CN106883749A - A kind of LED UV woodenware aqueous priming paints and preparation method thereof - Google Patents
A kind of LED UV woodenware aqueous priming paints and preparation method thereof Download PDFInfo
- Publication number
- CN106883749A CN106883749A CN201710074186.9A CN201710074186A CN106883749A CN 106883749 A CN106883749 A CN 106883749A CN 201710074186 A CN201710074186 A CN 201710074186A CN 106883749 A CN106883749 A CN 106883749A
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- led
- product
- woodenware
- priming paint
- aqueous priming
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
Abstract
The invention discloses a kind of LED UV woodenware aqueous priming paints, by weight percentage, it is prepared from by the raw material of following component:Aqueous polyurethane acrylic acid dispersion 50% 80%;Defoamer 0.1% 0.2%;Dispersant 0.1% 0.2%;Levelling agent 0.1% 0.2%;Coalescents 3% 6%;Thickener 0.3% 0.6%;Talcum powder 15% 20%;PH conditioning agents 0.3% 0.6%;Light trigger 1% 5%;Deionized water 10% 20%.A kind of LED UV woodenware aqueous priming paints that the present invention is provided, curing rate is fast, environmental protection, and obtained LED UV woodenware aqueous priming paints are limited without workpiece type shape.
Description
Technical field
The present invention relates to priming paint preparation field, especially a kind of LED-UV woodenware aqueous priming paint and preparation method thereof.
Background technology
Traditional mercury lamp solidification does not adapt to life from market plane, energy-conservation, easy construction and environmental requirement all angles
Force of labor develops the requirement with the epoch.Traditional mercury lamp solidifies high energy consumption, equipment high investment, and flat board, resistance to can only be confined to using base material
In hot substrate, existing market has been substantially saturated, and profit significantly declines.Under this historical background, Rong Jia R&D teams are absorbed in grinds
Study carefully removable cold light source curing technology, obtain and be smoothly applied to successfully and by it surfacing treatment.So make market plane without
Limitation expands, and in original base than mercury lamp energy-conserving and environment-protective, may move, and does not have heat radiation, deeply traditional mercury lamp can be reached
The field arrived:Traditional-family fits up, special-shaped furniture surface treatment, energy-conservation.Normal temperature rapid curing, unlike heat cure heated substrate and
Surrounding space, inherits and has developed UV curing technologies and water paint technology many advantages, especially environmentally safe, to human body
Health is substantially free of volatile organic solvent without influence, does not result in air pollution, also reduces and harm and fire are endangered
Dangerous, production efficiency is high, and energy consumption is low, and uv equipment, and investment technology is relatively low, easily realizes production line balance, factory building
Floor space is small, can save great amount of investment.Without solvent, pollution is reduced, save resources consider most economical.
As countries in the world ecological environmental protection is paid attention to, strict legislation limitation, photocuring product are carried out to atmosphere pollution
Superiority.The U.S., Europe, Japan and other countries are using photocuring technology as one of reduction VOC emission important means.China is certainly
Since reform and opening-up, national economy is rapidly developed, and in order to realize sustainable development, builds a Harmonious Society, and increases to environment
Administer and protect, this is without suspected of photocuring product offer opportunity, it is believed that, with national development, social progress, man and nature
Get along amiably and peacefully, environmental protection photocuring industry is bound to all enter with day, thriving.
The content of the invention
In view of this, it is an object of the invention to provide a kind of LED-UV woodenware aqueous priming paint and preparation method thereof, solidification
Speed is fast, environmental protection, and obtained LED-UV woodenware aqueous priming paint is limited without workpiece type shape.
The technical scheme is that:A kind of LED-UV woodenware aqueous priming paint, by weight percentage, by following component
Raw material is prepared from:
Aqueous polyurethane acrylic acid dispersion 50%-80%;
Defoamer 0.1%-0.2%;
Dispersant 0.1%-0.2%;
Levelling agent 0.1%-0.2%;
Coalescents 3%-6%;
Thickener 0.3%-0.6%;
Talcum powder 15%-20%;
PH conditioning agents 0.3%-0.6%;
Light trigger 1%-5%;
Deionized water 10%-20%.
Preferably, the LED-UV woodenware aqueous priming paint, by weight percentage, by the raw material preparation of following component
Into:
Aqueous polyurethane acrylic acid dispersion 60%-70%;
Defoamer 0.1%-0.15%;
Dispersant 0.14%-0.2%;
Levelling agent 0.16%-0.2%;
Coalescents 4%-6%;
Thickener 0.4%-0.6%;
Talcum powder 15%-17%;
PH conditioning agents 0.4%-0.6%;
Light trigger 3%-5%;
Deionized water 10%-15%.
Preferably, the aqueous polyurethane acrylic acid dispersion can be using German Cohan wound company or BASF Aktiengesellschaft
Or the product of dutch royal DSM group production.
Preferably, the defoamer, dispersant, levelling agent can use Di Gao companies of Germany or Bi Ke companies of Germany or Taiwan
The product of this De Qian company of hamming production.
Preferably, the light trigger is benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkane
One or more combination in base benzophenone or acyl group oxidation of ketones thing or benzophenone or thioxanthone or iron arene, it is described light-initiated
Agent can use the new light of Tianjin Jiu new materials limited company or Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai
The product of Chemical Co., Ltd.'s production.
Preferably, the PH conditioning agents are that the trade mark of LG-DOW company production is the product of AMP-95.
Preferably, the coalescents are that the trade mark of LG-DOW company production is the product of DPM or DPNB.
Preferably, the thickener is that the trade mark of German Ming Ling chemical companies production is the product of PUR-40.
A kind of preparation method of LED-UV woodenware aqueous priming paint, comprises the following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
Compared with prior art, the present invention has the advantages that:A kind of LED-UV woodenware that the present invention is provided is aqueous
The preparation method of priming paint, can accelerate curing rate, environmental protection, to human body non-hazardous, and obtained LED-UV woodenware water
Property priming paint limited without workpiece type shape, finish paint good toughness, industrial prospect is wide.
Specific embodiment
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of LED-UV woodenware aqueous priming paint, by weight percentage, is prepared from by the raw material of following component, such as table 1:
Table 1
Aqueous polyurethane acrylic acid dispersion | 65% |
Defoamer | 0.1% |
Dispersant | 0.2% |
Levelling agent | 0.2% |
Coalescents | 6.0% |
Thickener | 0.6% |
PH conditioning agents | 0.6% |
Talcum powder | 15% |
Light trigger | 3.0% |
Deionized water | 12.3% |
Wherein, above-mentioned aqueous polyurethane acrylic acid dispersion can be using German Cohan wound company or BASF Aktiengesellschaft or Holland
The product of imperial DSM group production.
Defoamer, dispersant, levelling agent can use Di Gao companies of Germany or Bi Ke companies of Germany or this moral of Taiwan hamming modest
The product of company's production.
Light trigger is benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkyl phenones or acyl
One or more combination in base oxidation of ketones thing or benzophenone or thioxanthone or iron arene, light trigger can be long using Tianjin
Day new material limited company or Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai Xinguang Chemical Co., Ltd.'s life
The product of product.
PH conditioning agents are that the trade mark of LG-DOW company production is the product of AMP-95.
Coalescents are that the trade mark of LG-DOW company production is the product of DPM or DPNB.
Thickener is that the trade mark of German Ming Ling chemical companies production is the product of PUR-40.
A kind of preparation method of the LED-UV woodenware aqueous priming paints being formulated described in use embodiment 1, comprises the following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
Embodiment 2
A kind of LED-UV woodenware aqueous priming paint, by weight percentage, is prepared from by the raw material of following component, such as table 2:
Table 2
Aqueous polyurethane acrylic acid dispersion | 63% |
Defoamer | 0.2% |
Dispersant | 0.2% |
Levelling agent | 0.2% |
Coalescents | 6.0% |
Thickener | 0.6% |
PH conditioning agents | 0.6% |
Talcum powder | 17% |
Light trigger | 3.0% |
Deionized water | 10.3% |
Wherein, above-mentioned aqueous polyurethane acrylic acid dispersion can be using German Cohan wound company or BASF Aktiengesellschaft or Holland
The product of imperial DSM group production.
Defoamer, dispersant, levelling agent can use Di Gao companies of Germany or Bi Ke companies of Germany or this moral of Taiwan hamming modest
The product of company's production.
Light trigger is benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkyl phenones or acyl
One or more combination in base oxidation of ketones thing or benzophenone or thioxanthone or iron arene, light trigger can be long using Tianjin
Day new material limited company or Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai Xinguang Chemical Co., Ltd.'s life
The product of product.
PH conditioning agents are that the trade mark of LG-DOW company production is the product of AMP-95.
Coalescents are that the trade mark of LG-DOW company production is the product of DPM or DPNB.
Thickener is that the trade mark of German Ming Ling chemical companies production is the product of PUR-40.
A kind of preparation method of the LED-UV woodenware aqueous priming paints being formulated described in use embodiment 2, comprises the following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
Embodiment 3
A kind of LED-UV woodenware aqueous priming paint, by weight percentage, is prepared from by the raw material of following component, such as table 3:
Table 3
Aqueous polyurethane acrylic acid dispersion | 50% |
Defoamer | 0.1% |
Dispersant | 0.2% |
Levelling agent | 0.2% |
Coalescents | 6.0% |
Thickener | 0.6% |
PH conditioning agents | 0.6% |
Talcum powder | 15% |
Light trigger | 3.0% |
Deionized water | 12.3% |
Wherein, above-mentioned aqueous polyurethane acrylic acid dispersion can be using German Cohan wound company or BASF Aktiengesellschaft or Holland
The product of imperial DSM group production.
Defoamer, dispersant, levelling agent can use Di Gao companies of Germany or Bi Ke companies of Germany or this moral of Taiwan hamming modest
The product of company's production.
Light trigger is benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkyl phenones or acyl
One or more combination in base oxidation of ketones thing or benzophenone or thioxanthone or iron arene, light trigger can be long using Tianjin
Day new material limited company or Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai Xinguang Chemical Co., Ltd.'s life
The product of product.
PH conditioning agents are that the trade mark of LG-DOW company production is the product of AMP-95.
Coalescents are that the trade mark of LG-DOW company production is the product of DPM or DPNB.
Thickener is that the trade mark of German Ming Ling chemical companies production is the product of PUR-40.
A kind of preparation method of the LED-UV woodenware aqueous priming paints being formulated described in use embodiment 3, comprises the following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
Embodiment 4
A kind of LED-UV woodenware aqueous priming paint, by weight percentage, is prepared from by the raw material of following component, such as table 4:
Table 4
Aqueous polyurethane acrylic acid dispersion | 80% |
Defoamer | 0.2% |
Dispersant | 0.2% |
Levelling agent | 0.2% |
Coalescents | 6.0% |
Thickener | 0.6% |
PH conditioning agents | 0.6% |
Talcum powder | 17% |
Light trigger | 3.0% |
Deionized water | 10.3% |
Wherein, above-mentioned aqueous polyurethane acrylic acid dispersion can be using German Cohan wound company or BASF Aktiengesellschaft or Holland
The product of imperial DSM group production.
Defoamer, dispersant, levelling agent can use Di Gao companies of Germany or Bi Ke companies of Germany or this moral of Taiwan hamming modest
The product of company's production.
Light trigger is benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkyl phenones or acyl
One or more combination in base oxidation of ketones thing or benzophenone or thioxanthone or iron arene, light trigger can be long using Tianjin
Day new material limited company or Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai Xinguang Chemical Co., Ltd.'s life
The product of product.
PH conditioning agents are that the trade mark of LG-DOW company production is the product of AMP-95.
Coalescents are that the trade mark of LG-DOW company production is the product of DPM or DPNB.
Thickener is that the trade mark of German Ming Ling chemical companies production is the product of PUR-40.
A kind of preparation method of the LED-UV woodenware aqueous priming paints being formulated described in use embodiment 4, comprises the following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
LED-UV woodenware aqueous priming paint obtained in above-described embodiment 1-4 is as follows with the performance test results contrast of commercially available prod
Table 5;
Table 5
As can be seen from the above table, a kind of LED-UV woodenware aqueous priming paint that the present invention is provided and preparation method thereof, can accelerate solid
Change speed, environmental protection is limited human body non-hazardous, and obtained LED-UV woodenware aqueous priming paint, finish paint without workpiece type shape
Good toughness, industrial prospect is wide.
The above embodiments are only the preferred embodiments of the present invention, it is impossible to interest field of the invention is limited with this, because
This, modification, equivalent variations, improvement for being made according to scope of the present invention patent etc. still belong to the scope that the present invention is covered.
Claims (9)
1. a kind of LED-UV woodenware aqueous priming paint, it is characterised in that by weight percentage, prepared by the raw material of following component and
Into:
Aqueous polyurethane acrylic acid dispersion 50%-80%;
Defoamer 0.1%-0.2%;
Dispersant 0.1%-0.2%;
Levelling agent 0.1%-0.2%;
Coalescents 3%-6%;
Thickener 0.3%-0.6%;
Talcum powder 15%-20%;
PH conditioning agents 0.3%-0.6%;
Light trigger 1%-5%;
Deionized water 10%-20%.
2. a kind of LED-UV woodenware aqueous priming paint according to claim 1, it is characterised in that by weight percentage, by
The raw material of following component is prepared from:
Aqueous polyurethane acrylic acid dispersion 60%-70%;
Defoamer 0.1%-0.15%;
Dispersant 0.14%-0.2%;
Levelling agent 0.16%-0.2%;
Coalescents 4%-6%;
Thickener 0.4%-0.6%;
Talcum powder 15%-17%;
PH conditioning agents 0.4%-0.6%;
Light trigger 3%-5%;
Deionized water 10%-15%.
3. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the aqueous polyurethane
Acrylic acid dispersion can be using German Cohan wound company or the product of BASF Aktiengesellschaft or the production of dutch royal DSM group
Product.
4. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the defoamer, dispersion
Agent, levelling agent can be using Di Gao companies of Germany or the products of Bi Ke companies of Germany or the production of this De Qian company of Taiwan hamming.
5. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the light trigger is
Benzoin and derivative or benzil and derivative or hydroxyalkyl phenones or amine alkyl phenones or acyl group oxidation of ketones thing or hexichol first
One or more combination in ketone or thioxanthone or iron arene, the light trigger can be had using the long day new material share in Tianjin
Limit company or the product of Changzhou Tronly New Electronic Materials Co., Ltd. or Shanghai Xinguang Chemical Co., Ltd.'s production.
6. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the PH conditioning agents are
The trade mark of LG-DOW company production is the product of AMP-95.
7. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the coalescents are
The trade mark of LG-DOW company production is the product of DPM or DPNB.
8. a kind of LED-UV woodenware aqueous priming paint according to claim 1 and 2, it is characterised in that the thickener is moral
The trade mark of Guo Mingling chemical companies production is the product of PUR-40.
9. a kind of preparation method of the LED-UV woodenware aqueous priming paint as described in claim any one of 1-8, it is characterised in that bag
Include following steps:
(1)Start dispersion machine adjust rotating speed to 800-1000 revs/min, sequentially added under this rotating speed the deionized water and into
In film auxiliary agent and aqueous polyurethane acrylic acid dispersion, stir 5-10 minutes;
(2)Adjustment dispersing speed adds the talcum powder and dispersant to 1000-1200 revs/min under this rotating speed, at a high speed
Stirring 5-10 minutes;
(3)Adjustment dispersing speed adds the light trigger and PH conditioning agents, middling speed to 1000 revs/min under this rotating speed
Stirring 5-10 minutes, until paint liquid fineness reaches 15um;
(4)Adjustment dispersing speed adds to 800-1000 revs/min after the thickener adjustment viscosity is first added under this rotating speed
Enter the defoamer, levelling agent, stir 10-20 minutes, obtain final product.
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CN201710074186.9A CN106883749A (en) | 2017-02-10 | 2017-02-10 | A kind of LED UV woodenware aqueous priming paints and preparation method thereof |
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CN201710074186.9A CN106883749A (en) | 2017-02-10 | 2017-02-10 | A kind of LED UV woodenware aqueous priming paints and preparation method thereof |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101735676A (en) * | 2008-11-14 | 2010-06-16 | 上海富臣化工有限公司 | Aqueous ultraviolet-curable transparent middle coating primer with high solid content and preparation method thereof |
CN103320005A (en) * | 2013-06-28 | 2013-09-25 | 江苏海田技术有限公司 | Ultraviolet (UV)-waterborne spraying primer |
CN103484011A (en) * | 2012-06-13 | 2014-01-01 | 展辰涂料集团股份有限公司 | Water-based ultraviolet curing coating |
-
2017
- 2017-02-10 CN CN201710074186.9A patent/CN106883749A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101735676A (en) * | 2008-11-14 | 2010-06-16 | 上海富臣化工有限公司 | Aqueous ultraviolet-curable transparent middle coating primer with high solid content and preparation method thereof |
CN103484011A (en) * | 2012-06-13 | 2014-01-01 | 展辰涂料集团股份有限公司 | Water-based ultraviolet curing coating |
CN103320005A (en) * | 2013-06-28 | 2013-09-25 | 江苏海田技术有限公司 | Ultraviolet (UV)-waterborne spraying primer |
Non-Patent Citations (1)
Title |
---|
金养智等: "《光固化材料性能及应用手册》", 31 July 2010, 化学工业出版社 * |
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