CN106925564A - A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave - Google Patents
A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave Download PDFInfo
- Publication number
- CN106925564A CN106925564A CN201511021251.9A CN201511021251A CN106925564A CN 106925564 A CN106925564 A CN 106925564A CN 201511021251 A CN201511021251 A CN 201511021251A CN 106925564 A CN106925564 A CN 106925564A
- Authority
- CN
- China
- Prior art keywords
- thin section
- petrographic thin
- thermometric
- micro
- unloading piece
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
Abstract
The invention belongs to sample preparation technology field, and in particular to a kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave.The present invention is comprised the following steps：Step 1, tool equipment prepare；Step 2, heating unloading piece；Step 3, ultrasonic wave cleaning；Step 4, dry arrangement.The present invention can improve the cleannes of petrographic thin section after operating efficiency and cleaning, it is to avoid the directly contact of human body and organic solvent.
Description
Technical field
The invention belongs to sample preparation technology field, and in particular to one kind is used for the micro- survey of inclusion enclave
The quick unloading piece of petrographic thin section and cleaning method of temperature.
Background technology
Fluid inclusion microthermometry is research on mineral deposits, and especially BIFhosted gold deposit research is adopted extensively
Research method.By fluid inclusion microthermometry, the formation of BIFhosted gold deposit can be obtained
Temperature, Salinity Data, it is possible to calculate the pressure of formation of ore deposits, and then estimate the shape in mineral deposit
Into depth, a kind of method being widely used in the mineral deposit research for being different type, different mineral.
Fluid inclusion microthermometry needs to carry out a series of samples preparation flow, including fluid bag
Wrap up in preparation, optical identification, unloading piece, cleaning, the cold and hot micro- thermometric of body piece.
In the prior art, to the cleaning of fluid inclusion piece, using artificial mechanism manner of cleaning up.
The fluid inclusion piece of Canadian resin-bonding will be used, by organic solvent (alcohol or acetone)
Some hours are soaked, after manually it is separated with glass slide afterwards, further using organic examination
After the petrographic thin section for unloading is rinsed in agent (alcohol or acetone), then petrographic thin section is pressed with hand
Mechanical friction is carried out on polishing cloth, to reach the purpose of cleaning petrographic thin section.This operation stream
Journey is less efficient, and the petrographic thin section obtained after cleaning usually remains substantial amounts of adhesive, seriously
The follow-up thermometric work of influence.Meanwhile, it is difficult to avoid that human body with organic solvent in operating process
Frequently contact, causes the potential threat to health of human body.
The content of the invention
Present invention solves the technical problem that：The present invention provides a kind of for the micro- thermometric of inclusion enclave
The quick unloading piece of petrographic thin section and cleaning method, it is possible to increase petrographic thin section after operating efficiency and cleaning
Cleannes, it is to avoid the directly contact of human body and organic solvent.
The technical solution adopted by the present invention：
A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave, including
Following steps：Step 1, tool equipment prepare；Step 2, heating unloading piece；It is step 3, super
Sound wave is cleaned；Step 4, dry arrangement.
, it is necessary to the capital equipment and articles for use that prepare include in the step 1：Alcolhol burner 1,
1 bottle of absolute ethyl alcohol, small beaker 1,1, ultrasonic activation instrument, tweezers 2, pocket knife 1
It is individual, heat-insulated water-stop sheet 2, marking pen 2, plastics valve bag is some.
The step 2 is comprised the following steps：
Step 2.1, the fluid inclusion piece that will be ground, are picked up, as what is lighted with tweezers
Uniform baking glass slide side on alcolhol burner, until adhesive melts, petrographic thin section loosens and is
Only；
Step 2.2, the petrographic thin section and glass slide that will be loosened after heating with pocket knife are peeled off, will
Petrographic thin section after stripping is put into the small beaker for filling absolute ethyl alcohol, and the glass after heating is carried
Piece is as on heat-insulated water-stop sheet；
Step 2.3, with marking pen be placed with peel off after petrographic thin section beaker on marked phase
The sample number into spectrum answered.
The step 3 is concretely comprised the following steps：
Clear water is added in supersonic wave cleaning machine, will fill what is peeled off in absolute ethyl alcohol and step 2
Petrographic thin section beaker is put into the basket in supersonic wave cleaning machine, and the petrographic thin section to peeling off is carried out
Ultrasonic activation is cleaned.
The step 4 is comprised the following steps：
Step 4.1, after step 3 end after, the beaker of absolute ethyl alcohol and petrographic thin section will be filled
Take out, be put on heat-insulated water-stop sheet, taken the petrographic thin section after ultrasonic wave is cleaned with tweezers
Go out, as on heat-insulated water-stop sheet, wait is dried；
Step 4.2, will dry after petrographic thin section, be fitted into plastics valve bag, use marking pen
The good corresponding sample number into spectrum of mark, completes operating process.
The concentration of the absolute ethyl alcohol is 95%；Heat-insulated water-stop sheet is microcrystal glass plate.
The clear water submergence basket height 2/3 of addition.
Beneficial effects of the present invention：
(1) present invention provides a kind of quick unloading piece of petrographic thin section for the micro- thermometric of inclusion enclave
And cleaning method, being capable of the unloading of lifting fluid inclusion enclave piece and the operating efficiency cleaned；
(2) present invention provides a kind of quick unloading piece of petrographic thin section for the micro- thermometric of inclusion enclave
And cleaning method, it is possible to increase the cleannes of petrographic thin section after cleaning；
(3) present invention provides a kind of quick unloading piece of petrographic thin section for the micro- thermometric of inclusion enclave
And cleaning method, the directly contact of human body and organic solvent can be avoided, it is to avoid organic solvent pair
The potential hazard of health.
Specific embodiment
The micro- thermometric of inclusion enclave is used for one kind that the present invention is provided below according to specific embodiment
The quick unloading piece of petrographic thin section and cleaning method be described further.
A kind of quick unloading piece of petrographic thin section for the micro- thermometric of inclusion enclave that the present invention is provided and
Cleaning method, comprises the following steps：
Step 1, tool equipment prepare：
Needing the capital equipment and articles for use of preparation includes：Alcolhol burner 1,1 bottle of absolute ethyl alcohol,
Small beaker 1,1, ultrasonic activation instrument, tweezers 2,1, pocket knife, heat-insulated water-stop sheet
2, marking pen 2, plastics valve bag is some.
Step 2, heating unloading piece：
Step 2.1, the fluid inclusion piece that will be ground, are picked up, as what is lighted with tweezers
Uniform baking glass slide side on alcolhol burner, until adhesive melts, petrographic thin section loosens and is
Only, generally require 3-5 seconds；
Step 2.2, the petrographic thin section and glass slide that will quickly be loosened after heating with pocket knife are peeled off,
Petrographic thin section after stripping is put into the small beaker for filling absolute ethyl alcohol, by the glass after heating
Slide glass is as on heat-insulated water-stop sheet；
Step 2.3, with marking pen be placed with peel off after petrographic thin section beaker on marked phase
The sample number into spectrum answered.
Step 3, ultrasonic wave cleaning：
Proper amount of clear water (being advisable to submerge basket height 2/3) is added in supersonic wave cleaning machine,
The petrographic thin section beaker peeled off in absolute ethyl alcohol and step 2 will be filled and be put into supersonic wave cleaning machine
In basket in, set time of vibration, to peel off petrographic thin section carry out ultrasonic activation cleaning,
The time of usual ultrasonic activation cleaning is 5 minutes.
Step 4, dry arrangement：
Step 4.1, after ultrasonic wave cleaning terminates, absolute ethyl alcohol and petrographic thin section will be filled
Beaker takes out, and is put on heat-insulated water-stop sheet, with tweezers that the rock after ultrasonic wave is cleaned is thin
Piece is taken out, and as on heat-insulated water-stop sheet, wait is dried；
Step 4.2, will dry after petrographic thin section, be fitted into plastics valve bag, use marking pen
The good corresponding sample number into spectrum of mark, completes operating process.
The concentration of absolute ethyl alcohol is 95%；Heat-insulated water-stop sheet is microcrystal glass plate.
Claims (7)
1. a kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave, its
It is characterised by：Comprise the following steps：
Step (1), tool equipment prepare；Step (2), heating unloading piece；It is step (3), super
Sound wave is cleaned；Step (4), dry arrangement.
2. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 1 is fast
Fast unloading piece and cleaning method, it is characterised in that：, it is necessary to the master for preparing in the step (1)
Wanting equipment and articles for use includes：Alcolhol burner 1,1 bottle of absolute ethyl alcohol, small beaker 1, ultrasound
Ripple vibration gauge 1, tweezers 2,1, pocket knife, heat-insulated water-stop sheet 2, marking pen 2,
Plastics valve bag is some.
3. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 1 is fast
Fast unloading piece and cleaning method, it is characterised in that：The step (2) comprises the following steps：
Step (2.1), the fluid inclusion piece that will be ground, are picked up with tweezers, as lighting
Alcolhol burner on uniform baking glass slide side, until adhesive melts, petrographic thin section loosens
Untill；
Step (2.2), the petrographic thin section and glass slide that will be loosened after heating with pocket knife are peeled off,
Petrographic thin section after stripping is put into the small beaker for filling absolute ethyl alcohol, by the glass after heating
Slide glass is as on heat-insulated water-stop sheet；
Step (2.3), with marking pen be placed with peel off after petrographic thin section beaker on mark
Corresponding sample number into spectrum.
4. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 1 is fast
Fast unloading piece and cleaning method, it is characterised in that：Step (3) concretely comprise the following steps：
Clear water is added in supersonic wave cleaning machine, stripping in absolute ethyl alcohol and step (2) will be filled
From petrographic thin section beaker be put into the basket in supersonic wave cleaning machine, to peel off petrographic thin section
Carry out ultrasonic activation cleaning.
5. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 1 is fast
Fast unloading piece and cleaning method, it is characterised in that：The step (4) comprises the following steps：
Step (4.1), after step (3) terminates, absolute ethyl alcohol and petrographic thin section will be filled
Beaker take out, be put on heat-insulated water-stop sheet, with tweezers by the rock after ultrasonic wave is cleaned
Thin slice is taken out, and as on heat-insulated water-stop sheet, wait is dried；
Step (4.2), will dry after petrographic thin section, be fitted into plastics valve bag, use mark
The good corresponding sample number into spectrum of pen mark, completes operating process.
6. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 2 is fast
Fast unloading piece and cleaning method, it is characterised in that：
The concentration of the absolute ethyl alcohol is 95%；Heat-insulated water-stop sheet is microcrystal glass plate.
7. a kind of petrographic thin section for the micro- thermometric of inclusion enclave according to claim 4 is fast
Fast unloading piece and cleaning method, it is characterised in that：The clear water submergence basket height 2/3 of addition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511021251.9A CN106925564A (en) | 2015-12-30 | 2015-12-30 | A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511021251.9A CN106925564A (en) | 2015-12-30 | 2015-12-30 | A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave |
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| Publication Number | Publication Date |
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| CN106925564A true CN106925564A (en) | 2017-07-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201511021251.9A Pending CN106925564A (en) | 2015-12-30 | 2015-12-30 | A kind of quick unloading piece of petrographic thin section and cleaning method for the micro- thermometric of inclusion enclave |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109856105A (en) * | 2017-11-30 | 2019-06-07 | 核工业北京地质研究院 | A kind of Microscopic Identification method of clay mineral |
| CN111751176A (en) * | 2019-03-26 | 2020-10-09 | 中国石油化工股份有限公司 | Slice moving device for rock inclusion slice |
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| WO2009014120A1 (en) * | 2007-07-25 | 2009-01-29 | Jokoh Co., Ltd. | Intrabath cleaning for tissue piece treating device |
| CN102554750A (en) * | 2010-12-29 | 2012-07-11 | 北京有色金属研究总院 | Double-surface polishing method for gallium antimonide wafer |
| CN103013813A (en) * | 2012-12-18 | 2013-04-03 | 中国科学院半导体研究所 | Method for manufacturing digital PCR (polymerase chain reaction) chip based on 3D (three-dimensional) printing platform |
| CN103157624A (en) * | 2011-12-19 | 2013-06-19 | 天津天维移动通讯终端检测有限公司 | Component cleaning method before component performance test |
| CN103489819A (en) * | 2013-09-18 | 2014-01-01 | 中国东方电气集团有限公司 | Method for temporarily bonding and debonding slice applied to semiconductor manufacturing process |
| CN103712841A (en) * | 2014-01-06 | 2014-04-09 | 中国石油大学(华东) | Production method for rock salt fluid inclusion flakes |
| CN104568545A (en) * | 2015-01-20 | 2015-04-29 | 中国石油大学(华东) | Manufacturing method of shale rock lamina |
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2015
- 2015-12-30 CN CN201511021251.9A patent/CN106925564A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3209841A1 (en) * | 1980-12-17 | 1983-09-29 | Hermann Julius Dr. 8400 Regensburg Berger | Method for embedding at least one tissue sample in paraffin and apparatus for carrying out this method |
| WO2009014120A1 (en) * | 2007-07-25 | 2009-01-29 | Jokoh Co., Ltd. | Intrabath cleaning for tissue piece treating device |
| CN102554750A (en) * | 2010-12-29 | 2012-07-11 | 北京有色金属研究总院 | Double-surface polishing method for gallium antimonide wafer |
| CN103157624A (en) * | 2011-12-19 | 2013-06-19 | 天津天维移动通讯终端检测有限公司 | Component cleaning method before component performance test |
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| CN103712841A (en) * | 2014-01-06 | 2014-04-09 | 中国石油大学(华东) | Production method for rock salt fluid inclusion flakes |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109856105A (en) * | 2017-11-30 | 2019-06-07 | 核工业北京地质研究院 | A kind of Microscopic Identification method of clay mineral |
| CN111751176A (en) * | 2019-03-26 | 2020-10-09 | 中国石油化工股份有限公司 | Slice moving device for rock inclusion slice |
| CN111751176B (en) * | 2019-03-26 | 2024-02-23 | 中国石油化工股份有限公司 | Rock inclusion thin slice moves piece device |
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Application publication date: 20170707 |