CN106962920A - A kind of fermented type pomegranate dark plum medicinal extract and preparation method thereof - Google Patents

A kind of fermented type pomegranate dark plum medicinal extract and preparation method thereof Download PDF

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Publication number
CN106962920A
CN106962920A CN201710124841.7A CN201710124841A CN106962920A CN 106962920 A CN106962920 A CN 106962920A CN 201710124841 A CN201710124841 A CN 201710124841A CN 106962920 A CN106962920 A CN 106962920A
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parts
pomegranate
dark plum
medicinal extract
fermented type
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CN106962920B (en
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马嫄
罗鸣
古小露
焦文成
王晓敏
耿福能
徐娟
史敏娟
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SICHUAN FNY BIOTECHNOLOGY Co Ltd
Xihua University
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SICHUAN FNY BIOTECHNOLOGY Co Ltd
Xihua University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2400/00Lactic or propionic acid bacteria
    • A23V2400/11Lactobacillus
    • A23V2400/113Acidophilus

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  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The present invention relates to food and its manufacture field, specifically related to a kind of fermented type pomegranate dark plum medicinal extract and preparation method thereof, is prepared from by 30 60 parts of pomegranate, 10 30 parts of dark plum, 2 10 parts of passionflower, water-soluble 2 20 parts of sugar-type compound, 15 parts of rose, 15 parts of Roselle, 15 parts of sweet osmanthus, 15 parts of lotus leaf.Fermented type pomegranate dark plum medicinal extract of the present invention, by the way that the flowers and fruits such as pomegranate, dark plum, passionflower, sweet osmanthus are scientifically merged, mouthfeel more horn of plenty is with rich flavor;Several flowers and fruits it is compound, can supplement the nutriment of needed by human body comprehensively, strengthen body immunity, with tonifying middle-Jiao and Qi, astringe the lung promote the production of body fluid, the health-care efficacy such as poison expelling and beautifying, anti-aging, hypotensive, its preparation method is scientific and reasonable simultaneously, is with a wide range of applications and edibility.

Description

A kind of fermented type pomegranate dark plum medicinal extract and preparation method thereof
Technical field
The present invention relates to food and its manufacture field, and in particular to a kind of fermented type pomegranate dark plum medicinal extract and its preparation side Method.
Background technology
Pomegranate is with a long history in China's culture, at present a kind about more than 70, and nutrition is especially enriched.Contain in pomegranate fruit There are the mineral matters such as abundant vitamin, organic acid, carbohydrate, protein, fat, and calcium, phosphorus, potassium.In its pericarp containing tannin, The compositions such as flavonoids, alkaloid, with obvious relieving diarrhea with astringents and bacteriostasis.In addition, containing several amino acids in juice of my pomegranate And trace element, there are aid digestion, anti-gastric-ulcer, softening blood vessel, reducing blood lipid and blood glucose, reduce a variety of functions such as cholesterol.It can prevent Only coronary heart disease, hypertension, can reach the effect that stomach invigorating is refreshed oneself, whetted the appetite.
Dark plum is also known as plum fruit, smoked plum, is rose family Prunus green plum tree fruit.Contain abundant Chinese holly edge in dark plum pulp The compositions such as acid, malic acid, butanedioic acid, carbohydrate, sitosterol, vitamin C, there is strengthening the spleen and stomach, the effect of mending nourishing liver and kidney.
Passionflower also known as passion fruit or passion fruit, its fruit juice contain more than 60 kinds of volatile compound, amino acid content also phase When abundant, also containing multivitamin and mineral matter element, its natural Normal juice is unique strong with its own bright-coloured color and luster Fragrant local flavor, abundant nutrition and the health-care effect to human body, are referred to as natural nutrition concentrate.
The now utilization of current dark plum and passionflower is limited only to beverage, preserved fruit and dried fruit class, and we commercially see Pomegranate product have beverage, fruit wine, jam, dried fruit, fruit tea etc., as be developed into extract product utilization only document and specially See on industry books, in the market, which has no, sells.And pomegranate of the nutritional ingredient equivalent to 2-5g contained by pomegranate medicinal extract 1g, eat Mode has the advantage for exempting to decoct, while being conducive to playing the pleiotropism of some compositions, can make the nutritional ingredient contained by pomegranate Farthest utilized.
The content of the invention
In order to solve the above problems, it is an object of the invention to provide a kind of fermented type pomegranate dark plum medicinal extract, to fill up city The blank of pomegranate medicinal extract on field.
To achieve the above object, the technical solution adopted by the present invention is:A kind of fermented type pomegranate dark plum medicinal extract, by weighing as follows Measure the raw material composition of number:30-60 parts of pomegranate, 10-30 parts of dark plum, 2-10 parts of passionflower, water-soluble 2-20 parts of sugar-type compound, 1-5 parts of rose, 1-5 parts of Roselle, 1-5 parts of sweet osmanthus, 1-5 parts of lotus leaf.
Further, it is made up of the raw material of following parts by weight:42 parts of pomegranate, 23 parts of dark plum, 8 parts of passionflower, water solubility 10 parts of sugar-type compound, 4 parts of rose, 4 parts of Roselle, 4 parts of sweet osmanthus, 3 parts of lotus leaf.
Further, the sugar in the water-soluble sugar-type compound is one kind or several in monosaccharide and disaccharide, sugar alcohol or oligosaccharides Plant mixture.
The present invention also provides a kind of preparation method of fermented type pomegranate dark plum medicinal extract, and step includes:
(1) pomegranate and passionflower of maturation are selected, demucilage and pericarp is cleaned, fruit is made in pulp mashing, clarification, filtering Slurry, peel crushing slagging;
(2) dark plum pulp is peeled, the water with adding 10 times of quality after rose, Roselle, lotus leaf difference ultramicro grinding, in 50 DEG C infusion 1h, filtering removes filter residue;
(3) it is respectively 1 by solid-liquid ratio by the pulp obtained by step (1), (2):10 add 80% absolute ethyl alcohol, at 50 DEG C Extract and compound flower fruit juice is obtained after clarified solution is mixed after 4h, suction filtration;
(4) 1.0-3.0% lactobacillus acidophilus is added in broken pomegranate peel residue and passionflower skin slag, in 37 DEG C of fermentations 2-3 days, fermentation Miao's liquid is made;
(5) fermentation Miao's liquid is mixed with compound flower fruit juice, concentrated with Rotary Evaporators;
(6) water-soluble sugar-type compound is added, low temperature infusion adds sweet osmanthus, stir to obtain medicinal extract liquid to thick;
(7) medicinal extract liquid, the rear demoulding to be formed, cooling are poured into a mould by moulding machine at 80-120 DEG C;
(8) packed after medicinal extract solid being dried in vacuo into 30min, 135 DEG C of sterilization 3-5s at 45 DEG C.
In the present invention, supercritical carbon dioxide extracting can be used after compound flower fruit juice and fermentation Miao liquid mixing, leaching is made Cream liquid, supercritical carbon dioxide extracting condition is:Temperature 45 C, pressure 14MPa, CO2Flow be 37L/h, time be 3.5h.
Further, in step (7), cast medicinal extract shape according to mold shape be tablet form, piece caryogram or Grain type.
The method have the benefit that:Fermented type pomegranate dark plum medicinal extract of the present invention, by by pomegranate, dark plum, west kind The flowers and fruits such as lotus, sweet osmanthus are scientifically merged, mouthfeel more horn of plenty, with rich flavor;Being combined for several flowers and fruits, can be supplemented comprehensively The nutriment of needed by human body, strengthen body immunity, with tonifying middle-Jiao and Qi, astringe the lung promote the production of body fluid, poison expelling and beautifying, anti-aging, drop blood The health-care efficacies such as pressure, while its preparation method is scientific and reasonable, are with a wide range of applications and edibility.
The present invention is handled by lactic fermentation, makes product while having pomegranate, dark plum, passionflower and ferment local-flavor, sour-sweet Tasty, fragrance enriches;And rich in full pomegranate, full passionflower, the nutritional ingredient of dark plum, the nutritional ingredient human body of its product is easy to Absorb, with healthcare function, biological transformation ratio is high the features such as.Granatum and passion flower-fruit peel are maximally utilized simultaneously, make money Source makes full use of, and realizes the theory of green production.
Fermented type pomegranate dark plum medicinal extract of the present invention, because melting mixing and forming process are in the hard of routine in preparation process Easily it is continuously finished in the way of hard candy is processed on sugared casting machine, has the advantages that speed of production is fast, produces batch flexibly.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment 1
A kind of fermented type pomegranate dark plum medicinal extract, is made up of the raw material of following weight:Pomegranate 4kg, dark plum 2.5kg, passionflower 0.8kg, water-soluble sugar-type compound 1.0kg, rose 0.4kg, Roselle 0.4kg, sweet osmanthus 0.4kg, lotus leaf 0.3kg.
Wherein, water miscible sugar-type compound is one or more of mixtures in monosaccharide and disaccharide, sugar alcohol or oligosaccharides etc..
A kind of preparation method of fermented type pomegranate dark plum medicinal extract is carried out by following steps:
(1) pretreatment of raw material:The pomegranate and passionflower of maturation are selected, cleans, digs out pulp, pericarp is cleaned.Select organic The abundant dark plum of acid content, cleans, peels pulp;
(2) zymotic fluid processed:Granatum, passion flower-fruit peel are crushed, 1.0-3.0% lactobacillus acidophilus leavening is added (viable count is 3.0 × 1015Individual/mL), fermented 2-3 days at 37 DEG C, filtering obtains fermentation Miao's liquid;
(3) juice is taken:Pomegranate and passionflower pulp are beaten with beater, pulp is made in clarification, filtering;By dark plum pulp, Rose, Roselle, lotus leaf are carried out after ultramicro grinding respectively, plus 10 times of quality water, in 50 DEG C of infusion 1h, filtering removes filter Slag;
(4) extract:It is stripped with 80% ethanol, solid-liquid ratio is 1:10,4h is extracted at 50 DEG C, suction filtration must be combined flowers and fruits Juice;
(5) concentrate:Fermentation Miao's liquid and compound flower fruit juice are well mixed, concentrated in Rotary Evaporators, side concentration Side stir, until concentrate to it is thick when stop;
(6) injection or extrusion moulding:In the way of hard candy processing sizing, company is poured into by moulding head in 80-120 DEG C In the model disk of reforwarding row, room temperature sizing is then rapidly cooled to, then is deviate from out of mould, the leaching of fermented type pomegranate dark plum is produced Cream;
(7) sterilization pack:Medicinal extract solid is dried in vacuo 30min at 45 DEG C, then in 135 DEG C of ultra high temperature sterilization 3-5s, it is cold But pack, preserve at room temperature afterwards.
A kind of fermented type pomegranate dark plum medicinal extract experiment:
The pomegranate dark plum medicinal extract for taking 6g specifications to pack, soaks 10min with 100 DEG C of drinking water of 100mL, is gently agitated for, to soup Color uniformly no longer changes colour, and experiment is repeated 6 times altogether.Its organoleptic indicator and physical and chemical index are determined respectively.
(1) subjective appreciation
Sensory evaluation is carried out with commenting to the smell of fermented type pomegranate dark plum medicinal extract of the present invention, three aspects of mouthfeel and color and luster Point, full marks are 100 points, and subjective appreciation group is made up of laboratory academics and students, totally 8 people.Subjective appreciation personnel are by passing through one The laboratory member composition of fixed ex-period training.
(2) physical and chemical index is analyzed
Project
Moisture/% 5.3
Tannin/mg/g 85.8
Organic acid/% 10.7
Flavonoid substances/mg/kg 73.2
Soluble solid/% 17.5
pH 3.75
Embodiment 2
The present embodiment and the difference of embodiment 1 are:Extraction conditions are:Solid-liquid ratio is 1:15, extract 3h at 40 DEG C.
Embodiment 3
A kind of fermented type pomegranate dark plum medicinal extract, is made up of the raw material of following weight:Pomegranate 4kg, dark plum 2.5kg, passionflower 0.8kg, water-soluble sugar-type compound 1.0kg, rose 0.4kg, Roselle 0.4kg, sweet osmanthus 0.4kg, lotus leaf 0.3kg.
Wherein, water miscible sugar-type compound is one or more of mixtures in monosaccharide and disaccharide, sugar alcohol or oligosaccharides etc.;
A kind of preparation method of fermented type pomegranate dark plum medicinal extract is carried out by following steps:
(1) pretreatment of raw material:The pomegranate and passionflower of maturation are selected, cleans, digs out pulp, clean pericarp selects organic acid The dark plum of rich content, cleans, peels pulp;
(2) zymotic fluid processed:Granatum, passion flower-fruit peel are crushed, 1.0-3.0% lactobacillus acidophilus leavening is added (viable count is 3.0 × 1015Individual/mL), fermented 2-3 days at 37 DEG C, filtering obtains fermentation Miao's liquid;
(3) juice is taken:Pomegranate and passionflower pulp are beaten with beater, pulp is made in clarification, filtering;By dark plum pulp, Rose, Roselle, lotus leaf are carried out after ultramicro grinding respectively, plus 10 times of quality water, in 50 DEG C of infusion 1h, filtering removes filter residue And mix to obtain compound flower fruit juice with pulp;
(4) fermentation Miao's liquid and compound flower fruit juice are well mixed, are placed in extractor, sealed.Separator I and separation are set The temperature of device II is 55 DEG C and 50 DEG C;Pressure is set to be 7MPa and 5MPa respectively, temperature to be extracted is proceeded by when reaching 45 DEG C Extraction.It is 14MPa, CO to set extracting pressure2Flow is 37L/h, and extraction time is 3.5h;
(5) extract and water-soluble sugar-type compound are well mixed, add sweet osmanthus;
(6) injection or extrusion moulding:In the way of hard candy processing sizing, company is poured into by moulding head at 80-120 DEG C In the model disk of reforwarding row, room temperature sizing is then rapidly cooled to, then is deviate from out of mould, the leaching of fermented type pomegranate dark plum is produced Cream;
(7) sterilization pack:Medicinal extract solid is dried in vacuo 30min at 45 DEG C, then in 135 DEG C of ultra high temperature sterilization 3-5s, it is cold But pack, preserve at room temperature afterwards.
Embodiment 4
The present embodiment and the difference of embodiment 3 are:Granatum passes through ferment treatment with passion flower-fruit peel, goes astringent taste, specifically Operation is as follows:
A kind of fermented type pomegranate dark plum medicinal extract, is made up of the raw material of following weight:Pomegranate 4kg, dark plum 2.5kg, passionflower 0.8kg, water-soluble sugar-type compound 1.0kg, rose 0.4kg, Roselle 0.4kg, sweet osmanthus 0.4kg, lotus leaf 0.3kg.
Wherein, water miscible sugar-type compound is one or more of mixtures in monosaccharide and disaccharide, sugar alcohol or oligosaccharides etc.;
A kind of preparation method of fermented type pomegranate dark plum medicinal extract is carried out by following steps:
(1) pretreatment of raw material:The pomegranate and passionflower of maturation are selected, cleans, digs out pulp, clean pericarp selects organic acid The dark plum of rich content, cleans, peels pulp;
(2) zymotic fluid processed:Granatum and passion flower-fruit peel are cleaned, crushed, then acquisition decomposed solution is decomposed with cellulase; Decomposed solution is freezed successively, melts processing 2-4 time, (viable count is addition 1.0-3.0% lactobacillus acidophilus leavening 3.0×1015Individual/mL), fermented 2-3 days at 37 DEG C, filtering obtains fermentation Miao's liquid;
(3) juice is taken:Pomegranate and passionflower pulp are beaten with beater, pulp is made in clarification, filtering;By dark plum pulp, Rose, Roselle, lotus leaf are carried out after ultramicro grinding respectively, plus 10 times of quality water, in 50 DEG C of infusion 1h, filtering removes filter residue And mix to obtain compound flower fruit juice with pulp;
(4) fermentation Miao's liquid and compound flower fruit juice are well mixed, are placed in extractor, sealed.Separator I and separation are set The temperature of device II is 55 DEG C and 50 DEG C;Pressure is set to be 7MPa and 5MPa respectively, temperature to be extracted is proceeded by when reaching 45 DEG C Extraction.It is 14MPa, CO to set extracting pressure2Flow is 37L h, and extraction time is 3.5h;
(5) extract and water-soluble sugar-type compound are well mixed, add sweet osmanthus;
(6) injection or extrusion moulding:In the way of hard candy processing sizing, company is poured into by moulding head at 80-120 DEG C In the model disk of reforwarding row, room temperature sizing is then rapidly cooled to, then is deviate from out of mould, the leaching of fermented type pomegranate dark plum is produced Cream;
(7) sterilization pack:Medicinal extract solid is dried in vacuo 30min at 45 DEG C, then in 135 DEG C of ultra high temperature sterilization 3-5s, it is cold But pack, preserve at room temperature afterwards.
Those skilled in the art of the present technique are appreciated that unless otherwise defined, all terms used herein (including technology art Language and scientific terminology) with the general understanding identical meaning with the those of ordinary skill in art of the present invention.Should also Understand, those terms defined in such as general dictionary, which should be understood that, to be had and the meaning in the context of prior art The consistent meaning of justice, and unless defined as here, will not be explained with idealization or excessively formal implication.
It should be noted last that:Above example is only used to illustrative and not limiting technical scheme, although ginseng The present invention is described in detail according to above-described embodiment, it will be apparent to an ordinarily skilled person in the art that:Still can be to this Invention is modified or equivalent substitution, any modification or partial replacement without departing from the spirit and scope of the present invention, and its is equal It should cover among scope of the presently claimed invention.

Claims (7)

1. a kind of fermented type pomegranate dark plum medicinal extract, it is characterised in that be made up of the raw material of following parts by weight:30-60 parts of pomegranate, 10-30 parts of dark plum, 2-10 parts of passionflower, water-soluble 2-20 parts of sugar-type compound, 1-5 parts of rose, 1-5 parts of Roselle, sweet osmanthus 1-5 parts, 1-5 parts of lotus leaf.
2. fermented type pomegranate dark plum medicinal extract according to claim 1, it is characterised in that by the raw material group of following parts by weight Into:42 parts of pomegranate, 23 parts of dark plum, 8 parts of passionflower, water-soluble 10 parts of sugar-type compound, 4 parts of rose, 4 parts of Roselle, sweet osmanthus 4 Part, 3 parts of lotus leaf.
3. fermented type pomegranate dark plum medicinal extract according to claim 1 or claim 2, it is characterised in that the water-soluble sugar-type compound In sugar be monosaccharide and disaccharide, sugar alcohol or oligosaccharides in one or more of mixtures.
4. a kind of preparation method of fermented type pomegranate dark plum medicinal extract, it is characterised in that step includes:
(1) pomegranate and passionflower of maturation are selected, demucilage and pericarp is cleaned, pulp is made in pulp mashing, clarification, filtering, Peel crushing slagging;
(2) dark plum pulp is peeled, the water with adding 10 times of quality after rose, Roselle, lotus leaf difference ultramicro grinding is endured in 50 DEG C 1h is boiled, filtering removes filter residue;
(3) it is respectively 1 by solid-liquid ratio by the pulp obtained by step (1), (2):10 add 80% absolute ethyl alcohol, in 50 DEG C of extractings Compound flower fruit juice is obtained after clarified solution is mixed after 4h, suction filtration;
(4) 1.0-3.0% lactobacillus acidophilus is added in broken pomegranate peel residue and passionflower skin slag, ferment 2-3 in 37 DEG C My god, fermentation Miao's liquid is made;
(5) fermentation Miao's liquid is mixed with compound flower fruit juice, concentrated with Rotary Evaporators;
(6) water-soluble sugar-type compound is added, low temperature infusion adds sweet osmanthus, stir to obtain medicinal extract liquid to thick;
(7) medicinal extract liquid, the rear demoulding to be formed, cooling are poured into a mould by moulding machine at 80-120 DEG C;
(8) packed after medicinal extract solid being dried in vacuo into 30min, 135 DEG C of sterilization 3-5s at 45 DEG C.
5. fermented type pomegranate dark plum medicinal extract preparation method according to claim 4, it is characterised in that:In step (5), compound flower Fruit juice and fermentation Miao liquid carry out supercritical carbon dioxide extracting after mixing, and medicinal extract liquid is made.
6. the preparation method of fermented type pomegranate dark plum medicinal extract according to claim 5, it is characterised in that the overcritical dioxy Changing carbon extraction conditions is:Temperature 45 C, pressure 14MPa, CO2Flow be 37L/h, time be 3.5h.
7. according to the preparation method of any one of the claim 4-6 fermented type pomegranate dark plum medicinal extract, it is characterised in that step (7) in, the medicinal extract shape poured into a mould is tablet form, piece caryogram or granular pattern according to mold shape.
CN201710124841.7A 2017-03-03 2017-03-03 Fermented pomegranate dark plum extract and preparation method thereof Active CN106962920B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104194934A (en) * 2014-08-29 2014-12-10 杨祝华 Preparation method of lotus extractum
CN104232313A (en) * 2014-09-25 2014-12-24 秦富英 Flowery extract
CN105559003A (en) * 2015-12-30 2016-05-11 重庆市日用化学工业研究所 Preparation method of sweet-scented osmanthus medicinal extract
CN106071021A (en) * 2016-07-19 2016-11-09 西华大学 A kind of compound fruitcake of Fructus Mume Herba Passiflorae Caeruleae and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104194934A (en) * 2014-08-29 2014-12-10 杨祝华 Preparation method of lotus extractum
CN104232313A (en) * 2014-09-25 2014-12-24 秦富英 Flowery extract
CN105559003A (en) * 2015-12-30 2016-05-11 重庆市日用化学工业研究所 Preparation method of sweet-scented osmanthus medicinal extract
CN106071021A (en) * 2016-07-19 2016-11-09 西华大学 A kind of compound fruitcake of Fructus Mume Herba Passiflorae Caeruleae and preparation method thereof

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* Cited by examiner, † Cited by third party
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