CN106905762A - A kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof - Google Patents
A kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof Download PDFInfo
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- CN106905762A CN106905762A CN201710197597.7A CN201710197597A CN106905762A CN 106905762 A CN106905762 A CN 106905762A CN 201710197597 A CN201710197597 A CN 201710197597A CN 106905762 A CN106905762 A CN 106905762A
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- chinese ink
- prepared chinese
- resistance
- dizzy dye
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof, the prepared Chinese ink of the resistance to dizzy dye is made up of the raw material of following weight portion：12 16 parts of carbon black, 10 15 parts of gelatine, 47 parts of silicate, 6 10 parts of ammonium chloride, 0.1 0.4 parts of camphorated oil, 0.1 0.5 parts of OIT, 0.2 0.5 parts of AEO, 0.3 0.8 parts of prodan, 60 70 parts of water, prepared Chinese ink stable performance prepared by the present invention, it is difficult layering, drawn a picture on paper, prepared Chinese ink will not occur diffusion dizzy dye after meeting water so that painting and calligraphy pieces can be saved preferably.
Description
Technical field
The present invention relates to prepared Chinese ink technical field, and in particular to a kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof.
Background technology
Ink is one of writing brush, ink stick, ink slab and paper, is indispensable element in Chinese Painting and Calligraphy works, and its traditional material has china ink stick and ink
Juice.China ink stick needs to be ground when in use, time-consuming, laborious very inconvenience.Clear and Bright thanks to Song beams brother's initiative ground second during the time ruled by Emperor Guang Xu
For painting and calligraphy creation material-prepared Chinese ink, due to that need not grind and easy to use, popularized in painting and calligraphy creation quickly.The biography of prepared Chinese ink
System processing technology is usually tung oil cigarette carbon black and animal gelatin as primary raw material mixes with a certain proportion of water, is added appropriate
Aromatic, becomes painting and calligraphy creation prepared Chinese ink after mixing.But existing prepared Chinese ink has still suffered from problems since the birth, such as in calligraphy
Prepared Chinese ink diffusion of the water loading on paper is met in production process or after the completion of calligraphy work dizzy dye occurs, influence the effect of calligraphy,
So as to limit the preservation of calligraphy creation, particularly painting and calligraphy pieces, after water is met, painting and calligraphy pieces are damaged completely, the treasure of forefathers
Product ruin once.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of prepared Chinese ink of resistance to dizzy dye, calligraphy wound is carried out using the prepared Chinese ink
Make, meet water indiffusion and dizzy dye phenomenon occurs.
To realize object above, the present invention is achieved by the following technical programs：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：Carbon black 12-16 parts, gelatine 10-15 parts, silicic acid
Salt 4-7 parts, ammonium chloride 6-10 parts, camphorated oil 0.1-0.4 parts, OIT 0.1-0.5 parts, AEO 0.2-
0.5 part, prodan 0.3-0.8 parts, water 60-70 parts.
Preferably, it is made up of the raw material of following weight portion：15 parts of carbon black, 12 parts of gelatine, 6 parts of silicate, 8 parts of ammonium chloride,
0.2 part of camphorated oil, 0.3 part of OIT, 0.3 part of AEO, 0.4 part of prodan, 65 parts of water.
Preferably, the silicate is selected from sodium metasilicate or potassium silicate.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 30-40 DEG C is heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains
Solution I；
2) excess water is heated to 80-90 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to dissolving
Stir, stand, be cooled to 30-40 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, high-speed stirred 20-30min, obtain final product.
Preferably, the step 3) high speed speed of agitator be 1200-1500rpm.
Beneficial effect of the present invention：The present invention add silicate in water have good colloidal dispersion, suspension and
Thickening property, it can occur coagulation in the presence of prodan and form protective layer on ink marks surface, effectively prevent moisture
The infiltration of son, the prepared Chinese ink prepared with the present invention is drawn a picture on paper, and prepared Chinese ink will not occur diffusion dizzy dye after meeting water so that painting and calligraphy are made
Product can be saved preferably.
Specific embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：15 parts of carbon black, 12 parts of gelatine, 6 parts of silicate,
8 parts of ammonium chloride, 0.2 part of camphorated oil, 0.3 part of OIT, 0.3 part of AEO, 0.4 part of prodan, water
65 parts.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 35 DEG C are heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains molten
Liquid I；
2) excess water is heated to 90 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Mix uniform, stand, be cooled to 35 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, control rotating speed to stir 30min for 1200rpm, obtain final product.
Embodiment 2：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：13 parts of carbon black, 14 parts of gelatine, 5 parts of sodium metasilicate,
7 parts of ammonium chloride, 0.1 part of camphorated oil, 0.1 part of OIT, 0.4 part of AEO, 0.3 part of prodan, water
62 parts.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 40 DEG C are heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains molten
Liquid I；
2) excess water is heated to 90 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Mix uniform, stand, be cooled to 40 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, control rotating speed to stir 25min for 1400rpm, obtain final product.
Embodiment 3：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：15 parts of carbon black, 11 parts of gelatine, 7 parts of sodium metasilicate,
8 parts of ammonium chloride, 0.2 part of camphorated oil, 0.2 part of OIT, 0.3 part of AEO, 0.5 part of prodan, water
68 parts.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 35 DEG C are heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains molten
Liquid I；
2) excess water is heated to 85 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Mix uniform, stand, be cooled to 35 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, control rotating speed to stir 25min for 1300rpm, obtain final product.
Embodiment 4：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：12 parts of carbon black, 15 parts of gelatine, 4 parts of potassium silicate,
10 parts of ammonium chloride, 0.1 part of camphorated oil, 0.5 part of OIT, 0.2 part of AEO, 0.8 part of prodan, water
60 parts.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 40 DEG C are heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains molten
Liquid I；
2) excess water is heated to 80 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Mix uniform, stand, be cooled to 30 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, control rotating speed to stir 20min for 1500rpm, obtain final product.
Embodiment 5：
A kind of prepared Chinese ink of resistance to dizzy dye, is made up of the raw material of following weight portion：16 parts of carbon black, 10 parts of gelatine, 7 parts of potassium silicate,
6 parts of ammonium chloride, 0.4 part of camphorated oil, 0.1 part of OIT, 0.5 part of AEO, 0.3 part of prodan, water
70 parts.
The preparation method of the prepared Chinese ink of resistance to dizzy dye, comprises the following steps：
1) suitable quantity of water is taken, 30 DEG C are heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains molten
Liquid I；
2) excess water is heated to 80 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Mix uniform, stand, be cooled to 30 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, poly alkyl alcohol
Oxygen vinethene, prodan, control rotating speed to stir 30min for 1200rpm, obtain final product.
Embodiment of the present invention 1-5 prepare resistance to dizzy dye prepared Chinese ink stable performance, at normal temperatures sealing preserve do not produce within three months
Life is precipitated, and each performance indications are not changed in, and after creating into painting and calligraphy, is met water and is difficult dizzy dye, so that the more conducively preservation of calligraphy and painting.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating
In any this actual relation or order.And, term " including ", "comprising" or its any other variant be intended to
Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those
Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention has been described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent to which part technical characteristic；And these modification or
Replace, do not make the spirit and scope of the essence disengaging various embodiments of the present invention technical scheme of appropriate technical solution.
Claims (5)
1. a kind of prepared Chinese ink of resistance to dizzy dye, it is characterised in that be made up of the raw material of following weight portion：Carbon black 12-16 parts, gelatine 10-
15 parts, silicate 4-7 parts, ammonium chloride 6-10 parts, camphorated oil 0.1-0.4 parts, OIT 0.1-0.5 parts, fatty alcohol polyoxy
Vinethene 0.2-0.5 parts, prodan 0.3-0.8 parts, water 60-70 parts.
2. the prepared Chinese ink of resistance to dizzy dye as claimed in claim 1, it is characterised in that be made up of the raw material of following weight portion：Carbon black 15
Part, 12 parts of gelatine, 6 parts of silicate, 8 parts of ammonium chloride, 0.2 part of camphorated oil, 0.3 part of OIT, AEO
0.3 part, 0.4 part of prodan, 65 parts of water.
3. the prepared Chinese ink of resistance to dizzy dye as claimed in claim 2, it is characterised in that the silicate is selected from sodium metasilicate or potassium silicate.
4. the preparation method of the prepared Chinese ink of the resistance to dizzy dye as described in claim 1-3 is any, it is characterised in that comprise the following steps：
1) suitable quantity of water is taken, 30-40 DEG C is heated to, ammonium chloride and silicate is added thereto to, stirring makes it fully dissolve, obtains solution
Ⅰ；
2) excess water is heated to 80-90 DEG C, is added thereto to gelatine, stirring adds carbon black, camphorated oil to continue to stir to dissolving
Uniformly, stand, be cooled to 30-40 DEG C, obtain solution II；
3) solution I is slowly added into solution II, it is stirring while adding, it is added thereto to OIT, fatty alcohol polyoxy second
Alkene ether, prodan, high-speed stirred 20-30min, obtain final product.
5. the prepared Chinese ink of resistance to dizzy dye as claimed in claim 4, it is characterised in that the step 3) high speed speed of agitator is
1200-1500rpm。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710197597.7A CN106905762A (en) | 2017-03-29 | 2017-03-29 | A kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710197597.7A CN106905762A (en) | 2017-03-29 | 2017-03-29 | A kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106905762A true CN106905762A (en) | 2017-06-30 |
Family
ID=59195524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710197597.7A Pending CN106905762A (en) | 2017-03-29 | 2017-03-29 | A kind of prepared Chinese ink of resistance to dizzy dye and preparation method thereof |
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| CN (1) | CN106905762A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108864820A (en) * | 2018-06-27 | 2018-11-23 | 广州市美帮祈富文仪有限公司 | A kind of painting appliance has the anti-of dispersibility to eat color ink juice and its manufacturing method by mistake |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05331404A (en) * | 1992-06-01 | 1993-12-14 | Zebura Kk | Gel-like pigment ink for water-based ball point pen |
| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
-
2017
- 2017-03-29 CN CN201710197597.7A patent/CN106905762A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05331404A (en) * | 1992-06-01 | 1993-12-14 | Zebura Kk | Gel-like pigment ink for water-based ball point pen |
| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 夏正兵等: "《建筑材料（第2版）》", 31 August 2016, 东南大学出版社 * |
| 李东光等: "《精细化工产品配方与工艺（一）》", 30 June 2000, 化学工业出版社 * |
| 葛霖: "《筑炉手册》", 30 April 1996, 冶金工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108864820A (en) * | 2018-06-27 | 2018-11-23 | 广州市美帮祈富文仪有限公司 | A kind of painting appliance has the anti-of dispersibility to eat color ink juice and its manufacturing method by mistake |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170630 |
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| RJ01 | Rejection of invention patent application after publication |