CN106957734A - Environment-protection detergent powder - Google Patents
Environment-protection detergent powder Download PDFInfo
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- CN106957734A CN106957734A CN201710147176.3A CN201710147176A CN106957734A CN 106957734 A CN106957734 A CN 106957734A CN 201710147176 A CN201710147176 A CN 201710147176A CN 106957734 A CN106957734 A CN 106957734A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2089—Ether acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3945—Organic per-compounds
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of environment-protection detergent powder, the preparation method of the environment-protection detergent powder includes following raw materials：Plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, sodium carboxymethylcellulose, bentonite, water.Environment-protection detergent powder of the present invention, it can quickly and thoroughly remove the greasy dirt being attached on clothing, sweat stain and other pollutants, antibiotic property is good, so as to improve the detersive efficiency of clothing, preparation process is using natural plant extracts and the surfactant of green, safe, non-stimulated to human body skin, the waste water of washing is environmentally safe.
Description
Technical field
The present invention relates to detergent technical field, and in particular to a kind of environment-protection detergent powder.
Background technology
Washing powder is one of essential cleaning supplies of people's daily life already.With people's consumption concept into
It is ripe, the requirement of national low-carbon economy, energy-saving, water-saving and emission-reducing trend of the times, traditional washing powder is generally synthetic detergent powder, with
Its highly energy-consuming, accumulating packing cost are high, all rich in unfavorable environmentally friendly, alkaline higher damaging laundry and the filler inefficient cycle of phosphorus aluminium etc.
Many shortcomings, are increasingly not suitable with the requirement of era development.
Chemical washing powder is synthesized with its cheap, cleaning performance well all the time in occupation of the city of household cleaning product
.Synthetic detergent powder usually contain surfactant, alkaline agent, complexing agent, protease, fluorescent whitening agent, filler etc. it is main into
Part, whitening type washing powder can also add the bleaching agents such as peroxide.Institute in the waste water after clothes is cleaned with synthesis chemical washing powder
The chemical substance contained easily causes environmental pollution, and it all has large effect to water original, fish, soil, crops etc..Washing
Afterwards on clothes synthetic detergent powder residual can all have an impact to human body skin and nervous system, especially to child and bear a pretty, delicate skin easily
Allergy personage influence is bigger.Such as sodium alkyl benzene sulfonate is the principal surfactant for synthesizing chemical washing powder, and it has collaboration
Carcinogenic effect.Benzene is the benzene remained on a kind of liposoluble substance, the clothing of non-rinsed clean, can not only stimulate skin to cause scabies
Itch, and can be penetrated into by skin in human body, accumulate over a long period, may induce an illness.The conventional fluorescent whitening agent of washing powder is to cause
Cancer material, can be distorted human body cell, can also trigger dermatitis and pruitus.Modern medicine proves, LAS (alkylbenzenes
Sodium sulfonate), AES (sodium sulfate of polyethenoxy ether of fatty alcohol), the raw material such as AS (sodium alkyl sulfate) can also cause under fecundity
The toxic and side effects such as drop, injury liver kidney, contaminated blood, infringement lymphatic system reduction immunity.In order to solve the residual of synthetic detergent powder
The problems such as staying and pollute, urgent need works out a kind of environmentally friendly skin-care washing powder.
The content of the invention
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of environment-protection detergent powder, including following raw materials：Percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl are fine
The plain sodium of dimension, bentonite, water.
A kind of environment-protection detergent powder, including following raw materials：Plant extracts, percarbamide, cocoyl glucoside, antiscaling dispersion
Agent, sodium carboxymethylcellulose, bentonite, water.
Preferably, a kind of environment-protection detergent powder, includes the raw material of following weight parts：30-40 parts of plant extracts, percarbamide
10-20 parts, 10-20 parts of cocoyl glucoside, 1-5 parts of dirt dispersion agent, 0.1-1 parts of sodium carboxymethylcellulose, bentonite 8-15
Part, 10-30 parts of water.
Preferably, the preparation method of the plant extracts comprises the following steps：
(1) gleditsia sinensis, Saponaria officinalis, polygala, balloonflower root, Salvia japonica, crush as 60-100 mesh, obtain plant mixture；
(2) plant mixture is soaked in organic solvent 10-20 minutes, obtains mixed solution；
(3) mixed solution is handled into 5-10min in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, is filtered after extraction, obtain filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
Preferably, the preparation method of the plant extracts comprises the following steps：
(1) 40-50 parts of gleditsia sinensis, 20-30 parts of Saponaria officinalis, 10-20 parts of polygala, 10-20 parts of balloonflower root, rat-tail are weighed by weight
It is careless 5-10 parts, crush as 60-100 mesh, obtain plant mixture；
(2) plant mixture is soaked to 10-20 minutes, the wherein matter of plant mixture and organic solvent in organic solvent
Amount is than being 1：(8-12), obtains mixed solution；
(3) mixed solution is handled into 5-10min, magnetic field intensity 2200GS-2400GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, first in 40-50 DEG C of microwave abstracting
1-3 minutes, then in 20-30 DEG C of microwave abstracting 5-10 minutes, filtering obtained filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
Preferably, described organic solvent is the ethanol water that volume fraction is 30-40%.
Preferably, the power 400-600W of the microwave abstracting.
Preferably, the dirt dispersion agent is sodium citrate and/or sodium humate.It is highly preferred that the dirt dispersion agent
For sodium citrate and sodium humate (1-3) in mass ratio:1 mixes.
Environment-protection detergent powder of the present invention, can quickly and thoroughly remove the greasy dirt being attached on clothing, sweat stain and other dirts
Thing is contaminated, antibiotic property is good, so as to improve the detersive efficiency of clothing, preparation process is lived using the surface of natural plant extracts and green
Property agent, safe, non-stimulated to human body skin, the waste water of washing is environmentally safe.
Embodiment
Detergency ability is tested：With reference to GB/T13174-2008《Dress material with detergent detergency and circulate scourability survey
It is fixed》Method tests the clean result of environment-protection detergent powder prepared by each embodiment.
Method of testing：Using B values (whiteness holding ratio) as the evaluation index of clean result, as B >=1.0, detergent
Detergency is qualified；During B ＜ 1.0, detergent detergency is unqualified.
Test sample includes JB-01 (carbon black greasy dirt cloth), JB-02 (albumen soiled cotton), JB-03 (sebum soiled cotton).
Wash conditions：Washing powder concentration 0.2% in cleaning solution, 30 DEG C of wash temperature, wash time 20min, the water hardness
250mg/kg。
Anti-microbial property test：Using QB/T2738-2012《The evaluation method of daily chemical products antibacterial bacteriostatic effect》To each reality
The anti-microbial property for applying the environment-protection detergent powder of example preparation is tested.The microorganism tested：Escherichia coli (ATCC 25922)；It is withered
Careless bacillus (ATCC 9372)；Staphylococcus aureus (ATCC 6538).
Ethanol, No. CAS：64-17-5.
Percarbamide, No. CAS：124-43-6.Carbamide percarbonate outward appearance is white crystalline powder, and nontoxic odorlessness is readily soluble
Yu Shui, the aqueous solution has the property of urea and hydrogen peroxide concurrently.Urea, H are decomposed into water2O2And elemental oxygen, and slowly release oxygen
Gas.Its active o content is high, and the solubility in water is big, and pH value of water solution weakly acidic pH, good stability, the effectiveness time is long, no pair
Effect, Nonpoisonous, non-environmental-pollution.
Cocoyl glucoside, No. CAS：141464-42-8, is a kind of green surfactant, sends out triumphant using Shanghai and changes
The APG0814 of work Co., Ltd production.
Sodium humate, No. CAS：68131-04-4.
Sodium citrate, No. CAS：6132-04-3.
Sodium carboxymethylcellulose, No. CAS：9004-32-4, the carboxylic first provided using Shandong Xi Tang bio tech ltd
Base sodium cellulosate.
Bentonite, No. CAS：1302-78-9, the bentonite provided using Luoshan County green hill town Li Hui bentonites factory, particle diameter
325-800 mesh.
The fruit of gleditsia sinensis, i.e. honey locust Gleditsia sinensis Lam., be medicine food, health products, cosmetics and
The natural material of articles for washing；Gleditsia sinensis Seeds can promoting digestion appetizing, and containing a kind of natural plant gum, Fructus Gleditsia acupuncture (soap pin) includes Huang
Ketone glucoside, phenols, amino acid have very high economic worth.Gleditsia sinensis has antibacterial action, and gleditsia sinensis has naturally to many bacteriums, fungi
Suppression and sterilized effect.
Saponaria officinalis, Classification system：The dried leaf of Saponaria officinalis is used in Saponaria officinalis, the present invention.
Polygala is milk wort polygala Polyyala tenuifolia Willd. or ovum leaf polygala Polygala
Sibirica L. dry root.
Balloonflower root, Campanulaceae balloonflower root Platycodon grandiflorum (Jacq.) A DC. dry root.
Salvia japonica, Classification system：The dried leaf of Salvia japonica is used in Salvia japonica Thunb., the present invention.Rat-tail
Grass is a kind of perennial fragrant plant, and Salvia japonica essential oil has the effect of anti-inflammation.Cytothesis can be promoted, maintenance skin is thin
Born of the same parents organize, and purify greasy scalp, regulation skin oil and fat secretion, the skin problem reduced inflammation with swelling.Help improve oiliness
The skin problem such as skin, acne, acne.Salvia japonica essential oil has the effect of beautifying face and moistering lotion, additionally it is possible to anti-inflammation.
Microwave abstracting equipment, the model KL-2D- provided using the industrial microwave equipment Co., Ltd of the triumphant rib in Guangzhou
80CQ microwave abstracting equipment.
Embodiment 1
A kind of raw material of environment-protection detergent powder (parts by weight)：35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts comprises the following steps：
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of polygala, 15 parts of balloonflower root, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is soaked 15 minutes in volume fraction is 35% ethanol water, wherein plant mixes
The mass ratio of thing and ethanol water is 1：10, obtain mixed solution；
(3) mixed solution is used into 300 mesh filter-cloth filtering wastes, obtains filtrate, be in pressure 0.06MPa, temperature by filtrate
It is the thick paste that density is 1.30g/mL (20 DEG C) that vacuum-concentrcted is carried out under conditions of at 40 DEG C, is freeze-dried at -20 DEG C
After 12 hours, to plant extracts.
A kind of preparation method of environment-protection detergent powder comprises the following steps：
(1) dispensing：Weigh plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose
Sodium, bentonite, water, are well mixed, obtain mixture；
(2) granulate：Distributed slurry be spray-dried to obtain environment-protection detergent powder.
Embodiment 2
A kind of raw material of environment-protection detergent powder (parts by weight)：35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts comprises the following steps：
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of polygala, 15 parts of balloonflower root, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is soaked 15 minutes in volume fraction is 35% ethanol water, wherein plant mixes
The mass ratio of thing and ethanol water is 1：10, obtain mixed solution；
(3) mixed solution is handled into 8min, magnetic field intensity 2300GS in magnetic field；
(4) mixed solution that will be handled through step (3) uses 300 mesh filter-cloth filtering wastes, obtains filtrate；Filtrate is in pressure
0.06MPa, temperature be at 40 DEG C under conditions of to carry out vacuum-concentrcted be the thick paste that density is 1.30g/mL (20 DEG C) ,-
After being freeze-dried 12 hours at 20 DEG C, to plant extracts.
A kind of preparation method of environment-protection detergent powder：
(1) dispensing：Weigh plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose
Sodium, bentonite, water, are well mixed, obtain mixture；
(2) granulate：Distributed slurry be spray-dried to obtain environment-protection detergent powder.
Embodiment 3
It is substantially the same manner as Example 2, differ only in：
The step of preparation method of the plant extracts (3) is：Mixed solution is handled into 8min in magnetic field, magnetic field is strong
Spend 2200GS.
Embodiment 4
It is substantially the same manner as Example 2, differ only in：
The step of preparation method of the plant extracts (3) is：Mixed solution is handled into 8min in magnetic field, magnetic field is strong
Spend 2400GS.
Embodiment 5
A kind of raw material of environment-protection detergent powder (parts by weight)：35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts comprises the following steps：
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of polygala, 15 parts of balloonflower root, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is soaked 15 minutes in volume fraction is 35% ethanol water, wherein plant mixes
The mass ratio of thing and ethanol water is 1：10, obtain mixed solution；
(3) mixed solution is handled into 8min, magnetic field intensity 2300GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, the power of microwave abstracting is
500W, in 45 DEG C of microwave abstractings 10 minutes, using 300 mesh filter-cloth filtering wastes, obtains filtrate；
(5) by filtrate be at 40 DEG C in pressure 0.06MPa, temperature under conditions of carry out vacuum-concentrcted be that density is
1.30g/mL (20 DEG C) thick paste, after being freeze-dried 12 hours at -20 DEG C, to plant extracts.
A kind of preparation method of environment-protection detergent powder：
(1) dispensing：Weigh plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose
Sodium, bentonite, water, are well mixed, obtain mixture；
(2) granulate：Distributed slurry be spray-dried to obtain environment-protection detergent powder.
Embodiment 6
It is substantially the same manner as Example 2, differ only in：
The step of preparation method of the plant extracts (4) is：The mixed solution handled through step (3) is added to micro-
In ripple extraction equipment, the power of microwave abstracting was 500W, in 25 DEG C of microwave abstractings 10 minutes, using 300 mesh filter-cloth filtering wastes,
Obtain filtrate.
Embodiment 7
It is substantially the same manner as Example 2, differ only in：
The step of preparation method of the plant extracts (4) is：The mixed solution handled through step (3) is added to micro-
In ripple extraction equipment, the power of microwave abstracting is 500W, first in 45 DEG C of microwave abstractings 2 minutes, then in 25 DEG C of 8 points of microwave abstractings
Clock, using 300 mesh filter-cloth filtering wastes, obtains filtrate.
Embodiment 8
A kind of raw material of environment-protection detergent powder (parts by weight)：35 parts of plant extracts, 15 parts of percarbamide, cocoyl glucoside
15 parts, 3 parts of dirt dispersion agent, 0.5 part of sodium carboxymethylcellulose, 12 parts of bentonite, 20 parts of water.
The dirt dispersion agent is sodium humate.
The preparation method of the plant extracts comprises the following steps：
(1) 45 parts of gleditsia sinensis, 25 parts of Saponaria officinalis, 15 parts of polygala, 15 parts of balloonflower root, 8 parts of Salvia japonica are weighed by weight, are crushed and are
80 mesh, obtain plant mixture；
(2) plant mixture is soaked 15 minutes in volume fraction is 35% ethanol water, wherein plant mixes
The mass ratio of thing and ethanol water is 1：10, obtain mixed solution；
(3) mixed solution is added in microwave abstracting equipment, the power of microwave abstracting is 500W, first in 45 DEG C of microwave extractions
Take 2 minutes, then in 25 DEG C of microwave abstractings 8 minutes, using 300 mesh filter-cloth filtering wastes, obtain filtrate；
(4) by filtrate be at 40 DEG C in pressure 0.06MPa, temperature under conditions of carry out vacuum-concentrcted be that density is
1.30g/mL (20 DEG C) thick paste, after being freeze-dried 12 hours at -20 DEG C, to plant extracts.
A kind of preparation method of environment-protection detergent powder：
(1) dispensing：Weigh plant extracts, percarbamide, cocoyl glucoside, dirt dispersion agent, carboxymethyl cellulose
Sodium, bentonite, water, are well mixed, obtain mixture；
(2) granulate：Distributed slurry be spray-dried to obtain environment-protection detergent powder.
Embodiment 9
It is substantially the same manner as Example 7, differ only in：
The dirt dispersion agent is sodium citrate.Detergency ability is tested：JB01 1.45, JB02 1.27, JB03 1.30；
Bactericidal property test result：Sterilizing rate to Escherichia coli (ATCC 25922) is 92.8%, to hay bacillus (ATCC 9372)
Sterilizing rate be 93.1%, be 94.2% to the sterilizing rate of staphylococcus aureus (ATCC 6538).
Embodiment 10
It is substantially the same manner as Example 7, differ only in：
The dirt dispersion agent is sodium citrate and sodium humate in mass ratio 2:1 mixes.Detergency ability test knot
Really：JB01 values 1.61, JB02 1.38, JB03 1.44.Bactericidal property test result：Escherichia coli (ATCC 25922) are killed
Bacterium rate is 99.8%, and the sterilizing rate to hay bacillus (ATCC 9372) is 99.6%, to staphylococcus aureus (ATCC
6538) sterilizing rate is 99.9%.
Test case 1
Detergency ability test is carried out to the environment-protection detergent powder of embodiment 1-8 preparation.Concrete outcome is shown in Table 1.
Table 1：Detergency ability test result table
Embodiment 2-4 employs magnetic field processing mixed solution, the environment friendly laundry of preparation in the preparation process of plant extracts
The clean effect of powder is substantially better than embodiment 1.Intensity to magnetic field is optimized, and is found when magnetic field intensity is 2300GS, system
Standby washing powder clean effect is best.
The preparation process of embodiment 5-7 plant extracts uses microwave abstracting, the clean effect of the environment-protection detergent powder of preparation
It is substantially better than embodiment 1-4, and to carry out microwave abstracting effect stage by stage best for embodiment 7.
The preparation process of the plant extracts of embodiment 7 handles mixed solution and stage by stage microwave abstracting using magnetic field, prepares
Environment-protection detergent powder clean effect be better than embodiment 1-4 and embodiment 8.
Test case 2
Bactericidal property test is carried out to the environment-protection detergent powder of embodiment 1-8 preparation.Concrete outcome is shown in Table 2.
The sterilizing rate of table 2 tests table
| Escherichia coli, % | Hay bacillus, % | Staphylococcus aureus, % | |
| Embodiment 1 | 65.3 | 63.4 | 67.8 |
| Embodiment 2 | 79.5 | 78.1 | 80.1 |
| Embodiment 3 | 74.2 | 75.9 | 76.4 |
| Embodiment 4 | 76.7 | 74.6 | 75.3 |
| Embodiment 5 | 86.2 | 87.8 | 88.6 |
| Embodiment 6 | 84.6 | 85.1 | 84.2 |
| Embodiment 7 | 91.5 | 92.3 | 93.8 |
| Embodiment 8 | 81.2 | 83.6 | 82.6 |
Claims (8)
1. a kind of environment-protection detergent powder, it is characterised in that including following raw materials：Percarbamide, cocoyl glucoside, antiscaling dispersion
Agent, sodium carboxymethylcellulose, bentonite, water.
2. a kind of environment-protection detergent powder, it is characterised in that including following raw materials：Plant extracts, percarbamide, cocoyl glucose
Glycosides, dirt dispersion agent, sodium carboxymethylcellulose, bentonite, water.
3. a kind of environment-protection detergent powder, it is characterised in that the raw material including following weight parts：30-40 parts of plant extracts, excessively phosphinylidyne
10-20 parts of amine, 10-20 parts of cocoyl glucoside, 1-5 parts of dirt dispersion agent, 0.1-1 parts of sodium carboxymethylcellulose, bentonite 8-
15 parts, 10-30 parts of water.
4. environment-protection detergent powder as claimed in claim 3, it is characterised in that the preparation method of the plant extracts includes following
Step：
(1) gleditsia sinensis, Saponaria officinalis, polygala, balloonflower root, Salvia japonica, crush as 60-100 mesh, obtain plant mixture；
(2) plant mixture is soaked in organic solvent 10-20 minutes, obtains mixed solution；
(3) mixed solution is handled into 5-10min in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, is filtered after extraction, obtain filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
5. environment-protection detergent powder as claimed in claim 3, it is characterised in that the preparation method of the plant extracts includes following
Step：
(1) 40-50 parts of gleditsia sinensis, 20-30 parts of Saponaria officinalis, 10-20 parts of polygala, 10-20 parts of balloonflower root, Salvia japonica 5- are weighed by weight
10 parts, crush as 60-100 mesh, obtain plant mixture；
(2) plant mixture is soaked to 10-20 minutes, the wherein mass ratio of plant mixture and organic solvent in organic solvent
For 1：(8-12), obtains mixed solution；
(3) mixed solution is handled into 5-10min, magnetic field intensity 2200GS-2400GS in magnetic field；
(4) mixed solution handled through step (3) is added in microwave abstracting equipment, first in 40-50 DEG C of 1-3 points of microwave abstracting
Clock, then in 20-30 DEG C of microwave abstracting 5-10 minutes, filtering obtained filtrate；
(5) filtrate decompression is concentrated, is freeze-dried, obtains plant extracts.
6. environment-protection detergent powder as claimed in claim 5, it is characterised in that described organic solvent is that volume fraction is 30-
40% ethanol water.
7. environment-protection detergent powder as claimed in claim 5, it is characterised in that the power 400-600W of the microwave abstracting.
8. the environment-protection detergent powder as described in claim 3 or 5, it is characterised in that the dirt dispersion agent be sodium citrate and/or
Sodium humate.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN109457467B (en) * | 2018-12-03 | 2021-11-05 | 广东三兴高新材料科技有限公司 | Mild environment-friendly decontamination finishing agent for cotton fabric |
| CN111334380A (en) * | 2020-02-26 | 2020-06-26 | 惠州市康洁洗涤用品有限公司 | Sterilizing environment-friendly washing powder |
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