CN106978009A - A kind of prepared Chinese ink of high gloss and preparation method thereof - Google Patents
A kind of prepared Chinese ink of high gloss and preparation method thereof Download PDFInfo
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- CN106978009A CN106978009A CN201710329989.4A CN201710329989A CN106978009A CN 106978009 A CN106978009 A CN 106978009A CN 201710329989 A CN201710329989 A CN 201710329989A CN 106978009 A CN106978009 A CN 106978009A
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- prepared chinese
- chinese ink
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- deionized water
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
Abstract
The present invention provides a kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：10 15 parts of colouring agent, 10 15 parts of Arabic gum, 10 15 parts of graphene dispersing solution, 13 parts of lignosulfonates, 25 parts of borax, 25 parts of AEO, 0.05 0.2 parts of aromatic, 15 25 parts of deionized water, the invention also discloses its preparation method.Prepared Chinese ink writing attachment fastness produced by the present invention is high, and light is elegant, painting and calligraphy all suitable, ink markss are easily done, are easy to open up and mount, and with certain antibacterial ability, beneficial to the permanent preservation of prepared Chinese ink.
Description
Technical field
The present invention relates to prepared Chinese ink technical field, and in particular to a kind of prepared Chinese ink of high gloss and preparation method thereof.
Background technology
Prepared Chinese ink has long history in China, is indispensable element in Chinese Painting and Calligraphy works, the calligraphy of Chinese,
Drawing all be unable to do without prepared Chinese ink, is typically all with ink in rice paper, newsprint or common paper.The prepared Chinese ink used on domestic market
It is made up of mostly the raw material such as charcoal or black smoke, animal glue and anticorrosive additive, existing prepared Chinese ink, which is existed, to be had the disadvantage：In conventional writing paper
Or drawing brightness or fastness are inadequate on rice paper.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of prepared Chinese ink of high gloss and preparation method thereof.
To realize object above, the present invention is achieved by the following technical programs：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：10-15 parts of colouring agent, Arabic gum 10-15
Part, 10-15 parts of graphene dispersing solution, 1-3 parts of lignosulfonates, 2-5 parts of borax, 2-5 parts of AEO, fragrance
0.05-0.2 parts of agent, 15-25 parts of deionized water.
Preferably, it is made up of the raw material of following parts by weight：13 parts of colouring agent, 14 parts of Arabic gum, graphene dispersing solution 12
Part, 2 parts of lignosulfonates, 4 parts of borax, 3 parts of AEO, 0.1 part of aromatic, 20 parts of deionized water.
Preferably, the preparation method of the graphene dispersing solution is as follows：Graphene is added in deionized water, is heated to
40-50 DEG C of ultrasonic disperse 40-60min, adds neopelex and sodium borohydride thereto, and ultrasonic 30-40min disperses
Mixing, centrifugation, takes upper liquid, produces.
Preferably, the graphene and the mass ratio of deionized water are 2-3：2.
Preferably, the centrifugation rate is 600-800rpm.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 80-90 DEG C, Arabic gum is added thereto, stirred to molten
Solution, is cooled to normal temperature, obtains solution I；
2) add a colorant in balance deionized water, the ultrasonic disperse 30-40min at 40-50 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 10-20min after adding every time, then to it
Middle addition graphene dispersing solution, ultrasonic disperse 10-20min is eventually adding lignosulfonates, AEO, virtue
Pastil, stirs 20-30min, produces.
Beneficial effect of the present invention：The graphene dispersing solution added in prepared Chinese ink of the present invention is in addition to antibacterial characteristics, additionally it is possible to
The glossiness of prepared Chinese ink is significantly improved, lignosulfonates can improve the rate of drying of ink marks, and obtained prepared Chinese ink writes attachment fastness
Height, light is elegant, painting and calligraphy all suitable, ink markss are easily done, are easy to open up and mount, and with certain antibacterial ability, beneficial to the long Kubo of prepared Chinese ink
Deposit.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：13 parts of colouring agent, 14 parts of Arabic gum, stone
Black 12 parts of alkene dispersion liquid, 2 parts of lignosulfonates, 4 parts of borax, 3 parts of AEO, 0.1 part of aromatic, deionization
20 parts of water.
The preparation method of graphene dispersing solution is as follows：In the deionized water that graphene is added to etc. to quality, 45 are heated to
DEG C ultrasonic disperse 50min, adds neopelex and sodium borohydride thereto, ultrasonic 30min dispersion mixings, centrifugation,
It is 700rpm to control centrifugation rate, takes upper liquid, produces.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 85 DEG C, Arabic gum is added thereto, stirring is extremely dissolved,
Normal temperature is cooled to, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 35min at 45 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 15min after adding every time, then thereto
Graphene dispersing solution is added, ultrasonic disperse 20min is eventually adding lignosulfonates, AEO, aromatic,
20min is stirred, is produced.
Embodiment 2：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：12 parts of colouring agent, 12 parts of Arabic gum, stone
Black 11 parts of alkene dispersion liquid, 2 parts of lignosulfonates, 3 parts of borax, 3.5 parts of AEO, 0.1 part of aromatic, go from
Sub- 18 parts of water.
The preparation method of graphene dispersing solution is as follows：By graphene according to 2：3 mass ratio is added in deionized water, plus
Heat adds neopelex and sodium borohydride to 40 DEG C of ultrasonic disperse 60min thereto, ultrasonic 30min dispersion mixings,
Centrifugation, it is 800rpm to control centrifugation rate, takes upper liquid, produces.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 80 DEG C, Arabic gum is added thereto, stirring is extremely dissolved,
Normal temperature is cooled to, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 40min at 40 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 10min after adding every time, then thereto
Graphene dispersing solution is added, ultrasonic disperse 20min is eventually adding lignosulfonates, AEO, aromatic,
30min is stirred, is produced.
Embodiment 3：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：14 parts of colouring agent, 12 parts of Arabic gum, stone
Black 12 parts of alkene dispersion liquid, 1.5 parts of lignosulfonates, 3.5 parts of borax, 3 parts of AEO, 0.15 part of aromatic,
22 parts of deionized water.
The preparation method of graphene dispersing solution is as follows：By graphene according to 4:5 mass ratio is added in deionized water, plus
Heat adds neopelex and sodium borohydride to 50 DEG C of ultrasonic disperse 40min thereto, ultrasonic 40min dispersion mixings,
Centrifugation, it is 600rpm to control centrifugation rate, takes upper liquid, produces.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 90 DEG C, Arabic gum is added thereto, stirring is extremely dissolved,
Normal temperature is cooled to, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 30min at 50 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 15min after adding every time, then thereto
Graphene dispersing solution is added, ultrasonic disperse 15min is eventually adding lignosulfonates, AEO, aromatic,
20min is stirred, is produced.
Embodiment 4：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：10 parts of colouring agent, 15 parts of Arabic gum, stone
Black 10 parts of alkene dispersion liquid, 3 parts of lignosulfonates, 2 parts of borax, 5 parts of AEO, 0.05 part of aromatic, go from
Sub- 25 parts of water.
The preparation method of graphene dispersing solution is as follows：By graphene according to 2:3 mass ratio is added in deionized water, plus
Heat adds neopelex and sodium borohydride to 40 DEG C of ultrasonic disperse 50min thereto, ultrasonic 35min dispersion mixings,
Centrifugation, it is 700rpm to control centrifugation rate, takes upper liquid, produces.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 85 DEG C, Arabic gum is added thereto, stirring is extremely dissolved,
Normal temperature is cooled to, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 30min at 45 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 10min after adding every time, then thereto
Graphene dispersing solution is added, ultrasonic disperse 20min is eventually adding lignosulfonates, AEO, aromatic,
20min is stirred, is produced.
Embodiment 5：
A kind of prepared Chinese ink of high gloss, is made up of the raw material of following parts by weight：15 parts of colouring agent, 10 parts of Arabic gum, stone
Black 15 parts of alkene dispersion liquid, 1 part of lignosulfonates, 5 parts of borax, 2 parts of AEO, 0.2 part of aromatic, deionization
15 parts of water.
The preparation method of graphene dispersing solution is as follows：By graphene according to 1:1 mass ratio is added in deionized water, heating
To 40 DEG C of ultrasonic disperse 60min, neopelex and sodium borohydride are added thereto, ultrasonic 40min dispersion mixings, from
The heart, it is 800rpm to control centrifugation rate, takes upper liquid, produces.
The preparation method of the prepared Chinese ink of high gloss, step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 85 DEG C, Arabic gum is added thereto, stirring is extremely dissolved,
Normal temperature is cooled to, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 30min at 40 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, ultrasonic disperse 20min after adding every time, then thereto
Graphene dispersing solution is added, ultrasonic disperse 20min is eventually adding lignosulfonates, AEO, aromatic,
20min is stirred, is produced.
Glossiness performance test is carried out to prepared Chinese ink prepared by the embodiment of the present invention, carried out using QB/T2860-2007 standards
Color detects that prepared Chinese ink color and luster prepared by 1-5 of the embodiment of the present invention is all higher than 1.46, and the prepared Chinese ink prepared with the embodiment of the present invention
Write on blank sheet of paper, after natural drying, ink marks is black and light.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those
Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (6)
1. a kind of prepared Chinese ink of high gloss, it is characterised in that be made up of the raw material of following parts by weight：10-15 parts of colouring agent, I
Primary glue 10-15 parts, 10-15 parts of graphene dispersing solution, 1-3 parts of lignosulfonates, 2-5 parts of borax, AEO
2-5 parts, 0.05-0.2 parts of aromatic, 15-25 parts of deionized water.
2. the prepared Chinese ink of high gloss as claimed in claim 1, it is characterised in that be made up of the raw material of following parts by weight：Coloring
13 parts of agent, 14 parts of Arabic gum, 12 parts of graphene dispersing solution, 2 parts of lignosulfonates, 4 parts of borax, AEO
3 parts, 0.1 part of aromatic, 20 parts of deionized water.
3. the prepared Chinese ink of high gloss as claimed in claim 2, it is characterised in that the preparation method of the graphene dispersing solution is such as
Under：Graphene is added in deionized water, 40-50 DEG C of ultrasonic disperse 40-60min is heated to, dodecyl is added thereto
Benzene sulfonic acid sodium salt and sodium borohydride, ultrasonic 30-40min dispersion mixings, centrifugation take upper liquid, produced.
4. the prepared Chinese ink of high gloss as claimed in claim 3, it is characterised in that the graphene and the mass ratio of deionized water
For 2-3：2.
5. the prepared Chinese ink of high gloss as claimed in claim 3, it is characterised in that the centrifugation rate is 600-800rpm.
6. the preparation method of the prepared Chinese ink of the high gloss as described in claim 1-5 is any, it is characterised in that step is as follows：
1) borax is dissolved in appropriate amount of deionized water, is heated to 80-90 DEG C, Arabic gum is added thereto, stirring is cold to dissolving
But to normal temperature, solution I is obtained；
2) add a colorant in balance deionized water, the ultrasonic disperse 30-40min at 40-50 DEG C obtains solution II；
3) solution II is slowly added into solution I in three times, then ultrasonic disperse 10-20min after adding every time adds thereto
Enter graphene dispersing solution, ultrasonic disperse 10-20min is eventually adding lignosulfonates, AEO, aromatic,
20-30min is stirred, is produced.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710329989.4A CN106978009A (en) | 2017-05-11 | 2017-05-11 | A kind of prepared Chinese ink of high gloss and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710329989.4A CN106978009A (en) | 2017-05-11 | 2017-05-11 | A kind of prepared Chinese ink of high gloss and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN106978009A true CN106978009A (en) | 2017-07-25 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710329989.4A Pending CN106978009A (en) | 2017-05-11 | 2017-05-11 | A kind of prepared Chinese ink of high gloss and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111423766A (en) * | 2020-05-12 | 2020-07-17 | 同曦集团有限公司 | Graphene modified ink and preparation method thereof |
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|---|---|---|---|---|
| CN1958687A (en) * | 2006-11-21 | 2007-05-09 | 祁育新 | Multifunctional prepared Chinese ink |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
| CN104058392A (en) * | 2014-06-12 | 2014-09-24 | 同济大学 | Method for preparing graphene colloid dispersion liquid |
| CN105907175A (en) * | 2016-06-30 | 2016-08-31 | 叶文佳 | Bright carbonic ink |
| CN106519840A (en) * | 2016-10-31 | 2017-03-22 | 陈少双 | Plastic paint and preparation method thereof |
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2017
- 2017-05-11 CN CN201710329989.4A patent/CN106978009A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1958687A (en) * | 2006-11-21 | 2007-05-09 | 祁育新 | Multifunctional prepared Chinese ink |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
| CN104058392A (en) * | 2014-06-12 | 2014-09-24 | 同济大学 | Method for preparing graphene colloid dispersion liquid |
| CN105907175A (en) * | 2016-06-30 | 2016-08-31 | 叶文佳 | Bright carbonic ink |
| CN106519840A (en) * | 2016-10-31 | 2017-03-22 | 陈少双 | Plastic paint and preparation method thereof |
Non-Patent Citations (2)
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|---|
| 候海云等: "《表面活性剂物理化学基础》", 31 August 2014, 西安交通大学出版社 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111423766A (en) * | 2020-05-12 | 2020-07-17 | 同曦集团有限公司 | Graphene modified ink and preparation method thereof |
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Application publication date: 20170725 |
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