CN106902379B - A kind of konjaku glucomannan environmental protection diaper and preparation method thereof - Google Patents

A kind of konjaku glucomannan environmental protection diaper and preparation method thereof Download PDF

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CN106902379B
CN106902379B CN201710115501.8A CN201710115501A CN106902379B CN 106902379 B CN106902379 B CN 106902379B CN 201710115501 A CN201710115501 A CN 201710115501A CN 106902379 B CN106902379 B CN 106902379B
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konjaku glucomannan
preparation
diaper
environmental protection
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CN106902379A (en
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庞杰
王林
童彩玲
吴佳煜
倪永升
穆若郡
刘畅达
龚静妮
洪馨
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Jiangxi Ruiteng new material development Co.,Ltd.
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Fujian Agriculture and Forestry University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/22Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
    • A61L15/28Polysaccharides or their derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/18Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing inorganic materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/20Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing organic materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/44Medicaments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/62Compostable, hydrosoluble or hydrodegradable materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/20Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
    • A61L2300/30Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/404Biocides, antimicrobial agents, antiseptic agents

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
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Abstract

The present invention relates to a kind of konjaku glucomannan environmental protection diapers and preparation method thereof.The preparation method of konjaku glucomannan environmental protection diaper, including prepare colloidal sol, prepare auxiliary material, prepare konjaku glucomannan complex liquid, the preparation on surface layer, preparation middle layer, waterproof infiltration layer preparation, prepare environmentally friendly diaper.The present invention using konjaku glucomannan there are the physicochemical properties such as viscosity is high, water suction is more, expansion is fast to improve the bioavilability and retentiveness of konjaku glucomannan by electrospun nanofibers film;Konjaku glucomannan nano fibrous membrane/bottom counnter attack infiltration layer space structure is sufficient, breathes freely, antibacterial, is aided with menthol, Cortex Phellodendri, honeysuckle, Moschus etc., also have many advantages, such as it is refrigerant, solve prickly heat, be anti-inflammatory antibacterial.It is convenient, at low cost that the present invention draws materials, and has the advantages that antibiotic property is good, preparation process is simple, nontoxic, biodegradable and bioavilability is good.

Description

A kind of konjaku glucomannan environmental protection diaper and preparation method thereof
Technical field
The present invention relates to a kind of articless for babies and preparation method thereof, and in particular to a kind of konjaku glucomannan environmental protection diaper And preparation method thereof, belong to articles for babies technical field.
Background technique
As the improvement of people's living standards, the development of diaper product reaches its maturity, it is deep to be liked by the majority of consumers. Diaper made from conventional method is made of surface soft cotton layer, absorbent core layer, waterproof layer and bottom cloth layer.Urine currently on the market The hygroscopic agent overwhelming majority used in not wet is hydroscopic high-molecular resin, and water imbibition is high, but since super absorbent resin is tool There are many low crosslinking degree of hydrophilic radical or the high molecular polymers of partially crystallizable, therefore inevitably contain some pairs of skins Influential chemical substance.Also appearance uses modified starch to substitute hydroscopic high-molecular resin as the hygroscopic agent of diaper, to the greatest extent at present Nothing is to the harmful substance of skin in pipe modified starch, but its water imbibition is undesirable, meanwhile, modified starch is expensive, it is difficult to push away Extensively.
Konjaku glucomannan is cheap, from a wealth of sources, has very high retentiveness, dilatancy, thickening property, but konjaku Portugal There are many limitations for the conventional machining techniques of sweet glycan, keep konjaku glucomannan utilization efficiency extremely low, and functional characteristic is not yet It can highlight.
Application No. is 201610182215.9 patent of invention " vapor-permeable type diaper " (applyings date: 2016.03.28), are situated between Continued a kind of vapor-permeable type diaper, and skin care layer of cloth, absorbent core layer and waterproof layer of cloth, the absorbent core layer are arranged from top to bottom and includes The first layer of cloth, the second layer of cloth and the third layer of cloth being arranged from top to bottom, first layer of cloth and second layer of cloth pass through elasticity The first beanbag of multiple accommodating water-absorbent materials is made in linear slit, and second layer of cloth and the third layer of cloth pass through elastic sewer At the second beanbag of multiple accommodating water-absorbent materials, first beanbag and the second beanbag are arranged in a staggered manner, solve existing The problem of baby's diaper poor air permeability.But production method is excessively complicated, and without antibiotic property, level of application is by very big limit System.
Application No. is 201410453036.5 patent of invention " a kind of baby's diaper and preparation method thereof " (applying date: 2014.09.09), a kind of antibacterial, ventilative baby's diaper product are provided, by selecting suitable antibacterial agent, to liner parent Water non-woven fabrics carries out antibacterial pretreatment, makes it have high-efficiency antimicrobial, breathes freely comfortably, can the advantages of not stimulating, have no toxic side effect Effectively prevention infant skin infection.But this diaper is complicated for operation, high financial profit, is not suitable for large scale investment production.
Application No. is 201320093594.6 patent " a kind of bacteriostasis and health-care baby diaper " (applying date: 2013.03.01), a kind of bacteriostasis and health-care baby's diaper with health care and therapeutic effect is described, by increasing in soft cotton layer If one layer of bacteriostasis and health-care layer for being coated with chitin fiber extract, plays effective inhibition to bacterium, and chitin fiber Chitosan element in extract and other effects composition has anti-inflammatory, promotes the growth of epithelium, accelerate the Healing of wound, meanwhile, Also there is chitin fiber removing toxic substances to seep rash, treat atropurpureus macula, sore, eczema and other effects.But such diaper is excessively complicated, Inconvenience is used, and bioavilability is not high.
With the development of economy, the continuous improvement of quality of life, people have higher requirement to diaper.To meet baby Child's demand, urgent need provide a kind of product for having further effect than traditional diaper, promote refrigerant, antibacterial, solve prickly heat Effect provides the space of development for Konjac Glucomannan.
Summary of the invention
The object of the present invention is to provide a kind of konjaku glucomannan environmental protection diapers and preparation method thereof, to solve existing skill The deficiency of art.The affinity of product of the present invention is high, not only can refrigerant, solution prickly heat, antibacterial compared to other diapers, moreover it is possible to thoroughly Gas significantly improves the effect of anti-bacterial, anti-itching, improves bioavilability.
To achieve the above object, the present invention adopts the following technical scheme that.
A kind of preparation method of konjaku glucomannan environmental protection diaper of the present invention, it is characterised in that preparation step is as follows:
(1) it prepares colloidal sol: by quality component, taking 10-20 parts of konjaku glucomannans, 300-500 parts of deionized waters are added, stir Dissolution is mixed, colloidal sol is made;
(2) auxiliary material is prepared: by 3-5 parts of sodium citrates, 1-3 portions of Cortex Phellodendris, 5-7 parts of menthols, 3-5 portions of honeysuckles, 2-4 portions of musk deers Perfume (or spice) crushes, and crosses 80 meshes, spare;
(3) it prepares konjaku glucomannan complex liquid: taking 15-25 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, And deionized water is added, it stirs evenly, forms the medical fluid that mass fraction is 100 parts, medical fluid is set in supercentrifuge, with 2000- 3000r/min centrifugation degassing 30-40min, obtains konjaku glucomannan complex liquid;
(4) preparation on surface layer: 8-12 parts of colloidal sol in step (1) are taken in sterile syringe, with ES series electrostatic spinning Equipment prepares konjaku glucomannan nano fibrous membrane, and the surface layer of environmentally friendly diaper is made;
(5) it prepares middle layer: taking 0.8-1.2 parts of konjaku glucomannan complex liquid of step (3), 40-50 DEG C of water-bath side is stirred It mixes side to be added in 98.8-99.2 parts of deionized waters, 0.5-1.5h is stirred with the speed of 300-400r/min, is subsequently placed in 50- After vacuumizing 5-15min in 60 DEG C of vacuum drying ovens, with ES series electrospinning device, prepares konjaku glucomannan load medicine and receive Rice tunica fibrosa, is made the middle layer of environmentally friendly diaper;
(6) preparation of waterproof infiltration layer: 0.8-1.2 parts of colloidal sol in step (1) are taken to gather with sodium alginate 0.2-0.4 parts, shell It is 0.2-0.6 parts sugared, 0.4-0.6 parts of calcium chloride, dissolve blending film forming, the waterproof infiltration layer of environmentally friendly diaper is made;
(7) prepare environmentally friendly diaper: surface layer that step (4) (5) (6) is obtained, middle layer, waterproof infiltration layer are urinated not as environmental protection Three layers are fixed together using elastica, konjaku glucomannan environmental protection diaper are made by wet structural framework.
Advantages of the present invention: a kind of konjaku glucomannan environmental protection diaper of the invention has using konjaku glucomannan The physicochemical properties such as viscosity is high, water suction is more, expansion is fast improve konjaku glucomannan by electrospun nanofibers film Bioavilability and retentiveness;Konjaku glucomannan nano fibrous membrane/bottom counnter attack infiltration layer space structure is sufficient, breathes freely, is anti- Bacterium, while also there is refrigerant, solution prickly heat and gas permeability.Konjaku glucomannan performance is stablized, manufactured konjaku glucomannan environmental protection Type diaper bioavilability is high, anti-microbial property is good and water imbibition is strong.Konjaku glucomannan environment-friendly type diaper of the invention, Middle menthol acts on skin or mucous membrane, there is refrigerant itching-relieving action;Cortex Phellodendri, honeysuckle can strengthen immunity, anti-inflammatory, it is antipyretic, only Blood etc.;Moschus is anti-inflammatory antibacterial.The present invention have draw materials it is convenient, at low cost, antibiotic property is good, preparation process is simple and it is nontoxic, The biodegradable and good advantage of bioavilability.
Konjaku glucomannan environmental protection diaper of the invention and existing diaper correlated performance test comparison knot on the market Fruit is as shown in table 1.
The konjaku glucomannan environmental protection diaper of the invention of table 1 and existing diaper correlated performance test comparison on the market As a result
By above-mentioned test comparison, konjaku glucomannan environmental protection diaper of the invention, bioavilability, antibiotic property, All other diapers are more excellent more on the market in the indexs such as water imbibition, potential market.
Specific embodiment
In order to sufficiently disclose a kind of konjaku glucomannan environmental protection diaper and preparation method thereof of the invention, below with reference to reality Applying example, invention is further described in detail.
Embodiment 1, a kind of preparation method of konjaku glucomannan environmental protection diaper, comprising the following steps:
(1) it prepares colloidal sol: taking 15 parts of konjaku glucomannans, 400 parts of deionized waters are added, colloidal sol is made in stirring and dissolving;
(2) it prepares auxiliary material: 4 parts of sodium citrates, 2 portions of Cortex Phellodendris, 6 parts of menthols, 4 portions of honeysuckles, 3 parts of Moschus crushes, mistake 80 meshes, it is spare;
(3) it prepares konjaku glucomannan complex liquid: taking 15 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, and Deionized water is added, stirs evenly, forms the medical fluid that mass fraction is 100 parts, medical fluid is set in supercentrifuge, with 2500r/min Centrifugation degassing 35min, obtains konjaku glucomannan complex liquid;
(4) preparation on surface layer: 10 parts of colloidal sol in step (1) are taken in sterile syringe, is set with ES series electrostatic spinning Standby konjaku glucomannan nano fibrous membrane is prepared, the surface layer of environmentally friendly diaper is made;
(5) it prepares middle layer: taking 1.0 parts of konjaku glucomannan complex liquids in step (3), 45 DEG C of water-baths are added while stirring Into 99.0 parts of deionized waters, 1.0h is stirred with the speed of 300-400r/min, is subsequently placed in 55 DEG C of vacuum drying ovens and takes out After vacuum 10min, konjaku glucomannan medicament-carrying nano-fiber membrane is prepared with ES series electrospinning device, environmentally friendly diaper is made Middle layer;
(6) preparation of waterproof infiltration layer: removing 1.0 parts of the colloidal sol and 0.3 part of sodium alginate in step (1), 0.4 part of chitosan, 0.5 part of calcium chloride dissolves blending film forming, and the waterproof infiltration layer of environmentally friendly diaper is made.
(7) prepare environmentally friendly diaper: surface layer that step (4) (5) (6) is obtained, middle layer, waterproof infiltration layer are urinated not as environmental protection Three layers are fixed together using elastica, konjaku glucomannan environmental protection diaper are made by wet structural framework.
Embodiment 2, a kind of preparation method of konjaku glucomannan environmental protection diaper, comprising the following steps:
(1) it prepares colloidal sol: taking 10 parts of konjaku glucomannans, 300 parts of deionized waters are added, colloidal sol is made in stirring and dissolving;
(2) it prepares auxiliary material: 3 parts of sodium citrates, 1 portion of Cortex Phellodendri, 5 parts of menthols, 3 portions of honeysuckles, 2 parts of Moschus crushes, mistake 80 meshes, it is spare;
(3) it prepares konjaku glucomannan complex liquid: taking 20 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, and Deionized water is added, stirs evenly, forms the medical fluid that mass fraction is 100 parts, medical fluid is set in supercentrifuge, with 2000r/min Centrifugation degassing 30min, obtains konjaku glucomannan complex liquid;
(4) preparation on surface layer: 8 parts of colloidal sol in step (1) are taken in sterile syringe, with ES series electrospinning device Konjaku glucomannan nano fibrous membrane is prepared, the surface layer of environmentally friendly diaper is made;
(5) it prepares middle layer: taking 0.8 part of konjaku glucomannan complex liquid in step (3), 40 DEG C of water-baths are added while stirring Into 98.8 parts of deionized waters, 0.5h is stirred with the speed of 300r/min, is subsequently placed in 50 DEG C of vacuum drying ovens and vacuumizes After 5min, with ES series electrospinning device, konjaku glucomannan medicament-carrying nano-fiber membrane is prepared, is made in environmentally friendly diaper Interbed;
(6) preparation of waterproof infiltration layer: removing 0.8 part of the colloidal sol and 0.2 part of sodium alginate in step (1), 0.2 part of chitosan, 0.4 part of calcium chloride dissolves blending film forming, and the waterproof infiltration layer of environmentally friendly diaper is made.
(7) prepare environmentally friendly diaper: surface layer that step (4) (5) (6) is obtained, middle layer, waterproof infiltration layer are urinated not as environmental protection Three layers are fixed together using elastica, konjaku glucomannan environmental protection diaper are made by wet structural framework.
Embodiment 3, a kind of preparation method of konjaku glucomannan environmental protection diaper, comprising the following steps:
(1) it prepares colloidal sol: taking 20 parts of konjaku glucomannans, 500 parts of deionized waters are added, colloidal sol is made in stirring and dissolving;
(2) it prepares auxiliary material: 5 parts of sodium citrates, 3 portions of Cortex Phellodendris, 7 parts of menthols, 5 portions of honeysuckles, 4 parts of Moschus crushes, mistake 80 meshes, it is spare;
(3) it prepares konjaku glucomannan complex liquid: taking 25 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, and Deionized water is added, stirs evenly, forms the medical fluid that mass fraction is 100 parts, medical fluid is set in supercentrifuge, with 3000r/min Centrifugation degassing 40min, obtains konjaku glucomannan complex liquid;
(4) preparation on surface layer: 12 parts of colloidal sol in step (1) are taken in sterile syringe, is set with ES series electrostatic spinning Standby konjaku glucomannan nano fibrous membrane is prepared, the surface layer of environmentally friendly diaper is made;
(5) it prepares middle layer: taking 1.2 parts of konjaku glucomannan complex liquids in step (3), 50 DEG C of water-baths add while stirring Enter into 99.2 parts of deionized waters, 1.5h is stirred with the speed of 400r/min, is subsequently placed in 60 DEG C of vacuum drying ovens and takes out very After empty 15min, konjaku glucomannan medicament-carrying nano-fiber membrane is prepared with ES series electrospinning device, environmentally friendly diaper is made Middle layer;
(6) preparation of waterproof infiltration layer: removing 1.2 parts of the colloidal sol and 0.4 part of sodium alginate in step (1), 0.6 part of chitosan, 0.6 part of calcium chloride dissolves blending film forming, and the waterproof infiltration layer of environmentally friendly diaper is made.
(7) prepare environmentally friendly diaper: surface layer that step (4) (5) (6) is obtained, middle layer, waterproof infiltration layer are urinated not as environmental protection Three layers are fixed together using elastica, konjaku glucomannan environmental protection diaper are made by wet structural framework.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, is all covered by the present invention.

Claims (7)

1. a kind of preparation method of konjaku glucomannan environmental protection diaper, it is characterised in that preparation step is as follows:
(1) it prepares colloidal sol: by quality component, taking 10-20 parts of konjaku glucomannans, 300-500 parts of deionized waters are added, stir molten Solution, is made colloidal sol;
(2) auxiliary material is prepared: by 3-5 parts of sodium citrates, 1-3 portions of Cortex Phellodendris, 5-7 parts of menthols, 3-5 portions of honeysuckles, 2-4 parts of Moschus, It crushes, crosses 80 meshes, it is spare;
(3) it prepares konjaku glucomannan complex liquid: taking 15-25 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, and add Enter deionized water, stir evenly, forms the medical fluid that mass fraction is 100 parts, medical fluid is set in supercentrifuge, with 2000-3000r/ Min centrifugation degassing 30-40min, obtains konjaku glucomannan complex liquid;
(4) preparation on surface layer: 8-12 parts of colloidal sol in step (1) are taken in sterile syringe, with ES series electrospinning device Konjaku glucomannan nano fibrous membrane is prepared, the surface layer of environmentally friendly diaper is made;
(5) it prepares middle layer: taking 0.8-1.2 parts of konjaku glucomannan complex liquid of step (3), 40-50 DEG C of water-bath is while stirring It is added in 98.8-99.2 parts of deionized waters, 0.5-1.5h is stirred with the speed of 300-400r/min, is subsequently placed in 50-60 DEG C After vacuumizing 5-15min in vacuum drying oven, with ES series electrospinning device, it is fine to prepare konjaku glucomannan medicament-carried nano Film is tieed up, the middle layer of environmentally friendly diaper is made;
(6) 0.8-1.2 parts of colloidal sol and sodium alginate 0.2-0.4 parts, chitosan in step (1) preparation of waterproof infiltration layer: are taken 0.2-0.6 parts, 0.4-0.6 parts of calcium chloride dissolve blending film forming, the waterproof infiltration layer of environmentally friendly diaper are made;
(7) prepare environmentally friendly diaper: surface layer that step (4) (5) (6) is obtained, middle layer, waterproof infiltration layer are as environmental protection diaper Three layers are fixed together using elastica, konjaku glucomannan environmental protection diaper are made by structural framework.
2. a kind of preparation method of konjaku glucomannan environmental protection diaper according to claim 1, it is characterised in that described It prepares colloidal sol: taking 15 parts of konjaku glucomannans, 400 parts of deionized waters are added, colloidal sol is made in stirring and dissolving.
3. a kind of preparation method of konjaku glucomannan environmental protection diaper according to claim 1, it is characterised in that described It prepares auxiliary material: 4 parts of sodium citrates, 2 portions of Cortex Phellodendris, 6 parts of menthols, 4 portions of honeysuckles, 3 parts of Moschus crushing, cross 80 meshes.
4. a kind of preparation method of konjaku glucomannan environmental protection diaper according to claim 1, it is characterised in that described It prepares konjaku glucomannan complex liquid: taking 15 parts of colloidal sol of step (1), the auxiliary material of step (2) is added, and deionization is added Water stirs evenly, and forms the medical fluid that mass fraction is 100 parts, sets medical fluid in supercentrifuge, is centrifuged and is deaerated with 2500r/min 35min obtains konjaku glucomannan complex liquid.
5. a kind of preparation method of konjaku glucomannan environmental protection diaper according to claim 1, it is characterised in that described Preparation middle layer: 1.0 parts of konjaku glucomannan complex liquids in step (3) are taken, 45 DEG C of water-baths are added to 99.0 parts while stirring and go In ionized water, 1.0h is stirred with the speed of 300-400r/min, is subsequently placed in 55 DEG C of vacuum drying ovens and vacuumizes 10min Afterwards, konjaku glucomannan medicament-carrying nano-fiber membrane is prepared with ES series electrospinning device, the middle layer of environmentally friendly diaper is made.
6. a kind of preparation method of konjaku glucomannan environmental protection diaper according to claim 1, it is characterised in that described The preparation of waterproof infiltration layer: 1.0 parts of colloidal sol and the 0.3 part of sodium alginate in step (1), 0.4 part of chitosan, 0.5 part of calcium chloride are taken Blending film forming is dissolved, the waterproof infiltration layer of environmentally friendly diaper is made.
7. the konjaku glucomannan environmental protection diaper that either as described in claim 1-6 prepared by method.
CN201710115501.8A 2017-03-01 2017-03-01 A kind of konjaku glucomannan environmental protection diaper and preparation method thereof Active CN106902379B (en)

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CN107375736A (en) * 2017-07-21 2017-11-24 福建农林大学 A kind of konjaku glucomannan medicine pastes and preparation method thereof more enough
CN107307062B (en) * 2017-08-08 2020-06-16 福建农林大学 Konjac glucomannan shrimp preservative and preparation method thereof
CN109825955B (en) * 2019-02-03 2021-09-17 南通纺织丝绸产业技术研究院 Antibacterial and anti-allergic paper diaper for adults and preparation method thereof
CN112155860A (en) * 2020-09-30 2021-01-01 陈孝庆 Antibacterial environment-friendly diaper with strong hygroscopicity
CN112976703B (en) * 2021-02-25 2021-10-01 徐州中国矿大岩土工程新技术发展有限公司 Modular plant-growing blanket

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CN1197676A (en) * 1997-04-27 1998-11-04 李向东 Dressing made of konjak and its preparation
CN1218658A (en) * 1998-11-16 1999-06-09 张慧荣 Personal health article using konjak as raw material
CN2512413Y (en) * 2001-11-01 2002-09-25 上海兰格科技有限公司 Antiseptic high absorption composite material
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