CN106890477B - Cortex Eucommiae natural medicinal ingredients extraction process and its extract equipment - Google Patents
Cortex Eucommiae natural medicinal ingredients extraction process and its extract equipment Download PDFInfo
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- CN106890477B CN106890477B CN201710043738.XA CN201710043738A CN106890477B CN 106890477 B CN106890477 B CN 106890477B CN 201710043738 A CN201710043738 A CN 201710043738A CN 106890477 B CN106890477 B CN 106890477B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
- B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01D11/02—Solvent extraction of solids
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Abstract
A kind of Cortex Eucommiae natural medicinal ingredients extraction process, the following steps are included: (1) Cortex Eucommiae raw material enzymolysis processing, (2) separation, filtering of enzymolysis liquid, (3) filtering enzymolysis liquid low temperature concentration, (4) disinfection of concentrate room temperature, precipitation and separation, (5) drug ingedient refine.A kind of Cortex Eucommiae natural medicinal ingredients extract equipment, including gutta-percha and natural medicinal ingredients separator, gutta-percha and natural medicinal ingredients separator side are equipped with spiral centrifugal separator, spiral centrifugal separator side is equipped with sand core and filtering bag filter, the side of sand core and filtering bag filter is equipped with membrane filter, membrane filter side is equipped with drug vacuum concentrator, drug vacuum concentrator side is equipped with the stainless-steel vacuum blender with stirring, stainless-steel vacuum blender side is equipped with Cortex Eucommiae natural drug fine powder load device, the side of Cortex Eucommiae natural drug fine powder load device is equipped with ethyl alcohol purification equipment；The present invention can fast and efficiently extract the Cortex Eucommiae natural medicinal ingredients in enzymolysis liquid.
Description
Technical field
The present invention relates to a kind of drug extraction process and equipment, it is especially a kind of for Cortex Eucommiae natural medicinal ingredients extract
Technique and the equipment of extraction.
Background technique
Eucommiaceae plant Cortex Eucommiae (Eucommia ulmoides Oliver), is the distinctive medicinal material in China and economic resources,
The characteristics of integrating economic forest and Timber stands, Cortex Eucommiae also have many days for having special efficacy to human body other than gutta-percha
Right active medicine, have on the market Hydrolyze method, alcohol extracting method, three kinds of enzymatic isolation method Cortex Eucommiae raw material is decomposed, with water extraction and alcohol extracting
Method is compared, and the natural products in enzymolysis and extraction Cortex Eucommiae is much more.It is analyzed from extraction components, all substances can be in enzymatic hydrolysis
Corresponding substance peak is found in chromatographic absorption peak, and is also only present in enzyme-extracting solution there are four types of substance, so enzymatic hydrolysis mentions
The type for the Cortex Eucommiae natural products for taking method to extract is apparently higher than the extracting method of pure water, that is to say, that is apparently higher than common Du
Secondary decocting for Chinese herbal medicine method, and extracted amount is also more much higher than decocting method；Alcohol dissolves the very capable of chlorophyll, it is likely to chlorophyll
Interference, but chlorophyll have bitter taste be unfavorable for Cortex Eucommiae drug administration, nevertheless, the substance classes of alcohol extract still do not have
The Cortex Eucommiae natural products substance for having enzymatic isolation method to extract is more, so often being carried out at enzymatic hydrolysis using enzymatic isolation method to Cortex Eucommiae raw material on the market
Reason, however Cortex Eucommiae natural drug abstraction process is complicated, is all to be carried out using distinct device substep to Cortex Eucommiae natural drug on the market,
It can not effectively integrate and reach whole process progress, human interference is bigger, low efficiency, and the amount of substance of extraction is few, cannot
Enough a large amount of, high efficiency extraction Cortex Eucommiae natural medicinal ingredients, and substep extracts Cortex Eucommiae natural drug the requirements for people are relatively high,
To cause extraction cost high, and the waste that each step generates can not be used effectively, to cause the very big of resource
Waste.
Summary of the invention
The shortcomings that the invention solves the above-mentioned prior arts provides a kind of a large amount of, high efficiency extraction Cortex Eucommiae natural drug fine powder
Cortex Eucommiae natural medicinal ingredients extraction process and its extract equipment, meet manufacturing enterprise for Cortex Eucommiae natural drug extracted amount
Greatly, demand at low cost.
The technical scheme adopted by the invention to solve the technical problem: this Cortex Eucommiae natural medicinal ingredients extraction process, including
Following steps:
(1) Cortex Eucommiae raw material Cortex Eucommiae raw material enzymolysis processing: is put into the interior bucket of gutta-percha and natural medicinal ingredients separator
Place, add water to submerge Cortex Eucommiae raw material, gradually respectively by containing protease, cellulase, pectase, cutinase solution according to 1:1
Proportion carry out being mixed into mixed solution, PH buffer is configured to using food-grade citric acid and sodium citrate and is poured into mixed liquor
In, being made into pH value is 3.2,4.0,5.5 3 kind of enzymatic hydrolysis solution, and enzymatic hydrolysis solution is poured into gutta-percha and natural medicinal ingredients separate
In the water of device, enzymatic hydrolysis is constantly stirred to Cortex Eucommiae raw material, and molten to the enzymatic hydrolysis in gutta-percha and natural medicinal ingredients separator
Liquid carries out heating water bath, and for heating and temperature control at 40 DEG C~50 DEG C, every kind of enzyme digestion reaction time is 4~6 hours；
(2) separation, filtering of enzymolysis liquid: Cortex Eucommiae colloid stays in gutta-percha and natural medicinal ingredients point after Cortex Eucommiae raw material enzymatic hydrolysis
From device, its interior enzymolysis liquid be discharged by the leakage fluid dram of gutta-percha and natural medicinal ingredients separator and pass through spiral continuously from
Heart separation removes slag and clast, and the separating liquid after spiral centrifugal slagging-off carries out sand core and filter bag carries out coarse filtration, by coarse filtration
Enzymolysis liquid is filtered by membrane filter again, obtains the brown clear solution transparent, without suspended solid residue by refined filtration；
(3) filtering enzymolysis liquid low temperature concentration；Clear and transparent brown solution injection of medicine vacuum concentrator (5), drug
Vacuum concentrator (5) carries out cryogenic vacuum concentration to the enzymolysis liquid of filtering；
(4) disinfection of concentrate room temperature, precipitation and separation: the enzymolysis liquid injection of medicine precipitation and separation device (6) after low temperature is concentrated
In, 95% edible ethanol is added and constantly the enzymolysis liquid after concentration is stirred under normal pressure, the rear static enzyme made after concentration
Significantly reducing in liquid underflow without effective component solubility is solved, is precipitated from the concentrated extract of enzyme-extracting solution, and molecular state
Natural Cortex Eucommiae drug ingedient then can be sufficiently mixed and dissolve with ethanol solution under conditions of being sufficiently stirred；
(5) drug ingedient refines: extracting supernatant liquor, supernatant liquor is then injected into the load of Cortex Eucommiae natural drug fine powder
In device (7), cyclodextrin is loaded to supernatant and carries out heating water bath processing under vacuum conditions, heating and temperature control is at 55 DEG C
~60 DEG C, the alcohol and residual moisture in clear liquid are evaporated, and obtain Cortex Eucommiae fine powder.
This Cortex Eucommiae natural medicinal ingredients extract equipment, including gutta-percha and natural medicinal ingredients separator, gutta-percha
Be equipped with spiral centrifugal separator with the side of natural medicinal ingredients separator, the side of spiral centrifugal separator be equipped with sand core and
The side of filtering bag filter, sand core and filtering bag filter is equipped with membrane filter, and the side of membrane filter is concentrated in vacuo equipped with drug
Device, the side of drug vacuum concentrator are provided with the stainless-steel vacuum blender of rabbling mechanism, the side of stainless-steel vacuum blender
Portion is equipped with ethyl alcohol purification equipment, and the side of stainless-steel vacuum blender is equipped with Cortex Eucommiae natural drug fine powder load device；Gutta-percha
Enzymolysis liquid holding vessel, spiral centrifugal separator and sand are equipped between natural medicinal ingredients separator and spiral centrifugal separator
It is equipped with coarse filtration liquid holding vessel between core and filtering bag filter, refined filtration liquid is equipped between sand core and filtering bag filter and membrane filter and is stored up
Tank is deposited, fine filtrate holding vessel is equipped between membrane filter and drug vacuum concentrator, the side of drug vacuum concentrator is equipped with
Hot-water cylinder and water tank with heating function and temperature controller；The leakage fluid dram and enzymatic hydrolysis of gutta-percha and natural medicinal ingredients separator
Communicating pipe one is installed between the top of liquid holding vessel, the inlet of the bottom of enzymolysis liquid holding vessel and spiral centrifugal separator it
Between communicating pipe two is installed, between the liquid outlet of spiral centrifugal separator and the top of coarse filtration liquid holding vessel be installed communicating pipe
Three, communicating pipe four, sand core and filter bag are installed between the bottom of coarse filtration liquid holding vessel and sand core and the inlet of filtering bag filter
Communicating pipe five, the bottom of refined filtration liquid holding vessel and film mistake are installed between the liquid outlet of filter and the top of refined filtration liquid holding vessel
Communicating pipe six, the company of being equipped between membrane filter liquid outlet and the top of fine filtrate holding vessel are installed between filter inlet
Siphunculus seven, is equipped with triple valve at the inlet of drug vacuum concentrator, the bottom of fine filtrate holding vessel and triple valve one end
Communicating pipe eight is installed between entrance, is installed between another end opening of triple valve and the input end of stainless-steel vacuum blender
There is communicating pipe nine, hot water conveying pipe and efferent duct, drug vacuum concentrator are installed between hot-water cylinder and drug vacuum concentrator
Water storage cavity and water storage pot bottom between communicating pipe ten is installed, at the top of the bottom of water tank and hot-water cylinder between be equipped with and be connected to
Guan Shiyi；Cortex Eucommiae natural drug fine powder load device includes the bucket with opening, is fixed with a cavity in the cavity of bucket
It is divided into two-part partition up and down, the circle shape partition of tapered setting is equipped at the cavity above partition, encloses the top of shape partition
End is fixed on the inner peripheral wall of bucket, and the bottom end of circle shape partition is fixed on the top surface of partition, on the inside of circle shape partition and outer
Side is respectively the cavity one and cavity two separated, is provided with the through-hole being connected to cavity one on partition, the opening of bucket is equipped with
For the end cap of closed opening, it is fixed with bracket on bucket, band valve cylinder is fixed on bracket, the piston rod with valve cylinder is solid
It is scheduled on end cap top surface, vertical bar is rotatably connected on end cap, the bottom end of vertical bar is rotatably connected to the briquetting with taper, the cone of briquetting
It spends identical as the circle taper of shape partition and cooperates with the inner surface of circle shape partition, vertical bar is electric by the servo for being fixed on end cap top
Machine drives, and stirring sheet is fixed in the bottom wheel profile surface of vertical bar, installs having heaters in cavity two；The side of bucket be equipped with by
The alcohol vapour collector that condenser, cooler, separator, accumulator form, the condenser and cavity of alcohol vapour collector
It is connected with connecting tube between one, between the accumulator and ethyl alcohol purification equipment of alcohol vapour collector is installed communicating pipe 12；
Liquid suction pipe is installed between stainless-steel vacuum blender and Cortex Eucommiae natural drug fine powder load device；Triple valve and drug vacuum are dense
Solenoid valve one is installed between the inlet of contracting device, solenoid valve two is installed on communicating pipe one, drawing liquid is installed on communicating pipe two
Pump one is equipped with drawing liquid pump two on communicating pipe three, drawing liquid pump three is equipped on communicating pipe four, is equipped with drawing liquid pump on communicating pipe five
Four, drawing liquid pump five is installed on communicating pipe six, drawing liquid pump six is installed on communicating pipe seven, solenoid valve is installed on communicating pipe nine
Three, drawing liquid pump 12 is installed on communicating pipe ten, drawing liquid pump is installed on liquid suction pipe, drawing liquid pump is installed on communicating pipe 11
Eight, drawing liquid pump nine is installed on communicating pipe 12, apparatus for vacuum producing is installed on Cortex Eucommiae natural drug fine powder load device.Here it shuts out
Secondary glue and natural medicinal ingredients separator are using application No. is 201521047806.2 products；Here spiral centrifugal separator
For equipment general on the market, Science and Technology Co., Ltd., Zhejiang sky environmental protection equipment Co., Ltd are protected using Zhejiang threefold ring
The product of equal companies；Here sand core and filtering bag filter are common apparatus on the market, and the limited public affairs of filtering technique are quite strangled using Shanghai
The equipment of department, Wuxi Hua Ao environmental protection equipment Chang Deng company；Membrane filter is product general on the market, using Hefei wind and cloud film point
Product from companies such as Technology Co., Ltd., Hangzhou triumphant conjunctiva isolation technics Co., Ltds；Drug vacuum concentrator is on the market
General product, using the production of the companies such as Shanghai Jia Pai automation equipment Co., Ltd, Hefei calf light industry and machinery Co., Ltd
Product；Stainless-steel vacuum blender common apparatus on the market, using Dongguan Dongzheng Environmental Protection Equipment Technology Products Co., Ltd., the huge person of outstanding talent in Wenzhou
The product of the companies such as mechanical Science and Technology Ltd.；Here ethyl alcohol purification equipment is common apparatus on the market, dry using Hangzhou Qianjiang
The product of the companies such as dry equipment Co., Ltd, the European rich Machinery Co., Ltd. in Zhengzhou.Cortex Eucommiae natural drug fine powder load device
Use process: being injected into the supernatant of the natural medicinal ingredients containing Cortex Eucommiae in cavity one by liquid suction pipe, and Cyclodextrin is passed through Sheng
Feed opening on charging basket is added in cavity one, and is started servo motor and driven vertical bar rotation, not using the stirring sheet on vertical bar
Disconnected stirring cyclodextrin and supernatant make its mixing, and at the same time, heating agent and starting in heating cavity two vacuumize machine,
It extracts the air in cavity one out, so that cavity one is in class vacuum state and make the heating agent in cavity two by the control of temperature controller
Temperature control the mixture between 55 DEG C~60 DEG C to continuous heating water bath supernatant and cyclodextrin always, and then not
Disconnected to evaporate ethyl alcohol and residual moisture, the alcohol vapour and residual moisture of evaporation carry out condensation by alcohol vapour collector and become liquid
It collects, the Cortex Eucommiae fine powder particle for becoming dry shape after the ethanol evaporation in mixture (containing supernatant and Cyclodextrin) is complete can be gathered in
At this moment the bottom of circle shape partition funnel-shaped stops heater heating, and stop apparatus for vacuum producing work, starting band valve gas
Cylinder, briquetting move up, to make Cortex Eucommiae fine powder be discharged in charge cask from through hole by gravity；Alcohol vapour collector is city
Wuxi City can be selected along demulcen Equipment Limited, the product of Tai'an Teng Yang General Devices Co., Ltd. in the universal product on face；
When briquetting is pressed in circle shape partition and closes through-hole, servo motor can drive vertical bar to rotate and stirring sheet is driven to rotate, at this moment
Briquetting is motionless；Apparatus for vacuum producing is the universal product on the market, and the production of Dongguan City great Lang Hao Bao vacuum equipment manufactory can be selected
Product.
It is further perfect, between the bottom of water tank and gutta-percha and natural medicinal ingredients separator be installed communicating pipe
13, drawing liquid pump ten is installed on communicating pipe 13.Here the effect of communicating pipe 13 and drawing liquid pump ten is can to store up being located at
It deposits the water in tank and is pumped into the enzyme digestion reaction for being used for Cortex Eucommiae raw material in gutta-percha and natural medicinal ingredients separator.
It is further perfect, vibrator is installed on bucket.Here the effect of vibrator be can accelerate Cortex Eucommiae fine powder from
It is fallen in charge cask in cavity one by through-hole, and Cortex Eucommiae fine powder can be made more thoroughly to fall to charge cask
It is interior.
It is further perfect, between the liquid storing barrel and stainless-steel vacuum blender of ethyl alcohol purification equipment be installed communicating pipe ten
Four, drawing liquid pump 11 is installed on communicating pipe 14.Here the effect of communicating pipe 14 and drawing liquid pump 11 is, can be ethyl alcohol
High-purity edible ethanol after purification in equipment for purifying is after being newly injected into and carrying out in stainless-steel vacuum blender to concentration
What enzymolysis liquid underflow carried out reduces precipitation processing without effective component solubility.
It is further perfect, temperature controller is installed on cavity two.Here the effect of temperature controller is to can be convenient control cavity two
The temperature of interior heating agent.
Further perfect, the side of Cortex Eucommiae natural drug fine powder load device is equipped with support plate, is equipped with PLC in support plate
Controller, PLC controller and gutta-percha and natural medicinal ingredients separator, spiral centrifugal separator, drug vacuum concentrator,
Ethyl alcohol purification equipment, Cortex Eucommiae natural drug fine powder load device, hot-water cylinder, each drawing liquid pump and triple valve, solenoid valve one, solenoid valve
Two, three connection of solenoid valve.Here PLC controller is programmable logic controller (PLC) general on the market, be can be selected on the market
General Mitsubishi PLC, Schneider PLC, still brands, the PLC controller such as Nikon Unitronics, Delta PLC and Matsushita PLC pass through
A drawing liquid pump and electric control part are controlled to reach the extraction and processing fine powder processing to Cortex Eucommiae natural medicinal ingredients, automation
Height, recruitment are few, can greatly improve the fine powder quantity of Cortex Eucommiae natural medicinal ingredients extraction, facilitate the raising of Cortex Eucommiae fine powder quality simultaneously
And reduce production cost；Here triple valve is three-way magnetic valve.
The invention has the advantages that: structure of the invention is ingenious in design, reasonable, utilizes Cortex Eucommiae colloid extraction element, spiral
Whizzer, sand core and filtering bag filter, sand core and filtering bag filter, membrane filter, drug vacuum concentrator, stainless steel are true
Empty blender, ethyl alcohol purification equipment, interconnection and synergistic effect between Cortex Eucommiae natural drug fine powder load device, can be fast
Speed, efficiently the Cortex Eucommiae natural medicinal ingredients in Cortex Eucommiae raw material, pass through filtering, concentration, refinement, fine powder extract integration stream
Journey not only substantially increases fine powder extraction efficiency, but also quality is higher, is worthy of popularization.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is the topology view of drug vacuum concentrator in the present invention；
Fig. 3 is the topology view of Cortex Eucommiae natural drug fine powder load device in the present invention；
Fig. 4 is state diagram when Cortex Eucommiae natural drug fine powder load device upper holder block lifts in the present invention.
Description of symbols: gutta-percha and natural medicinal ingredients separator 1, spiral centrifugal separator 2, sand core and filter bag
Filter 3, membrane filter 4, drug vacuum concentrator 5, stainless-steel vacuum blender 6, Cortex Eucommiae natural drug fine powder load device
7, bucket 7-1, partition 7-2 enclose shape partition 7-3, one 7-4 of cavity, cavity two 7-5, end cap 7-6, bracket 7-7, band valve cylinder
7-8, vertical bar 7-9, briquetting 7-10, alcohol vapour collector 7-11, connecting tube 7-12, enzymolysis liquid holding vessel 8, coarse filtration liquid holding vessel
9, refined filtration liquid holding vessel 10, fine filtrate holding vessel 11, hot-water cylinder 12, water tank 13, ethyl alcohol purification equipment a, communicating pipe 1,
Communicating pipe 2 15, communicating pipe 3 16, communicating pipe 4 17, communicating pipe 5 18, communicating pipe 6 19, communicating pipe 7 20, triple valve 21, even
Siphunculus 8 22, communicating pipe 9 23, liquid suction pipe 24, hot water conveying pipe 25, efferent duct 26, communicating pipe 10, communicating pipe 11, even
Siphunculus 12, solenoid valve 1,12 c of drawing liquid pump, drawing liquid pump 1, drawing liquid pump 2 32, drawing liquid pump 3 33, drawing liquid pump four
34, drawing liquid pump 5 35, drawing liquid pump 6 36, solenoid valve 3 37, drawing liquid pump 8 38, drawing liquid pump 9 39, apparatus for vacuum producing 40, solenoid valve two
41, communicating pipe 13, drawing liquid pump 10, vibrator 44, communicating pipe 14, drawing liquid pump 11, support plate 47, PLC control
Device 48 processed.
Specific embodiment
The present invention will be further explained below with reference to the attached drawings:
Referring to attached drawing: this Cortex Eucommiae natural medicinal ingredients extraction process, comprising the following steps:
(1) Cortex Eucommiae raw material Cortex Eucommiae raw material enzymolysis processing: is put into the interior bucket of gutta-percha and natural medicinal ingredients separator 1
Place, add water to submerge Cortex Eucommiae raw material, gradually respectively by containing protease, cellulase, pectase, cutinase solution according to 1:1
Proportion carry out being mixed into mixed solution, PH buffer is configured to using food-grade citric acid and sodium citrate and is poured into mixed liquor
In, being made into pH value is 3.2,4.0,5.5 3 kind of enzymatic hydrolysis solution, and enzymatic hydrolysis solution is poured into gutta-percha and natural medicinal ingredients separate
In the water of device 1, enzymatic hydrolysis is constantly stirred to Cortex Eucommiae raw material, and to the enzymatic hydrolysis in gutta-percha and natural medicinal ingredients separator 1
Solution carries out heating water bath, and for heating and temperature control at 40~50 DEG C, every kind of enzyme digestion reaction time is 4~6 hours；
(2) separation, filtering of enzymolysis liquid: Cortex Eucommiae colloid stays in gutta-percha and natural medicinal ingredients point after Cortex Eucommiae raw material enzymatic hydrolysis
From in device 1, enzymolysis liquid is discharged by the leakage fluid dram of gutta-percha and natural medicinal ingredients separator 1 and to pass through spiral continuous
Centrifuge separation removes slag and clast, and the separating liquid after spiral centrifugal slagging-off carries out sand core and filter bag carries out coarse filtration, by coarse filtration
Enzymolysis liquid again by membrane filter filter, obtain the brown clear solution transparent, without suspended solid residue by refined filtration；
(3) filtering enzymolysis liquid low temperature concentration；Clear and transparent brown solution injection of medicine vacuum concentrator 5, drug is true
The enzymolysis liquid of 5 pairs of empty inspissator filterings carries out cryogenic vacuum concentration；
(4) disinfection of concentrate room temperature, precipitation and separation: in the enzymolysis liquid injection of medicine precipitation and separation device 6 after low temperature is concentrated,
95% edible ethanol is added and constantly the enzymolysis liquid after concentration is stirred under normal pressure, the rear static enzymolysis liquid made after concentration
Significantly reducing in underflow without effective component solubility, precipitates from the concentrated extract of enzyme-extracting solution, and the day of molecular state
Right Cortex Eucommiae drug ingedient then can be sufficiently mixed and dissolve with ethanol solution under conditions of being sufficiently stirred；
(5) drug ingedient refines: extracting supernatant liquor, supernatant liquor is then injected into the load of Cortex Eucommiae natural drug fine powder
In device 7, to supernatant load cyclodextrin and under vacuum conditions progress heating water bath processing, heating and temperature control 55 DEG C~
60 DEG C, the alcohol and residual moisture in clear liquid are evaporated, and obtain Cortex Eucommiae fine powder.
This Cortex Eucommiae natural medicinal ingredients extract equipment, including gutta-percha and natural medicinal ingredients separator 1, gutta-percha
It is equipped with spiral centrifugal separator 2 with the side of natural medicinal ingredients separator 1, the side of spiral centrifugal separator 2 is equipped with sand
The side of core and filtering bag filter 3, sand core and filtering bag filter 3 is equipped with membrane filter 4, and the side of membrane filter 4 is equipped with drug
Vacuum concentrator 5, the side of drug vacuum concentrator 5 are provided with the stainless-steel vacuum blender 6 of rabbling mechanism, stainless-steel vacuum
The side of blender 6 is equipped with ethyl alcohol purification equipment a, and the side of stainless-steel vacuum blender 6 is negative equipped with Cortex Eucommiae natural drug fine powder
It carries and sets 7；Enzymolysis liquid holding vessel 8 is equipped between gutta-percha and natural medicinal ingredients separator 1 and spiral centrifugal separator 2,
Coarse filtration liquid holding vessel 9, sand core and filtering bag filter 3 and film are equipped between spiral centrifugal separator 2 and sand core and filtering bag filter 3
It is equipped with refined filtration liquid holding vessel 10 between filter 4, fine filtrate is equipped between membrane filter 4 and drug vacuum concentrator 5 and is stored
The side of tank 11, drug vacuum concentrator 5 is equipped with hot-water cylinder 12 and water tank 13 with heating function and temperature controller；Gutta-percha and
Communicating pipe 1, enzymolysis liquid are installed between the leakage fluid dram of natural medicinal ingredients separator 1 and the top of enzymolysis liquid holding vessel 8
Communicating pipe 2 15 is installed between the bottom of holding vessel 8 and the inlet of spiral centrifugal separator 2, spiral centrifugal separator 2
Communicating pipe 3 16, the bottom of coarse filtration liquid holding vessel 9 and sand core and filter are installed between liquid outlet and the top of coarse filtration liquid holding vessel 9
Communicating pipe 4 17, the liquid outlet and refined filtration liquid holding vessel of sand core and filtering bag filter 3 are installed between the inlet of bag type filter 3
Communicating pipe 5 18 is installed between 10 top, is equipped between 4 inlet of bottom and membrane filter of refined filtration liquid holding vessel 10
Communicating pipe 6 19 between 4 liquid outlet of membrane filter and the top of fine filtrate holding vessel 11 be installed communicating pipe 7 20, drug is true
Triple valve 21, the bottom of fine filtrate holding vessel 11 and the entrance of 21 one end of triple valve are equipped at the inlet of empty inspissator 5
Between communicating pipe 8 22 is installed, installed between another end opening of triple valve 21 and the input end of stainless-steel vacuum blender 6
There is communicating pipe 9 23, hot water conveying pipe 25 and efferent duct 26 is installed, drug is true between hot-water cylinder 12 and drug vacuum concentrator 5
Communicating pipe 10, the bottom of water tank 13 and hot-water cylinder 12 are installed between 13 bottom of water storage cavity and water tank of empty inspissator 5
Communicating pipe 11 is installed between top；Cortex Eucommiae natural drug fine powder load device 7 includes the bucket 7-1 with opening, is contained
It is fixed in the cavity of charging basket 7-1 and cavity is divided into two-part partition 7-2 up and down, be equipped at the cavity above partition 7-2
The top of the circle shape partition 7-3 of tapered setting, circle shape partition 7-3 are fixed on the inner peripheral wall of bucket 7-1, enclose shape partition
The bottom end of 7-3 is fixed on the top surface of partition 7-2, and on the inside of circle shape partition 7-3 and outside is respectively one 7-4 of cavity and chamber separated
The through-hole 7-2a being connected to one 7-4 of cavity is provided on body two 7-5, partition 7-2, the opening of bucket 7-1 is equipped with for closed
It is fixed with bracket 7-7 on the end cap 7-6 of opening, bucket 7-1, band valve cylinder 7-8, band valve cylinder 7-8 are fixed on bracket 7-7
Piston rod be fixed on the top surface end cap 7-6, be rotatably connected to vertical bar 7-9 on end cap 7-6, the bottom end rotation connection of vertical bar 7-9
There is a briquetting 7-10 with taper, the taper of briquetting 7-10 is identical as the circle taper of shape partition 7-3 and interior table with circle shape partition 7-3
Face cooperation, vertical bar 7-9 is driven by being fixed on the servo motor 7-14 on the top end cap 7-6, solid in the bottom wheel profile surface of vertical bar 7-9
Surely there is stirring sheet 7-15, having heaters 7-13 is installed in two 7-5 of cavity；The side of bucket 7-1 is equipped with by condenser, cooling
The condenser and one 7- of cavity of the alcohol vapour collector 7-11 that device, separator, accumulator form, alcohol vapour collector 7-11
It is connected with connecting tube 7-12 between 4, is equipped with and is connected between the accumulator and ethyl alcohol purification equipment a of alcohol vapour collector 7-11
Pipe 12；Liquid suction pipe 24 is installed between stainless-steel vacuum blender 6 and Cortex Eucommiae natural drug fine powder load device 7；Threeway
Solenoid valve 1 is installed between valve 21 and the inlet of drug vacuum concentrator 5, solenoid valve two is installed on communicating pipe 1
41, drawing liquid pump 1 is installed on communicating pipe 2 15, drawing liquid pump 2 32 is installed on communicating pipe 3 16, is installed on communicating pipe 4 17
There is drawing liquid pump 3 33, drawing liquid pump 4 34 is installed on communicating pipe 5 18, drawing liquid pump 5 35, communicating pipe are installed on communicating pipe 6 19
Drawing liquid pump 6 36 is installed on 7 20, solenoid valve 3 37 is installed on communicating pipe 9 23, drawing liquid pump is installed on communicating pipe 10
12 c are equipped with drawing liquid pump b on liquid suction pipe 24, drawing liquid pump 8 38 are equipped on communicating pipe 11, is pacified on communicating pipe 12
Equipped with drawing liquid pump 9 39, apparatus for vacuum producing 40 is installed on Cortex Eucommiae natural drug fine powder load device 7.
Communicating pipe 13 is installed between the bottom of water tank 13 and gutta-percha and natural medicinal ingredients separator 1,
Drawing liquid pump 10 is installed on communicating pipe 13.
Vibrator 44 is installed on bucket 7-1.
Communicating pipe 14, communicating pipe are installed between the liquid storing barrel and stainless-steel vacuum blender 6 of ethyl alcohol purification equipment a
Drawing liquid pump 11 is installed on 14.
Temperature controller 7-16 is installed on two 7-5 of cavity.
The side of Cortex Eucommiae natural drug fine powder load device 7 is equipped with support plate 47, is equipped with PLC controller in support plate 47
48, PLC controller 48 and gutta-percha and natural medicinal ingredients separator 1, spiral centrifugal separator 2, drug vacuum concentrator
5, ethyl alcohol purification equipment a, Cortex Eucommiae natural drug fine powder load device 7, hot-water cylinder 12, each drawing liquid pump and triple valve 21, solenoid valve
One 30, solenoid valve 2 41,3 37 connection of solenoid valve.
The process of equipment extraction Cortex Eucommiae natural drug fine powder: Cortex Eucommiae raw material is put into gutta-percha and natural medicinal ingredients
In the screen roller of separator 1, drawing liquid pump 43 is then started by PLC controller 48, the water being located in water tank 13 is taken out
Enter into 1 liquid holding groove of gutta-percha and natural medicinal ingredients separator, gutta-percha and natural medicinal ingredients separator 1 add good liquid
Afterwards, gradually respectively by containing protease, cellulase, pectase, cutinase solution according to the proportion of 1:1 be mixed into it is mixed
Close solution, PH buffer is configured to using food-grade citric acid and sodium citrate and is poured into mixed liquor, be made into pH value be 3.2,
4.0,5.5 3 kinds of enzymatic hydrolysis solution, enzymatic hydrolysis solution is poured into the water of gutta-percha and natural medicinal ingredients separator 1, to Du
Secondary raw material constantly stirs enzymatic hydrolysis, and then PLC controller 48 controls the servo electricity on gutta-percha and natural medicinal ingredients separator 1
Machine rotation constantly carries out Cortex Eucommiae raw material so that the screen roller of gutta-percha and natural medicinal ingredients separator 1 be driven to rotate
Stirring enzymatic hydrolysis, while heating water bath, heating temperature are carried out to the enzymatic hydrolysis solution in gutta-percha and natural medicinal ingredients separator 1
At 40 DEG C~50 DEG C, every kind of enzyme digestion reaction time is 4~6 hours for control, in order to improve enzymatic hydrolysis amount, can use multiple gutta-percha
The mode that Cortex Eucommiae raw material is digested with natural medicinal ingredients separator 1 carries out, after reaching 4~6 hours enzymolysis times, PLC control
Device control solenoid valve 2 41 processed is opened, and the enzymolysis liquid for having digested Cortex Eucommiae raw material is stored into storage in enzymolysis liquid holding vessel 8 and (is located at
The Folium glue wire of screen roller is separately taken out Folium glue wire purification plants and is separately purified, and what the present invention introduced is Cortex Eucommiae day
The extraction of right drug ingedient is not described Folium glue wire purifying here), the enzymolysis liquid in enzymolysis liquid holding vessel 8 is logical
It crosses drawing liquid pump 1 and enzymolysis liquid is pumped into (the spiral centrifugal separator 2 of the control of PLC controller 48 at this time of spiral centrifugal separator 2
Motor operation) in carry out slag and the processing of big clast, filtered enzymolysis liquid is pumped into coarse filtration liquid by drawing liquid pump 2 32
Then the enzymolysis liquid being located in coarse filtration liquid holding vessel 9 is pumped into sand core and filter bag by drawing liquid pump 3 33 by storage in holding vessel 9
It carefully being filtered in filter 3, the enzymolysis liquid being carefully obtained by filtration is sent in refined filtration liquid holding vessel 10 by drawing liquid pump 4 34 and stores,
Then the enzymolysis liquid being located in refined filtration liquid holding vessel 10 is sent in membrane filter 4 by drawing liquid pump 5 35 and carries out fine mistake
Filter, the solution obtained by fine filtering are stored into fine filtrate holding vessel 12 by drawing liquid pump 6 36, and starting drug is true
Apparatus for vacuum producing in empty inspissator 5, at this moment triple valve 21 is between 5 inlet of communicating pipe 8 22 and drug vacuum concentrator
Route is dense drug vacuum is pumped into positioned at enzymolysis liquid in fine filtrate holding vessel 12 using negative pressure caused by apparatus for vacuum producing
The heating of contracting device 5 is indoor, closes communicating pipe 8 22 and 5 feed liquor of drug vacuum concentrator after the completion of extraction by solenoid valve 1
Route between mouthful, to reach to heating room vacuumize process, heating room passes through the continuous heat cycles of hot-water cylinder 12, so that
It heats indoor temperature on drug vacuum concentrator 5 to be controlled always at 55 DEG C~60 DEG C, concentration time was controlled at 3~4 hours, dense
It has contracted after enzymolysis liquid, triple valve 21 opens 5 inlet of drug vacuum concentrator and the route between communicating pipe 9 23, at this moment starts
Apparatus for vacuum producing on stainless-steel vacuum blender 6, using negative pressure the enzymolysis liquid after the concentration being located in drug vacuum concentrator 5
It is drawn into the tank body of stainless-steel vacuum blender 6, after sucking is good, closes solenoid valve 3 37, and take out by drawing liquid pump 11
The high concentration edible ethanol in ethyl alcohol purification equipment a is taken to inject in stainless-steel vacuum blender 6, pumping high-concentration edible ethanol is complete
Bi Hou, it is then continuous using the rabbling mechanism on stainless-steel vacuum blender 6 to 6 vacuumize process of stainless-steel vacuum blender
Concentrate after enzymatic hydrolysis is stirred, under the effect of high concentration edible ethanol, these are dissolved in enzymolysis liquid without drug effect
The polymer solubility of ingredient significantly reduces, and can precipitate from the concentrated extract of enzyme-extracting solution, and natural Du of molecular state
Secondary drug ingedient can be then sufficiently mixed under conditions of being sufficiently stirred with high concentration edible ethanol solution, and be dissolved in the molten of ethyl alcohol
(high concentration edible ethanol not only has the function of dissolving Cortex Eucommiae natural medicinal ingredients, but also the effect with sterilizing in liquid
Fruit), mixing time control control stops stirring after 1 hour, time are arrived, and waiting makes solution in stationary state for 15 minutes, at this moment,
The macromolecule polyalcohol of metabolite of no effective component can precipitate in solid form, have drug effect to be divided into secondary
Metabolite is dissolved in high concentration edible ethanol, positioned at the brown clear liquid shape in the top of sediment, starts Cortex Eucommiae natural drug
Apparatus for vacuum producing 40 on fine powder load device 7, due to negative pressure, brownish supernatant is drawn into Cortex Eucommiae day by liquid suction pipe 24
A certain amount of Cyclodextrin is manually added in one 7-4 of cavity of right drug fine powder load device 7 and by feed opening, at the same time,
Heater 7-13 heating on Cortex Eucommiae natural drug fine powder load device 7 is located at the heating agent in two 7-5 of cavity, and temperature control exists
55 DEG C~60 DEG C, meanwhile, PLC controller 48 starts servo motor 7-14 rotation, and vertical bar 7-9 is driven to rotate and drive stirring sheet 2-
15 are stirred continuously Cyclodextrin is mixed with supernatant, and the mixture of Cyclodextrin and supernatant is stirred while being heated,
The heated rapid evaporation of ethyl alcohol and residual moisture in mixture, steam are condensed by alcohol vapour collector 7-11, are become
Liquid is collected again, and after ethanol evaporation is complete, mixture is by being dried just at Cortex Eucommiae natural drug fine powder, Cortex Eucommiae crude drug
Object fine powder all gathers the circle bottom shape partition 7-3, and the at this moment starting of PLC controller 48 band valve cylinder 7-8 drives vertical bar 7-9 to move up,
And briquetting 7-10 is opened, Cortex Eucommiae natural drug fine powder is drained into charge cask by through-hole 7-2a, at this point, PLC controller 48
Vibrator 44 is controlled to work, so that it is drained into Cortex Eucommiae natural drug fine powder more rapidly, efficiently, without remaining in charge cask,
Ethanol liquid in alcohol vapour collector 7-11 is stored by the purification of ethyl alcohol purification equipment a, can be utilized again；
Condensed water in drug vacuum concentrator 5, which can be also drawn into water tank 13, to be reused；So that Cortex Eucommiae natural drug
In ingredient fine powder extraction process, waste can be recycled utilization, to reach, environmental protection, energy conservation, extraction efficiency is high, is produced into
This low effect is worthy of popularization.
Although the present invention has been illustrated and described with reference to preferred embodiments, this profession ordinary skill
Personnel are it is to be appreciated that within the scope of the claims, can make various variation in form and details.
Claims (6)
1. a kind of Cortex Eucommiae natural medicinal ingredients extract equipment, including gutta-percha and natural medicinal ingredients separator (1), Du
The side of secondary glue and natural medicinal ingredients separator (1) is equipped with spiral centrifugal separator (2), the spiral centrifugal separator
(2) side is equipped with sand core and filtering bag filter (3), and the side of the sand core and filtering bag filter (3) is equipped with membrane filter
(4), the side of the membrane filter (4) is equipped with drug vacuum concentrator (5), and the side of the drug vacuum concentrator (5) is matched
There is the stainless-steel vacuum blender (6) with rabbling mechanism, the side of the stainless-steel vacuum blender (6) is set equipped with ethyl alcohol purification
Standby (a), it is characterized in that: the side of the stainless-steel vacuum blender (6) is equipped with Cortex Eucommiae natural drug fine powder load device (7)；
Enzymolysis liquid is equipped between the gutta-percha and natural medicinal ingredients separator (1) and spiral centrifugal separator (2) to store
Tank (8) is equipped with coarse filtration liquid holding vessel (9) between the spiral centrifugal separator (2) and sand core and filtering bag filter (3), described
Refined filtration liquid holding vessel (10), the membrane filter (4) and medicine are equipped between sand core and filtering bag filter (3) and membrane filter (4)
Fine filtrate holding vessel (11) is equipped between object vacuum concentrator (5), the side of the drug vacuum concentrator (5) is equipped with band and adds
The hot-water cylinder (12) and water tank (13) of heat function and temperature controller；The gutta-percha and natural medicinal ingredients separator (1)
Communicating pipe one (14), the bottom of the enzymolysis liquid holding vessel (8) are installed between leakage fluid dram and the top of enzymolysis liquid holding vessel (8)
Be installed between the inlet of spiral centrifugal separator (2), the spiral centrifugal separator (2) goes out liquid communicating pipe two (15)
Communicating pipe three (16), the bottom of the coarse filtration liquid holding vessel (9) and sand are installed between mouth and the top of coarse filtration liquid holding vessel (9)
Communicating pipe four (17), the liquid out of the sand core and filtering bag filter (3) are installed between core and the inlet of filtering bag filter (3)
Mouthful between the top of refined filtration liquid holding vessel (10) be installed communicating pipe five (18), the bottom of the refined filtration liquid holding vessel (10) and
Communicating pipe six (19), membrane filter (4) liquid outlet and fine filtrate holding vessel are installed between membrane filter (4) inlet
(11) communicating pipe seven (20) is installed between top, is equipped with triple valve at the inlet of the drug vacuum concentrator (5)
(21), between the bottom of the fine filtrate holding vessel (11) and the entrance of triple valve (21) one end be installed communicating pipe eight
(22), between another end opening of the triple valve (21) and the input end of stainless-steel vacuum blender (6) be installed communicating pipe
Nine (23) are equipped with hot water conveying pipe (25) and efferent duct (26) between the hot-water cylinder (12) and drug vacuum concentrator (5),
Communicating pipe ten (27), the water storage are installed between the water storage cavity and water tank (13) bottom of the drug vacuum concentrator (5)
Between at the top of the bottom of tank (13) and hot-water cylinder (12) be installed communicating pipe 11 (28)；
The Cortex Eucommiae natural drug fine powder load device (7) includes the bucket (7-1) with opening, the bucket (7-1)
It is fixed in cavity and cavity is divided into two-part partition (7-2) up and down, be equipped at the cavity above the partition (7-2) and be in
The top of the circle shape partition (7-3) of taper setting, circle shape partition (7-3) is fixed on the inner peripheral wall of bucket (7-1),
The bottom end of circle shape partition (7-3) is fixed on the top surface of partition (7-2), on the inside of the circle shape partition (7-3) and outside point
The cavity one (7-4) and cavity two (7-5) that Wei do not separate are provided with the through-hole being connected to cavity one (7-4) on the partition (7-2)
(7-2a), the opening of the bucket (7-1) are equipped with the end cap (7-6) for closed opening, consolidate on the bucket (7-1)
Surely have bracket (7-7), band valve cylinder (7-8) is fixed on the bracket (7-7), the piston rod of the band valve cylinder (7-8) is solid
It is scheduled on the top surface end cap (7-6), is rotatably connected to vertical bar (7-9) on the end cap (7-6), the bottom end of the vertical bar (7-9) turns
It is dynamic to be connected with the briquetting (7-10) with taper, the taper of the briquetting (7-10) it is identical as the taper of shape partition (7-3) is enclosed and with
The inner surface cooperation of shape partition (7-3) is enclosed, the vertical bar (7-9) is by being fixed on the servo motor (7- on the top end cap (7-6)
14) it drives, is fixed with stirring sheet (7-15) in the bottom wheel profile surface of the vertical bar (7-9), is equipped in the cavity two (7-5)
Heater (7-13)；The side of the bucket (7-1) is equipped with the ethyl alcohol being made of condenser, cooler, separator, accumulator
Steam accumulator (7-11) is connected between the condenser and cavity one (7-4) of the alcohol vapour collector (7-11) and connect
It manages (7-12), between the accumulator and ethyl alcohol purification equipment (a) of the alcohol vapour collector (7-11) is installed communicating pipe ten
Two (29)；
Liquid suction pipe (24) are installed between the stainless-steel vacuum blender (6) and Cortex Eucommiae natural drug fine powder load device (7)；
Solenoid valve one (30), the communicating pipe one are installed between the triple valve (21) and the inlet of drug vacuum concentrator (5)
(14) solenoid valve two (41) is installed on, drawing liquid pump one (31), the communicating pipe three are installed on the communicating pipe two (15)
(16) drawing liquid pump two (32) is installed on, drawing liquid pump three (33), the communicating pipe five are installed on the communicating pipe four (17)
(18) drawing liquid pump four (34) is installed on, drawing liquid pump five (35), the communicating pipe seven are installed on the communicating pipe six (19)
(20) drawing liquid pump six (36) is installed on, solenoid valve three (37), the communicating pipe ten are installed on the communicating pipe nine (23)
(27) drawing liquid pump 12 (c) is installed on, drawing liquid pump (b), the communicating pipe 11 (28) are installed on the liquid suction pipe (24)
On drawing liquid pump eight (38) is installed, drawing liquid pump nine (39), the Cortex Eucommiae natural drug are installed on the communicating pipe 12 (29)
Apparatus for vacuum producing (40) are installed on fine powder load device (7).
2. Cortex Eucommiae natural medicinal ingredients extract equipment according to claim 1, it is characterized in that: the bottom of the water tank (13)
Communicating pipe 13 (42), the communicating pipe 13 are installed between portion and gutta-percha and natural medicinal ingredients separator (1)
(42) drawing liquid pump ten (43) is installed on.
3. Cortex Eucommiae natural medicinal ingredients extract equipment according to claim 2, it is characterized in that: on the bucket (7-1)
Vibrator (44) are installed.
4. Cortex Eucommiae natural medicinal ingredients extract equipment according to claim 3, it is characterized in that: the ethyl alcohol purification equipment
(a) be installed, on the communicating pipe 14 (45) communicating pipe 14 (45) between liquid storing barrel and stainless-steel vacuum blender (6)
Drawing liquid pump 11 (46) is installed.
5. Cortex Eucommiae natural medicinal ingredients extract equipment according to claim 4, it is characterized in that: on the cavity two (7-5)
Temperature controller (7-16) is installed.
6. Cortex Eucommiae natural medicinal ingredients extract equipment according to claim 5, it is characterized in that: the Cortex Eucommiae natural drug is smart
The side of powder load device (7) is equipped with support plate (47), is equipped with PLC controller (48), the PLC on the support plate (47)
Controller (48) and gutta-percha and natural medicinal ingredients separator (1), spiral centrifugal separator (2), drug vacuum concentrator
(5), ethyl alcohol purification equipment (a), Cortex Eucommiae natural drug fine powder load device (7), hot-water cylinder (12), each drawing liquid pump and triple valve
(21), solenoid valve one (30), solenoid valve two (41), solenoid valve three (37) connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710043738.XA CN106890477B (en) | 2017-01-19 | 2017-01-19 | Cortex Eucommiae natural medicinal ingredients extraction process and its extract equipment |
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|---|---|---|---|
| CN201710043738.XA CN106890477B (en) | 2017-01-19 | 2017-01-19 | Cortex Eucommiae natural medicinal ingredients extraction process and its extract equipment |
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| CN106890477B true CN106890477B (en) | 2019-10-15 |
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| CN108783350B (en) * | 2018-05-16 | 2021-12-24 | 虎林市森源天然食品有限责任公司 | Honey concentration method with active invertase retained by membrane filtration |
| CN112716906A (en) * | 2021-01-17 | 2021-04-30 | 洪学云 | Preparation method of phospholipid chitosan medicine |
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| US20020146466A1 (en) * | 2001-02-05 | 2002-10-10 | Nobuyoshi Kuboyama | Solid form compositions containing an extract of a raw material as the active ingredient and process of preparing the same |
| CN103550951A (en) * | 2013-11-20 | 2014-02-05 | 青岛农业大学 | Novel method for extracting or purifying effective components of traditional Chinese medicine |
| CN203694667U (en) * | 2014-01-25 | 2014-07-09 | 青岛科技大学 | Natural eucommia ulmoides rubber liquid extraction separation equipment |
| CN105561628B (en) * | 2015-12-16 | 2018-06-19 | 浙江旭源杜仲生物科技有限公司 | Plant colloid extraction process and separation equipment |
| CN205603495U (en) * | 2016-05-16 | 2016-09-28 | 浙江旭源杜仲生物科技有限公司 | Enzymolysis is supplementary eluriates separation purification equipment who detaches residue in gutta -percha |
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