 2022-04-15 | 2022-07-29 | 王涛 | Multiphase cosmetic and application thereof |
| CN114795979B (en) * | 2022-04-15 | 2024-03-15 | 王涛 | Multiphase cosmetic and application thereof |
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| CN107007479B (en) | 2019-08-20 |
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