CN106955249A - 一种含有树莓的膏状面膜 - Google Patents
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Abstract
本发明提供了一种含有树莓的膏状面膜。将树莓花色苷提取物、树莓果油和树莓多糖等组份配伍使用后制备的膏状面膜,具有良好的美白、保湿、抗衰老、防晒等功效。
Description
技术领域
本发明涉及一种含有树莓的膏状面膜。
背景技术
树莓(Rubus idaeus L.)又名山莓、悬钩子、覆盆子等,属蔷薇科悬钩子属。树莓主要分布于北半球温带和寒带,其果实为多浆小聚合果,味甜微酸。树莓含有果油、有机酸、黄酮、花青素,多酚、维生素、矿质元素、挥发油、鞣质等多种活性成分,具有极高的营养价值和医疗保健作用,被誉为“黄金水果”。
目前,还未见将树莓的多种活性成分配伍运用的报道。
发明内容
本发明提供了一种含有树莓的膏状面膜,它含有如下质量配比的组份:
其中,树莓花色苷提取物选自3.0~5.0份、树莓果油选自1.0~3.0份、树莓多糖选自5.0~10.0份、枸杞子水提物1~3份、玫瑰花水提物1~3份。
本发明一个具体实施方式中,选取的组份配比如下:
配比一:
配比二:
制备方法同上。
配比三:
制备方法同上。
配比四:
进一步地,树莓花色苷提取物选自4.0±0.5份、树莓果油选自2.0±0.5份、树莓多糖选自8.0±0.5份、枸杞子水提物2.0±0.5份、玫瑰花水提物2.0±0.5份。本发明在实际使用过程中发现,若将树莓各部位按照该配比与枸杞子水提物、玫瑰花水提物进行组合使用,其护肤效果显著优于其他配伍关系。
其中,所述树莓为蔷薇科悬钩子属植物的果实。
本发明所使用的树莓花色苷提取物、树莓果油、树莓多糖、枸杞子水提物、玫瑰花水提物可以在市售商品中购买,也可以根据目前公开的技术进行制备,本发明一个具体实施方式中,所述树莓花色苷提取物的制备方法如下:取树莓,加水提取,水提物上大孔树脂柱,先用水洗除杂,再用60~80%v/v乙醇洗脱,收集乙醇洗脱部位,干燥即得。
其中,所述树莓多糖的制备方法如下:取树莓,石油醚或乙醚脱脂后,用75%~95%v/v乙醇提取,过滤,滤渣加水提取,取水提液浓缩后,加乙醇或含水乙醇至含醇量达到70%~85%v/v,取固形物即为树莓多糖。
其中,所述树莓果油的制备方法如下:取树莓,采用超临界CO2萃取进行提取,提取后,再经两级减压分离得到树莓果油;其中,萃取条件如下:萃取釜压力为15~45Mpa、温度为30~55℃、CO2流量为20~60L/h、萃取时间为40~120min;两级减压分离条件如下:以压力为5~7Mpa、温度为40~50℃作为一级减压分离,以压力为3~5Mpa、温度为30~40℃作为二级减压分离。
枸杞子水提物,即采用水加热至50~70℃进行提取,提取液减压浓缩,干燥即得。
玫瑰花水提物,即采用水加热至50~70℃进行提取,提取液减压浓缩,干燥即得。
本发明还提供了上述膏状面膜的制备方法,它包括如下操作步骤:
(1)取树莓果油、生育酚、氢化小麦胚芽油、鲸蜡、硬脂醇、鲸蜡硬脂基葡糖苷,作为油相备用;
(2)取树莓花色苷提取物、树莓多糖、枸杞子水提物、玫瑰花水提物、甘油、海藻酸钠、透明质酸钠、EDTA二钠和部分水,作为水相备用;
(3)取丁二醇、丙二醇、二氧化钛作为C相备用;
(4)取C相研磨均匀,将A、B相加热,均质,降温冷却,即得膏状面膜。
本发明还提供了上述膏状面膜在制备具有补水保湿、美白、抗衰老、防晒功效的护肤品中的用途。
本发明研究发现,将树莓花色苷提取物、树莓果油和树莓多糖等组份配伍使用后制备的膏状面膜,具有良好的美白、保湿、抗衰老、防晒等功效。
另外,在本发明基础上,面膜中还可以添加一些已知的护肤物质,如珍珠粉、尿囊素等。
另外,组合物或乳液中还可以添加适量的天然防腐剂、抗氧化剂等辅料。
具体实施方式
实施例1本发明膏状面膜的制备及功效研究
工艺流程:
(1)取树莓果油、生育酚、氢化小麦胚芽油、鲸蜡硬脂醇、鲸蜡硬脂基葡糖苷,作为油相备用;
(2)取树莓花色苷提取物、树莓多糖、甘油、海藻酸钠、透明质酸钠、EDTA二钠和部分水,作为水相备用;
(3)取丁二醇、丙二醇、二氧化钛作为C相备用;
(4)取C相研磨均匀,将A、B相加热,均质,降温冷却,即得膏状面膜。
为了测试本发明的保湿效果,进行了试用调查实验:
1.调查对象:选取同一地区的不同肤质的志愿试用者共60人;
2.调查时间:连续30天
使用产品:A产品:本发明实施例1制备的膏状面膜;B产品为对照例膏状面膜:对照例膏状面膜中仅如下部分与实施例1不同:树莓花色苷提取物5.0g、树莓果油4.0g、树莓多糖5.0g,其余同实施例1。
3.测试方法:30人使用A产品,其余30人使用B产品,A产品组中途退出2例,B产品组中途退出1例。各组试用者清洁脸部后,分别将产品涂抹在脸部皮肤,观察并调查使用效果,试用者使用期间不知道每一组的成分配比,每天晚上睡前使用一次,每次敷贴10~30min。
4.测试结果统计如下:
表1
*良好:试用者认为皮肤有明显的改善效果;一般:试用者皮肤有改善,但自我感觉作用并不是非常突出;无影响:试用者认为皮肤无任何改善。
5.反馈结论:
试用者均表示,A、B两种产品的可抑制黑色素的形成,可祛斑美白、延缓衰老、补水保湿,使肌肤光泽富有弹性。
另外,A产品美白抗衰老保湿效果很好,连续使用二周后皮肤就已经出现了明显改善,细纹减少,肌肤具有弹性和光泽,且美白效果极好,好评率高达90%以上。B产品有一定的防皱保湿效果,面部细纹有所减少,好评率为70~86%,但是美白、抗衰老和保湿效果却不及A产品。
实施例2本发明膏状面膜的制备及功效研究
制备方法同上。
实施例3本发明膏状面膜的制备及功效研究
制备方法同上。
实施例4发明膏状面膜的制备及功效研究
制备方法同上。
Claims (9)
1.一种含有树莓的膏状面膜,其特征在于:它含有如下质量配比的组份:
2.根据权利要求1所述的含有树莓的膏状面膜,其特征在于:树莓花色苷提取物选自3.0~5.0份、树莓果油选自1.0~3.0份、树莓多糖选自5.0~10.0份、枸杞子水提物1~3份、玫瑰花水提物1~3份。
3.根据权利要求2所述的含有树莓的膏状面膜,其特征在于:树莓花色苷提取物选自4.0±0.5份、树莓果油选自2.0±0.5份、树莓多糖选自8.0±0.5份、枸杞子水提物2.0±0.5份、玫瑰花水提物2.0±0.5份。
4.根据权利要求1所述的含有树莓的膏状面膜,其特征在于:所述树莓为蔷薇科悬钩子属植物的果实。
5.根据权利要求1~4任意一项所述的含有树莓的膏状面膜,其特征在于:所述树莓花色苷提取物的制备方法如下:
取树莓,加水提取,水提物上大孔树脂柱,先用水洗除杂,再用60~80%v/v乙醇洗脱,收集乙醇洗脱部位,干燥即得。
6.根据权利要求1~4任意一项所述的含有树莓的膏状面膜,其特征在于:所述树莓多糖的制备方法如下:
取树莓,石油醚或乙醚脱脂后,用75%~95%v/v乙醇提取,过滤,滤渣加水提取,取水提液浓缩后,加乙醇或含水乙醇至含醇量达到70%~85%v/v,取固形物即为树莓多糖。
7.根据权利要求1~4任意一项所述的含有树莓的膏状面膜,其特征在于:所述树莓果油的制备方法如下:
取树莓,采用超临界CO2萃取进行提取,提取后,再经两级减压分离得到树莓果油;其中,萃取条件如下:萃取釜压力为15~45Mpa、温度为30~55℃、CO2流量为20~60L/h、萃取时间为40~120min;两级减压分离条件如下:以压力为5~7Mpa、温度为40~50℃作为一级减压分离,以压力为3~5Mpa、温度为30~40℃作为二级减压分离。
8.权利要求1所述膏状面膜的制备方法,其特征在于:它包括如下操作步骤:
(1)取树莓果油、生育酚、氢化小麦胚芽油、鲸蜡硬脂醇、鲸蜡硬脂基葡糖苷,作为A相备用;
(2)取树莓花色苷提取物、树莓多糖、枸杞子水提物、玫瑰花水提物、甘油、海藻酸钠、透明质酸钠、EDTA二钠和部分水,作为B相备用;
(3)取丁二醇、丙二醇、二氧化钛作为C相备用;
(4)取C相研磨均匀,将A、B相加热,均质,降温冷却,即得膏状面膜。
9.权利要求1~7任意一项所述膏状面膜在制备具有补水保湿、美白、抗衰老、防晒功效的护肤品中的用途。
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108498404A (zh) * | 2018-05-29 | 2018-09-07 | 华中农业大学 | 一种具有美白功能的树莓提取物 |
CN108938502A (zh) * | 2018-09-29 | 2018-12-07 | 中北大学 | 一种可食用水晶面膜及其制备方法 |
CN110139569A (zh) * | 2017-08-09 | 2019-08-16 | 奥比托有限公司 | 黑树莓提取物、含有黑树莓提取物的美白剂和饮食品、黑树莓提取物的制造方法和使用了黑树莓提取物的美白方法 |
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