CN106982831A - A kind of composition and application process that purple spot of soybean is treated based on guaiacol - Google Patents

A kind of composition and application process that purple spot of soybean is treated based on guaiacol Download PDF

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Publication number
CN106982831A
CN106982831A CN201710235431.XA CN201710235431A CN106982831A CN 106982831 A CN106982831 A CN 106982831A CN 201710235431 A CN201710235431 A CN 201710235431A CN 106982831 A CN106982831 A CN 106982831A
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CN
China
Prior art keywords
guaiacol
soybean
composition
purple spot
procymidone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
CN201710235431.XA
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Chinese (zh)
Inventor
黄朝纲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Golden Phoenix Agrochemical Co Ltd
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Jiangsu Golden Phoenix Agrochemical Co Ltd
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Publication date
Application filed by Jiangsu Golden Phoenix Agrochemical Co Ltd filed Critical Jiangsu Golden Phoenix Agrochemical Co Ltd
Priority to CN201710235431.XA priority Critical patent/CN106982831A/en
Publication of CN106982831A publication Critical patent/CN106982831A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08Oxygen or sulfur directly attached to an aromatic ring system
    • A01N31/16Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/32Cyclic imides of polybasic carboxylic acids or thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of composition and application process that purple spot of soybean is treated based on guaiacol, guaiacol is applied to agriculture field, composition is made by a certain percentage with procymidone, for treating purple spot of soybean, guaiacol new application is developed, purple spot of soybean can effectively be treated, the resistance against diseases of crop is improved, and it is compared with other existing agricultural chemicals single doses, and prevention effect is more preferable, production cost is relatively low, is worthy to be popularized.

Description

A kind of composition and application process that purple spot of soybean is treated based on guaiacol
Technical field
The application of purple spot of soybean and administration side are being prevented and treated the present invention relates to pesticide field, more particularly to guaiacol mixture Method.
Background technology
Guaiacol is a kind of white or slightly yellow crystallization or colourless to pale yellow transparent oily liquids, there is special aroma Taste, scientific name guaiacol, glycerin ether, guaiacol glycerol ether, adjacent hydroxyl glycerin ether etc., guaiaci lignum is present in nature It is a kind of important fine-chemical intermediate in resin, pine tar and hardwood empyreumatic oil, is widely used in medicine, spices and dyestuff Synthesis, rarely have the document and technology for using it for other field in existing production and living.
The content of the invention
The present invention develops guaiacol in agriculture field, the application especially in terms of purple spot of soybean is prevented and treated, and There is provided its application process, blank of the guaiacol in the field purposes has been filled up, it is of the invention by guaiacol and procymidone system Into composition, phase composition includes guaiacol and procymidone, and the mass ratio of the guaiacol and procymidone is 1/10-10.
Preferably, the guaiacol and procymidone ratio are 1-5.
Preferably, wherein Determination of Guaiacol is 10%, procymidone content is 10%.
Preferably, also including the one or more in dispersant, sticker, bleeding agent, emulsifying agent, preservative, antifreezing agent.
Preferably, the procymidone and guaiacol mixture are processed into one kind in suspending agent, aqua, soluble liquid.
Preferably, the suspending agent includes sodium alginate 0.1%-25%, anion surfactant;The anion table Face activating agent includes lignosulfonates 0.1%-25%.
Preferably, treating the application process of the composition of purple spot of soybean based on guaiacol;Comprise the following steps:
S1., the procymidone and guaiacol mixture are processed into one kind in suspending agent, aqua, soluble liquid;
S2. dispenser, takes the guaiacol decoction that step S1 is configured to carry out spray pesticide or pouring to soybean.
Preferably, spray value is 500~800L/ hm in the step S22, atomisation pressure is 0.3~0.8kPa, dispenser Number of times is 2~3 times.
The guaiacol decoction mechanism of action:
(1)Suppress RNA reverse transcriptase RTASE activity, prevent virion from synthesizing;
(2)Absorption of the virion on cell is prevented, virus is reduced and contaminates probability;
(3) oxidation resistance in enhancing plant, reduces injury of the virus dip-dye to plant;
(4) resistance against diseases of plant is improved.
The present invention develops guaiacol in preventive and therapeutic effect of the agriculture field particularly with purple spot of soybean, can be made into conventional The formulations of pesticide, it is mashed up in proportion with procymidone, prevention effect more more preferable than single dose is reached, while adding chitosan and other auxiliary agents Make the increase of guaiacol decoction viscosity, can preferably be attached to crop surface, beneficial to drug absorption, meanwhile, chitosan also has one Fixed auxiliary is antibacterial, the effect of desinsection, and moderate cost, is worthy to be popularized.
Embodiment
Embodiment one
Guaiacol and procymidone are made to the composition for the treatment of purple spot of soybean, its composition includes guaiacol and procymidone, The mass ratio of the guaiacol and procymidone is 1/10-10.
More specifically, the guaiacol and procymidone mass ratio are 1-5.
More specifically, wherein Determination of Guaiacol is 10%, and procymidone content is 10%.
More specifically, in addition to one kind in dispersant, sticker, bleeding agent, emulsifying agent, preservative, antifreezing agent or It is a variety of.
More specifically, procymidone and the guaiacol mixture is processed into one in suspending agent, aqua, soluble liquid Kind.
More specifically, the suspending agent includes sodium alginate 0.1%-25%, anion surfactant;It is described it is cloudy from Sub- surfactant includes lignosulfonates 0.1%-25%.
More specifically, the application process of the composition of purple spot of soybean is treated based on guaiacol;Comprise the following steps:
S1., the procymidone and guaiacol mixture are processed into one kind in suspending agent, aqua, soluble liquid;
S2. dispenser, takes the guaiacol decoction that step S1 is configured to carry out spray pesticide or pouring to soybean.
More specifically, spray value is 300~400L/ hm in the step S22, atomisation pressure is 0.3~0.8kPa, Spraying times are 2~3 times.
Embodiment two
Guaiacol, procymidone single dose are determined using Plating, and two kinds of single doses press 1: 10,1: 5,1:3、1:2、1∶1、2∶1、 9 kinds of mixture samples of 3: 1,5: 1,10: 1 ratio composition are to the Antibacterial Activity of purple spot of soybean pathogenic bacteria mycelial growth, record And relatively more each drug concentration suppresses the bacteriostasis rate of purple spot of soybean pathogenic bacteria mycelial growth.
Result of the test shows that procymidone has preferable bacteriostatic activity to the mycelial growth of purple spot of soybean pathogenic bacteria, and Guaiacol is relatively low to the bacteriostatic activity of purple spot of soybean pathogenic bacteria.Procymidone shows to the bacteriostatic activity of purple spot of soybean pathogenic bacteria Write the bacteriostatic activity higher than guaiacol.
With probit analysis, calculate procymidone, guaiacol and its mixture and suppress the life of purple spot of soybean pathogenic bacteria mycelia Long toxicity regression formula.Result of calculation shows that procymidone has to the mycelial growth of purple spot of soybean pathogenic bacteria preferably to be suppressed to live Property, guaiacol is substantially less than procymidone to the inhibitory activity of purple spot of soybean pathogenic bacteria mycelial growth.
With the EC of each mixture50Value is calculated the co-toxicity coefficient of mixture by the abundant methods of Sun Yun, is as a result shown, when procymidone and guaiaci lignum When phenol is with 1: 10 mixture, the CTC values of its mixture are less than 80, illustrate its mixture procymidone and guaiacol by 1: 10 mixture to soybean The bacteriostatic activity of purple spot pathogenic bacteria shows as antagonism;When procymidone and guaiacol are with 1: 5,1:3、1:2nd, 1: 1 mixture When, the CTC values of its mixture are all higher than 120, and with 1:1 is highest, illustrates procymidone and guaiacol in these ratio mixtures pair The bacteriostatic activity of purple spot of soybean pathogenic bacteria shows as synergistic effect;When procymidone and guaiacol are with 10: 1 mixture, it is mixed The CTC values of agent are more than 80 and less than 120, illustrate procymidone with guaiacol by 10: 1,2: 1,3:1、5:1 ratio mixture is to soybean The bacteriostatic activity of purple spot pathogenic bacteria shows as summation action, therefore, configuration guaiacol procymidone treatment purple spot of soybean Composition procymidone and both guaiacol ratio 1: 5,1:3、1:2nd, choose among 1: 1, bactericidal activity is higher, wherein with 1:1 is optimum proportioning.
Preferred embodiments of the present invention are these are only, therefore the scope that the present invention is implemented can not be limited according to this, i.e., according to the present invention Equivalence changes and decoration that description is made, should all belong in the range of present invention covering.

Claims (9)

1. a kind of composition that purple spot of soybean is treated based on guaiacol, it is characterised in that:Including guaiacol and procymidone, The mass ratio of the guaiacol and procymidone is 1/10-10.
2. the composition as claimed in claim 1 that purple spot of soybean is treated based on guaiacol, it is characterised in that:It is described more to create Wooden phenol and procymidone ratio is 1-5.
3. the composition as claimed in claim 2 that purple spot of soybean is treated based on guaiacol, it is characterised in that:Wherein more create Wooden phenol content is 10%, and procymidone content is 10%.
4. the composition as claimed in claim 3 that purple spot of soybean is treated based on guaiacol, it is characterised in that:Also include dividing One or more in powder, sticker, bleeding agent, emulsifying agent, preservative, antifreezing agent.
5. the composition as claimed in claim 4 that purple spot of soybean is treated based on guaiacol, it is characterised in that:The corruption is mould Profit and guaiacol mixture are processed into one kind in suspending agent, aqua or soluble liquid.
6. the composition as claimed in claim 5 that purple spot of soybean is treated based on guaiacol, it is characterised in that:It is described to suspend Agent includes anion surfactant, sodium alginate 0.1%-25%.
7. the composition as claimed in claim 6 that purple spot of soybean is treated based on guaiacol, it is characterised in that:It is described it is cloudy from Sub- surfactant includes lignosulfonates 0.1%-25%.
8. a kind of application process of the composition as claimed in claim 7 that purple spot of soybean is treated based on guaiacol;Including Following steps:
S1., the procymidone and guaiacol mixture are processed into one kind in suspending agent, aqua or soluble liquid;
S2. dispenser, the guaiacol decoction for taking step S1 to be configured carries out spray pesticide or pouring after diluting to soybean.
9. a kind of application process of the composition as claimed in claim 8 that purple spot of soybean is treated based on guaiacol;It is described Atomisation pressure is 0.3~0.8kPa in step S2, and spraying times are 2~3 times.
CN201710235431.XA 2017-04-12 2017-04-12 A kind of composition and application process that purple spot of soybean is treated based on guaiacol Withdrawn CN106982831A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0748217A (en) * 1993-08-04 1995-02-21 Matsukaade:Kk Antibacterial agent
CN103918653A (en) * 2014-03-31 2014-07-16 海利尔药业集团股份有限公司 Bactericidal composition containing picoxystrobin and procymidone
CN104521957A (en) * 2014-12-09 2015-04-22 安徽扬子化工有限公司 Applications of guaiacol in rice stripe disease

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0748217A (en) * 1993-08-04 1995-02-21 Matsukaade:Kk Antibacterial agent
CN103918653A (en) * 2014-03-31 2014-07-16 海利尔药业集团股份有限公司 Bactericidal composition containing picoxystrobin and procymidone
CN104521957A (en) * 2014-12-09 2015-04-22 安徽扬子化工有限公司 Applications of guaiacol in rice stripe disease

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Application publication date: 20170728