CN106957734B - Environment-protection detergent powder - Google Patents
Environment-protection detergent powder Download PDFInfo
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- CN106957734B CN106957734B CN201710147176.3A CN201710147176A CN106957734B CN 106957734 B CN106957734 B CN 106957734B CN 201710147176 A CN201710147176 A CN 201710147176A CN 106957734 B CN106957734 B CN 106957734B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2089—Ether acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3945—Organic per-compounds
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of environment-protection detergent powder, the preparation method of the environment-protection detergent powder includes including following raw materials: plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, sodium carboxymethylcellulose, bentonite, water.Environment-protection detergent powder of the present invention, it can quickly and thoroughly remove the greasy dirt being attached on clothing, sweat stain and other pollutants, antibiotic property is good, to improve the detersive efficiency of clothing, preparation process is using natural plant extracts and green surfactant, it is highly-safe, the waste water no pollution to the environment of washing non-stimulated to human skin.
Description
Technical field
The present invention relates to detergent technical fields, and in particular to a kind of environment-protection detergent powder.
Background technique
Washing powder is one of essential cleaning supplies of people's daily life already.With people consumption concept at
Ripe, the requirement of national low-carbon economy, energy-saving, water-saving and emission-reducing trend of the times, traditional washing powder is mostly synthetic detergent powder, with
Its highly energy-consuming, storage and transportation packing cost are high, all rich in the unfavorable environmental protection of phosphorus aluminium, the higher damaging laundry of alkalinity and filler inefficient cycle etc.
More disadvantages are increasingly not suitable with the requirement of era development.
Synthesis chemical washing powder is cheap with its, cleaning effect is good all the time in occupation of the city of household cleaning product
?.Synthetic detergent powder usually contain surfactant, alkaline agent, complexing agent, protease, fluorescent whitening agent, filler etc. mainly at
Part, whitening type washing powder can also add the bleaching agents such as peroxide.Institute in waste water after cleaning clothes with synthesis chemical washing powder
The chemical substance contained be easy to cause environmental pollution, all has large effect to water original, fish, soil, crops etc..Washing
Afterwards on clothes synthetic detergent powder residual can all have an impact to human skin and nervous system, especially to child and bear a pretty, delicate skin easily
Allergy personage influences bigger.For example sodium alkyl benzene sulfonate is the principal surfactant for synthesizing chemical washing powder, has collaboration
Carcinogenic effect.Benzene is a kind of liposoluble substance, and remaining benzene on the clothing of non-rinsed clean can not only stimulate skin to cause scabies
Itch, and can be penetrated into human body by skin, accumulates over a long period, may induce disease.The common fluorescent whitening agent of washing powder is to cause
Cancer substance can be such that human body cell is distorted, also can trigger dermatitis and pruitus.Modern medicine proves, LAS (alkylbenzene
Sodium sulfonate), AES (sodium sulfate of polyethenoxy ether of fatty alcohol), the raw materials such as AS (sodium alkyl sulfate) can also cause under fecundity
Drop, injury liver kidney, contaminated blood, damage lymphatic system reduce the toxic side effects such as immunity.In order to solve the residual of synthetic detergent powder
The problems such as staying and polluting is badly in need of developing a kind of environmentally friendly skin-care washing powder.
Summary of the invention
To achieve the above object, the present invention adopts the following technical scheme:
A kind of environment-protection detergent powder, including following raw materials: percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl are fine
Tie up plain sodium, bentonite, water.
A kind of environment-protection detergent powder, including following raw materials: plant extracts, percarbamide, cocoyl glucoside, antiscaling dispersion
Agent, sodium carboxymethylcellulose, bentonite, water.
Preferably, a kind of environment-protection detergent powder, the raw material including following weight parts: 30-40 parts of plant extracts, percarbamide
10-20 parts, 10-20 parts of cocoyl glucoside, 1-5 parts of dirt dispersion agent, 0.1-1 parts of sodium carboxymethylcellulose, bentonite 8-15
Part, 10-30 parts of water.
Preferably, the plant extracts preparation method the following steps are included:
(1) gleditsia sinensis, Saponaria officinalis, Radix Polygalae, campanulaceae, Salvia japonica crush as 60-100 mesh, obtain plant mixture；
(2) plant mixture is impregnated 10-20 minutes in organic solvent, obtains mixed solution；
(3) mixed solution is handled into 5-10min in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, is filtered after extraction, obtains filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
Preferably, the plant extracts preparation method the following steps are included:
(1) 40-50 parts of gleditsia sinensis, 20-30 parts of Saponaria officinalis, 10-20 parts of Radix Polygalae, 10-20 parts of campanulaceae, rat-tail are weighed by weight
It is 5-10 parts careless, it crushes as 60-100 mesh, obtains plant mixture；
(2) plant mixture impregnated to 10-20 minutes in organic solvent, wherein the matter of plant mixture and organic solvent
Amount is than being 1:(8-12), obtain mixed solution；
(3) mixed solution is handled into 5-10min, magnetic field strength 2200GS-2400GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, first in 40-50 DEG C of microwave abstracting
1-3 minutes, then 20-30 DEG C microwave abstracting 5-10 minutes, filtering, obtain filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
Preferably, the organic solvent is the ethanol water that volume fraction is 30-40%.
Preferably, the power 400-600W of the microwave abstracting.
Preferably, the dirt dispersion agent is sodium citrate and/or sodium humate.It is highly preferred that the dirt dispersion agent
For sodium citrate and sodium humate (1-3) in mass ratio: 1 mixes.
Environment-protection detergent powder of the present invention can quickly and thoroughly remove the greasy dirt being attached on clothing, sweat stain and other dirts
Object is contaminated, antibiotic property is good, to improve the detersive efficiency of clothing, preparation process is living using the surface of natural plant extracts and green
Property agent, highly-safe, the waste water no pollution to the environment of washing non-stimulated to human skin.
Specific embodiment
Detergency ability test: referring to GB/T13174-2008 " dress material detergent detergency and the survey for recycling scourability
Method tests the washing effect of the environment-protection detergent powder of each embodiment preparation calmly ".
Test method: using B value (whiteness holding ratio) as the evaluation index of washing effect, as B >=1.0, detergent
Detergency is qualified；When B < 1.0, detergent detergency is unqualified.
Test sample includes JB-01 (carbon black greasy dirt cloth), JB-02 (albumen soiled cotton), JB-03 (sebum soiled cotton).
Wash conditions: washing powder concentration 0.2% in cleaning solution, 30 DEG C of wash temperature, wash time 20min, the water hardness
250mg/kg。
Anti-microbial property test: using QB/T2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect " to each reality
The anti-microbial property for applying the environment-protection detergent powder of example preparation is tested.The microorganism tested: Escherichia coli (ATCC 25922)；It is withered
Straw bacterium (ATCC 9372)；Staphylococcus aureus (ATCC 6538).
Ethyl alcohol, No. CAS: 64-17-5.
Percarbamide, No. CAS: 124-43-6.Carbamide percarbonate appearance is white crystalline powder, and nontoxic odorlessness is readily soluble
Yu Shui, aqueous solution have the property of urea and hydrogen peroxide concurrently.It is decomposed into urea, H in water2O2And elemental oxygen, and slowly release oxygen
Gas.Its active o content is high, and solubility in water is big, and pH value of water solution weakly acidic pH, stability is good, and the effectiveness time is long, no pair
Effect, Nonpoisonous, non-environmental-pollution.
Cocoyl glucoside, No. CAS: 141464-42-8, it is a kind of surfactant of green, sends out change triumphant using Shanghai
The APG0814 of work Co., Ltd production.
Sodium humate, No. CAS: 68131-04-4.
Sodium citrate, No. CAS: 6132-04-3.
Sodium carboxymethylcellulose, No. CAS: 9004-32-4, the carboxylic first provided using Shandong Xi Tang Biotechnology Co., Ltd
Base sodium cellulosate.
Bentonite, No. CAS: 1302-78-9, the bentonite provided using Luoshan County green hill town Li Hui bentonite factory, partial size
325-800 mesh.
Gleditsia sinensis, the i.e. fruit of honey locust Gleditsia sinensis Lam., be medicine food, health care product, cosmetics and
The natural material of articles for washing；Gleditsia sinensis Seeds can promoting digestion appetizing, and contain a kind of natural plant gum, Fructus Gleditsia acupuncture (soap needle) includes Huang
Ketone glucoside, phenols, amino acid have very high economic value.Gleditsia sinensis has antibacterial action, and gleditsia sinensis has naturally many bacteriums, fungi
Inhibition and sterilization effect.
Saponaria officinalis, Classification system: Saponaria officinalis, the present invention in use Saponaria officinalis dried leaf.
Radix Polygalae is milk wort Radix Polygalae Polyyala tenuifolia Willd. or ovum leaf Radix Polygalae Polygala
The dry root of sibirica L..
Campanulaceae, the dry root of Campanulaceae campanulaceae Platycodon grandiflorum (Jacq.) A DC..
Salvia japonica, Classification system: Salvia japonica Thunb., the present invention in use Salvia japonica dried leaf.Rat-tail
Grass is a kind of perennial fragrant plant, and Salvia japonica essential oil has the function of antibacterial anti-inflammatory.It can promote cytothesis, maintenance skin is thin
Born of the same parents' tissue, purifies greasy scalp, adjusts skin oil and fat secretion, mitigates the skin problem of inflammation and swelling.Help improve oiliness
The skin problem such as skin, acne, acne.Salvia japonica essential oil has the effect of beautifying face and moistering lotion, additionally it is possible to antibacterial anti-inflammatory.
Microwave abstracting equipment, the model KL-2D- provided using the industrial microwave equipment Co., Ltd of the triumphant rib in Guangzhou
The microwave abstracting equipment of 80CQ.
Embodiment 1
A kind of raw material of environment-protection detergent powder (parts by weight): 35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts the following steps are included:
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of Radix Polygalae, 15 parts of campanulaceae, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is impregnated 15 minutes in the ethanol water that volume fraction is 35%, wherein plant mixes
The mass ratio of object and ethanol water is 1:10, obtains mixed solution；
(3) mixed solution is used into 300 mesh filter-cloth filtering wastes, obtains filtrate, is in pressure 0.06MPa, temperature by filtrate
It is the thick paste that density is 1.30g/mL (20 DEG C) that vacuum-concentrcted is carried out under conditions of at 40 DEG C, is freeze-dried at -20 DEG C
After 12 hours, plant extracts is arrived.
A kind of preparation method of environment-protection detergent powder the following steps are included:
(1) plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose ingredient: are weighed
Sodium, bentonite, water are uniformly mixed, obtain mixture；
(2) it is granulated: distributed slurry being spray-dried to obtain environment-protection detergent powder.
Embodiment 2
A kind of raw material of environment-protection detergent powder (parts by weight): 35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts the following steps are included:
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of Radix Polygalae, 15 parts of campanulaceae, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is impregnated 15 minutes in the ethanol water that volume fraction is 35%, wherein plant mixes
The mass ratio of object and ethanol water is 1:10, obtains mixed solution；
(3) mixed solution is handled into 8min, magnetic field strength 2300GS in magnetic field；
(4) mixed solution that will be handled through step (3) uses 300 mesh filter-cloth filtering wastes, obtains filtrate；Filtrate is in pressure
0.06MPa, temperature be at 40 DEG C under conditions of to carry out vacuum-concentrcted be thick paste that density is 1.30g/mL (20 DEG C) ,-
After being freeze-dried 12 hours at 20 DEG C, plant extracts is arrived.
A kind of preparation method of environment-protection detergent powder:
(1) plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose ingredient: are weighed
Sodium, bentonite, water are uniformly mixed, obtain mixture；
(2) it is granulated: distributed slurry being spray-dried to obtain environment-protection detergent powder.
Embodiment 3
Substantially the same manner as Example 2, difference is only that:
The step of preparation method of the plant extracts (3) are as follows: mixed solution is handled into 8min in magnetic field, magnetic field is strong
Spend 2200GS.
Embodiment 4
Substantially the same manner as Example 2, difference is only that:
The step of preparation method of the plant extracts (3) are as follows: mixed solution is handled into 8min in magnetic field, magnetic field is strong
Spend 2400GS.
Embodiment 5
A kind of raw material of environment-protection detergent powder (parts by weight): 35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts the following steps are included:
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of Radix Polygalae, 15 parts of campanulaceae, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is impregnated 15 minutes in the ethanol water that volume fraction is 35%, wherein plant mixes
The mass ratio of object and ethanol water is 1:10, obtains mixed solution；
(3) mixed solution is handled into 8min, magnetic field strength 2300GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, the power of microwave abstracting is
500W, 45 DEG C microwave abstracting 10 minutes, using 300 mesh filter-cloth filtering wastes, obtain filtrate；
(5) filtrate is carried out vacuum-concentrcted under conditions of pressure 0.06MPa, temperature are at 40 DEG C is that density is
The thick paste of 1.30g/mL (20 DEG C) after being freeze-dried 12 hours at -20 DEG C, arrives plant extracts.
A kind of preparation method of environment-protection detergent powder:
(1) plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose ingredient: are weighed
Sodium, bentonite, water are uniformly mixed, obtain mixture；
(2) it is granulated: distributed slurry being spray-dried to obtain environment-protection detergent powder.
Embodiment 6
Substantially the same manner as Example 2, difference is only that:
The step of preparation method of the plant extracts (4) are as follows: be added to the mixed solution handled through step (3) micro-
In wave extraction equipment, the power of microwave abstracting is 500W, 25 DEG C microwave abstracting 10 minutes, using 300 mesh filter-cloth filtering wastes,
Obtain filtrate.
Embodiment 7
Substantially the same manner as Example 2, difference is only that:
The step of preparation method of the plant extracts (4) are as follows: be added to the mixed solution handled through step (3) micro-
In wave extraction equipment, the power of microwave abstracting is 500W, first 45 DEG C microwave abstracting 2 minutes, then divide in 25 DEG C of microwave abstractings 8
Clock obtains filtrate using 300 mesh filter-cloth filtering wastes.
Embodiment 8
A kind of raw material of environment-protection detergent powder (parts by weight): 35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts the following steps are included:
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of Radix Polygalae, 15 parts of campanulaceae, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is impregnated 15 minutes in the ethanol water that volume fraction is 35%, wherein plant mixes
The mass ratio of object and ethanol water is 1:10, obtains mixed solution；
(3) mixed solution is added in microwave abstracting equipment, the power of microwave abstracting is 500W, is first extracted in 45 DEG C of microwaves
Take 2 minutes, then 25 DEG C microwave abstracting 8 minutes, using 300 mesh filter-cloth filtering wastes, obtain filtrate；
(4) filtrate is carried out vacuum-concentrcted under conditions of pressure 0.06MPa, temperature are at 40 DEG C is that density is
The thick paste of 1.30g/mL (20 DEG C) after being freeze-dried 12 hours at -20 DEG C, arrives plant extracts.
A kind of preparation method of environment-protection detergent powder:
(1) plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose ingredient: are weighed
Sodium, bentonite, water are uniformly mixed, obtain mixture；
(2) it is granulated: distributed slurry being spray-dried to obtain environment-protection detergent powder.
Embodiment 9
Substantially the same manner as Example 7, difference is only that:
The dirt dispersion agent is sodium citrate.Detergency ability test: JB01 1.45, JB02 1.27, JB03 1.30；
Bactericidal property test result: the sterilizing rate to Escherichia coli (ATCC 25922) is 92.8%, to hay bacillus (ATCC 9372)
Sterilizing rate be 93.1%, be 94.2% to the sterilizing rate of staphylococcus aureus (ATCC 6538).
Embodiment 10
Substantially the same manner as Example 7, difference is only that:
The dirt dispersion agent is that sodium citrate and sodium humate 2:1 in mass ratio are mixed.Detergency ability test knot
Fruit: JB01 value 1.61, JB02 1.38, JB03 1.44.Bactericidal property test result: Escherichia coli (ATCC 25922) are killed
Bacterium rate is 99.8%, and the sterilizing rate to hay bacillus (ATCC 9372) is 99.6%, to staphylococcus aureus (ATCC
6538) sterilizing rate is 99.9%.
Test case 1
Detergency ability test is carried out to the environment-protection detergent powder of the preparation of embodiment 1-8.Concrete outcome is shown in Table 1.
Table 1: detergency ability test result table
Embodiment 2-4 uses magnetic field in the preparation process of plant extracts and handles mixed solution, the environment friendly laundry of preparation
The clean effect of powder is substantially better than embodiment 1.The intensity in magnetic field is optimized, discovery is when magnetic field strength is 2300GS, system
Standby washing powder clean effect is best.
The preparation process of embodiment 5-7 plant extracts uses microwave abstracting, the clean effect of the environment-protection detergent powder of preparation
It is substantially better than embodiment 1-4, and to carry out microwave abstracting effect stage by stage best for embodiment 7.
The preparation process of 7 plant extracts of embodiment handles mixed solution and stage by stage microwave abstracting, preparation using magnetic field
Environment-protection detergent powder clean effect be better than embodiment 1-4 and embodiment 8.
Test case 2
Bactericidal property test is carried out to the environment-protection detergent powder of the preparation of embodiment 1-8.Concrete outcome is shown in Table 2.
2 sterilizing rate of table tests table
| Escherichia coli, % | Hay bacillus, % | Staphylococcus aureus, % | |
| Embodiment 1 | 65.3 | 63.4 | 67.8 |
| Embodiment 2 | 79.5 | 78.1 | 80.1 |
| Embodiment 3 | 74.2 | 75.9 | 76.4 |
| Embodiment 4 | 76.7 | 74.6 | 75.3 |
| Embodiment 5 | 86.2 | 87.8 | 88.6 |
| Embodiment 6 | 84.6 | 85.1 | 84.2 |
| Embodiment 7 | 91.5 | 92.3 | 93.8 |
| Embodiment 8 | 81.2 | 83.6 | 82.6 |
Claims (4)
1. a kind of environment-protection detergent powder, which is characterized in that the raw material including following weight parts: 30-40 parts of plant extracts crosses phosphinylidyne
10-20 parts of amine, 10-20 parts of cocoyl glucoside, 1-5 parts of dirt dispersion agent, 0.1-1 parts of sodium carboxymethylcellulose, bentonite 8-
15 parts, 10-30 parts of water；
The preparation method of the plant extracts the following steps are included:
(1) 40-50 parts of gleditsia sinensis, 20-30 parts of Saponaria officinalis, 10-20 parts of Radix Polygalae, 10-20 parts of campanulaceae, Salvia japonica 5- are weighed by weight
It 10 parts, crushes as 60-100 mesh, obtains plant mixture；
(2) plant mixture impregnated to 10-20 minutes in organic solvent, wherein the mass ratio of plant mixture and organic solvent
For 1:(8-12), mixed solution is obtained；
(3) mixed solution is handled into 5-10min, magnetic field strength 2200GS-2400GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, first at 40-50 DEG C of microwave abstracting 1-3 points
Clock, then 20-30 DEG C microwave abstracting 5-10 minutes, filtering, obtain filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
2. environment-protection detergent powder as described in claim 1, which is characterized in that the organic solvent is that volume fraction is 30-
40% ethanol water.
3. environment-protection detergent powder as described in claim 1, which is characterized in that the power 400-600W of the microwave abstracting.
4. environment-protection detergent powder as described in claim 1, which is characterized in that the dirt dispersion agent is sodium citrate and/or corruption
Grow sour sodium.
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| CN201710147176.3A CN106957734B (en) | 2017-03-13 | 2017-03-13 | Environment-protection detergent powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107760474A (en) * | 2017-09-15 | 2018-03-06 | 安徽省力天新材料股份有限公司 | One kind is felt at ease Traditional Chinese medicine laundry detergent of reposing |
| CN109457467B (en) * | 2018-12-03 | 2021-11-05 | 广东三兴高新材料科技有限公司 | Mild environment-friendly decontamination finishing agent for cotton fabric |
| CN111334380A (en) * | 2020-02-26 | 2020-06-26 | 惠州市康洁洗涤用品有限公司 | Sterilizing environment-friendly washing powder |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099411A (en) * | 1994-06-24 | 1995-03-01 | 黄德丰 | Harmless washing powder |
| DE202006007594U1 (en) * | 2006-05-12 | 2006-07-13 | Remsgold-Chemie Gmbh & Co | Cleaning agent containing saponin, useful as e.g. bleach and water-free fine detergent, bleach-free wash cream and dishwasher detergents, comprises a surfactant and/or a dispersing agent |
| CN102242021B (en) * | 2011-05-31 | 2012-11-21 | 廊坊乐万家联合家化有限公司 | Oxygen-containing concentrated laundry powder |
| CN102965217A (en) * | 2012-12-03 | 2013-03-13 | 晓健科技（大连）有限公司 | Soapberry liquid laundry detergent |
| CN104324065A (en) * | 2014-10-27 | 2015-02-04 | 福州品行科技发展有限公司 | Composition having function of improving sleep and preparation method thereof |
| CN104450252A (en) * | 2014-11-19 | 2015-03-25 | 苏州佑君环境科技有限公司 | Environment-friendly purification washing paste and preparation method thereof |
-
2017
- 2017-03-13 CN CN201710147176.3A patent/CN106957734B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099411A (en) * | 1994-06-24 | 1995-03-01 | 黄德丰 | Harmless washing powder |
| DE202006007594U1 (en) * | 2006-05-12 | 2006-07-13 | Remsgold-Chemie Gmbh & Co | Cleaning agent containing saponin, useful as e.g. bleach and water-free fine detergent, bleach-free wash cream and dishwasher detergents, comprises a surfactant and/or a dispersing agent |
| CN102242021B (en) * | 2011-05-31 | 2012-11-21 | 廊坊乐万家联合家化有限公司 | Oxygen-containing concentrated laundry powder |
| CN102965217A (en) * | 2012-12-03 | 2013-03-13 | 晓健科技（大连）有限公司 | Soapberry liquid laundry detergent |
| CN104324065A (en) * | 2014-10-27 | 2015-02-04 | 福州品行科技发展有限公司 | Composition having function of improving sleep and preparation method thereof |
| CN104450252A (en) * | 2014-11-19 | 2015-03-25 | 苏州佑君环境科技有限公司 | Environment-friendly purification washing paste and preparation method thereof |
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