CN106898948B - Super-radiance light emitting diode or laser epitaxial structure and preparation method thereof - Google Patents
Super-radiance light emitting diode or laser epitaxial structure and preparation method thereof Download PDFInfo
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- CN106898948B CN106898948B CN201510953170.6A CN201510953170A CN106898948B CN 106898948 B CN106898948 B CN 106898948B CN 201510953170 A CN201510953170 A CN 201510953170A CN 106898948 B CN106898948 B CN 106898948B
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01S—DEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
- H01S5/00—Semiconductor lasers
- H01S5/30—Structure or shape of the active region; Materials used for the active region
- H01S5/34—Structure or shape of the active region; Materials used for the active region comprising quantum well or superlattice structures, e.g. single quantum well [SQW] lasers, multiple quantum well [MQW] lasers or graded index separate confinement heterostructure [GRINSCH] lasers
- H01S5/343—Structure or shape of the active region; Materials used for the active region comprising quantum well or superlattice structures, e.g. single quantum well [SQW] lasers, multiple quantum well [MQW] lasers or graded index separate confinement heterostructure [GRINSCH] lasers in AIIIBV compounds, e.g. AlGaAs-laser, InP-based laser
- H01S5/34333—Structure or shape of the active region; Materials used for the active region comprising quantum well or superlattice structures, e.g. single quantum well [SQW] lasers, multiple quantum well [MQW] lasers or graded index separate confinement heterostructure [GRINSCH] lasers in AIIIBV compounds, e.g. AlGaAs-laser, InP-based laser with a well layer based on Ga(In)N or Ga(In)P, e.g. blue laser
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Abstract
The invention discloses a kind of super-radiance light emitting diode or laser epitaxial structures and preparation method thereof.The epitaxial structure includes the Si substrate set gradually from top to bottom, AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, ducting layer on N-shaped or i type InGaN lower waveguide layer, active area, p-type or i type InGaN, p-type AlGaN electronic barrier layer, optical confinement layer, p-type or N-shaped GaN or InGaN contact layer on p-type AlGaN.Preferably, the active area uses i type InGaN/GaN multiple quantum wells or quantum dot active region.The thickness and the super-radiance light emitting diode of the GaN ducting layer or the ridged item of laser are wide quite.By the epitaxial structure of the invention, the carrier of injection can be effectively limited in very thin active area, the light intensity of its compound generation can expand in first wave guide structure from active area, and because GaN ducting layer therein is thicker, which can significantly improve the beam quality of super-radiance light emitting diode, laser.
Description
Technical field
Present invention relates particularly to a kind of super-radiance light emitting diode or the epitaxial structures and its preparation process of laser, belong to
Semiconductor photoelectronic device field.
Background technique
Super-radiance light emitting diode has many advantages, such as that wide spectrum, power are big as a kind of special light sources.Semiconductor laser
Be widely used in due to the advantages that small in size, light-weight, photoelectric conversion efficiency is high, the service life is long and tunable wave length pumping,
The military fields such as communication, material processing, medical and laser ranging, laser radar, laser guidance and laser night vision.But it partly leads
In body laser on vertical pn-junction in-plane (lateral x), since active area thickness d is relatively thin, diffraction is very strong, thus
Beam divergence angle is larger, and usually 30~45 °.And on being parallel to pn-junction lateral (y), wide item is usually several microns, this ratio
Active layer thickness d is several times greater, and to more than ten times, diffraction is relatively weak, and correspondingly its dispersion angle is 10~20 °.Therefore, lead to
What normal semiconductor laser issued is the fan-like beam of the ellipse of a branch of (30~45 °) × (10~20 °), as shown in Figure 2.
In most of important application occasions, such as light-pumped solid state laser, focusing, collimation, fiber coupling, the light beam of semiconductor laser
It requires using lens system collimation, focusing or shaping, this significantly limits it in the direct application in many fields.Therefore,
Beam quality is improved, the direct application range of high power semiconductor lasers can be not only extended, design optics can also be exempted
The trouble of orthopedic systems, meaning is very great, and this is also this field one of problem urgently to be resolved.
Summary of the invention
The main purpose of the present invention is to provide a kind of super-radiance light emitting diode or laser epitaxial structure and its preparations
Method, to overcome deficiency in the prior art.
For realization aforementioned invention purpose, the technical solution adopted by the present invention includes:
The embodiment of the invention provides a kind of super-radiance light emitting diode or laser epitaxial structures comprising from top to bottom
Wave under the Si substrate, AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or the i type InGaN that set gradually
Ducting layer on conducting shell, active area, p-type or i type InGaN, p-type AlGaN electronic barrier layer, optical confinement layer, p-type on p-type AlGaN
Or N-shaped GaN or InGaN contact layer;Wherein the AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer form first wave guide knot
Structure, the InGaN ducting layer constitute second waveguide structure.
In some more preferred embodiments, the active area uses i type InGaN/GaN multiple quantum wells or quantum dot
Active area.
In some more preferred embodiments, the super-radiance light emitting diode or laser have ridge structure,
The thickness and the super-radiance light emitting diode of the GaN ducting layer or the ridged item of laser are wide quite." suitable " herein
It is interpreted as " of substantially equal ", such as can be the two thickness difference within 1 μm.
The embodiment of the invention also provides a kind of sides for preparing the super-radiance light emitting diode or laser epitaxial structure
Method comprising: AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or i are sequentially formed on a si substrate
Ducting layer, p-type AlGaN electronic barrier layer, p-type AlGaN glazing on type InGaN lower waveguide layer, active area, p-type or i type InGaN
Learn limiting layer, p-type or N-shaped GaN or InGaN contact layer;Wherein the AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer group
At first wave guide structure, the InGaN ducting layer constitutes second waveguide structure.
Compared with prior art, the present invention at least have the advantages that by using on Si substrate AlGaN buffer layer,
GaN ducting layer and N-shaped AlGaN layer are as super-radiance light emitting diode or the first wave guide structure of laser epitaxial structure, InGaN
Ducting layer is as second waveguide structure, and since GaN ducting layer is thicker (wide quite with ridged item), which can significantly be mentioned
High light beam quality (i.e. far-field spot is closer round).
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of laser in an exemplary embodiments of the invention;
Fig. 2 is a kind of far-field spot figure of conventional semiconductor laser;
Description of symbols: Si substrate 101, AlN buffer layer 102, the first AlGaN layer 103, the second AlGaN layer 104, GaN
The upper ducting layer 109 of ducting layer 105, N-shaped AlGaN layer 106, InGaN lower waveguide layer 107, active area 108, InGaN, p-type AlGaN
Optical confinement layer 111, p-type GaN contact layer 112 on electronic barrier layer 110, p-type AlGaN.
Specific embodiment
The one aspect of the embodiment of the present invention provides a kind of super-radiance light emitting diode or laser epitaxial structure, from
Under to it is upper successively include: Si substrate, AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped GaN (or AlGaN) layer, N-shaped
(or i type) InGaN lower waveguide layer, i type InGaN/GaN multiple quantum wells/quantum dot active region, the upper waveguide of p-type (or i type) InGaN
Optical confinement layer, p-type (or N-shaped) GaN (or InGaN) contact layer on layer, p-type AlGaN electronic barrier layer, p-type AlGaN.
Wherein, the AlN buffer layer on Si substrate and AlGaN buffer layer can be used as super-radiance light emitting diode or laser
Lower light field limiting layer (Cladding layer), which can significantly improve the light limitation capability of active area.
Meanwhile AlGaN buffer layer, GaN ducting layer and the N-shaped AlGaN layer on Si substrate can be used as superradiation light-emitting two
The first wave guide structure of pole pipe or laser structure, InGaN ducting layer is as second waveguide structure.
By the use of heretofore described epitaxial structure, the carrier of injection, which can be effectively limited in, very thin to be had
In source region (about 10~100nm, preferably smaller than 100nm), the light intensity of their compound generations can expand to first wave from active area
In guide structure, since the GaN ducting layer in first wave guide structure is thicker (wide quite with ridged item), which can be significant
Improve the beam quality of super-radiance light emitting diode, laser (i.e. far-field spot is closer round).
The embodiment of the present invention is prepared outside the super-radiance light emitting diode or laser another aspect provides a kind of
The method for prolonging structure, may include steps of:
1) use Si body material as substrate;
2) use AlN layers as buffer layer on Si;
3) use AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer as first wave guide structure;
4) use N-shaped (or i type) InGaN as lower waveguide layer;
5) use i type InGaN/GaN Quantum Well or quantum dot as active area;
6) use p-type (or i type) InGaN as upper ducting layer;
7) use p-type AlGaN as electronic barrier layer;
8) use p-type AlGaN as upper optical confinement layer;
9) use p-type (either N-shaped) GaN (or InGaN) as contact layer.
Further, in abovementioned steps 3) in, the doping of GaN can be N-shaped or undoped.
Further, in abovementioned steps 4) in, the doping of InGaN can be N-shaped or undoped, component can with gradual change,
The mode of gradual change can be that step can also be continous way.
Further, in abovementioned steps 5) in, it can be used InGaN/GaN Quantum Well as active area blue wave band,
And it can be used InGaN/GaN Quantum Well or quantum dot as active area green light and red spectral band.
Further, in abovementioned steps 6) in, the doping of InGaN can be p-type or undoped, component can with gradual change,
The mode of gradual change can be that step can also be continous way.
Further, in abovementioned steps 7) in, AlGaN electronic barrier layer can use superlattices, can also use thick-layer.
Further, in abovementioned steps 8) in, p-type AlGaN upper limiting layer material can be used AlGaN/GaN superlattices or
AlGaN thick-layer also includes the AlGaN material using Al component-gradient.
Further, in abovementioned steps 9) in, N-shaped also can be used in addition to using p-type GaN (or InGaN) in contact layer
Material use tunnel junctions realize contact.
Below with reference to an exemplary embodiments, the technical scheme of the present invention will be further described:
The embodiment is related to a kind of ridge blue laser (excitation wavelength~450nm), and epitaxial structure can refer to Fig. 1 institute
Show, that is, include be sequentially formed on Si substrate 101 AlN buffer layer 102, the first AlGaN layer 103, the second AlGaN layer 104,
The upper ducting layer 109 of GaN ducting layer 105, N-shaped AlGaN layer 106, InGaN lower waveguide layer 107, active area 108, InGaN, p-type
Optical confinement layer 111, p-type GaN contact layer 112 on AlGaN electronic barrier layer 110, p-type AlGaN.
It is a kind of to grow that form the technique of the epitaxial structure may include following steps using MOCVD:
1) the AlN buffer layer of thickness about 265nm is grown in Si body substrate;
2) AlGaN layer of thickness about 210nm is grown, Al group is divided into 50%;
3) AlGaN layer of thickness about 325nm is grown, Al group is divided into 20%;
4) thick about 3.0 μm of the GaN ducting layer of growth, this layer undope;
5) thick about 1.5 μm of the AlGaN layer of growth, mixing Si concentration is 3 × 1018/cm3;
7) the InGaN lower waveguide layer for growing thickness about 80nm, mixing Si concentration is 5 × 1017/cm3;
8) multi-quantum well active region is grown, the group of well layer InGaN is divided into 16%, and 2 pairs in total;
9) ducting layer on the InGaN of thickness about 100nm is grown, this layer undopes;
10) the p-type AlGaN electronic barrier layer for growing thickness about 20nm, mixing Mg concentration is 2 × 1019/cm3;
11) optical confinement layer on the p-type AlGaN of thickness about 600nm is grown, mixing Si concentration is 1 × 1019/cm3;
12) the p-type GaN contact layer for growing thickness about 20nm, mixing Mg concentration is 5 × 1019/cm3。
After the growth for completing aforementioned epitaxial structure, also make to be formed into using various suitable methods known in the art
Product device, process flow may include the following operation successively carried out: top electrode production;Litho pattern;Ridge etching, ridge
About 4 μm of width;Substrate thinning;Lower electrode fabrication;Cleaved cavity surface, chamber are about 600 μm;Cavity surface film coating, front and back Cavity surface plate height respectively
Reflectance coating is 90%, 70%;Sliver.
The ridge blue laser is tested it can be found that its excitation wavelength about 450.5nm, threshold current density is about
3.2kA/cm2, threshold operative voltage about 4.7V, the symmetry of far-field spot is more preferable, approximate circle.
The above is only a specific embodiment of the invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (17)
1. a kind of epitaxial structure of super-radiance light emitting diode, it is characterised in that including set gradually from top to bottom Si substrate,
AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or i type InGaN lower waveguide layer, active area, p-type
Or optical confinement layer, p-type or N-shaped GaN or InGaN on ducting layer on i type InGaN, p-type AlGaN electronic barrier layer, p-type AlGaN
Contact layer;Wherein the AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer form first wave guide structure, the InGaN wave
Conducting shell constitutes second waveguide structure;The super-radiance light emitting diode has inclination or curved ridge structure, and contact thereon is
Positive electrode, lower contact is negative electrode or positive and negative electrode is contact in the same direction;Also, thickness and the institute of the GaN ducting layer
The ridged item for stating super-radiance light emitting diode is wide quite.
2. the epitaxial structure of super-radiance light emitting diode according to claim 1, it is characterised in that: the active area uses
I type InGaN/GaN multiple quantum wells or quantum dot active region.
3. a kind of epitaxial structure of laser, it is characterised in that including set gradually from top to bottom Si substrate, AlN buffer layer,
AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or i type InGaN lower waveguide layer, active area, p-type or i type InGaN
Upper ducting layer, p-type AlGaN electronic barrier layer, optical confinement layer, p-type or N-shaped GaN or InGaN contact layer on p-type AlGaN;Its
Described in AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer form first wave guide structure, the InGaN ducting layer constitutes the
Two waveguiding structures;The laser has ridge structure, and contact thereon is positive electrode, and lower contact is negative electrode or positive and negative electricity
Pole is contact in the same direction;Also, the ridged item of the thickness of the GaN ducting layer and the laser is wide quite.
4. the epitaxial structure of laser according to claim 3, it is characterised in that: the active area uses i type InGaN/
GaN multiple quantum wells or quantum dot active region.
5. the epitaxial structure of laser according to claim 3, it is characterised in that: the laser is that Si base is blue, green, red
Optical band laser, launch wavelength are 400nm~700nm.
6. a kind of preparation method of the epitaxial structure of super-radiance light emitting diode, characterized by comprising: on a si substrate successively
Form AlN buffer layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or i type InGaN lower waveguide layer, active
Ducting layer on area, p-type or i type InGaN, p-type AlGaN electronic barrier layer, optical confinement layer, p-type or N-shaped GaN on p-type AlGaN
Or InGaN contact layer;Wherein the AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer form first wave guide structure, described
InGaN ducting layer constitutes second waveguide structure;The super-radiance light emitting diode has inclination or curved ridge structure, thereon
Contact is positive electrode, and lower contact is negative electrode or positive and negative electrode is contact in the same direction;The thickness of the GaN ducting layer and institute
The ridged item for stating super-radiance light emitting diode is wide quite.
7. preparation method according to claim 6, it is characterised in that: the active area uses i type InGaN/GaN Multiple-quantum
Trap or quantum dot active region.
8. preparation method according to claim 6, it is characterised in that: the material of the GaN ducting layer be selected from n-type doping or
The undoped GaN of person.
9. preparation method according to claim 6, it is characterised in that: the group in the upper ducting layer and/or lower waveguide layer
Part is in step or continous way gradual change.
10. preparation method according to claim 6, it is characterised in that: the electronic barrier layer have superlattice structure or
Thick-layer structure.
11. preparation method according to claim 6, it is characterised in that: the material of the upper optical confinement layer is selected from
The AlGaN material of AlGaN/GaN superlattices, AlGaN thick-layer or Al component-gradient.
12. a kind of preparation method of the epitaxial structure of laser, characterized by comprising: it is slow to sequentially form AlN on a si substrate
Rush layer, AlGaN buffer layer, GaN ducting layer, N-shaped AlGaN layer, N-shaped or i type InGaN lower waveguide layer, active area, p-type or i type
The upper ducting layer of InGaN, p-type AlGaN electronic barrier layer, optical confinement layer, p-type or N-shaped GaN or InGaN contact on p-type AlGaN
Layer;Wherein the AlGaN buffer layer, GaN ducting layer and N-shaped AlGaN layer form first wave guide structure, the InGaN ducting layer
Constitute second waveguide structure;The laser has ridge structure, and contact thereon is positive electrode, and lower contact is negative electrode, or
Positive and negative electrode is contact in the same direction;The thickness of the GaN ducting layer and the ridged item of the laser are wide quite.
13. preparation method according to claim 12, it is characterised in that: the active area uses i type InGaN/GaN volume
Sub- trap or quantum dot active region.
14. preparation method according to claim 12, it is characterised in that: the material of the GaN ducting layer is selected from n-type doping
Or undoped GaN.
15. preparation method according to claim 12, it is characterised in that: in the upper ducting layer and/or lower waveguide layer
Component is in step or continous way gradual change.
16. preparation method according to claim 12, it is characterised in that: the electronic barrier layer have superlattice structure or
Thick-layer structure.
17. preparation method according to claim 12, it is characterised in that: the material of the upper optical confinement layer is selected from
The AlGaN material of AlGaN/GaN superlattices, AlGaN thick-layer or Al component-gradient.
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CN108767659A (en) * | 2018-06-04 | 2018-11-06 | 清华大学 | A method of utilizing two-dimensional material interlayer epitaxial growth laser |
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